#------------------------------------------------------------------------------ #$Date: 2021-12-03 22:04:43 +0200 (Fri, 03 Dec 2021) $ #$Revision: 271010 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/91/4519126.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519126 loop_ _publ_author_name 'Seal, Nilanjan' 'Neogi, Subhadip' _publ_section_title ; Intrinsic-Unsaturation-Enriched Biporous and Chemorobust Cu(II) Framework for Efficient Catalytic CO2 Fixation and Pore-Fitting Actuated Size-Exclusive Hantzsch Condensation with Mechanistic Validation. ; _journal_issue 46 _journal_name_full 'ACS applied materials & interfaces' _journal_page_first 55123 _journal_page_last 55135 _journal_paper_doi 10.1021/acsami.1c16984 _journal_volume 13 _journal_year 2021 _chemical_formula_moiety 'C19 H22 F N O4' _chemical_formula_sum 'C19 H22 F N O4' _chemical_formula_weight 347.38 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_date 2021-05-20 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _cell_angle_alpha 90.00 _cell_angle_beta 94.101(3) _cell_angle_gamma 90.00 _cell_formula_units_Z 4 _cell_length_a 9.8320(9) _cell_length_b 7.4081(6) _cell_length_c 24.865(2) _cell_measurement_reflns_used 23753 _cell_measurement_temperature 300.15 _cell_measurement_theta_max 27.47 _cell_measurement_theta_min 2.55 _cell_volume 1806.4(3) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 300.15 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0711 _diffrn_reflns_av_unetI/netI 0.0585 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 9 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 23753 _diffrn_reflns_theta_full 27.47 _diffrn_reflns_theta_max 27.47 _diffrn_reflns_theta_min 2.55 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.096 _exptl_absorpt_correction_T_max 0.9957 _exptl_absorpt_correction_T_min 0.9640 _exptl_crystal_colour 'pale yellow' _exptl_crystal_density_diffrn 1.277 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 736 _exptl_crystal_size_max 0.385 _exptl_crystal_size_mid 0.205 _exptl_crystal_size_min 0.045 _refine_diff_density_max 0.232 _refine_diff_density_min -0.177 _refine_diff_density_rms 0.040 _refine_ls_extinction_coef 0.006(2) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.015 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 231 _refine_ls_number_reflns 4122 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.015 _refine_ls_R_factor_all 0.1427 _refine_ls_R_factor_gt 0.0622 _refine_ls_shift/su_max 0.0002 _refine_ls_shift/su_mean 0.0001 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0791P)^2^+0.7098P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1511 _refine_ls_wR_factor_ref 0.1993 _reflns_number_gt 2049 _reflns_number_total 4122 _reflns_threshold_expression >2sigma(I) _iucr_refine_instructions_details ; REM Old TITL NS6107_0m in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.248, Rweak 0.027, Alpha 0.037, Orientation as input REM Formula found by SHELXT: C19 N O5 REM ##### REM NS6107_0m_a.res in P2(1)/c REM R1 = 0.0702 for 2053 Fo > 4sig(Fo) and 0.1516 for all 4126 data REM 230 parameters refined using 0 restraints REM Highest difference peak 0.314, deepest hole -0.209, 1-sigma level 0.048 REM NS6107_0m_a.res in P2(1)/c REM R1 = 0.0702 for 2053 Fo > 4sig(Fo) and 0.1516 for all 4126 data REM 230 