#------------------------------------------------------------------------------ #$Date: 2025-09-04 17:45:24 +0300 (Thu, 04 Sep 2025) $ #$Revision: 302014 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/95/4519505.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519505 _cell_angle_alpha 90.000 _cell_angle_beta 93.236 _cell_angle_gamma 90.000 _cell_length_a 18.3022 _cell_length_b 4.0961 _cell_length_c 11.4591 _exptl_crystal_F_000 420.40 _reflns_d_resolution_high 0.8196 _cod_data_source_file 11-1b_1c_038RZ2F_062RZ1F_jw27511.fcf _cod_data_source_block jw27511 _shelx_title ' jw27511_a.res in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 113.35 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 35.52 31.07 1.01 o 3 0 0 1236.81 1271.47 31.09 o 4 0 0 1090.52 1026.55 26.36 o 5 0 0 153.14 171.35 4.08 o 6 0 0 110.22 120.14 3.23 o 7 0 0 4531.30 4026.74 91.91 o 8 0 0 41.54 60.95 1.96 o 9 0 0 474.96 536.32 11.32 o 10 0 0 1294.56 1404.53 27.66 o 11 0 0 684.86 641.31 13.49 o 12 0 0 75.75 75.77 1.93 o 13 0 0 0.78 0.89 0.73 o 14 0 0 732.73 739.26 16.72 o 15 0 0 92.90 89.09 3.10 o 16 0 0 18.12 17.08 1.66 o 17 0 0 9.90 10.19 1.47 o 18 0 0 0.24 0.06 1.12 o 19 0 0 22.50 26.57 2.02 o 20 0 0 0.59 -0.75 0.88 o 21 0 0 17.86 16.61 1.69 o 22 0 0 20.94 23.92 1.75 o 1 1 0 1107.09 1002.73 15.36 o 2 1 0 3503.85 3330.87 49.44 o 3 1 0 2658.47 2634.01 36.30 o 4 1 0 294.14 259.46 4.13 o 5 1 0 129.72 128.12 2.04 o 6 1 0 1520.68 1457.54 21.72 o 7 1 0 49.43 46.70 0.93 o 8 1 0 182.55 209.70 3.14 o 9 1 0 275.30 232.66 3.86 o 10 1 0 44.22 36.70 0.90 o 11 1 0 137.48 132.46 2.16 o 12 1 0 0.36 1.10 0.53 o 13 1 0 397.75 397.08 6.89 o 14 1 0 89.33 89.96 2.18 o 15 1 0 62.89 64.30 1.86 o 16 1 0 181.81 181.14 3.89 o 17 1 0 140.68 140.31 3.26 o 18 1 0 4.39 4.46 0.83 o 19 1 0 0.95 1.06 0.78 o 20 1 0 18.92 25.02 1.69 o 21 1 0 3.27 2.28 1.07 o 0 2 0 159.52 184.45 4.19 o 1 2 0 1038.94 912.01 13.06 o 2 2 0 3.14 3.37 0.35 o 3 2 0 4.72 3.50 0.38 o 4 2 0 184.58 221.20 3.32 o 5 2 0 2.75 4.92 0.41 o 6 2 0 173.78 149.79 2.35 o 7 2 0 285.86 252.16 3.81 o 8 2 0 324.72 319.15 4.81 o 9 2 0 17.62 15.09 0.71 o 10 2 0 104.22 95.65 2.10 o 11 2 0 65.70 65.82 1.75 o 12 2 0 113.98 106.03 2.59 o 13 2 0 169.30 149.77 4.91 o 14 2 0 445.82 452.03 10.42 o 15 2 0 99.98 103.01 3.39 