#------------------------------------------------------------------------------ #$Date: 2025-09-04 19:25:05 +0300 (Thu, 04 Sep 2025) $ #$Revision: 302020 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/51/95/4519511.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4519511 _cell_angle_alpha 103.086 _cell_angle_beta 93.763 _cell_angle_gamma 100.454 _cell_length_a 3.8274 _cell_length_b 7.5328 _cell_length_c 14.9381 _exptl_crystal_F_000 224.00 _reflns_d_resolution_high 0.8199 _cod_data_source_file 03-4BrCA-jw24094-P-1.fcf _cod_data_source_block jw24094 _shelx_title ' jw24094_a.res in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 155.21 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 457.63 329.39 2.71 o 2 0 0 27.45 32.20 1.62 o -2 1 0 732.45 626.30 6.90 o -1 1 0 14462.34 17075.00 89.28 o 0 1 0 232.88 155.41 2.19 o 1 1 0 3.00 11.63 0.77 o 2 1 0 738.02 729.78 8.35 o 3 1 0 734.48 704.56 6.78 o -3 2 0 477.53 458.95 5.10 o -2 2 0 947.66 875.78 9.62 o -1 2 0 686.49 654.73 5.92 o 0 2 0 401.97 577.81 5.25 o 1 2 0 1341.47 1394.99 11.32 o 2 2 0 2068.89 1950.79 16.86 o 3 2 0 1172.61 1129.59 8.85 o 4 2 0 25.48 14.20 1.64 o -4 3 0 280.05 323.95 4.89 o -3 3 0 294.16 275.58 3.09 o -2 3 0 469.43 443.34 6.39 o -1 3 0 519.32 677.90 7.22 o 0 3 0 549.65 453.26 5.25 o 1 3 0 2131.29 2130.69 17.34 o 2 3 0 1358.14 1321.79 15.33 o 3 3 0 6.47 10.37 0.77 o -4 4 0 327.35 362.64 3.72 o -3 4 0 114.52 116.46 1.86 o -2 4 0 199.20 218.96 5.94 o -1 4 0 112.14 60.29 3.15 o 0 4 0 740.42 623.07 9.63 o 1 4 0 572.92 566.50 7.67 o 2 4 0 0.10 4.16 0.63 o 3 4 0 492.25 486.12 4.37 o -4 5 0 1.17 2.92 0.53 o -3 5 0 85.79 86.35 1.50 o -2 5 0 312.72 264.10 2.67 o -1 5 0 543.68 470.50 9.03 o 0 5 0 254.25 224.31 5.95 o 1 5 0 11.14 15.93 0.96 o 2 5 0 793.60 828.98 6.24 o 3 5 0 13.46 21.47 1.02 o -4 6 0 34.55 35.89 1.06 o -3 6 0 457.92 446.20 4.08 o -2 6 0 580.33 549.91 4.74 o -1 6 0 241.99 227.27 3.43 o 0 6 0 86.96 78.71 1.76 o 1 6 0 372.73 369.61 4.10 o 2 6 0 2.94 3.07 0.41 o -3 7 0 253.00 255.88 2.43 o -2 7 0 140.65 141.04 2.20 o -1 7 0 221.28 195.79 3.07 o 0 7 0 117.19 117.52 2.23 o 1 7 0 40.03 50.40 1.28 o 2 7 0 73.62 