parameters refined using 0 restraints REM Highest difference peak 0.314, deepest hole -0.209, 1-sigma level 0.048 TITL NS6107_0m_a.res in P2(1)/c CELL 0.71073 9.8320 7.4081 24.8652 90.000 94.101 90.000 ZERR 4.0000 0.0009 0.0006 0.0021 0.000 0.003 0.000 LATT 1 SYMM -X, 0.5+Y, 0.5-Z SFAC C H N O F UNIT 76 88 4 16 4 MERG 2 FMAP 2 GRID PLAN 20 TEMP 27 SIZE 0.045 0.205 0.385 BOND $H OMIT 1 2 6 OMIT 0 3 6 OMIT -3 6 3 OMIT 6 3 0 L.S. 4 ACTA WGHT 0.079100 0.709800 EXTI 0.005725 FVAR 0.59907 O001 4 0.584405 0.207152 0.656378 11.00000 0.06164 0.06006 = 0.07146 0.00616 -0.02275 0.00177 F002 5 -0.010957 0.281989 0.757147 11.00000 0.08540 0.12770 = 0.07335 0.01280 0.02218 -0.00202 O003 4 0.150640 0.199818 0.464589 11.00000 0.09510 0.04005 = 0.05679 -0.00206 -0.03356 -0.00507 O004 4 0.268938 0.011896 0.519150 11.00000 0.11022 0.03299 = 0.07008 -0.00002 -0.03168 0.00065 O005 4 0.666569 0.486816 0.663596 11.00000 0.08076 0.07878 = 0.07754 -0.00150 -0.03011 -0.02135 N006 3 0.340938 0.630928 0.548853 11.00000 0.07310 0.03017 = 0.06486 -0.00091 -0.01416 -0.00203 AFIX 43 H006 2 0.314919 0.740588 0.543268 11.00000 -1.20000 AFIX 0 C007 1 0.252428 0.278815 0.634687 11.00000 0.05467 0.03941 = 0.04418 0.00112 -0.01022 -0.00529 C008 1 0.356892 0.287038 0.591645 11.00000 0.05708 0.03582 = 0.04582 -0.00064 -0.01315 0.00163 AFIX 13 H008 2 0.402551 0.169594 0.590758 11.00000 -1.20000 AFIX 0 C009 1 0.289802 0.324011 0.536054 11.00000 0.05710 0.03451 = 0.04454 0.00085 -0.00861 0.00231 C00A 1 0.464505 0.429784 0.606742 11.00000 0.05054 0.04433 = 0.04416 -0.00627 -0.00512 -0.00219 C00B 1 0.276239 0.496631 0.518245 11.00000 0.06203 0.03756 = 0.04484 0.00057 -0.00867 0.00104 C00C 1 0.237844 0.165340 0.506659 11.00000 0.06528 0.03930 = 0.04204 0.00077 -0.00844 -0.00088 C00D 1 0.444978 0.599170 0.587893 11.00000 0.05682 0.04120 = 0.05505 -0.00844 -0.00183 -0.00550 C00E 1 0.580066 0.383260 0.644611 11.00000 0.05253 0.05987 = 0.04998 -0.00500 -0.00371 -0.00389 C00F 1 0.134972 0.382689 0.631164 11.00000 0.06913 0.05241 = 0.05380 0.00875 -0.00399 0.00484 AFIX 43 H00F 2 0.115703 0.453615 0.600709 11.00000 -1.20000 AFIX 0 C00G 1 0.276151 0.174021 0.680321 11.00000 0.05508 0.06796 = 0.06279 0.01784 -0.00800 -0.00024 AFIX 43 H00G 2 0.353149 0.100804 0.683410 11.00000 -1.20000 AFIX 0 C00H 1 0.076242 0.280468 0.716081 11.00000 0.06479 0.07861 = 0.05065 0.00147 -0.00020 -0.01056 C00I 1 0.199466 0.567105 0.468308 11.00000 0.09039 0.04472 = 0.05581 0.00778 -0.01477 0.00405 AFIX 137 H00A 2 0.227058 0.689082 0.461911 11.00000 -1.50000 H00B 2 0.103405 0.564187 0.472973 11.00000 -1.50000 H00C 2 0.218800 0.493149 0.438082 11.00000 -1.50000 AFIX 0 C00J 1 0.045913 0.383934 0.671472 11.00000 0.06976 0.06342 = 0.06735 0.00834 0.00100 0.01114 AFIX 43 H00J 2 -0.032943 0.453602 0.668344 11.00000 -1.20000 AFIX 0 C00K 1 0.189241 0.174555 0.721445 11.00000 0.06685 0.08871 = 0.05753 0.02522 -0.01067 -0.00639 AFIX 43 H00K 2 0.207493 0.104194 0.752088 11.00000 -1.20000 AFIX 0 C00L 1 0.525767 0.765174 0.603885 11.00000 0.08792 0.04955 = 0.08139 -0.00976 -0.00802 -0.01596 AFIX 137 H00D 2 0.619960 0.733368 0.611099 11.00000 -1.50000 H00E 2 0.491587 0.816599 0.635692 11.00000 -1.50000 H00H 2 0.517389 0.851651 0.575084 11.00000 -1.50000 AFIX 0 C00M 1 0.101422 0.048460 0.431494 11.00000 0.11238 0.04264 = 0.06507 -0.00483 -0.02889 -0.00966 AFIX 23 H00I 2 0.050399 -0.034334 0.452599 11.00000 -1.20000 H00L 2 0.177503 -0.016354 0.417879 11.00000 -1.20000 AFIX 0 C00N 1 0.688207 0.146074 0.697286 11.00000 0.06378 0.08812 = 0.08313 0.01006 -0.02957 0.01102 AFIX 23 H00M 2 0.770232 0.217431 0.694783 11.00000 -1.20000 H00N 2 0.710706 0.021107 0.690381 11.00000 -1.20000 AFIX 0 C00O 1 0.642156 0.161823 0.751886 11.00000 0.10105 0.13719 = 0.07481 0.02835 -0.01678 0.00858 AFIX 137 H00O 2 0.621585 0.285755 0.759144 11.00000 -1.50000 H00P 2 0.712860 0.120353 0.777557 11.00000 -1.50000 H00Q 2 0.561872 0.089674 0.754707 11.00000 -1.50000 AFIX 0 C00P 1 0.013529 0.121618 0.386700 11.00000 0.16180 0.07721 = 0.09755 -0.01281 -0.07089 -0.00272 AFIX 137 H00R 2 0.064956 0.203732 0.366229 11.00000 -1.50000 H00S 2 -0.061779 0.184435 0.400638 11.00000 -1.50000 H00T 2 -0.020223 0.024660 0.363861 11.00000 -1.50000 HKLF 4 REM NS6107_0m_a.res in P2(1)/c REM R1 = 0.0622 for 2049 Fo > 4sig(Fo) and 0.1427 for all 4122 data REM 231 parameters refined using 0 restraints END WGHT 0.0708 0.7367 REM Highest difference peak 0.232, deepest hole -0.177, 1-sigma level 0.040 Q1 1 0.3629 0.7461 0.5259 11.00000 0.05 0.23 Q2 1 0.5713 0.7545 0.6479 11.00000 0.05 0.21 Q3 1 0.4576 0.8617 0.6060 11.00000 0.05 0.20 Q4 1 0.6030 0.0265 0.7284 11.00000 0.05 0.19 Q5 1 0.2924 0.3942 0.5223 11.00000 0.05 0.18 Q6 1 0.4362 0.9111 0.5992 11.00000 0.05 0.18 Q7 1 0.1204 0.4564 0.4575 11.00000 0.05 0.17 Q8 1 0.0393 0.3067 0.7935 11.00000 0.05 0.17 Q9 1 0.4555 0.9507 0.5926 11.00000 0.05 0.16 Q10 1 0.1490 0.0605 0.3899 11.00000 0.05 0.16 Q11 1 0.1375 0.6800 0.4786 11.00000 0.05 0.15 Q12 1 0.3197 0.3178 0.5581 11.00000 0.05 0.15 Q13 1 0.6749 0.2567 0.7163 11.00000 0.05 0.15 Q14 1 -0.1668 0.4074 0.6717 11.00000 0.05 0.13 Q15 1 0.5458 0.2976 0.6801 11.00000 0.05 0.13 Q16 1 0.1279 -0.0408 0.4343 11.00000 0.05 0.13 Q17 1 0.4410 0.1479 0.5784 11.00000 0.05 0.13 Q18 1 0.2608 0.2637 0.5296 11.00000 0.05 0.12 Q19 1 -0.0001 0.2617 0.3786 11.00000 0.05 0.12 Q20 1 -0.0255 0.0777 0.4419 11.00000 0.05 0.12 ; _cod_data_source_file am1c16984_si_004.cif _cod_data_source_block 2b _cod_original_cell_volume 1806.5(3) _cod_database_code 4519126 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C008(H008) 2.b Secondary CH2 refined with riding coordinates: C00M(H00I,H00L), C00N(H00M,H00N) 2.c Aromatic/amide H refined with riding coordinates: N006(H006), C00F(H00F), C00G(H00G), C00J(H00J), C00K(H00K) 2.d Idealised Me refined as rotating group: C00I(H00A,H00B,H00C), C00L(H00D,H00E,H00H), C00O(H00O,H00P,H00Q), C00P(H00R, H00S,H00T) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 'x, y, z' 2 '-x, y+1/2, -z+1/2' 3 '-x, -y, -z' 4 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_calc_flag _atom_site_disorder_assembly _atom_site_disorder_group _atom_site_refinement_flags_posn O001 O 0.5844(2) 0.2072(3) 0.65638(8) 0.0657(6) Uani 1 d . . . F002 F -0.0110(2) 0.2820(3) 0.75715(8) 0.0947(7) Uani 1 d . . . O003 O 0.1506(2) 0.1998(2) 0.46459(8) 0.0659(6) Uani 1 d . . . O004 O 0.2689(2) 0.0119(2) 0.51915(9) 0.0729(7) Uani 1 d . . . O005 O 0.6666(2) 0.4868(3) 0.66360(9) 0.0807(7) Uani 1 d . . . N006 N 0.3409(2) 0.6309(3) 0.54885(9) 0.0570(7) Uani 1 d . . . H006 H 0.3149 0.7406 0.5433 0.068 Uiso 1 calc . . R C007 C 0.2524(3) 0.2788(3) 0.63469(11) 0.0467(7) Uani 1 d . . . C008 C 