#------------------------------------------------------------------------------ #$Date: 2017-05-23 06:34:29 +0300 (Tue, 23 May 2017) $ #$Revision: 196895 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/05/62/7056209.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7056209 loop_ _publ_author_name 'Hadjikakou, Sotiris K.' 'Banti, C. N.' 'Kourkoumelis, Nikolaos' 'Raptopoulou, Catherine' 'Psycharis, Vassilis' _publ_section_title ; N-(4-hydroxyphenyl)acetamide against di-iodine towards polyiodide dianion ; _journal_name_full 'New J. Chem.' _journal_paper_doi 10.1039/C7NJ01117B _journal_year 2017 _chemical_formula_sum 'C16 H19 I4 N2 O4' _chemical_formula_weight 810.93 _space_group_crystal_system monoclinic _space_group_IT_number 13 _space_group_name_Hall '-P 2yac' _space_group_name_H-M_alt 'P 1 2/n 1' _symmetry_space_group_name_Hall '-P 2yac' _symmetry_space_group_name_H-M 'P 1 2/n 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2014/6 _audit_update_record ; 2016-12-12 deposited with the CCDC. 2017-05-22 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 97.777(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.1757(6) _cell_length_b 9.6136(3) _cell_length_c 17.0845(6) _cell_measurement_reflns_used 8976 _cell_measurement_temperature 160(2) _cell_measurement_theta_max 27.58 _cell_measurement_theta_min 3.21 _cell_volume 2306.85(15) _computing_cell_refinement 'CrystalClear, Rigaku MSC, 2005' _computing_data_collection 'CrystalClear, Rigaku MSC, 2005' _computing_data_reduction 'CrystalClear, Rigaku MSC, 2005' _computing_structure_refinement 'SHELXL-2014/6 (Sheldrick, 2014)' _computing_structure_solution 'CrystalClear, Rigaku MSC, 2005' _diffrn_ambient_temperature 160(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Rigaku R-AXIS SPIDER IPDS' _diffrn_measurement_method '\q scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0346 _diffrn_reflns_av_unetI/netI 0.0379 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 14491 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.000 _diffrn_reflns_theta_min 3.207 _diffrn_source ; fine-focus sealed tube with graphite monochromator ; _exptl_absorpt_coefficient_mu 5.425 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.365 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'CrystalClear, Rigaku MSC, 2005' _exptl_crystal_colour black _exptl_crystal_density_diffrn 2.335 _exptl_crystal_description parallelepide _exptl_crystal_F_000 1492 _exptl_crystal_size_max 0.28 _exptl_crystal_size_mid 0.24 _exptl_crystal_size_min 0.18 _refine_diff_density_max 1.593 _refine_diff_density_min -0.465 _refine_diff_density_rms 0.119 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.050 