76.11 1.57 o -2 8 0 127.60 110.37 2.17 o -1 8 0 161.92 157.51 2.27 o 0 8 0 305.20 306.76 3.61 o 1 8 0 69.73 65.59 1.97 o 1 -9 1 72.22 76.47 1.61 o -1 -8 1 19.71 15.49 0.87 o 0 -8 1 369.51 383.62 4.37 o 1 -8 1 339.71 351.88 6.06 o 2 -8 1 44.07 56.47 1.30 o -2 -7 1 50.04 49.70 1.33 o -1 -7 1 497.90 492.68 5.59 o 0 -7 1 1175.64 1173.34 13.41 o 1 -7 1 156.82 155.98 2.79 o 2 -7 1 4.00 9.74 0.75 o 3 -7 1 264.12 249.64 2.36 o -2 -6 1 157.82 158.57 2.03 o -1 -6 1 1840.66 1845.98 14.56 o 0 -6 1 275.54 270.18 3.70 o 1 -6 1 37.98 54.97 1.66 o 2 -6 1 552.46 518.86 4.03 o 3 -6 1 188.69 195.15 2.97 o 4 -6 1 13.21 21.20 0.76 o -3 -5 1 28.36 37.89 1.20 o -2 -5 1 1175.90 1214.24 8.11 o -1 -5 1 114.67 106.09 2.26 o 0 -5 1 251.51 270.82 6.55 o 1 -5 1 1578.31 1612.00 21.26 o 2 -5 1 864.88 813.81 5.61 o 3 -5 1 289.67 299.90 3.00 o 4 -5 1 0.49 2.87 0.61 o -3 -4 1 379.81 391.15 3.82 o -2 -4 1 27.21 26.92 1.29 o -1 -4 1 188.56 189.31 4.48 o 0 -4 1 1827.03 1948.65 15.84 o 1 -4 1 1880.95 1832.62 22.65 o 2 -4 1 1460.65 1501.64 17.08 o 3 -4 1 33.70 39.95 1.15 o 4 -4 1 118.78 142.09 2.33 o -4 -3 1 81.34 76.42 6.96 o -3 -3 1 33.17 36.63 1.44 o -2 -3 1 12.79 15.95 2.05 o -1 -3 1 644.66 574.24 6.87 o 0 -3 1 1642.70 1650.05 12.34 o 1 -3 1 2009.07 2456.75 16.01 o 2 -3 1 305.86 398.38 6.45 o 3 -3 1 561.26 547.70 4.75 o 4 -3 1 283.52 310.00 5.43 o -4 -2 1 24.18 27.16 1.90 o -3 -2 1 27.36 32.55 1.36 o -2 -2 1 534.07 464.13 6.93 o -1 -2 1 874.68 759.10 6.97 o 0 -2 1 495.62 541.53 5.04 o 1 -2 1 508.77 670.97 7.85 o 2 -2 1 1114.58 1090.66 10.60 o 3 -2 1 895.25 800.58 8.02 o -3 -1 1 734.94 745.58 6.81 o -2 -1 1 817.73 692.66 8.00 o -1 -1 1 24.64 16.41 0.96 o 0 -1 1 45.04 148.23 2.45 o 1 -1 1 665.44 558.75 5.31 o 2 -1 1 1238.17 1111.32 13.09 o -2 0 1 105.35 94.14 2.41 o -1 0 1 24.97 93.21 1.93 o 0 0 1 594.87 413.97 4.42 o 1 0 1 636.20 459.89 3.77 o 2 0 1 93.88 69.76 2.55 o -3 1 1 164.20 173.34 7.64 o -2 1 1 643.02 613.88 7.64 o -1 1 1 1670.75 1645.33 10.64 o 0 1 1 1107.58 920.04 6.42 o 1 1 1 397.61 344.21 4.12 o 2 1 1 13.88 28.40 2.25 o 3 1 1 214.91 200.20 3.10 o -3 2 1 579.14 573.43 5.28 o -2 2 1 1804.28 1666.44 14.05 o -1 2 1 