0.3569(3) 0.2870(3) 0.59165(10) 0.0470(7) Uani 1 d . . . H008 H 0.4026 0.1696 0.5908 0.056 Uiso 1 calc . . R C009 C 0.2898(3) 0.3240(3) 0.53605(10) 0.0460(7) Uani 1 d . . . C00A C 0.4645(3) 0.4298(3) 0.60674(11) 0.0468(7) Uani 1 d . . . C00B C 0.2762(3) 0.4966(3) 0.51824(11) 0.0487(7) Uani 1 d . . . C00C C 0.2378(3) 0.1653(3) 0.50666(11) 0.0495(7) Uani 1 d . . . C00D C 0.4450(3) 0.5992(4) 0.58789(11) 0.0513(7) Uani 1 d . . . C00E C 0.5801(3) 0.3833(4) 0.64461(11) 0.0545(7) Uani 1 d . . . C00F C 0.1350(3) 0.3827(4) 0.63116(12) 0.0588(8) Uani 1 d . . . H00F H 0.1157 0.4536 0.6007 0.071 Uiso 1 calc . . R C00G C 0.2762(3) 0.1740(4) 0.68032(12) 0.0625(9) Uani 1 d . . . H00G H 0.3531 0.1008 0.6834 0.075 Uiso 1 calc . . R C00H C 0.0762(3) 0.2805(5) 0.71608(13) 0.0649(9) Uani 1 d . . . C00I C 0.1995(3) 0.5671(4) 0.46831(12) 0.0646(9) Uani 1 d . . . H00A H 0.2271 0.6891 0.4619 0.097 Uiso 1 calc . . GR H00B H 0.1034 0.5642 0.4730 0.097 Uiso 1 calc . . GR H00C H 0.2188 0.4931 0.4381 0.097 Uiso 1 calc . . GR C00J C 0.0459(4) 0.3839(4) 0.67147(13) 0.0670(9) Uani 1 d . . . H00J H -0.0329 0.4536 0.6683 0.080 Uiso 1 calc . . R C00K C 0.1892(4) 0.1746(5) 0.72145(14) 0.0718(10) Uani 1 d . . . H00K H 0.2075 0.1042 0.7521 0.086 Uiso 1 calc . . R C00L C 0.5258(4) 0.7652(4) 0.60388(14) 0.0736(10) Uani 1 d . . . H00D H 0.6200 0.7334 0.6111 0.110 Uiso 1 calc . . GR H00E H 0.4916 0.8166 0.6357 0.110 Uiso 1 calc . . GR H00H H 0.5174 0.8517 0.5751 0.110 Uiso 1 calc . . GR C00M C 0.1014(4) 0.0485(4) 0.43149(13) 0.0751(10) Uani 1 d . . . H00I H 0.0504 -0.0343 0.4526 0.090 Uiso 1 calc . . R H00L H 0.1775 -0.0164 0.4179 0.090 Uiso 1 calc . . R C00N C 0.6882(3) 0.1461(5) 0.69729(15) 0.0800(11) Uani 1 d . . . H00M H 0.7702 0.2174 0.6948 0.096 Uiso 1 calc . . R H00N H 0.7107 0.0211 0.6904 0.096 Uiso 1 calc . . R C00O C 0.6422(4) 0.1618(6) 0.75189(16) 0.1055(14) Uani 1 d . . . H00O H 0.6216 0.2858 0.7591 0.158 Uiso 1 calc . . GR H00P H 0.7129 0.1204 0.7776 0.158 Uiso 1 calc . . GR H00Q H 0.5619 0.0897 0.7547 0.158 Uiso 1 calc . . GR C00P C 0.0135(5) 0.1216(5) 0.38670(17) 0.1160(17) Uani 1 d . . . H00R H 0.0650 0.2037 0.3662 0.174 Uiso 1 calc . . GR H00S H -0.0618 0.1844 0.4006 0.174 Uiso 1 calc . . GR H00T H -0.0202 0.0247 0.3639 0.174 Uiso 1 calc . . GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0616(13) 0.0601(13) 0.0715(14) 0.0062(10) -0.0227(11) 0.0018(10) F002 0.0854(14) 0.1277(18) 0.0734(14) 0.0128(12) 0.0222(12) -0.0020(12) O003 0.0951(16) 0.0400(11) 0.0568(13) -0.0021(9) -0.0336(12) -0.0051(10) O004 0.1102(18) 0.0330(11) 0.0701(14) 0.0000(9) -0.0317(13) 0.0006(11) O005 0.0808(15) 0.0788(15) 0.0775(16) -0.0015(12) -0.0301(13) -0.0214(13) N006 0.0731(16) 0.0302(11) 0.0649(16) -0.0009(10) -0.0142(14) -0.0020(10) C007 0.0547(16) 0.0394(14) 0.0442(16) 0.0011(11) -0.0102(13) -0.0053(12) C008 0.0571(16) 0.0358(13) 0.0458(16) -0.0006(11) -0.0131(14) 0.0016(12) C009 0.0571(16) 0.0345(13) 0.0445(15) 0.0009(11) -0.0086(13) 0.0023(12) C00A 0.0505(15) 0.0443(15) 0.0442(15) -0.0063(12) -0.0051(13) -0.0022(12) C00B 0.0620(17) 0.0376(14) 0.0448(16) 0.0006(12) -0.0087(14) 0.0010(12) C00C 0.0653(18) 0.0393(15) 0.0420(15) 0.0008(12) -0.0084(14) -0.0009(13) C00D 0.0568(17) 0.0412(15) 0.0551(17) -0.0084(13) -0.0018(15) -0.0055(13) C00E 0.0525(17) 0.0599(18) 0.0500(17) -0.0050(14) -0.0037(15) -0.0039(14) C00F 