Crystallography Open Database

Information card for entry 7022836

Preview

Coordinates	7022836.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H106 N4 O2 Si2 Y2
Calculated formula	C66 H106 N4 O2 Si2 Y2
Title of publication	Rare-earth dichloro and bis(alkyl) complexes supported by bulky amido-imino ligand. Synthesis, structure, reactivity and catalytic activity in isoprene polymerization.
Authors of publication	Kissel, Alexander A.; Lyubov, Dmitry M.; Mahrova, Tatyana V.; Fukin, Georgy K.; Cherkasov, Anton V.; Glukhova, Tatyana A.; Cui, Dongmei; Trifonov, Alexander A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2013
Journal volume	42
Journal issue	25
Pages of publication	9211 - 9225
a	12.8326 ± 0.0006 Å
b	20.5123 ± 0.001 Å
c	13.8751 ± 0.0007 Å
α	90°
β	109.973 ± 0.001°
γ	90°
Cell volume	3432.6 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0687
Residual factor for significantly intense reflections	0.0465
Weighted residual factors for significantly intense reflections	0.116
Weighted residual factors for all reflections included in the refinement	0.1247
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179933 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/28.	7022836.cif
90357	2013-11-17	cif/ Adding structures of 7022831, 7022832, 7022833, 7022834, 7022835, 7022836, 7022837, 7022838 via cif-deposit CGI script.	7022836.cif