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Information card for entry 7049039
Preview
| Coordinates | 7049039.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C55 H59 B O5 Os P2 |
|---|---|
| Calculated formula | C55 H59 B O5 Os P2 |
| Title of publication | Pentamethylcyclopentadienyl osmium complexes that contain diazoalkane, dioxygen and allenylidene ligands: preparation and reactivity. |
| Authors of publication | Albertin, Gabriele; Antoniutti, Stefano; Castro, Jesús; Sibilla, Francesca |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2019 |
| Journal volume | 48 |
| Journal issue | 9 |
| Pages of publication | 3116 - 3131 |
| a | 16.9078 ± 0.0012 Å |
| b | 18.2131 ± 0.0014 Å |
| c | 34.414 ± 0.003 Å |
| α | 102.266 ± 0.002° |
| β | 96.846 ± 0.002° |
| γ | 105.345 ± 0.002° |
| Cell volume | 9811.9 ± 1.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0597 |
| Residual factor for significantly intense reflections | 0.0431 |
| Weighted residual factors for significantly intense reflections | 0.0918 |
| Weighted residual factors for all reflections included in the refinement | 0.0977 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.055 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 224321 (current) | 2019-11-08 | cif/ Updating files of 7049037, 7049038, 7049039 Original log message: Adding full bibliography for 7049037--7049039.cif. |
7049039.cif |
| 213676 | 2019-02-16 | cif/ Adding structures of 7049037, 7049038, 7049039 via cif-deposit CGI script. |
7049039.cif |
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Users of the data should acknowledge the original authors of the
structural data.