#------------------------------------------------------------------------------ #$Date: 2025-09-04 17:45:02 +0300 (Thu, 04 Sep 2025) $ #$Revision: 302012 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/95/4519503.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519503 _cell_angle_alpha 90.000 _cell_angle_beta 102.430 _cell_angle_gamma 90.000 _cell_length_a 18.4448 _cell_length_b 7.9586 _cell_length_c 11.9812 _exptl_crystal_F_000 841.12 _reflns_d_resolution_high 0.7833 _cod_data_source_file 09-1b_1d_069RZ2F_031TZ_jw27321.fcf _cod_data_source_block jw27321 _shelx_title ' jw27321 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 118.26 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 5 0 0 2677.67 3184.43 134.69 o 6 0 0 3466.23 3808.94 161.01 o 7 0 0 289.16 369.12 8.47 o 8 0 0 730.42 827.04 18.83 o 9 0 0 301.02 317.30 8.07 o 10 0 0 736.07 1161.28 44.57 o 11 0 0 479.50 448.88 8.03 o 13 0 0 963.78 863.05 15.30 o 14 0 0 472.86 511.41 9.20 o 15 0 0 424.88 477.14 9.61 o 16 0 0 267.59 203.00 4.28 o 17 0 0 16.32 19.16 0.72 o 18 0 0 21.12 23.49 0.80 o 19 0 0 241.49 263.38 7.76 o 20 0 0 16.92 17.65 0.80 o 21 0 0 283.06 288.58 7.30 o 22 0 0 174.23 155.62 4.74 o 1 1 0 699.43 170.87 9.21 o 4 1 0 32.40 51.37 1.00 o 5 1 0 596.37 584.19 8.71 o 6 1 0 515.67 589.15 8.37 o 8 1 0 2417.73 2759.30 75.25 o 9 1 0 1510.12 1581.39 62.18 o 10 1 0 648.43 911.16 13.62 o 11 1 0 1189.00 1246.30 21.98 o 12 1 0 1.23 1.78 0.18 o 13 1 0 139.43 116.00 1.68 o 14 1 0 464.63 420.84 5.74 o 15 1 0 642.99 676.69 9.01 o 16 1 0 570.76 493.97 7.03 o 17 1 0 310.28 326.84 5.46 o 18 1 0 112.32 106.92 1.83 o 19 1 0 33.87 30.06 0.78 o 20 1 0 165.98 170.47 3.00 o 21 1 0 96.51 98.56 2.02 o 22 1 0 12.88 13.82 0.91 o 1 2 0 867.41 494.51 9.75 o 3 2 0 273.65 502.59 7.50 o 4 2 0 669.94 803.72 22.27 o 5 2 0 385.02 350.00 4.90 o 6 2 0 281.05 285.31 4.69 o 7 2 0 1845.19 1657.14 64.92 o 8 2 0 577.17 662.85 11.48 o 9 2 0 451.55 442.85 6.70 o 10 2 0 413.55 431.74 6.56 o 11 2 0 0.91 3.67 0.22 o 12 2 0 9.56 22.78 0.68 o 13 2 0 8.91 8.72 0.33 o 14 2 0 1468.83 1416.77 19.76 o 15 2 0 803.10 754.52 10.63 o 16 2 0 8.08 9.95 0.38 o 17 2 0 23.84 23.93 0.62 o 18 2 0 51.85 58.02 1.11 o 19 2 0 125.75 134.81 2.44 o 20 2 0 13.44 12.70 0.74 o 21 