o 16 2 0 12.79 11.25 1.10 o 17 2 0 0.42 0.50 0.85 o 18 2 0 25.76 23.06 1.40 o 19 2 0 4.69 4.11 0.91 o 20 2 0 1.10 1.57 0.91 o 1 3 0 1.59 1.02 0.43 o 2 3 0 9.53 10.52 0.73 o 3 3 0 75.76 74.47 2.06 o 4 3 0 1.32 0.42 0.49 o 5 3 0 101.67 105.39 2.08 o 6 3 0 0.04 0.88 0.52 o 7 3 0 1.13 2.01 0.53 o 8 3 0 36.90 33.51 1.43 o 9 3 0 24.88 22.25 1.11 o 10 3 0 1.98 0.32 0.54 o 11 3 0 22.54 13.79 1.05 o 12 3 0 41.89 48.20 2.74 o 13 3 0 12.25 12.60 1.15 o 14 3 0 1.18 0.31 0.86 o 15 3 0 0.10 -1.52 2.01 o 16 3 0 12.03 6.62 1.92 o 17 3 0 4.73 0.34 1.04 o 0 4 0 1.70 2.23 0.72 o 1 4 0 16.68 18.32 0.89 o 2 4 0 15.33 14.23 0.88 o 3 4 0 1.18 1.46 0.56 o 4 4 0 7.31 6.05 0.67 o 5 4 0 0.01 0.48 0.61 o 6 4 0 22.63 25.29 1.13 o 7 4 0 2.27 2.03 0.75 o 8 4 0 0.26 -0.18 0.62 o 9 4 0 0.31 1.08 0.63 o 10 4 0 0.74 -0.12 0.74 o 11 4 0 9.13 7.02 1.40 o 12 4 0 31.17 45.46 2.60 o 13 4 0 2.63 2.08 0.87 o -21 1 1 3.02 2.88 1.05 o -20 1 1 1.61 1.03 0.81 o -19 1 1 13.64 14.27 1.33 o -18 1 1 67.54 64.74 2.98 o -17 1 1 7.31 8.53 1.08 o -16 1 1 0.74 -0.54 0.61 o -15 1 1 23.72 19.57 1.35 o -14 1 1 68.18 79.02 2.02 o -13 1 1 38.65 37.30 1.36 o -12 1 1 15.02 10.53 0.64 o -11 1 1 55.75 44.02 1.06 o -10 1 1 533.98 563.57 8.05 o -9 1 1 1046.10 954.97 12.56 o -8 1 1 324.70 280.92 3.72 o -7 1 1 93.10 117.61 1.77 o -6 1 1 188.41 195.88 3.01 o -5 1 1 1378.75 1313.74 19.12 o -4 1 1 21.19 11.99 0.48 o -3 1 1 633.44 535.74 9.43 o -2 1 1 772.03 639.74 11.20 o -1 1 1 1330.92 1288.04 22.37 o 0 1 1 12848.31 11641.16 433.96 o 1 1 1 723.63 793.89 12.96 o 2 1 1 3423.34 3207.06 50.30 o 3 1 1 152.57 111.97 1.83 o 4 1 1 691.06 670.79 9.59 o 5 1 1 657.12 517.94 8.29 o 6 1 1 1.72 6.21 0.37 o 7 1 1 33.69 32.97 0.75 o 8 1 1 69.48 94.13 1.64 o 9 1 1 978.26 950.71 13.65 o 10 1 1 668.21 618.43 9.03 o 11 1 1 26.81 15.04 0.69 o 12 1 1 356.42 352.47 4.96 o 13 1 1 17.30 18.50 0.94 o 14 1 1 38.62 37.46 1.45 o 15 1 1 1.40 0.45 0.64 o 16 1 1 26.50 27.30 1.12 o 17 1 1 11.16 12.04 0.86 o 18 1 1 8.12 4.11 0.90 o 19 1 1 3.51 3.65 0.87 o 20 1 1 4.23 2.89 0.89 o 21 1 1 0.25 0.87 0.95 o -20 2 1 0.21 -0.91 0.92 o -19 2 1 18.99 15.03 1.91 o -18 2 1 3.47 3.44 0.89 o -17 2 1 0.82 0.60 0.84 o -16 2 1 0.29 1.04 0.85 o -15 2 1 35.67 34.39 2.79 o -14 2 1 4.97 1.81 0.84 o -13 2 1 42.17 38.84 2.08 o -12 2 1 207.88 