2821.96 3036.87 19.22 o 0 2 1 2183.21 2672.87 18.14 o 1 2 1 111.44 123.44 2.86 o 2 2 1 301.07 247.21 5.64 o 3 2 1 319.08 317.05 3.67 o -4 3 1 46.18 59.10 1.77 o -3 3 1 768.57 749.53 6.06 o -2 3 1 1664.48 1627.28 14.74 o -1 3 1 1182.33 1489.94 13.12 o 0 3 1 1276.63 1696.94 13.86 o 1 3 1 827.05 739.94 8.12 o 2 3 1 540.60 504.30 7.03 o 3 3 1 89.81 94.53 1.96 o -4 4 1 384.86 433.05 4.52 o -3 4 1 420.79 425.59 3.95 o -2 4 1 213.53 249.02 6.51 o -1 4 1 1146.94 1378.25 14.73 o 0 4 1 1587.16 1501.85 13.67 o 1 4 1 1560.33 1481.98 13.69 o 2 4 1 318.41 328.22 3.49 o 3 4 1 8.50 9.39 0.73 o -4 5 1 61.67 84.10 1.74 o -3 5 1 42.23 39.61 1.19 o -2 5 1 151.61 159.03 1.98 o -1 5 1 1046.80 1033.63 14.02 o 0 5 1 1762.21 1689.31 19.04 o 1 5 1 394.13 415.19 4.30 o 2 5 1 2.71 5.96 0.63 o 3 5 1 466.42 443.32 6.59 o -3 6 1 1.07 5.44 0.50 o -2 6 1 249.48 250.21 2.93 o -1 6 1 920.72 852.36 7.91 o 0 6 1 132.92 145.51 2.43 o 1 6 1 49.70 50.79 1.46 o 2 6 1 783.56 757.31 6.82 o -3 7 1 66.60 78.66 1.22 o -2 7 1 547.15 518.15 5.00 o -1 7 1 11.94 18.01 1.11 o 0 7 1 29.00 32.51 1.28 o 1 7 1 609.28 591.51 6.19 o -2 8 1 1.87 6.43 0.86 o -1 8 1 10.31 17.06 0.97 o 0 8 1 230.77 235.30 2.78 o 1 8 1 301.01 284.35 4.89 o 1 -9 2 42.79 42.13 1.04 o -1 -8 2 23.34 27.95 1.05 o 0 -8 2 41.69 44.15 1.14 o 1 -8 2 255.10 248.85 3.08 o 2 -8 2 163.80 165.18 2.37 o -2 -7 2 9.88 12.34 0.80 o -1 -7 2 56.87 60.75 1.90 o 0 -7 2 10.29 13.37 1.38 o 1 -7 2 312.63 298.63 3.59 o 2 -7 2 361.19 336.39 3.84 o 3 -7 2 30.78 31.20 0.94 o -2 -6 2 124.17 133.35 1.92 o -1 -6 2 3.96 5.43 0.63 o 0 -6 2 959.92 944.19 7.67 o 1 -6 2 278.33 256.85 3.10 o 2 -6 2 45.34 45.61 1.10 o 3 -6 2 265.33 263.90 2.75 o 4 -6 2 230.00 226.28 3.78 o -3 -5 2 155.48 161.02 2.19 o -2 -5 2 136.00 135.84 2.12 o -1 -5 2 1787.94 1790.90 12.24 o 0 -5 2 218.55 219.25 8.84 o 1 -5 2 44.95 52.24 3.34 o 2 -5 2 316.43 285.56 2.71 o 3 -5 2 226.50 221.26 2.59 o 4 -5 2 138.84 141.09 2.11 o -3 -4 2 405.77 420.32 4.21 o -2 -4 2 1154.83 1192.30 7.81 o -1 -4 2 191.91 207.11 4.27 o 0 -4 2 374.31 417.47 6.66 o 1 -4 2 661.76 588.66 7.36 o 2 -4 2 248.77 179.39 5.16 o 3 -4 2 359.93 367.90 3.48 o 4 -4 2 17.92 21.95 