2 0 1.58 1.07 0.34 o 22 2 0 3.70 4.11 0.59 o 1 3 0 1326.02 1335.27 52.33 o 2 3 0 1656.62 1546.47 30.42 o 3 3 0 591.74 596.58 12.18 o 4 3 0 1640.75 1891.49 49.18 o 5 3 0 146.70 151.53 2.37 o 6 3 0 1773.41 2220.16 153.26 o 7 3 0 144.97 173.90 2.41 o 8 3 0 96.22 119.83 1.70 o 9 3 0 206.97 188.95 2.60 o 10 3 0 17.87 17.14 0.42 o 11 3 0 199.81 194.62 2.72 o 12 3 0 0.32 3.19 0.34 o 13 3 0 1884.65 1815.68 32.84 o 14 3 0 318.06 302.20 5.05 o 15 3 0 506.54 537.06 9.68 o 16 3 0 24.97 18.80 0.66 o 17 3 0 61.10 59.90 1.25 o 18 3 0 45.03 42.42 0.98 o 19 3 0 18.74 23.88 0.69 o 20 3 0 6.19 10.05 0.53 o 21 3 0 3.88 1.89 0.40 o 0 4 0 140.36 203.38 4.72 o 1 4 0 1187.02 1146.94 21.06 o 2 4 0 47.26 27.16 0.88 o 3 4 0 745.85 794.85 21.18 o 4 4 0 2000.13 1658.91 48.84 o 5 4 0 3201.63 3156.00 135.82 o 6 4 0 1.11 18.72 0.46 o 7 4 0 908.60 772.48 11.63 o 8 4 0 1161.60 1308.36 21.13 o 9 4 0 94.49 118.58 1.85 o 10 4 0 15.45 23.86 0.68 o 11 4 0 137.08 148.94 2.63 o 12 4 0 228.11 224.64 3.87 o 13 4 0 178.77 170.47 3.02 o 14 4 0 92.23 88.73 1.71 o 15 4 0 329.13 331.49 5.58 o 16 4 0 4.54 6.72 0.42 o 17 4 0 168.75 171.82 3.02 o 18 4 0 1.51 4.04 0.40 o 19 4 0 41.24 42.56 1.18 o 20 4 0 17.07 22.44 1.08 o 21 4 0 89.44 86.22 2.99 o 1 5 0 145.14 174.95 6.76 o 2 5 0 1.61 6.82 0.47 o 4 5 0 44.40 83.64 1.65 o 5 5 0 0.23 3.85 0.25 o 6 5 0 702.40 606.38 9.17 o 7 5 0 1403.04 1432.76 23.19 o 8 5 0 201.70 173.41 3.32 o 9 5 0 50.73 63.67 1.29 o 10 5 0 1.59 7.63 0.42 o 11 5 0 1.36 0.49 0.30 o 12 5 0 19.87 13.80 0.61 o 13 5 0 2.64 4.94 0.67 o 14 5 0 18.82 13.08 0.57 o 15 5 0 262.01 248.15 4.65 o 16 5 0 140.78 154.08 2.99 o 17 5 0 0.03 0.10 0.33 o 18 5 0 195.67 197.61 5.88 o 19 5 0 125.94 119.69 3.71 o 1 6 0 890.96 916.84 21.07 o 2 6 0 225.78 250.79 6.03 o 3 6 0 975.31 970.70 17.14 o 4 6 0 97.77 94.14 2.71 o 5 6 0 10.76 6.35 0.46 o 6 6 0 285.11 299.82 5.44 o 7 6 0 91.17 85.40 1.63 o 8 6 0 11.44 8.69 0.47 o 9 6 0 195.08 219.98 4.14 o 10 6 0 325.78 303.36 6.28 o 11 6 0 352.90 328.54 6.07 o 12 6 0 15.06 14.63 0.87 o 13 6 0 4.93 6.18 0.45 o 14 6 0 355.04 365.46 6.67 o 15 6 0 222.59 225.50 5.21 o 16 6 0 49.72 42.21 1.33 o 17 6 0 75.80 72.84 2.44 o 18 6 0 86.85 99.32 8.88 o 1 7 0 931.58 886.19 17.66 o 2 7 0 16.89 7.40 0.85 o 3 7 0 15.10 13.60 