205.06 4.41 o -11 2 1 129.82 139.32 2.81 o -10 2 1 3.77 3.19 0.47 o -9 2 1 15.36 19.60 0.74 o -8 2 1 802.58 801.36 11.62 o -7 2 1 160.40 149.16 2.44 o -6 2 1 238.18 188.88 2.89 o -5 2 1 263.78 239.53 3.60 o -4 2 1 1170.58 1116.94 15.28 o -3 2 1 181.05 159.86 2.52 o -2 2 1 65.36 89.90 1.53 o -1 2 1 480.76 439.53 6.33 o 0 2 1 18.33 24.21 0.67 o 1 2 1 33.50 32.70 1.13 o 2 2 1 127.65 136.28 1.94 o 3 2 1 106.91 111.38 1.69 o 4 2 1 746.23 757.83 10.46 o 5 2 1 23.72 25.08 0.78 o 6 2 1 193.12 196.27 2.98 o 7 2 1 294.02 279.23 4.16 o 8 2 1 155.96 130.79 2.10 o 9 2 1 5.62 6.03 0.49 o 10 2 1 326.49 329.62 5.20 o 11 2 1 284.33 289.63 4.93 o 12 2 1 28.59 23.10 1.06 o 13 2 1 0.62 0.54 0.61 o 14 2 1 9.62 8.90 0.91 o 15 2 1 77.26 84.21 2.41 o 16 2 1 19.87 15.98 1.04 o 17 2 1 1.09 -0.17 0.86 o 18 2 1 52.45 60.29 3.11 o 19 2 1 3.78 2.95 0.93 o 20 2 1 0.43 0.06 1.51 o -17 3 1 8.48 7.01 1.49 o -16 3 1 1.48 0.62 1.29 o -15 3 1 0.14 -0.13 0.93 o -14 3 1 33.99 26.35 2.88 o -13 3 1 0.35 1.43 1.02 o -12 3 1 137.66 147.05 4.87 o -11 3 1 1.45 1.44 0.82 o -10 3 1 142.28 163.41 3.95 o -9 3 1 150.21 143.58 3.11 o -8 3 1 9.04 13.89 0.84 o -7 3 1 63.69 58.82 1.58 o -6 3 1 452.16 427.83 8.28 o -5 3 1 201.04 207.41 3.65 o -4 3 1 105.79 110.17 2.34 o -3 3 1 217.84 243.52 4.46 o -2 3 1 108.78 102.42 2.30 o -1 3 1 41.30 33.84 1.10 o 0 3 1 0.13 0.41 0.40 o 1 3 1 191.70 175.94 3.21 o 2 3 1 317.27 276.36 4.63 o 3 3 1 3.01 3.60 0.62 o 4 3 1 395.14 402.73 7.80 o 5 3 1 483.08 444.51 8.06 o 6 3 1 43.62 49.41 1.48 o 7 3 1 0.29 0.44 0.52 o 8 3 1 108.71 108.72 3.60 o 9 3 1 176.55 176.40 4.42 o 10 3 1 91.87 92.11 2.50 o 11 3 1 3.20 2.21 0.67 o 12 3 1 7.49 5.67 1.05 o 13 3 1 61.49 55.65 2.86 o 14 3 1 103.51 100.76 3.87 o 15 3 1 0.98 1.95 1.06 o 16 3 1 7.38 5.60 1.12 o 17 3 1 5.56 4.89 1.35 o -13 4 1 7.29 3.69 1.42 o -12 4 1 25.02 14.26 1.90 o -11 4 1 7.86 7.41 1.03 o -10 4 1 3.37 4.02 0.89 o -9 4 1 9.94 11.96 1.06 o -8 4 1 55.51 57.11 2.61 o -7 4 1 44.73 45.30 1.91 o -6 4 1 1.70 1.65 0.64 o -5 4 1 17.62 22.08 1.27 o -4 4 1 93.22 83.80 2.16 o -3 4 1 127.09 145.94 3.00 o -2 4 1 0.16 0.68 0.50 o -1 4 1 44.35 37.97 1.22 o 0 4 1 27.52 22.77 1.05 o 1 4 1 7.38 10.07 0.79 o 2 4 1 10.79 15.63 0.92 o 3 4 1 34.34 34.09 1.31 o 4 4 1 65.22 74.86 2.16 o 5 4 1 10.58 10.98 1.11 o 6 4 1 61.16 