1.73 o -4 -3 2 287.07 250.21 6.34 o -3 -3 2 299.14 291.93 3.29 o -2 -3 2 234.69 261.57 5.82 o -1 -3 2 2252.82 2623.22 18.00 o 0 -3 2 3134.91 3557.69 36.25 o 1 -3 2 1059.12 982.26 8.49 o 2 -3 2 674.43 742.78 9.21 o 3 -3 2 50.40 50.35 1.21 o 4 -3 2 79.90 93.34 3.07 o -4 -2 2 105.55 97.63 5.43 o -3 -2 2 175.78 188.93 2.63 o -2 -2 2 2173.41 2308.50 22.76 o -1 -2 2 4220.52 4523.15 26.86 o 0 -2 2 2882.56 3652.70 46.78 o 1 -2 2 674.92 804.55 7.52 o 2 -2 2 6.62 9.11 1.39 o 3 -2 2 673.92 642.31 6.45 o -4 -1 2 41.69 49.96 4.10 o -3 -1 2 464.16 483.87 5.03 o -2 -1 2 1693.20 1589.46 14.02 o -1 -1 2 2295.42 2467.02 16.54 o 0 -1 2 147.62 199.52 3.49 o 1 -1 2 21.00 99.54 2.27 o 2 -1 2 6996.05 7476.49 51.83 o -3 0 2 521.56 538.15 5.99 o -2 0 2 1223.13 1197.19 11.17 o -1 0 2 132.95 164.27 2.35 o 0 0 2 227.09 176.32 2.00 o 1 0 2 24091.38 26239.40 245.69 o 2 0 2 553.67 415.25 6.32 o -3 1 2 750.41 815.18 8.20 o -2 1 2 171.85 210.26 3.80 o -1 1 2 943.77 893.60 7.06 o 0 1 2 11171.18 12456.19 132.41 o 1 1 2 1250.23 1063.79 8.64 o 2 1 2 76.97 62.71 3.25 o 3 1 2 120.47 118.17 2.48 o -4 2 2 302.23 343.47 5.77 o -3 2 2 6.94 13.53 0.93 o -2 2 2 423.06 383.36 5.46 o -1 2 2 857.11 693.72 7.74 o 0 2 2 2092.25 2102.03 15.71 o 1 2 2 27.37 73.31 2.42 o 2 2 2 266.91 249.43 8.61 o 3 2 2 655.46 649.90 6.17 o -4 3 2 56.89 70.64 1.92 o -3 3 2 328.89 338.34 3.47 o -2 3 2 656.40 544.80 9.06 o -1 3 2 1201.97 1199.44 10.48 o 0 3 2 77.12 148.93 3.19 o 1 3 2 80.24 60.72 2.95 o 2 3 2 834.96 840.65 6.46 o 3 3 2 616.81 613.98 5.29 o -4 4 2 147.54 171.71 2.58 o -3 4 2 907.51 846.07 11.83 o -2 4 2 315.50 281.27 8.09 o -1 4 2 4.14 18.11 1.63 o 0 4 2 4.80 10.37 1.28 o 1 4 2 466.91 401.40 6.92 o 2 4 2 441.17 447.12 4.30 o 3 4 2 30.52 34.73 1.28 o -4 5 2 518.93 566.71 4.62 o -3 5 2 12.20 14.54 0.81 o -2 5 2 3.93 9.24 0.68 o -1 5 2 220.27 158.04 7.97 o 0 5 2 502.45 423.19 9.75 o 1 5 2 360.59 342.66 4.29 o 2 5 2 10.66 15.21 0.89 o 3 5 2 239.54 207.30 2.07 o -3 6 2 16.33 15.89 0.78 o -2 6 2 536.31 517.12 4.84 o -1 6 2 696.65 654.17 5.69 o 0 6 2 410.03 386.11 4.17 o 1 6 2 6.87 6.72 0.74 o 2 6 2 57.23 61.41 1.36 o -3 7 2 229.81 229.88 2.71 o -2 7 