0.77 o 4 7 0 521.95 552.20 16.26 o 5 7 0 3.13 2.48 0.39 o 6 7 0 94.79 96.53 2.78 o 7 7 0 268.21 283.00 6.88 o 8 7 0 704.59 642.72 13.24 o 9 7 0 248.94 263.24 4.89 o 10 7 0 4.24 3.07 0.38 o 11 7 0 165.36 155.92 3.04 o 12 7 0 597.24 589.59 10.57 o 13 7 0 34.03 36.32 1.02 o 14 7 0 96.25 108.75 5.31 o 15 7 0 60.90 57.19 2.05 o 16 7 0 0.45 1.13 0.81 o 0 8 0 31.42 25.92 1.28 o 1 8 0 79.33 72.14 1.82 o 2 8 0 35.20 45.18 1.15 o 3 8 0 226.29 216.20 4.12 o 4 8 0 318.99 331.66 6.90 o 5 8 0 61.75 63.24 1.69 o 6 8 0 41.66 50.06 2.75 o 7 8 0 105.69 101.88 2.89 o 8 8 0 506.31 508.43 11.90 o 9 8 0 266.06 281.40 6.78 o 10 8 0 366.65 360.35 11.48 o 11 8 0 2.41 2.26 0.97 o 12 8 0 21.12 17.93 1.61 o 14 8 0 91.30 83.98 3.88 o 1 9 0 11.37 12.74 0.77 o 2 9 0 181.56 174.41 3.85 o 3 9 0 264.69 245.39 5.24 o 4 9 0 139.65 152.55 3.44 o 5 9 0 258.77 249.36 13.40 o 6 9 0 656.43 665.39 13.42 o 7 9 0 181.20 183.55 5.54 o 8 9 0 0.30 1.06 0.50 o 9 9 0 64.59 77.48 2.74 o 10 9 0 42.79 47.32 2.42 o -23 1 1 19.89 21.08 1.14 o -22 1 1 53.15 53.47 1.58 o -21 1 1 91.31 93.41 1.92 o -20 1 1 6.64 5.30 0.45 o -19 1 1 153.29 130.32 2.36 o -18 1 1 471.35 513.29 7.81 o -17 1 1 288.52 317.68 6.02 o -16 1 1 1012.22 851.16 11.98 o -15 1 1 18.43 35.40 0.77 o -14 1 1 147.13 172.89 2.33 o -13 1 1 1211.13 1152.24 16.11 o -12 1 1 447.77 397.03 6.04 o -11 1 1 467.63 494.48 7.45 o -10 1 1 403.85 481.75 7.25 o -9 1 1 2657.85 3139.95 72.57 o -8 1 1 86.35 47.53 0.79 o -7 1 1 2591.08 2522.94 59.90 o -6 1 1 1897.43 2269.83 54.68 o -5 1 1 57.59 23.94 0.46 o -4 1 1 442.76 309.98 5.02 o -3 1 1 23.82 60.78 1.13 o -2 1 1 426.56 558.86 10.98 o 3 1 1 1354.62 1977.49 93.51 o 4 1 1 839.38 1230.22 34.25 o 5 1 1 47.49 2.78 0.25 o 6 1 1 3347.43 5427.16 159.64 o 7 1 1 652.65 977.07 38.76 o 8 1 1 981.51 826.63 12.32 o 9 1 1 2978.02 3108.18 65.63 o 10 1 1 1467.23 1572.04 43.79 o 11 1 1 0.52 3.80 0.22 o 12 1 1 469.75 480.41 6.81 o 13 1 1 1922.23 1836.71 50.99 o 14 1 1 665.51 649.35 9.15 o 15 1 1 546.53 499.76 7.09 o 16 1 1 90.43 104.45 1.66 o 17 1 1 117.57 130.99 2.02 o 18 1 1 2.10 1.10 0.23 o 19 1 1 26.20 15.85 0.52 o 20 1 1 58.77 63.80 1.52 o 21 1 1 1.62 2.79 0.41 o 22 1 1 207.82 200.42 6.55 o -22 2 1 2.61 3.61 0.58 o -21 2 1 205.85 213.87 5.19 o -20 2 1 29.51 