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 289 _refine_ls_number_reflns 5000 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.050 _refine_ls_R_factor_all 0.0264 _refine_ls_R_factor_gt 0.0234 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0234P)^2^+1.0336P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0543 _refine_ls_wR_factor_ref 0.0557 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4551 _reflns_number_total 5000 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c7nj01117b2.cif _cod_data_source_block compound1 _cod_database_code 7056209 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelxl_version_number 2014/6 _shelx_res_file ; TITL *** HADJ2 *** P 2/n CELL 0.71073 14.1757 9.6136 17.0845 90.000 97.777 90.000 ZERR 4.00 0.0006 0.0003 0.0006 0.000 0.002 0.000 LATT 1 SYMM 1/2 - X, Y, 1/2 - Z SFAC C H N O I UNIT 64 76 8 16 16 OMIT -2.00 54.00 OMIT 8 6 6 ! 8.92 2947.59 31.37 0.086 1.0 OMIT 0 3 4 ! 309.37 164.35 6.70 0.020 2.5 OMIT -3 4 6 ! 621.08 367.43 6.49 0.030 1.7 FMAP 2 PLAN -20 EQIV $1 -x+2, -y+1, -z EQIV $2 -x, -y+1, -z+1 EQIV $3 -x+1, -y, -z EQIV $4 -x+1/2, y+1, -z+1/2 ACTA HTAB 2.00000 HTAB O1 O1_$1 HTAB O3 O3_$2 HTAB O2 O4 HTAB O4 I1 HTAB N1 I3_$3 HTAB N2 I2_$4 FMAP 2 ACTA HTAB 2 BOND $H L.S. 4 TEMP -113.00 WGHT 0.023400 1.033600 FVAR 0.82687 I1 5 0.437965 0.020831 0.311993 11.00000 0.03071 0.02876 = 0.04194 0.00180 0.01325 0.00049 I2 5 0.347646 0.056563 0.143498 11.00000 0.02888 0.01830 = 0.04922 -0.00560 0.01506 -0.00036 I3 5 0.252442 0.075155 -0.014093 11.00000 0.04319 0.03111 = 0.04307 -0.00468 0.01047 -0.00384 I4 5 0.657139 -0.038949 0.265138 11.00000 0.03255 0.03177 = 0.03606 0.00153 0.00630 -0.00416 N1 3 0.842062 0.295767 0.070780 11.00000 0.02589 0.02182 = 0.03222 0.00350 0.01210 0.00112 AFIX 43 H1 2 0.835405 0.204780 0.071385 11.00000 -1.30000 AFIX 0 O1 4 0.932915 0.469524 0.033465 11.00000 0.02919 0.02975 = 0.03983 0.00038 0.01869 -0.00185 O2 4 0.560647 0.567962 0.211275 11.00000 0.03865 0.03200 = 0.04997 -0.00220 0.02934 0.00172 C1 1 0.975585 0.234830 0.003070 11.00000 0.03003 0.03904 = 0.03477 0.00059 0.01390 0.00508 AFIX 33 H1A 2 0.951046 0.141411 0.011273 11.00000 -1.50000 H1B 2 0.974117 0.251783 -0.053645 11.00000 -1.50000 H1C 2 1.041261 0.242100 0.029377 11.00000 -1.50000 AFIX 0 C2 1 0.914867 0.340742 0.037058 11.00000 0.02368 0.03184 = 0.02254 0.00213 0.00640 0.00312 C3 1 0.772158 0.372052 0.106564 11.00000 0.02306 0.02512 = 0.02323 0.00190 0.01003 0.00374 C4 1 0.771020 0.516639 0.113758 11.00000 0.03384 0.02663 = 0.03477 -0.00111 0.01622 -0.00270 C5 1 0.699240 0.578625 0.149596 11.00000 0.03450 0.02525 = 0.04049 -0.00376 0.01820 -0.00341 C6 1 