2 391.55 393.63 4.48 o -1 7 2 259.98 255.73 3.34 o 0 7 2 59.16 51.37 1.41 o 1 7 2 9.72 14.80 0.86 o -2 8 2 67.69 71.98 1.41 o -1 8 2 18.78 14.98 0.83 o 0 8 2 100.16 104.58 2.13 o 0 -9 3 25.37 28.39 1.24 o 1 -9 3 179.15 152.32 3.11 o -1 -8 3 123.66 121.96 2.49 o 0 -8 3 49.93 55.74 2.37 o 1 -8 3 231.88 249.62 3.12 o 2 -8 3 310.19 309.65 3.78 o -2 -7 3 228.59 216.88 2.79 o -1 -7 3 60.69 59.18 1.53 o 0 -7 3 332.98 331.74 3.78 o 1 -7 3 1437.21 1441.09 10.56 o 2 -7 3 252.41 248.79 3.00 o 3 -7 3 32.15 38.03 1.07 o -2 -6 3 105.80 98.42 1.65 o -1 -6 3 117.98 102.08 2.71 o 0 -6 3 2777.66 2857.22 18.38 o 1 -6 3 507.38 475.80 4.77 o 2 -6 3 0.56 8.64 0.59 o 3 -6 3 193.38 184.43 2.33 o -3 -5 3 8.57 11.57 0.92 o -2 -5 3 52.35 54.55 1.39 o -1 -5 3 1987.40 2039.55 20.73 o 0 -5 3 392.42 350.87 6.81 o 1 -5 3 35.13 57.22 3.92 o 2 -5 3 711.94 710.66 5.27 o 3 -5 3 385.58 381.88 3.41 o 4 -5 3 242.36 245.07 3.55 o -3 -4 3 171.03 189.28 2.48 o -2 -4 3 710.67 746.04 6.71 o -1 -4 3 298.58 250.78 4.43 o 0 -4 3 2.32 16.16 1.46 o 1 -4 3 989.82 1098.28 9.87 o 2 -4 3 1164.71 1059.99 12.64 o 3 -4 3 1017.87 1023.90 7.42 o 4 -4 3 1.52 3.21 0.71 o -4 -3 3 208.65 201.62 3.03 o -3 -3 3 262.53 275.21 3.18 o -2 -3 3 406.43 365.66 6.87 o -1 -3 3 138.65 194.09 3.50 o 0 -3 3 347.72 319.87 5.00 o 1 -3 3 1520.91 1559.33 13.93 o 2 -3 3 1400.80 1412.60 20.44 o 3 -3 3 16.16 28.00 1.17 o 4 -3 3 99.71 106.21 4.37 o -4 -2 3 175.87 180.62 2.78 o -3 -2 3 242.40 260.25 3.15 o -2 -2 3 8.63 19.08 1.78 o -1 -2 3 436.62 377.84 4.48 o 0 -2 3 1331.95 1543.90 25.81 o 1 -2 3 669.02 610.71 6.98 o 2 -2 3 4.11 11.60 1.67 o 3 -2 3 242.89 221.70 3.18 o -4 -1 3 43.38 50.20 1.94 o -3 -1 3 126.27 143.71 2.35 o -2 -1 3 1184.37 1142.65 11.54 o -1 -1 3 1683.58 1585.51 11.39 o 0 -1 3 375.29 297.50 3.14 o 1 -1 3 687.52 923.56 8.65 o 2 -1 3 197.45 160.57 4.55 o -4 0 3 122.13 125.62 3.86 o -3 0 3 1060.51 1122.82 8.55 o -2 0 3 1016.38 836.89 8.69 o -1 0 3 1099.08 1139.22 9.01 o 0 0 3 315.01 477.62 4.33 o 1 0 3 147.00 89.40 2.06 o 2 0 3 375.30 282.14 5.19 o 3 0 3 183.86 167.19 3.28 o -4 1 3 364.82 374.08 5.11 o -3 1 3 244.40 218.02 3.11 o -2 1 3 941.15 960.64 10.81 o -1 1 3 656.62 852.23 7.58 o 0 1 3 871.28 860.96 12.88 o 1 1 3 901.52 765.05 7.87 o 2 1 3 734.79 684.97 10.06 o 3 1 3 59.24 62.27 1.83 o -4 2 3 64.05 78.19 2.02 o -3 2 3 417.16 449.35 4.14 o -2 2 3 481.70 542.40 8.13 o -1 2 3 2096.88 2179.32 16.82 o 0 2 3 3203.84 3376.37 21.67 o 1 2 3 2066.64 2261.57 16.76 o 2 2 3 0.28 9.19 2.51 o 3 2 3 37.54 41.12 1.59 o -4 3 3 128.20 150.47 2.52 o -3 3 3 2.21 8.35 0.65 o -2 3 3 1269.61 1150.69 15.14 o -1 3 3 2568.46 2633.99 20.81 o 0 3 3 1595.93 1857.10 17.29 o 1 3 3 259.76 356.79 5.99 o 2 3 3 211.32 209.88 2.68 o 3 3 3 237.84 240.11 3.07 o -4 4 3 173.90 174.21 2.83 o -3 4 3 736.09 766.95 6.06 o -2 4 3 797.32 721.22 13.90 o -1 4 3 538.16 593.51 9.63 o 0 4 3 321.20 417.44 8.75 o 1 4 3 704.35 658.50 15.73 o 2 4 3 760.09 767.51 5.91 o 3 4 3 236.52 239.24 2.69 o -4 5 3 550.36 588.11 5.59 o -3 5 3 190.17 194.33 2.41 o -2 5 3 227.87 220.05 2.40 o -1 5 3 4.92 11.77 1.41 o 0 5 3 635.07 657.82 6.33 o 1 5 3 1139.73 1135.22 8.72 o 2 5 3 302.49 303.37 2.94 o -3 6 3 87.75 82.20 1.39 o -2 6 3 24.99 23.39 1.16 o -1 6 3 144.22 152.96 2.74 o 0 6 3 929.97 901.28 7.25 o 1 6 3 148.76 150.97 2.61 o 2 6 3 0.20 1.50 0.40 o -3 7 3 0.15 3.57 0.43 o -2 7 3 53.36 61.12 1.63 o -1 7 3 690.44 630.78 5.88 o 0 7 3 57.65 64.22 1.51 o 1 7 3 1.17 1.83 0.32 o -2 8 3 372.82 343.65 3.81 o -1 8 3 53.46 60.03 1.46 o 0 8 3 0.11 2.32 0.36 o 0 -9 4 178.60 169.08 2.67 o 1 -9 4 88.97 92.72 1.99 o -1 -8 4 259.32 259.50 3.58 o 0 -8 4 133.73 136.85 2.39 o 1 -8 4 4.40 8.51 0.68 o 2 -8 4 79.45 85.56 1.82 o -2 -7 4 349.10 339.01 4.02 o -1 -7 4 104.71 102.29 1.88 o 0 -7 4 3.84 8.92 0.82 o 1 -7 4 17.96 22.87 1.29 o 2 -7 4 390.21 378.50 3.58 o 3 -7 4 325.22 309.21 2.56 o -2 -6 4 34.32 36.99 1.22 o -1 -6 4 42.52 49.93 1.63 o 0 -6 4 18.46 31.95 2.45 o 1 -6 4 1273.24 1256.64 10.12 o 2 -6 4 393.49 378.57 3.21 o 3 -6 4 0.92 5.38 0.47 o -3 -5 4 33.08 36.01 1.05 o -2 -5 4 143.27 157.47 2.20 o -1 -5 4 317.89 323.55 6.59 o 0 -5 4 2456.44 2467.23 31.27 o 1 -5 4 613.98 625.17 8.09 o 2 -5 4 7.67 17.57 0.79 o 3 -5 4 93.11 97.83 1.63 o 4 -5 4 84.31 98.42 1.65 o -3 -4 4 90.69 100.11 1.77 o -2 -4 4 970.45 1004.36 6.80 o -1 -4 