25.77 0.87 o -19 2 1 189.26 200.15 3.39 o -18 2 1 395.00 358.10 5.17 o -17 2 1 268.33 265.07 3.87 o -16 2 1 16.27 17.70 0.48 o -15 2 1 271.08 268.71 3.72 o -14 2 1 6.88 4.05 0.27 o -13 2 1 741.40 651.85 9.84 o -12 2 1 198.50 281.93 4.07 o -11 2 1 2244.15 2152.99 59.67 o -10 2 1 307.45 598.83 9.71 o -9 2 1 682.21 1194.09 47.64 o -8 2 1 4749.90 4656.24 223.12 o -7 2 1 3797.67 5130.93 181.52 o -6 2 1 4.67 18.07 0.70 o -5 2 1 63.79 133.41 2.45 o -4 2 1 2663.59 2926.19 129.04 o -3 2 1 21.50 37.41 1.46 o -2 2 1 2198.09 1.29 2.91 o 0 2 1 1757.77 746.34 26.04 o 1 2 1 115.74 144.04 3.80 o 2 2 1 2640.55 2314.60 98.35 o 3 2 1 154.93 151.32 2.52 o 6 2 1 1035.29 1087.05 24.71 o 7 2 1 93.27 118.43 1.77 o 8 2 1 27.25 22.00 0.43 o 9 2 1 201.57 230.56 2.98 o 10 2 1 379.92 388.39 5.52 o 11 2 1 139.29 129.22 1.97 o 12 2 1 144.16 139.09 2.00 o 13 2 1 660.16 638.96 9.63 o 14 2 1 6.57 20.48 0.71 o 15 2 1 18.89 11.98 0.79 o 16 2 1 58.76 63.86 1.18 o 17 2 1 63.27 48.84 0.98 o 18 2 1 26.82 27.57 0.95 o 19 2 1 15.91 17.70 0.59 o 20 2 1 20.27 19.03 0.62 o 21 2 1 32.99 38.02 1.08 o 22 2 1 36.62 43.60 2.42 o -22 3 1 3.73 2.45 0.50 o -21 3 1 73.53 74.40 1.79 o -20 3 1 95.43 79.10 2.02 o -19 3 1 23.18 25.68 0.88 o -18 3 1 13.00 11.46 0.61 o -17 3 1 8.26 7.76 0.47 o -16 3 1 19.71 21.55 0.57 o -15 3 1 1075.33 1024.31 14.39 o -14 3 1 2740.69 2589.51 58.92 o -13 3 1 583.63 559.05 7.48 o -12 3 1 1.48 3.10 0.40 o -11 3 1 2366.92 2143.50 64.60 o -10 3 1 527.64 597.85 8.44 o -9 3 1 0.19 2.28 0.19 o -8 3 1 33.78 50.50 0.82 o -7 3 1 180.24 191.49 3.00 o -6 3 1 74.51 68.31 1.09 o -5 3 1 23.44 17.48 0.43 o -4 3 1 9.13 37.09 2.03 o -3 3 1 3703.50 3176.84 134.69 o -2 3 1 1882.59 1757.56 39.14 o -1 3 1 267.12 171.03 2.83 o 0 3 1 400.29 424.61 7.54 o 1 3 1 1319.60 1168.60 46.03 o 2 3 1 230.20 265.23 6.18 o 3 3 1 360.66 288.95 5.81 o 4 3 1 902.44 1075.26 42.64 o 5 3 1 3169.77 3156.06 163.78 o 6 3 1 163.97 180.72 3.34 o 7 3 1 541.47 542.99 8.20 o 9 3 1 1635.52 1495.88 26.33 o 10 3 1 207.58 148.08 1.99 o 11 3 1 407.90 487.65 6.54 o 12 3 1 110.51 156.43 2.52 o 13 3 1 66.30 36.76 0.78 o 14 3 1 787.69 722.33 11.79 o 15 3 1 36.41 36.49 1.20 o 16 3 1 85.36 88.79 1.71 o 17 3 1 184.86 183.82 3.22 o 18 3 1 115.37 115.92 2.12 o 19 3 1 104.29 