Crystallography Open Database

Information card for entry 7007727

Preview

Coordinates	7007727.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H40 Cl3 N2 Sb
Calculated formula	C36 H40 Cl3 N2 Sb
SMILES	C12C(c3cccc4cccc1c34)=[N](c1c(cccc1C(C)C)C(C)C)[Sb](Cl)(Cl)(Cl)[N]=2c1c(cccc1C(C)C)C(C)C
Title of publication	Complexes of 1,2-bis(aryl-imino)acenaphthene (Ar-BIAN) ligands with some heavy p-block elements.
Authors of publication	Hill, Nicholas J.; Reeske, Gregor; Moore, Jennifer A.; Cowley, Alan H.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2006
Journal issue	40
Pages of publication	4838 - 4844
a	34.4781 ± 0.0006 Å
b	10.9074 ± 0.0002 Å
c	22.4939 ± 0.0005 Å
α	90°
β	106.887 ± 0.001°
γ	90°
Cell volume	8094.4 ± 0.3 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0743
Residual factor for significantly intense reflections	0.0484
Weighted residual factors for significantly intense reflections	0.1273
Weighted residual factors for all reflections included in the refinement	0.1382
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	7007727.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7007727.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7007727.cif
1504	2010-09-08	cif/7/ Adding data extracted from RSC 2005 and 2006 year publications.	7007727.cif