0.069(2) 0.0524(17) 0.0538(18) 0.0087(14) -0.0040(16) 0.0048(15) C00G 0.0551(18) 0.068(2) 0.063(2) 0.0178(16) -0.0080(17) -0.0002(15) C00H 0.065(2) 0.079(2) 0.0506(19) 0.0015(16) -0.0002(17) -0.0106(17) C00I 0.090(2) 0.0447(16) 0.0558(19) 0.0078(13) -0.0148(17) 0.0040(15) C00J 0.070(2) 0.063(2) 0.067(2) 0.0083(16) 0.0010(18) 0.0111(16) C00K 0.067(2) 0.089(2) 0.058(2) 0.0252(18) -0.0107(18) -0.0064(18) C00L 0.088(2) 0.0495(18) 0.081(2) -0.0098(16) -0.008(2) -0.0160(16) C00M 0.112(3) 0.0426(16) 0.065(2) -0.0048(15) -0.029(2) -0.0097(17) C00N 0.064(2) 0.088(3) 0.083(3) 0.010(2) -0.030(2) 0.0110(18) C00O 0.101(3) 0.137(4) 0.075(3) 0.028(3) -0.017(2) 0.009(3) C00P 0.162(4) 0.077(3) 0.098(3) -0.013(2) -0.071(3) -0.003(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C00E O001 C00N 117.7(2) . . ? C00C O003 C00M 117.9(2) . . ? C00B N006 H006 118.2 . . ? C00D N006 H006 118.2 . . ? C00D N006 C00B 123.7(2) . . ? C00F C007 C008 122.0(2) . . ? C00G C007 C008 120.8(2) . . ? C00G C007 C00F 117.1(3) . . ? C007 C008 H008 108.1 . . ? C009 C008 C007 112.0(2) . . ? C009 C008 H008 108.1 . . ? C009 C008 C00A 110.4(2) . . ? C00A C008 C007 110.1(2) . . ? C00A C008 H008 108.1 . . ? C00B C009 C008 119.7(2) . . ? C00B C009 C00C 125.0(2) . . ? C00C C009 C008 115.2(2) . . ? C00D C00A C008 118.8(2) . . ? C00D C00A C00E 121.8(2) . . ? C00E C00A C008 119.2(2) . . ? N006 C00B C00I 113.0(2) . . ? C009 C00B N006 118.0(2) . . ? C009 C00B C00I 129.1(2) . . ? O003 C00C C009 115.0(2) . . ? O004 C00C O003 121.2(2) . . ? O004 C00C C009 123.7(2) . . ? N006 C00D C00L 113.5(2) . . ? C00A C00D N006 118.9(2) . . ? C00A C00D C00L 127.6(3) . . ? O001 C00E C00A 112.4(2) . . ? O005 C00E O001 121.4(3) . . ? O005 C00E C00A 126.2(3) . . ? C007 C00F H00F 119.1 . . ? C00J C00F C007 121.9(3) . . ? C00J C00F H00F 119.1 . . ? C007 C00G H00G 119.0 . . ? C007 C00G C00K 122.0(3) . . ? C00K C00G H00G 119.0 . . ? C00J C00H F002 119.1(3) . . ? C00K C00H F002 118.6(3) . . ? C00K C00H C00J 122.3(3) . . ? C00B C00I H00A 109.5 . . ? C00B C00I H00B 109.5 . . ? C00B C00I H00C 109.5 . . ? H00A C00I H00B 109.5 . . ? H00A C00I H00C 109.5 . . ? H00B C00I H00C 109.5 . . ? C00F C00J H00J 120.8 . . ? C00H C00J C00F 118.3(3) . . ? C00H C00J H00J 120.8 . . ? C00G C00K H00K 120.8 . . ? C00H C00K C00G 118.3(3) . . ? C00H C00K H00K 120.8 . . ? C00D C00L H00D 109.5 . . ? C00D C00L H00E 109.5 . . ? C00D C00L H00H 109.5 . . ? H00D C00L H00E 109.5 . . ? H00D C00L H00H 109.5 . . ? H00E C00L H00H 109.5 . . ? O003 C00M H00I 110.2 . . ? O003 C00M H00L 110.2 . . ? O003 C00M C00P 107.4(3) . . ? H00I C00M H00L 108.5 . . ? C00P C00M H00I 110.2 . . ? C00P C00M H00L 110.2 . . ? O001 C00N H00M 109.2 . . ? O001 C00N H00N 109.2 . . ? O001 C00N C00O 111.9(3) . . ? H00M C00N H00N 107.9 . . ? C00O C00N H00M 109.2 . . ? C00O C00N H00N 109.2 . . ? C00N C00O H00O 109.5 . . ? C00N C00O H00P 109.5 . . ? C00N C00O H00Q 109.5 . . ? H00O C00O H00P 109.5 . . ? H00O C00O H00Q 109.5 . . ? H00P C00O H00Q 109.5 . . ? C00M C00P H00R 109.5 . . ? C00M C00P H00S 109.5 . . ? C00M C00P H00T 109.5 . . ? H00R C00P H00S 109.5 . . ? H00R C00P H00T 109.5 . . ? H00S C00P H00T 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O001 C00E 1.337(3) . ? O001 C00N 1.460(3) . ? F002 C00H 1.380(4) . ? O003 C00C 1.329(3) . ? O003 C00M 1.453(3) . ? O004 C00C 1.212(3) . ? O005 