Crystallography Open Database

Information card for entry 7024278

Preview

Coordinates	7024278.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C37 H52 Ge N2 O4
Calculated formula	C37 H52 Ge N2 O4
SMILES	[Ge]1(N(c2c(cccc2C(C)C)C(C)C)C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C)C(=C\C(=O)OCC)/C(=O)OCC
Title of publication	Reactivity of germanium(II) hydride with nitrous oxide, trimethylsilyl azide, ketones, and alkynes and the reaction of a methyl analogue with trimethylsilyl diazomethane.
Authors of publication	Jana, Anukul; Roesky, Herbert W.; Schulzke, Carola
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	1
Pages of publication	132 - 138
a	11.837 ± 0.002 Å
b	17.042 ± 0.003 Å
c	17.895 ± 0.004 Å
α	90°
β	103.69 ± 0.03°
γ	90°
Cell volume	3507.3 ± 1.2 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0472
Residual factor for significantly intense reflections	0.0341
Weighted residual factors for significantly intense reflections	0.0738
Weighted residual factors for all reflections included in the refinement	0.0777
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179947 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/42.	7024278.cif
92343	2014-01-12	cif/ Adding structures of 7024276, 7024277, 7024278, 7024279, 7024280 via cif-deposit CGI script.	7024278.cif