4 1897.35 1859.24 14.86 o 0 -4 4 1008.86 1180.09 15.62 o 1 -4 4 84.75 126.88 4.81 o 2 -4 4 316.17 275.05 6.18 o 3 -4 4 186.10 171.12 2.24 o 4 -4 4 286.63 270.31 3.55 o -4 -3 4 15.38 28.77 1.71 o -3 -3 4 660.84 690.01 5.45 o -2 -3 4 782.87 686.67 10.12 o -1 -3 4 1293.70 1511.76 11.98 o 0 -3 4 2196.41 3405.93 25.03 o 1 -3 4 2064.75 2306.75 17.49 o 2 -3 4 858.04 766.27 10.25 o 3 -3 4 487.96 484.61 4.37 o 4 -3 4 6.48 12.83 1.91 o -4 -2 4 290.27 294.25 3.63 o -3 -2 4 533.33 539.86 4.71 o -2 -2 4 743.63 788.57 9.27 o -1 -2 4 2617.40 3359.65 21.52 o 0 -2 4 4348.14 5667.30 33.18 o 1 -2 4 2499.57 2643.80 18.17 o 2 -2 4 553.83 538.72 9.60 o 3 -2 4 110.85 122.92 2.20 o -4 -1 4 397.62 399.88 4.53 o -3 -1 4 231.10 249.01 3.00 o -2 -1 4 231.62 219.24 4.44 o -1 -1 4 2343.01 2398.66 17.55 o 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63.56 2.11 o -1 -4 16 422.56 424.84 4.30 o 0 -4 16 106.38 104.15 1.91 o 1 -4 16 122.88 110.22 1.67 o -2 -3 16 294.68 295.79 3.46 o -1 -3 16 49.32 51.40 1.45 o 0 -3 16 325.43 305.73 4.54 o 1 -3 16 227.35 230.56 2.68 o -2 -2 16 8.57 10.89 1.38 o -1 -2 16 62.50 62.81 1.41 o 0 -2 16 329.13 329.68 3.55 o 1 -2 16 642.93 625.18 5.67 o -2 -1 16 0.85 1.93 0.34 o -1 -1 16 331.71 335.58 3.92 o 0 -1 16 210.13 218.20 2.70 o 1 -1 16 0.41 3.69 0.47 o -2 0 16 202.08 208.72 2.99 o -1 0 16 61.94 71.05 1.58 o 0 0 16 20.17 20.96 0.92 o 1 0 16 3.19 5.87 0.63 o -2 1 16 129.91 145.70 4.03 o -1 1 16 36.90 34.22 1.12 o 0 1 16 0.42 1.15 0.37 o 1 1 16 88.26 102.25 1.94 o -1 2 16 19.67 26.19 2.84 o 0 2 16 76.88 88.40 1.52 o 0 -5 17 228.04 238.23 2.81 o -1 -4 17 330.70 316.99 3.53 o 0 -4 17 220.09 223.34 3.01 o 1 -4 17 4.52 8.22 0.89 o -1 -3 17 145.62 150.89 2.46 o 0 -3 17 10.08 13.06 0.93 o 1 -3 17 14.52 20.21 0.76 o -1 -2 17 5.08 8.95 1.04 o 0 -2 17 65.57 69.91 1.45 o 1 -2 17 14.20 22.78 0.80 o -1 -1 17 222.43 208.58 2.76 o 0 -1 17 314.41 315.11 4.37 o 1 -1 17 220.51 214.81 2.61 o -1 0 17 389.87 368.46 4.02 o 0 0 17 108.83 115.08 1.94 o -1 1 17 110.35 111.97 1.74 o 0 1 17 6.59 6.28 0.51 o 0 -3 18 66.68 74.77 2.52 o -1 -2 18 33.03 33.58 2.18 o 0 -2 18 0.33 2.50 0.45 o 0 -1 18 165.43 180.51 5.81 o