61.59 2.90 o 7 4 1 116.69 96.42 3.91 o 8 4 1 48.15 52.81 3.03 o 9 4 1 3.89 2.46 0.68 o 10 4 1 59.42 47.80 3.80 o 11 4 1 65.93 85.35 3.82 o 12 4 1 7.89 14.00 1.51 o 13 4 1 6.39 4.22 1.00 o -22 0 2 1.24 2.61 1.15 o -21 0 2 21.98 20.75 3.22 o -20 0 2 21.45 28.97 1.90 o -19 0 2 0.35 1.33 1.78 o -18 0 2 95.61 104.63 3.88 o -17 0 2 32.63 31.97 2.60 o -16 0 2 585.01 576.19 16.34 o -15 0 2 226.92 238.43 7.57 o -14 0 2 532.16 554.64 13.56 o -13 0 2 156.32 143.07 3.82 o -12 0 2 65.94 51.42 1.87 o -11 0 2 451.02 418.90 9.23 o -10 0 2 1217.84 1065.14 23.44 o -9 0 2 128.22 213.92 4.86 o -8 0 2 1323.05 1364.63 31.59 o -7 0 2 3177.84 2855.75 61.67 o -6 0 2 205.22 203.79 4.30 o -5 0 2 112.53 108.96 2.49 o -4 0 2 1063.29 1032.83 25.43 o -3 0 2 327.02 461.19 16.70 o -2 0 2 3214.04 3203.73 78.27 o -1 0 2 7669.03 8662.70 211.12 o 0 0 2 32.12 76.15 2.08 o 1 0 2 7166.11 7459.40 196.36 o 2 0 2 1275.51 1160.68 28.66 o 3 0 2 7550.46 7963.13 194.19 o 4 0 2 154.60 185.46 3.51 o 5 0 2 149.96 155.30 3.20 o 6 0 2 235.64 309.83 5.48 o 7 0 2 4647.94 4488.19 74.93 o 8 0 2 80.89 89.08 2.09 o 9 0 2 513.27 551.03 10.37 o 10 0 2 1146.71 1106.37 24.26 o 11 0 2 227.58 214.80 4.83 o 12 0 2 49.07 56.04 1.88 o 13 0 2 12.01 15.81 1.06 o 14 0 2 1056.15 1114.82 24.65 o 15 0 2 119.96 110.42 5.15 o 16 0 2 21.36 16.69 1.53 o 17 0 2 54.49 55.93 2.41 o 18 0 2 116.94 128.61 4.21 o 19 0 2 7.31 4.27 1.08 o 20 0 2 0.01 -0.11 0.97 o 21 0 2 20.40 23.49 2.42 o -21 1 2 17.71 14.91 1.43 o -20 1 2 19.18 19.80 1.48 o -19 1 2 2.88 2.54 0.85 o -18 1 2 3.38 2.13 0.94 o -17 1 2 52.24 53.60 2.48 o -16 1 2 0.25 0.85 0.66 o -15 1 2 1.62 3.29 0.66 o -14 1 2 613.55 610.67 12.06 o -13 1 2 483.11 451.87 8.62 o -12 1 2 175.07 175.20 3.27 o -11 1 2 0.11 0.56 0.46 o -10 1 2 216.98 184.84 2.98 o -9 1 2 9.70 16.29 0.66 o -8 1 2 268.27 272.12 3.99 o -7 1 2 319.24 258.72 3.78 o -6 1 2 1408.21 1284.66 18.27 o -5 1 2 412.97 442.98 6.41 o -4 1 2 1657.43 1553.75 25.21 o -3 1 2 114.20 114.94 2.02 o -2 1 2 230.13 293.75 5.08 o -1 1 2 802.51 732.02 12.82 o 0 1 2 9544.28 9264.67 165.99 o 1 1 2 11556.41 11173.89 240.45 o 2 1 2 411.46 327.47 4.57 o 3 1 2 9.90 5.07 0.30 o 4 1 2 173.21 251.76 3.65 o 5 1 2 313.46 246.44 3.67 o 6 1 2 409.55 380.87 5.69 o 7 1 2 67.26 47.17 0.95 o 8 1 2 521.97 526.32 7.30 o 9 1 2 