C00E 1.215(3) . ? N006 H006 0.8600 . ? N006 C00B 1.380(3) . ? N006 C00D 1.379(3) . ? C007 C008 1.537(4) . ? C007 C00F 1.385(4) . ? C007 C00G 1.381(4) . ? C008 H008 0.9800 . ? C008 C009 1.513(3) . ? C008 C00A 1.524(3) . ? C009 C00B 1.357(3) . ? C009 C00C 1.457(4) . ? C00A C00D 1.348(4) . ? C00A C00E 1.464(4) . ? C00B C00I 1.500(4) . ? C00D C00L 1.502(4) . ? C00F H00F 0.9300 . ? C00F C00J 1.377(4) . ? C00G H00G 0.9300 . ? C00G C00K 1.379(4) . ? C00H C00J 1.364(4) . ? C00H C00K 1.359(5) . ? C00I H00A 0.9600 . ? C00I H00B 0.9600 . ? C00I H00C 0.9600 . ? C00J H00J 0.9300 . ? C00K H00K 0.9300 . ? C00L H00D 0.9600 . ? C00L H00E 0.9600 . ? C00L H00H 0.9600 . ? C00M H00I 0.9700 . ? C00M H00L 0.9700 . ? C00M C00P 1.464(5) . ? C00N H00M 0.9700 . ? C00N H00N 0.9700 . ? C00N C00O 1.466(5) . ? C00O H00O 0.9600 . ? C00O H00P 0.9600 . ? C00O H00Q 0.9600 . ? C00P H00R 0.9600 . ? C00P H00S 0.9600 . ? C00P H00T 0.9600 . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 2 0 0 737.43 17.1 -2 0 0 733.73 16.4 -2 0 0 705.73 16 -2 0 0 718.73 16.9 2 0 0 729.43 17.8 -3 0 0 1528.25 30.2 3 0 0 1542.75 28.5 3 0 0 1481.35 32.6 -3 0 0 1430.96 29.1 -3 0 0 1496.05 30.6 3 0 0 1550.74 31.6 -4 0 0 287.47 13.4 -4 0 0 288.97 13.8 4 0 0 297.17 14.7 4 0 0 262.47 12 4 0 0 281.47 15.1 -4 0 0 281.07 13.8 -5 0 0 14.3 3.8 -5 0 0 20.8 4.8 5 0 0 18 5.1 -5 0 0 16.8 4.1 5 0 0 15.9 3.6 5 0 0 9.9 3.9 -6 0 0 7.8 3.3 -6 0 0 6.9 3.3 6 0 0 5.9 3.2 -6 0 0 4.8 3 6 0 0 6.3 2.5 6 0 0 1.7 3.7 7 0 0 143.69 12.3 7 0 0 134.69 14.6 -7 0 0 144.99 12.6 -7 0 0 131.99 12.1 -8 0 0 12.7 4.2 8 0 0 15.3 5.8 8 0 0 7.1 4.1 -9 0 0 10.4 4.8 -9 0 0 13.8 5.5 9 0 0 12.3 5.6 10 0 0 24.2 7.3 -10 0 0 19.7 6.1 -10 0 0 10.4 5.8 -11 0 0 9.6 5.5 -11 0 0 11.8 5.2 11 0 0 7.5 5.3 12 0 0 -7.2 5.2 -12 0 0 4.4 4.7 -12 0 0 -6.1 5.5 0 -1 0 -0.2 0.2 0 -1 0 0.1 0.3 0 -1 0 0.4 0.5 0 -1 0 0.5 0.5 0 1 0 0.8 0.4 0 1 0 0 0.2 0 1 0 -0.3 0.5 0 1 0 0.7 0.4 1 -1 0 2027.4 29 1 -1 0 2041.7 29.3 1 -1 0 2012.6 30.3 1 -1 0 2031.2 33.8 -1 -1 0 2054.09 24.5 -1 1 0 2064.19 28.3 1 1 0 1998.6 29.2 1 1 0 2025.2 26.7 -1 1 0 2018.6 28.7 -1 1 0 1991.6 33 -1 1 0 2032.1 29.6 2 -1 0 3455.85 47 2 -1 0 3507.35 55.59 -2 -1 0 3438.66 41.4 -2 -1 0 3491.15 45 2 -1 0 3483.15 50.59 -2 1 0 3457.25 49.3 -2 1 0 3448.95 45.8 2 1 0 3538.85 40.5 2 1 0 3493.65 48.1 -2 1 0 3496.05 53.39 3 -1 0 439.36 17.1 -3 -1 0 413.16 11.7 -3 -1 0 403.36 13.6 3 -1 0 377.16 13.9 3 -1 0 405.66 17.6 -3 1 0 418.36 15.6 3 1 0 398.26 16.2 -3 1 0 423.06 17.2 -3 1 0 435.56 13 3 1 0 411.36 12.2 3 1 0 428.66 15.8 -4 -1 0 45.9 5.2 -4 -1 0 44.7 4.4 4 -1 0 46.8 7.7 4 -1 0 41.9 5.3 4 -1 0 57.79 8.9 -4 1 0 35.5 4.3 -4 1 0 31.4 5.5 4 1 0 37.4 6.3 4 1 0 45.3 7.3 -4 1 0 29.3 5.6 4 1 0 48.6 5.2 -5 -1 0 52.69 6.2 -5 -1 0 58.29 5.7 5 -1 0 54.09 9.4 5 -1 0 48.8 8.5 5 -1 0 52.49 6.5 5 1 0 53.69 6.3 -5 1 0 47.1 7.9 5 1 0 49.99 6.5 5 1 0 49.99 8.3 -5 1 0 51.09 5.9 -5 1 0 56.89 7.1 6 -1 0 58.99 10.6 -6 -1 0 54.89 6.9 -6 -1 0 40.6 6.5 6 -1 0 57.99 7.4 6 -1 0 44.7 9.6 -6 1 0 42.8 7.2 6 1 0 46.9 8.5 6 1 0 56.19 7.2 -6 1 0 48.5 8.4 -6 1 0 43.1 7.6 6 1 0 45.5 7.7 -7 -1 0 12.2 4 -7 -1 0 13.7 4.5 7 -1 0 17.2 5.2 7 -1 0 15.2 6.2 -7 1 0 10.4 4.2 7 1 0 21 5.9 7 1 0 20.6 6.4 -7 1 0 15.5 5.1 -7 1 0 14.9 5.9 -8 -1 0 -1 2.5 8 -1 0 -0.3 2 -8 -1 0 0.5 2.6 -8 1 0 -4.4 2.6 8 1 0 8.4 4.6 8 1 0 -1.8 1.7 -8 1 0 4.2 3.5 -9 -1 0 62.59 10.4 9 -1 0 