Crystallography Open Database

Information card for entry 7047196

Preview

Coordinates	7047196.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H84 N2 Si10
Calculated formula	C36 H84 N2 Si10
Title of publication	Dearomative cycloadditions of a silylene with pyrazine and quinoxaline.
Authors of publication	Ishida, Shintaro; Tamura, Tomofumi; Iwamoto, Takeaki
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	33
Pages of publication	11317 - 11321
a	21.0673 ± 0.0007 Å
b	9.5867 ± 0.0003 Å
c	16.1406 ± 0.0005 Å
α	90°
β	129.594 ± 0.001°
γ	90°
Cell volume	2511.98 ± 0.14 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	5
Hermann-Mauguin space group symbol	C 1 2 1
Hall space group symbol	C 2y
Residual factor for all reflections	0.0362
Residual factor for significantly intense reflections	0.0346
Weighted residual factors for significantly intense reflections	0.0839
Weighted residual factors for all reflections included in the refinement	0.0851
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229428 (current)	2019-11-17	cif/ Updating files of 7047196, 7047197 Original log message: Adding full bibliography for 7047196--7047197.cif.	7047196.cif
209329	2018-08-01	cif/ Adding structures of 7047196, 7047197 via cif-deposit CGI script.	7047196.cif