518.46 517.06 7.55 o 10 1 2 663.25 691.79 10.31 o 11 1 2 42.38 42.47 1.08 o 12 1 2 309.51 286.40 4.09 o 13 1 2 83.41 75.82 1.81 o 14 1 2 289.27 308.93 5.94 o 15 1 2 129.43 131.59 2.97 o 16 1 2 80.69 78.46 2.45 o 17 1 2 9.08 9.82 0.87 o 18 1 2 8.14 6.90 0.86 o 19 1 2 9.54 8.21 1.44 o 20 1 2 17.18 17.86 1.35 o 21 1 2 0.47 -0.06 0.94 o -20 2 2 0.00 -0.88 1.10 o -19 2 2 3.62 1.45 0.86 o -18 2 2 1.77 1.80 1.14 o -17 2 2 9.33 10.20 1.12 o -16 2 2 20.88 16.39 1.58 o -15 2 2 111.57 112.23 3.47 o -14 2 2 27.18 33.55 1.93 o -13 2 2 42.44 37.66 1.66 o -12 2 2 0.15 0.32 0.62 o -11 2 2 45.64 43.86 1.76 o -10 2 2 13.51 11.53 0.97 o -9 2 2 84.34 66.81 1.44 o -8 2 2 245.00 238.78 3.78 o -7 2 2 89.58 78.83 1.52 o -6 2 2 92.44 84.29 1.91 o -5 2 2 45.87 44.37 0.99 o -4 2 2 911.75 917.92 13.22 o -3 2 2 118.41 115.69 1.85 o -2 2 2 167.44 138.81 2.15 o -1 2 2 269.32 264.28 3.75 o 0 2 2 1121.11 1013.50 15.25 o 1 2 2 1103.21 1190.44 16.26 o 2 2 2 177.28 206.06 3.06 o 3 2 2 731.80 763.61 9.74 o 4 2 2 786.99 871.47 12.29 o 5 2 2 119.39 116.24 2.01 o 6 2 2 319.71 300.14 4.49 o 7 2 2 156.63 137.33 2.34 o 8 2 2 63.21 50.13 1.08 o 9 2 2 50.69 52.53 1.47 o 10 2 2 0.29 1.94 0.53 o 11 2 2 4.44 8.86 0.87 o 12 2 2 18.61 11.25 1.13 o 13 2 2 42.45 44.53 1.97 o 14 2 2 1.83 1.13 1.35 o 15 2 2 1.69 2.73 0.84 o 16 2 2 5.32 4.31 0.93 o 17 2 2 67.69 74.61 2.86 o 18 2 2 1.30 0.38 0.94 o 19 2 2 0.33 0.12 0.86 o 20 2 2 1.97 1.36 1.86 o -17 3 2 0.35 1.83 0.84 o -16 3 2 0.21 0.55 0.84 o -15 3 2 0.88 -0.23 1.21 o -14 3 2 2.08 3.36 0.94 o -13 3 2 66.01 45.05 3.71 o -12 3 2 59.75 53.15 2.70 o -11 3 2 3.06 3.56 0.82 o -10 3 2 0.70 0.36 0.59 o -9 3 2 13.22 14.25 0.90 o -8 3 2 6.94 7.02 0.63 o -7 3 2 29.75 28.25 1.27 o -6 3 2 98.65 85.72 2.25 o -5 3 2 77.12 78.17 1.76 o -4 3 2 7.87 13.58 0.71 o -3 3 2 23.99 33.60 1.04 o -2 3 2 6.81 8.45 0.59 o -1 3 2 6.47 7.83 0.62 o 0 3 2 45.49 47.15 1.17 o 1 3 2 56.04 58.54 1.50 o 2 3 2 218.31 234.89 4.30 o 3 3 2 46.12 50.82 1.51 o 4 3 2 6.09 6.44 0.64 o 5 3 2 1.52 0.75 0.51 o 6 3 2 0.06 -0.52 0.52 o 7 3 2 7.73 8.84 0.70 o 8 3 2 21.76 24.85 1.08 o 9 3 2 36.76 28.70 1.54 o 10 3 2 6.80 6.83 0.76 o 11 3 2 1.72 0.48 0.68 o 12 3 2 7.74 6.08 0.89 o 13 3 2 0.63 3.26 0.88 o 14 3 2 2.35 1.01 0.84 o 15 3 2 28.07 17.78 3.78 o 16 3 2 5.42 4.56 1.19 o 