49.5 10.5 -9 1 0 49 9.5 -9 1 0 47.5 10.5 9 1 0 51.29 10 9 1 0 55.79 10.2 -10 -1 0 65.69 11.9 10 -1 0 70.69 13.4 -10 -1 0 92.49 11.6 -10 1 0 72.49 12.9 10 1 0 77.99 13.3 -10 1 0 55.19 10.4 -11 -1 0 6.6 4.9 11 -1 0 -0.7 5 -11 -1 0 -3.8 3.4 -11 1 0 0.3 3.6 -11 1 0 -4.4 3.1 -12 -1 0 -6.6 3.9 -12 -1 0 -1.4 6.4 12 -1 0 -1 6 -12 1 0 2 5.1 -12 1 0 1.8 4.7 12 1 0 -0.6 4.6 0 -2 0 1264.37 26.8 0 -2 0 1234.58 26.7 0 -2 0 1228.38 19.4 0 -2 0 1229.68 16.6 0 2 0 1263.47 18.4 0 2 0 1241.18 26.8 0 2 0 1244.88 21.4 1 -2 0 1.4 1.2 1 -2 0 -0.2 0.6 1 -2 0 2.2 1.7 -1 -2 0 3.9 1.5 -1 -2 0 7.5 2.2 1 2 0 4.5 1.2 -1 2 0 1 1 -1 2 0 1.6 1.1 -1 2 0 3.1 1.6 1 2 0 2.7 1.6 1 2 0 2.3 1 -1 2 0 3.3 1.9 2 -2 0 326.17 16.4 2 -2 0 301.17 13.2 -2 -2 0 303.57 7.4 2 -2 0 303.97 12.6 -2 2 0 299.67 14.8 2 2 0 308.37 12.9 2 2 0 326.57 7.9 2 2 0 322.47 11.6 -2 2 0 309.07 11.7 -2 2 0 320.57 12.1 2 2 0 319.07 7.2 -2 2 0 297.47 12.6 -3 -2 0 9.2 1.9 3 -2 0 8.5 2.9 3 -2 0 9.4 3.7 3 -2 0 9 2.6 3 -2 0 2.8 2.3 3 2 0 9.1 3 3 2 0 9.3 1.5 -3 2 0 5.1 2.6 -3 2 0 5.3 2.2 -3 2 0 6.3 3 -4 -2 0 6.8 2.2 4 -2 0 -0.4 1.9 -4 -2 0 6.8 1.9 4 -2 0 7.1 3 4 -2 0 6.8 3.6 4 2 0 6.5 1.9 -4 2 0 1 2.6 -4 2 0 6.1 2 4 2 0 1.8 1.5 -4 2 0 5.8 2.4 4 2 0 4.3 2.6 5 -2 0 195.68 12.7 -5 -2 0 207.58 10.9 5 -2 0 202.58 15.2 -5 -2 0 203.38 11.1 5 -2 0 171.78 15.5 5 2 0 180.98 13.8 5 2 0 201.88 10.5 -5 2 0 196.08 14.9 5 2 0 188.58 14.5 -5 2 0 192.68 13.4 -5 2 0 192.58 10.6 -6 -2 0 0.5 1.5 -6 -2 0 0.7 2 6 -2 0 -4.8 2.9 6 -2 0 -1.9 2 6 -2 0 -0.5 2.1 -6 2 0 -0.5 1.6 -6 2 0 -0.2 2 -6 2 0 -1.4 2.4 6 2 0 -1.8 2.1 6 2 0 -0.7 2 6 2 0 -1.1 2.8 7 -2 0 0.9 2.6 -7 -2 0 4.4 2.6 -7 -2 0 3.5 2.1 7 2 0 3 2.8 -7 2 0 0 2.1 -7 2 0 6.1 3 -7 2 0 -2.9 2.8 7 2 0 -0.2 3.1 8 -2 0 12.8 5.4 -8 -2 0 23.7 6.1 -8 -2 0 25.1 5.6 -8 2 0 21.6 6.3 8 2 0 23.4 7 8 2 0 18.6 5.6 -8 2 0 10.2 4.8 -9 -2 0 2.6 3.5 9 -2 0 -0.6 3.4 -9 -2 0 3.6 4.4 9 2 0 3 4.6 9 2 0 8.4 4 -9 2 0 -0.5 2.4 -9 2 0 9.4 5.3 -10 -2 0 2.3 4.4 -10 -2 0 1.5 3.7 10 -2 0 -6 4.8 10 2 0 -0.1 2.9 10 2 0 -7.3 5.8 -10 2 0 -0.7 3.1 -10 2 0 1.2 3.8 -11 -2 0 2.9 4 -11 -2 0 2.6 5.9 11 -2 0 1.7 4.5 11 2 0 -7.1 3.4 -11 2 0 6.9 7.2 -11 2 0 -3.9 3.2 -12 -2 0 -7.6 6.1 -12 -2 0 -0.5 4.4 12 -2 0 7.2 7.8 -12 2 0 4.6 5.4 -12 2 0 6.4 5.5 12 2 0 2.2 5 0 -3 0 -1.8 1.2 0 -3 0 1.1 1.5 0 3 0 -1.1 0.9 0 3 0 -1.7 1.1 0 3 0 1.1 1.2 0 3 0 2.6 1.8 1 -3 0 566.04 15.9 1 -3 0 560.14 15 -1 -3 0 579.94 20.6 -1 -3 0 576.54 17.9 1 -3 0 548.35 22.4 1 -3 0 554.34 21 -1 3 0 577.64 21.4 1 3 0 536.25 15.9 -1 3 0 578.94 15.3 -1 3 0 570.64 21.2 1 3 0 563.04 21 -1 3 0 566.34 20.7 1 3 0 573.84 16.9 2 -3 0 225.98 13.6 2 -3 0 213.88 13.3 2 -3 0 238.58 15.9 -2 -3 0 246.48 13.2 2 -3 0 234.78 12 2 3 0 231.38 8.4 -2 3 0 229.68 12.1 2 3 0 215.28 13 -2 3 0 219.48 10.8 -2 3 0 242.38 14.9 2 3 0 230.48 10.9 -2 3 0 235.28 13.1 3 -3 0 57.39 6.8 3 -3 0 56.19 9.9 -3 -3 0 60.79 2.5 3 -3 0 74.59 8.2 3 -3 0 66.59 7.5 -3 3 0 57.89 6.1 3 3 0 71.19 3.4 3 3 0 54.39 2.6 3 3 0 73.89 7.2 3 3 0 61.59 7.1 -3 3 0 72.69 7.1 -3 3 0 81.59 9.3 4 -3 0 12.3 3.7 4 -3 0 14.8 4.6 4 -3 0 9 4 4 -3 0 19.4 5.4 -4 -3 0 13.3 2.2 4 3 0 10.3 3.7 -4 3 0 16.8 4.7 -4 3 0 15.7 5.1 4 3 0 12.1 1.7 -4 3 0 10.3 3.5 4 3 0 15.8 4.3 5 -3 0 19.6 8.1 5 -3 0 10.8 4.3 5 -3 0 13.1 4.9 5 -3 0 16.7 4.7 -5 -3 0 13.4 2.9 5 3 0 17.2 4.9 -5 3 0 14.9 4 5 3 0 17.5 6.9 -5 3 0 16 4.2 5 3 0 16.8 2.7 5 3 0 16.9 5.4 6 -3 0 12.2 3.8 