108.51 3.57 o 20 3 1 390.86 363.09 6.62 o 21 3 1 146.94 156.54 4.90 o -21 4 1 56.18 55.62 1.93 o -20 4 1 0.77 1.44 0.50 o -19 4 1 7.11 6.40 0.50 o -18 4 1 16.23 18.43 0.84 o -17 4 1 0.92 1.51 0.43 o -16 4 1 3.68 3.20 0.39 o -15 4 1 87.81 87.61 1.69 o -14 4 1 426.79 400.27 6.19 o -13 4 1 21.50 21.35 1.01 o -12 4 1 1901.18 1835.55 36.28 o -11 4 1 666.48 586.59 8.92 o -10 4 1 935.24 926.08 13.93 o -9 4 1 250.99 282.27 4.14 o -8 4 1 122.09 124.08 2.08 o -7 4 1 568.66 569.62 10.12 o -6 4 1 1317.55 1339.28 32.74 o -5 4 1 2925.13 2842.86 123.55 o -4 4 1 1400.09 1498.22 58.79 o -3 4 1 4282.50 3924.76 119.11 o -2 4 1 32.76 50.52 0.85 o -1 4 1 485.53 447.02 7.96 o 0 4 1 675.75 647.79 14.86 o 1 4 1 1201.73 1238.09 47.08 o 2 4 1 241.90 263.30 5.32 o 3 4 1 463.28 538.65 9.56 o 4 4 1 347.42 380.97 8.37 o 5 4 1 1631.31 1590.92 62.98 o 6 4 1 956.61 907.89 14.66 o 8 4 1 1.99 4.35 0.29 o 9 4 1 540.69 551.70 8.34 o 10 4 1 564.39 541.36 8.21 o 11 4 1 348.66 355.03 5.93 o 12 4 1 435.02 468.73 8.49 o 13 4 1 531.38 462.82 7.67 o 14 4 1 153.72 148.31 2.91 o 15 4 1 13.52 7.74 0.50 o 16 4 1 340.54 365.07 6.12 o 17 4 1 63.44 52.18 1.35 o 18 4 1 156.13 154.31 4.08 o 19 4 1 418.48 396.56 8.05 o 20 4 1 42.43 45.23 3.80 o -20 5 1 3.15 3.40 0.57 o -19 5 1 56.61 53.19 1.93 o -18 5 1 113.16 116.74 2.98 o -17 5 1 0.55 2.00 0.40 o -16 5 1 306.07 276.30 5.71 o -15 5 1 393.72 400.40 7.26 o -14 5 1 206.32 196.90 3.72 o -13 5 1 317.65 332.35 6.84 o -12 5 1 242.66 281.24 4.78 o -11 5 1 366.11 319.24 6.30 o -10 5 1 658.47 582.39 9.58 o -9 5 1 912.93 903.16 13.62 o -8 5 1 235.17 208.87 3.63 o -7 5 1 483.46 443.92 11.23 o -6 5 1 2167.95 2222.06 87.05 o -5 5 1 256.12 247.93 3.86 o -4 5 1 41.66 52.19 1.05 o -3 5 1 359.82 395.08 8.25 o -2 5 1 2.59 1.90 0.14 o -1 5 1 124.20 126.39 2.33 o 0 5 1 1546.18 1600.38 49.74 o 1 5 1 81.83 64.12 1.29 o 2 5 1 918.42 1143.54 22.55 o 3 5 1 12.98 13.88 0.45 o 5 5 1 8.27 4.18 0.35 o 6 5 1 692.85 824.29 13.37 o 7 5 1 358.39 352.55 5.86 o 8 5 1 182.50 192.88 3.59 o 9 5 1 2.00 5.45 0.51 o 10 5 1 471.33 436.26 7.94 o 11 5 1 20.18 14.06 0.68 o 12 5 1 2897.35 2883.88 113.53 o 13 5 1 657.49 593.26 10.69 o 14 5 1 0.43 0.94 0.33 o 15 5 1 266.74 269.14 5.56 o 16 5 1 48.28 42.00 1.05 o 17 5 1 1.00 2.85 0.41 o 