Crystallography Open Database

Information card for entry 7046185

Preview

Coordinates	7046185.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H23 Cl2 Fe N3 Si
Calculated formula	C24 H23 Cl2 Fe N3 Si
Title of publication	The coordination chemistry of the neutral tris-2-pyridyl silicon ligand [PhSi(6-Me-2-py)<sub>3</sub>].
Authors of publication	Plajer, Alex J.; Colebatch, Annie L.; Enders, Markus; García-Romero, Álvaro; Bond, Andrew D.; García-Rodríguez, Raúl; Wright, Dominic S.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	20
Pages of publication	7036 - 7043
a	20.9935 ± 0.0005 Å
b	10.2893 ± 0.0002 Å
c	22.4986 ± 0.0005 Å
α	90°
β	93.954 ± 0.001°
γ	90°
Cell volume	4848.32 ± 0.18 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0469
Residual factor for significantly intense reflections	0.034
Weighted residual factors for significantly intense reflections	0.0784
Weighted residual factors for all reflections included in the refinement	0.0838
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229701 (current)	2019-11-17	cif/ Updating files of 7046180, 7046181, 7046182, 7046183, 7046184, 7046185 Original log message: Adding full bibliography for 7046180--7046185.cif.	7046185.cif
207595	2018-05-01	cif/ Adding structures of 7046180, 7046181, 7046182, 7046183, 7046184, 7046185 via cif-deposit CGI script.	7046185.cif