6 -3 0 20.5 6.4 6 -3 0 11 4.1 -6 3 0 18.7 4.9 -6 3 0 18.7 5.9 -6 3 0 10.4 3.3 6 3 0 27.6 7.8 6 3 0 17.7 5.3 -7 -3 0 1.1 2 7 -3 0 5.5 3.6 7 -3 0 6.9 3.6 -7 3 0 3.6 3.4 7 3 0 2.4 3.4 -7 3 0 7.8 4.2 7 3 0 5.8 3 -8 -3 0 19.6 5 -8 -3 0 22.5 5.2 8 -3 0 19.4 6.4 8 -3 0 19.7 6.7 8 3 0 16.7 6 -8 3 0 7.2 4.8 -8 3 0 17.6 5.3 -8 3 0 20 6 8 3 0 4.3 4 -9 -3 0 1.5 3 9 -3 0 2.8 4.6 9 -3 0 4.4 4.5 -9 -3 0 4.1 3.3 -9 3 0 6.4 4.1 9 3 0 -3.2 4 -9 3 0 6.9 3.9 9 3 0 3.1 5 10 -3 0 1 4.9 -10 -3 0 -1.1 2.7 10 -3 0 4.9 4.5 -10 -3 0 7.6 4.1 -10 3 0 -7.3 4.4 10 3 0 0.3 5.4 10 3 0 1.8 2.8 -11 -3 0 12.1 5.9 11 -3 0 14.4 6.6 11 -3 0 10.2 6.6 -11 -3 0 12 5.2 -11 3 0 9.1 5.3 11 3 0 6.9 4.1 -11 3 0 20.3 9.4 -12 -3 0 -3.5 3.9 12 -3 0 1.1 7.3 12 -3 0 0.2 5 -12 3 0 5 6.3 12 3 0 5.9 5.8 -12 3 0 5.8 7.9 0 -4 0 50.79 8.3 0 -4 0 41 7.4 0 4 0 51.29 6.4 0 4 0 57.29 5.8 0 4 0 47.8 9 0 4 0 52.99 8.5 1 -4 0 0 1.6 1 -4 0 1.7 1.9 -1 -4 0 -2.2 1.2 1 -4 0 -0.9 1 1 -4 0 -0.8 1.9 -1 -4 0 2 2.1 1 4 0 -1.2 1.2 1 4 0 0.3 1.4 -1 4 0 -3.4 2.3 -1 4 0 0.5 0.8 -1 4 0 2.4 2.1 1 4 0 3.1 2.5 -1 4 0 2.9 2.5 2 -4 0 72.39 9 -2 -4 0 88.39 9 2 -4 0 75.29 6.8 2 -4 0 88.19 10.6 2 4 0 74.59 5.8 2 4 0 91.19 11 -2 4 0 78.89 7 -2 4 0 90.89 9.9 2 4 0 89.49 7.6 -2 4 0 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12.5 -5 2 2 160.28 13.4 4 -2 -2 27.4 6.6 4 -2 -2 25.7 5.2 4 -2 -2 26.5 5.4 -4 -2 2 27.1 3 4 -2 -2 27.5 5.4 -4 2 2 24.1 4.8 -4 2 2 18.9 4.8 -4 2 2 24.5 5 4 2 -2 26.4 4.8 4 2 -2 30.5 4.3 4 2 -2 26.8 5.9 3 -2 -2 708.43 25.8 3 -2 -2 696.83 21.9 3 -2 -2 688.13 21.5 3 2 -2 688.73 20.3 3 2 -2 696.13 16.9 3 2 -2 684.53 23.9 -3 2 2 677.43 23.8 -3 2 2 664.43 21.4 3 2 -2 681.73 17.7 -3 2 2 706.03 20.9 2 -2 -2 0.5 1.3 2 -2 -2 -0.8 0.6 2 -2 -2 0.2 1.3 2 -2 -2 -1.4 0.9 2 2 -2 1.6 1.3 -2 2 2 0.4 1 -2 2 2 -0.9 1.3 2 2 -2 -0.6 0.5 -2 2 2 -0.7 1 -2 2 2 -0.5 0.9 1 -2 -2 4 2.3 -1 -2 2 5 2 1 -2 -2 3.2 1.8 1 -2 -2 4.9 1.6 1 -2 -2 4.1 2.9 1 -2 -2 4.6 1.6 -1 2 2 1.4 1.6 -1 2 2 4.7 1.9 1 2 -2 3.8 1.9 -1 2 2 5.4 1.5 1 2 -2 1.8 1.5 -1 2 2 8.1 2.9 0 -2 2 1922.41 35.3 0 -2 -2 1921.11 35.2 0 -2 -2 1929.71 27.3 0 -2 2 1995.5 38.6 0 -2 -2 1910.21 32.1 0 2 -2 1997.9 23.3 0 2 -2 1972.6 38.5 0 2 2 2026.7 36.1 0 2 2 1933.71 34.2 0 2 -2 1946.01 22.8 0 2 -2 1942.01 35.5 0 2 2 1983.8 34.1 -1 -2 -2 1671.73 33.8 -1 -2 -2 1773.92 25 -1 -2 -2 1727.83 32.2 1 -2 2 1807.82 40 1 -2 2 1707.33 27.8 1 -2 2 1747.43 34.3 -1 2 -2 1762.52 29.1 1 2 2 1744.53 33.5 -1 2 -2 1721.23 38.4 -1 2 -2 1720.03 29.3 1 2 2 1718.73 23.1 -1 2 -2 1681.03 32.5 1 2 2 1739.03 33.4 2 -2 2 6.2 3.4 2 -2 2 9.3 2.7 -2 -2 -2 10.5 2.6 2 -2 2 5.6 2.1 2 -2 2 9.5 2.2 -2 2 -2 7.4 3 -2 2 -2 8.2 2 -2 2 -2 7.5 2.4 2 2 2 8.5 2.6 3 -2 2 54.09 4.8 3 -2 2 61.79 10 3 -2 2 55.99 6.6 3 -2 2 71.69 7.1 -3 -2 -2 60.89 5.8 -3 2 -2 50.69 4.1 3 2 2 50.79 6.3 -3 2 -2 44.5 7.5 -3 2 -2 53.79 6 4 -2 2 2014.7 48.9 -4 -2 -2 2037.7 41.4 4 -2 2 2048.2 38.8 4 -2 2 2121.29 55.69 -4 -2 -2 2019.5 30 4 2 2 2028 48.6 -4 2 -2 2060.59 51.69 -4 2 -2 2064.59 34.3 4 2 2 2032.6 32.7 -4 2 -2 2052.39 46.2 -5 -2 -2 58.69 6.8 5 -2 2 56.19 12.6 -5 -2 -2 45.8 4.4 5 -2 2 50.99 6.3 5 -2 2 46.1 8.9 -5 2 -2 57.59 5.8 -5 2 -2 40.8 8.5 5 2 2 51.89 9.5 5 2 2 44.6 5.4 5 2 2 38.9 8 -5 2 -2 36.8 6.9 6 -2 2 -4.2 1.6 -6 -2 -2 -0.1 2 6 -2 2 1.7 3.1 6 -2 2 -0.5 3.9 -6 -2 -2 0.4 1.2 6 2 2 -0.5 2.1 6 2 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