Crystallography Open Database

Information card for entry 7049021

Preview

Coordinates	7049021.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H52 Cu3 Ge N5 O66 Tb W12
Calculated formula	C30 H20 Cu3 Ge N5 O66 Tb W12
Title of publication	Organic-inorganic hybrids assembled from plenary Keggin-type germanotungstate units and 3d-4f heterometal clusters.
Authors of publication	Li, Huijie; Gong, Peijun; Jiang, Jun; Li, Yamin; Pang, Jingjing; Chen, Lijuan; Zhao, Junwei
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	11
Pages of publication	3730 - 3742
a	13.2757 ± 0.0005 Å
b	16.5995 ± 0.0006 Å
c	35.2571 ± 0.0013 Å
α	90°
β	100.05 ± 0.001°
γ	90°
Cell volume	7650.4 ± 0.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296.15 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0847
Residual factor for significantly intense reflections	0.061
Weighted residual factors for significantly intense reflections	0.1547
Weighted residual factors for all reflections included in the refinement	0.1666
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224546 (current)	2019-11-08	cif/ Updating files of 7049020, 7049021, 7049022, 7049023 Original log message: Adding full bibliography for 7049020--7049023.cif.	7049021.cif
213649	2019-02-15	cif/ Adding structures of 7049020, 7049021, 7049022, 7049023 via cif-deposit CGI script.	7049021.cif