17 3 2 4.45 4.62 2.02 o -13 4 2 34.02 30.20 4.30 o -12 4 2 0.23 0.31 1.12 o -11 4 2 14.44 9.35 1.54 o -10 4 2 3.32 1.60 1.03 o -9 4 2 0.01 -0.35 0.63 o -8 4 2 0.23 0.35 0.60 o -7 4 2 0.85 0.24 0.66 o -6 4 2 0.01 -0.04 0.57 o -5 4 2 0.03 -0.09 0.62 o -4 4 2 23.45 21.26 1.12 o -3 4 2 17.96 14.15 0.96 o -2 4 2 1.72 2.58 0.65 o -1 4 2 23.81 25.03 1.21 o 0 4 2 26.81 22.47 1.07 o 1 4 2 0.07 0.12 0.61 o 2 4 2 0.23 -0.20 0.59 o 3 4 2 0.32 0.59 0.56 o 4 4 2 3.76 2.97 0.68 o 5 4 2 27.88 32.05 1.83 o 6 4 2 0.33 1.14 0.64 o 7 4 2 1.20 1.13 0.65 o 8 4 2 0.11 -0.19 0.63 o 9 4 2 3.15 0.74 0.83 o 10 4 2 4.61 4.47 0.83 o 11 4 2 0.10 -0.34 0.77 o 12 4 2 0.14 -0.50 1.03 o -21 1 3 3.90 3.54 1.01 o -20 1 3 1.15 0.33 0.89 o -19 1 3 0.74 3.18 0.91 o -18 1 3 20.23 25.18 1.31 o -17 1 3 45.50 41.97 1.81 o -16 1 3 113.62 120.11 3.12 o -15 1 3 7.30 6.21 0.73 o -14 1 3 24.89 21.24 1.08 o -13 1 3 14.99 10.75 1.30 o -12 1 3 105.21 111.17 2.33 o -11 1 3 108.13 118.93 2.99 o -10 1 3 36.25 35.26 0.99 o -9 1 3 70.12 82.17 1.42 o -8 1 3 22.81 22.08 0.72 o -7 1 3 97.70 84.48 1.59 o -6 1 3 34.70 27.81 0.76 o -5 1 3 588.88 595.96 9.55 o -4 1 3 1786.97 1781.10 30.96 o -3 1 3 610.08 632.12 11.12 o -2 1 3 819.74 832.68 14.56 o -1 1 3 258.10 231.07 4.07 o 0 1 3 528.56 556.14 8.41 o 1 1 3 3559.87 3779.48 52.07 o 2 1 3 182.37 171.04 2.64 o 3 1 3 7.87 9.88 0.47 o 4 1 3 518.80 536.63 8.12 o 5 1 3 888.62 856.27 13.21 o 6 1 3 0.08 0.87 0.32 o 7 1 3 8.96 10.88 0.46 o 8 1 3 3.92 3.70 0.41 o 9 1 3 20.85 16.63 0.64 o 10 1 3 1.84 3.49 0.44 o 11 1 3 6.65 8.84 0.65 o 12 1 3 4.30 4.83 0.66 o 13 1 3 27.15 27.85 1.30 o 14 1 3 151.96 167.16 3.82 o 15 1 3 42.51 33.36 1.76 o 16 1 3 58.16 68.37 2.08 o 17 1 3 1.13 0.92 0.85 o 18 1 3 0.31 -0.21 1.02 o 19 1 3 0.26 -0.41 1.04 o 20 1 3 2.26 2.71 1.70 o 21 1 3 0.00 1.45 1.29 o -20 2 3 3.89 2.45 1.29 o -19 2 3 30.78 27.65 3.15 o -18 2 3 5.26 5.36 1.41 o -17 2 3 0.22 1.10 0.87 o -16 2 3 14.99 15.34 1.39 o -15 2 3 0.10 0.03 0.80 o -14 2 3 74.91 77.17 2.80 o -13 2 3 22.18 21.29 1.58 o -12 2 3 232.49 215.43 5.20 o -11 2 3 62.16 65.22 2.11 o -10 2 3 1.82 2.94 0.59 o -9 2 3 435.30 404.86 6.97 o -8 2 3 134.88 153.27 2.52 o -7 2 3 18.84 21.25 0.75 o -6 2 3 20.87 32.33 0.95 o -5 2 3 1048.86 1078.72 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