0.629519 0.499825 0.177656 11.00000 0.02648 0.02729 = 0.02801 -0.00048 0.01162 0.00058 C7 1 0.631319 0.355386 0.170479 11.00000 0.03137 0.03045 = 0.03535 0.00478 0.01830 -0.00378 C8 1 0.702337 0.292834 0.135229 11.00000 0.03115 0.02225 = 0.03461 0.00359 0.01438 -0.00144 N2 3 0.151974 0.683742 0.409897 11.00000 0.02574 0.01645 = 0.03933 0.00315 0.01657 0.00031 AFIX 43 H2 2 0.155905 0.773514 0.400807 11.00000 -1.30000 AFIX 0 O3 4 0.067361 0.521993 0.464763 11.00000 0.02800 0.02276 = 0.04199 0.00678 0.02099 0.00137 O4 4 0.442894 0.396528 0.290827 11.00000 0.03444 0.02517 = 0.04719 -0.00414 0.02449 -0.00013 C9 1 0.011803 0.757928 0.464374 11.00000 0.03294 0.02808 = 0.05811 0.00552 0.02505 0.00491 C10 1 0.078931 0.646676 0.446171 11.00000 0.02219 0.02498 = 0.03068 0.00215 0.00979 -0.00094 C11 1 0.225139 0.602022 0.383229 11.00000 0.02084 0.02059 = 0.02646 -0.00054 0.00991 -0.00141 C12 1 0.229362 0.457984 0.387387 11.00000 0.02869 0.02145 = 0.03848 0.00302 0.01749 -0.00390 C13 1 0.302856 0.389182 0.356695 11.00000 0.02861 0.01695 = 0.04330 -0.00160 0.01691 -0.00200 C14 1 0.370684 0.462326 0.322790 11.00000 0.02280 0.02430 = 0.02684 -0.00338 0.01053 0.00025 C15 1 0.367116 0.606555 0.319747 11.00000 0.02944 0.02530 = 0.03096 0.00171 0.01455 -0.00451 C16 1 0.294837 0.674984 0.350095 11.00000 0.02797 0.02029 = 0.03247 0.00192 0.01275 -0.00110 H1O 2 1.000000 0.500000 0.000000 10.50000 0.09702 H2O 2 0.529030 0.515579 0.233132 11.00000 0.04433 H3O 2 0.000000 0.500000 0.500000 10.50000 0.08460 H4 2 0.820814 0.575585 0.090855 11.00000 0.04126 H4O 2 0.441099 0.318348 0.292377 11.00000 0.03008 H5 2 0.700100 0.676051 0.156206 11.00000 0.03170 H7 2 0.584507 0.303150 0.187375 11.00000 0.03951 H8 2 0.707141 0.185472 0.129445 11.00000 0.01704 H9A 2 0.039125 0.846810 0.462569 11.00000 0.08558 H9B 2 -0.047792 0.755982 0.433704 11.00000 0.10102 H9C 2 -0.003827 0.753165 0.511196 11.00000 0.07750 H12 2 0.179447 0.402040 0.409662 11.00000 0.02841 H13 2 0.305475 0.294485 0.357452 11.00000 0.02726 H15 2 0.413123 0.658385 0.298154 11.00000 0.03284 H16 2 0.293188 0.778538 0.352712 11.00000 0.02558 HKLF 4 REM *** HADJ2 *** P 2/n REM R1 = 0.0234 for 4551 Fo > 4sig(Fo) and 0.0264 for all 5000 data REM 289 parameters refined using 0 restraints END WGHT 0.0241 1.0704 REM Instructions for potential hydrogen bonds HTAB N1 I3_$3 HTAB N2 I2_$4 HTAB O1 O1_$1 HTAB O2 O4 HTAB O3 O3_$2 HTAB C4 O1 HTAB O4 I1 HTAB C8 I3_$3 HTAB C8 I4 EQIV $5 -x+3/2, y, -z+1/2 HTAB C8 I4_$5 HTAB C9 I2_$4 HTAB C12 O3 EQIV $6 -x+1/2, y, -z+1/2 HTAB C13 I2_$6 EQIV $7 x, y+1, z HTAB C16 I1_$7 REM Highest difference peak 1.593, deepest hole -0.465, 1-sigma level 0.119 Q1 1 0.3083 0.0585 