18 5 1 4.21 8.69 0.60 o 19 5 1 19.53 13.40 1.61 o -18 6 1 15.52 23.74 1.61 o -17 6 1 245.80 210.72 8.65 o -16 6 1 42.01 38.96 1.30 o -15 6 1 164.70 175.98 4.35 o -14 6 1 79.26 72.42 1.88 o -13 6 1 398.59 404.39 7.35 o -12 6 1 5.04 4.89 0.39 o -11 6 1 304.25 298.43 6.20 o -10 6 1 31.06 39.16 0.97 o -9 6 1 204.74 237.88 4.09 o -8 6 1 918.33 798.81 14.28 o -7 6 1 621.60 655.79 11.74 o -6 6 1 116.36 93.20 1.76 o -5 6 1 212.72 171.03 2.96 o -4 6 1 223.42 253.97 8.65 o -3 6 1 195.38 244.09 7.25 o -2 6 1 176.29 216.93 5.28 o -1 6 1 159.44 163.75 4.07 o 1 6 1 533.69 500.23 11.65 o 2 6 1 906.42 1016.31 18.15 o 3 6 1 13.04 8.41 0.38 o 4 6 1 506.49 466.42 7.68 o 5 6 1 667.27 684.81 11.16 o 6 6 1 3.71 10.27 0.43 o 7 6 1 3.86 7.11 0.54 o 8 6 1 21.47 40.66 0.99 o 9 6 1 102.95 98.43 2.03 o 10 6 1 246.18 220.65 4.23 o 11 6 1 257.75 273.00 5.10 o 12 6 1 292.85 308.59 5.72 o 13 6 1 329.98 355.41 7.34 o 14 6 1 327.20 303.79 5.60 o 15 6 1 6.08 7.20 0.61 o 16 6 1 99.98 108.81 2.42 o 17 6 1 48.46 47.66 1.78 o -16 7 1 31.50 36.66 2.42 o -15 7 1 19.86 25.58 2.18 o -14 7 1 48.53 47.73 2.61 o -13 7 1 42.50 40.70 1.37 o -12 7 1 26.42 29.28 1.00 o -11 7 1 102.40 112.54 2.82 o -10 7 1 1.46 1.36 0.33 o -9 7 1 58.00 63.99 1.80 o -8 7 1 0.77 3.94 0.51 o -7 7 1 117.86 123.65 3.36 o -6 7 1 34.48 34.44 1.34 o -5 7 1 1.30 4.13 0.52 o -4 7 1 6.62 7.41 0.56 o -3 7 1 20.66 22.56 1.28 o -2 7 1 161.15 175.23 3.77 o -1 7 1 36.79 41.38 1.18 o 0 7 1 3.66 5.70 0.46 o 1 7 1 349.84 349.37 8.36 o 2 7 1 146.03 145.71 3.72 o 3 7 1 19.34 19.37 0.98 o 4 7 1 8.45 11.56 0.61 o 5 7 1 58.00 62.21 1.63 o 6 7 1 57.50 64.67 1.64 o 7 7 1 21.70 17.40 0.64 o 8 7 1 42.26 43.41 1.25 o 9 7 1 3.40 2.31 0.33 o 10 7 1 116.29 122.96 4.12 o 11 7 1 22.96 24.91 0.79 o 12 7 1 6.42 9.10 0.77 o 13 7 1 17.02 17.13 0.70 o 14 7 1 0.10 0.68 0.50 o 15 7 1 0.29 1.45 0.57 o 16 7 1 0.16 0.81 0.81 o -14 8 1 32.37 38.11 2.10 o -13 8 1 27.40 30.36 1.94 o -12 8 1 5.80 6.19 0.74 o -11 8 1 161.70 203.28 6.86 o -10 8 1 202.42 197.85 8.07 o -9 8 1 117.62 128.66 4.48 o -8 8 1 58.32 77.56 2.60 o -7 8 1 289.91 263.03 5.72 o -6 8 1 34.24 29.82 1.37 o -5 8 1 141.46 143.52 3.26 o -4 8 1 153.83 169.98 4.13 o -3 8 1 28.42 40.58 1.25 o -2 8 1 76.47 69.89 1.76 o -1 8 1 129.21 112.63 2.62 