Crystallography Open Database

Information card for entry 7028494

Preview

Coordinates	7028494.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C6 K7 Na4 O109 P2 Re2 W23
Calculated formula	C6 K7 Na4 O109 P2 Re2 W23
Title of publication	Complexation of metal carbonyl units with [α-PW11O39](7-) and [α2-P2W17O61](10-): insights into the chiral "twisted-sandwich" dimeric structures.
Authors of publication	Zhao, Chongchao; Glass, Elliot N.; Sumliner, Jordan M.; Bacsa, John; Kim, Daniel Taehyun; Guo, Weiwei; Hill, Craig L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2014
Journal volume	43
Journal issue	10
Pages of publication	4040 - 4047
a	13.0794 ± 0.0004 Å
b	19.8716 ± 0.0006 Å
c	21.3258 ± 0.0006 Å
α	76.506 ± 0.002°
β	84.428 ± 0.002°
γ	82.631 ± 0.002°
Cell volume	5332.3 ± 0.3 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173.15 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0803
Residual factor for significantly intense reflections	0.053
Weighted residual factors for significantly intense reflections	0.1166
Weighted residual factors for all reflections included in the refinement	0.1358
Goodness-of-fit parameter for all reflections included in the refinement	1.075
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179990 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/84.	7028494.cif
105344	2014-03-12	cif/ Adding structures of 7028494, 7028495, 7028496 via cif-deposit CGI script.	7028494.cif