Crystallography Open Database

Information card for entry 7054820

Preview

Coordinates	7054820.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H62 Ir Lu N3 Si
Calculated formula	C45 H60 Ir Lu N3 Si
Title of publication	Rare-earth‒iridium heterobimetallic complexes with bridging imido and silylmethyl ligands: synthesis, structure and reactivity
Authors of publication	Shima, Takanori; Yanagi, Takako; Hou, Zhaomin
Journal of publication	New J. Chem.
Year of publication	2015
Journal volume	39
Journal issue	10
Pages of publication	7608
a	46.05 ± 0.03 Å
b	9.62 ± 0.006 Å
c	19.635 ± 0.013 Å
α	90°
β	90.619 ± 0.011°
γ	90°
Cell volume	8698 ± 10 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.1749
Residual factor for significantly intense reflections	0.0524
Weighted residual factors for significantly intense reflections	0.0809
Weighted residual factors for all reflections included in the refinement	0.1112
Goodness-of-fit parameter for all reflections included in the refinement	0.885
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7054820.cif
162092	2015-10-09	cif/ Updating files of 7054818, 7054819, 7054820, 7054821, 7054822 Original log message: Adding full bibliography for 7054818--7054822.cif.	7054820.cif
135964	2015-05-09	cif/ Adding structures of 7054818, 7054819, 7054820, 7054821, 7054822 via cif-deposit CGI script.	7054820.cif