0.0982 11.00000 0.05 1.59 Q2 1 0.3997 0.0197 0.2660 11.00000 0.05 1.49 Q3 1 0.2136 0.0703 -0.0575 11.00000 0.05 1.41 Q4 1 0.1154 0.0368 -0.2784 11.00000 0.05 1.19 Q5 1 0.3017 0.0749 0.0379 11.00000 0.05 1.13 Q6 1 0.2008 0.0376 -0.1862 11.00000 0.05 1.10 Q7 1 0.3969 0.0525 0.1990 11.00000 0.05 0.98 Q8 1 0.4853 0.0234 0.3622 11.00000 0.05 0.96 Q9 1 0.2843 0.0413 -0.0280 11.00000 0.05 0.86 Q10 1 0.4594 0.0775 0.3056 11.00000 0.05 0.71 Q11 1 0.2286 0.0384 0.0019 11.00000 0.05 0.59 Q12 1 0.3246 0.0423 0.1654 11.00000 0.05 0.59 Q13 1 0.4177 0.0238 0.3289 11.00000 0.05 0.54 Q14 1 0.2073 0.0529 -0.1188 11.00000 0.05 0.45 Q15 1 0.1845 0.0551 -0.2587 11.00000 0.05 0.40 Q16 1 0.6580 0.5375 0.1543 11.00000 0.05 0.38 Q17 1 0.4584 -0.0426 0.3059 11.00000 0.05 0.37 Q18 1 0.2716 -0.1479 -0.0153 11.00000 0.05 0.37 Q19 1 0.2945 -0.0403 0.0389 11.00000 0.05 0.36 Q20 1 0.4017 0.1637 0.1978 11.00000 0.05 0.36 ; _shelx_res_checksum 65372 _shelx_hkl_file ; 0 0 3 25.2405 5.60038 1 0 0 -3 53.3052 5.47501 1 0 0 4 8905.34 266.283 1 0 0 -4 8726.06 256.955 1 0 0 5 17.5856 14.6301 1 0 0 -5 9.08212 13.385 1 0 0 650467.10 2241.66 1 0 0 -648706.00 2168.59 1 0 0 7 34.5462 15.9951 1 0 0 -7 13.2744 13.8608 1 0 0 810642.10 315.147 1 0 0 -8 9972.58 294.262 1 0 0 9-1.68151 19.3559 1 0 0 -9 46.6071 16.7154 1 0 0 10 114.727 17.6339 1 0 0 -10 137.857 15.8611 1 0 0 11 28.1685 24.2978 1 0 0 -11 17.8833 20.5195 1 0 0 12 816.96 52.0935 1 0 0 -12 812.045 45.3716 1 0 0 13-24.4873 31.9114 1 0 0 -13-9.09101 26.0449 1 0 0 14-0.55954 19.2067 1 0 0 -14 30.3054 15.7244 1 0 0 15-26.5976 27.9959 1 0 0 -15 4.30271 22.6944 1 0 0 16 1374.28 108.451 1 0 0 -16 1245.13 91.5622 1 0 0 17 25.7736 32.1995 1 0 0 -17-33.6145 26.5098 1 0 0 18 1799.57 157.472 1 0 0 -18 1494.03 133.528 1 0 0 19-0.90025 43.6181 1 0 0 -19 19.4441 34.2783 1 0 0 20-16.7785 36.2331 1 0 0 -20 24.4006 30.5241 1 0 0 21 14.7298 45.2521 1 0 0 -21 23.1022 37.3769 1 0 1 222243.90 658.382 1 0 -1 222618.20 701.79 1 0 1 -222866.90 724.425 1 0 -1 -221692.00 647.217 1 0 1 3 874.798 25.6567 1 0 -1 3 914.529 27.538 1 0 1 -3 887.119 26.2971 1 0 -1 -3 836.011 17.5348 1 0 1 433089.50 1253.42 1 0 -1 434444.00 1380.27 1 0 1 -433418.20 1276.71 1 0 -1 -432954.60 1245.26 1 0 1 513892.20 418.175 1 0 -1 514160.90 464.336 1 0 -1 -513736.90 411.40 1 0 1 -513609.40 440.553 1 0 1 615642.30 494.578 1 0 -1 615419.60 485.731 1 0 -1 -615224.60 457.779 1 0 1 -615066.60 504.246 1 0 1 7 51.8164 14.438 1 0 -1 7 19.8123 11.0919 1 0 1 -7 32.3037 9.90723 1 0 -1 -7 30.0849 8.02833 1 0 -1 813902.20 487.193 1 0 1 814133.10 433.872 1 0 -1 -813507.10 443.681 1 0 1 -813385.50 462.556 1 0 -1 9 667.971 52.115 1 0 1 9 703.692 43.8694 1 0 -1 -9 667.30 39.9833 1 