o 0 8 1 60.46 59.18 1.58 o 1 8 1 464.25 463.29 9.45 o 2 8 1 689.72 686.14 12.35 o 3 8 1 0.16 0.68 0.30 o 4 8 1 508.33 492.55 10.07 o 5 8 1 246.72 248.50 10.33 o 6 8 1 28.48 22.29 1.19 o 7 8 1 166.06 160.84 5.08 o 8 8 1 32.49 33.09 1.27 o 9 8 1 30.64 28.51 1.23 o 10 8 1 18.22 18.19 1.17 o 11 8 1 347.39 347.67 10.11 o 12 8 1 124.35 119.67 5.49 o 13 8 1 48.33 52.97 2.91 o -10 9 1 8.52 10.50 1.13 o -9 9 1 0.30 0.26 0.54 o -8 9 1 0.04 0.32 0.54 o -7 9 1 6.66 9.78 1.05 o -6 9 1 8.06 8.72 0.74 o -5 9 1 0.46 0.30 0.45 o -4 9 1 21.58 24.19 0.99 o -3 9 1 89.03 88.03 2.18 o -2 9 1 91.27 84.63 2.08 o -1 9 1 165.92 173.64 3.83 o 0 9 1 236.13 201.33 3.81 o 1 9 1 9.95 7.31 0.56 o 2 9 1 20.27 23.07 0.98 o 3 9 1 33.24 41.19 1.27 o 4 9 1 317.28 301.52 7.21 o 5 9 1 148.10 157.27 4.99 o 6 9 1 38.31 33.93 1.29 o 7 9 1 37.37 40.84 2.51 o 8 9 1 138.07 147.02 4.51 o 9 9 1 38.32 49.51 1.88 o -23 0 2 26.06 24.39 1.94 o -22 0 2 88.48 83.54 2.80 o -21 0 2 27.24 22.60 1.05 o -20 0 2 21.65 14.62 0.86 o -19 0 2 29.54 12.47 0.70 o -18 0 2 20.67 15.69 0.77 o -17 0 2 355.56 357.97 10.60 o -16 0 2 2803.24 2884.85 113.69 o -15 0 2 2307.05 2112.40 83.49 o -14 0 2 164.98 199.49 4.18 o -13 0 2 449.99 512.12 10.25 o -12 0 2 886.99 917.71 21.00 o -11 0 2 146.87 202.80 4.18 o -10 0 2 1738.75 2110.24 88.58 o -9 0 2 946.16 1114.85 53.60 o -8 0 2 304.07 364.71 8.85 o -7 0 2 235.47 238.40 4.80 o -5 0 2 675.29 967.63 24.29 o -4 0 2 273.61 227.56 6.45 o -2 0 2 644.26 574.93 22.61 o 0 0 2 129.78 150.24 4.23 o 1 0 2 743.75 560.79 20.01 o 2 0 2 398.25 475.82 10.88 o 3 0 2 2050.93 2118.21 198.97 o 4 0 2 3152.65 2513.24 108.69 o 7 0 2 3684.85 4159.21 128.68 o 8 0 2 2254.09 3245.14 106.07 o 9 0 2 13984.80 16142.76 461.81 o 10 0 2 239.68 331.69 6.68 o 11 0 2 802.16 841.41 19.24 o 12 0 2 39.71 44.14 1.34 o 13 0 2 774.78 708.98 14.09 o 14 0 2 1843.45 1780.47 40.47 o 15 0 2 25.49 48.47 1.26 o 16 0 2 522.05 415.48 11.82 o 17 0 2 57.77 68.34 1.63 o 18 0 2 236.75 282.97 5.83 o 19 0 2 253.55 212.92 4.46 o 20 0 2 26.40 30.39 1.63 o 21 0 2 50.17 62.58 2.22 o -23 1 2 85.04 68.02 3.05 o -22 1 2 34.76 40.40 1.30 o -21 1 2 71.19 74.94 1.62 o -20 1 2 0.04 0.94 0.25 o -19 1 2 3.95 3.88 0.39 o -18 1 2 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