0 1 -9 678.317 31.0281 1 0 1 10 178.829 30.6507 1 0 -1 10 201.34 22.6253 1 0 -1 -10 203.091 26.6201 1 0 1 -10 215.703 30.3237 1 0 1 11 552.478 51.0091 1 0 -1 11 658.572 58.675 1 0 1 -11 510.735 32.6752 1 0 -1 -11 459.163 28.8795 1 0 -1 12 5042.06 241.564 1 0 1 12 5329.58 225.465 1 0 1 -12 4831.52 214.669 1 0 -1 -12 4936.82 200.386 1 0 1 13 2440.46 99.7275 1 0 -1 13 2281.93 105.107 1 0 1 -13 2242.65 135.868 1 0 -1 -13 2227.90 87.4661 1 0 1 14 1324.48 103.112 1 0 -1 14 1278.14 112.054 1 0 1 -14 1171.31 94.3037 1 0 -1 -14 1287.08 84.2805 1 0 1 15 175.455 29.4415 1 0 -1 15 178.816 32.1418 1 0 -1 -15 162.556 38.7978 1 0 1 -15 173.395 43.0415 1 0 -1 16 2443.24 155.618 1 0 1 16 2536.77 145.166 1 0 1 -16 2303.92 133.662 1 0 -1 -16 2266.15 92.2716 1 0 1 17 10.8519 19.7518 1 0 -1 17-7.77887 34.7864 1 0 -1 -17 5.24037 25.8054 1 0 1 -17 40.5338 29.0023 1 0 -1 18 2181.09 127.554 1 0 1 18 2516.96 179.309 1 0 -1 -18 2107.40 105.882 1 0 1 -18 2086.06 111.248 1 0 1 19 525.624 59.7743 1 0 -1 19 539.295 100.365 1 0 1 -19 435.964 84.9506 1 0 -1 -19 476.817 78.3333 1 0 1 20 36.9135 45.6006 1 0 -1 20 70.6092 29.7598 1 0 1 -20 30.0021 25.0261 1 0 -1 -20 32.3686 24.1196 1 0 1 21 69.6472 35.6937 1 0 -1 21 125.39 61.231 1 0 1 -21 88.5287 51.8758 1 0 -1 -21 85.4322 47.9214 1 0 -2 0276006.023638.50 1 0 2 0279501.023959.70 1 0 -2 1 748.812 32.6126 1 0 2 1 657.623 18.3619 1 0 -2 -1 791.098 20.1679 1 0 2 -1 724.847 21.188 1 0 -2 251703.00 2140.51 1 0 2 238494.00 1539.04 1 0 2 -251861.00 2140.00 1 0 2 3 3443.69 78.5309 1 0 -2 3 3504.06 121.427 1 0 2 -3 3407.19 113.216 1 0 -2 4 9931.15 278.449 1 0 2 410083.00 251.786 1 0 2 -4 9563.33 294.611 1 0 -2 -4 9516.78 244.463 1 0 -2 541314.50 1781.38 1 0 2 541494.40 1660.56 1 0 -2 -539513.60 1596.58 1 0 2 -539914.30 1713.41 1 0 2 616340.00 481.142 1 0 -2 616313.30 565.637 1 0 2 -615256.80 493.095 1 0 -2 -615781.90 489.598 1 0 -2 7 134.872 27.2492 1 0 2 7 78.2413 16.193 1 0 -2 -7 152.697 15.5803 1 0 2 -7 105.564 14.907 1 0 2 8 2900.74 88.3142 1 0 -2 8 2802.11 115.20 1 0 2 -8 2695.37 104.111 1 0 -2 -8 2661.69 81.9109 1 0 -2 9 2903.89 121.91 1 0 2 9 2980.94 78.1324 1 0 -2 -9 2769.43 90.2167 1 0 2 -9 2766.63 84.275 1 0 2 10 10.8481 13.8513 1 0 -2 10-3.84755 11.463 1 0 2 -10 0.46031 9.95753 1 0 -2 -10-18.1954 11.7879 1 0 2 11 2932.94 122.43 1 0 -2 11 2864.91 107.656 1 0 2 -11 2670.74 130.853 1 0 -2 -11 2790.85 108.208 1 0 2 12 366.241 32.4862 1 0 -2 12 400.229 67.2487 1 0 2 -12 357.807 35.0427 1 0 -2 -12 352.315 44.1794 1 0 2 13 7266.46 302.725 1 0 -2 13 6840.84 337.787 1 0 2 -13 6471.76 302.251 1 0 -2 -13 6647.86 270.547 1 0 2 14 635.58 66.7282 1 0 -2 14 563.874 51.3776 1 0 2 -14 588.627 44.5681 1 0 -2 -14 552.616 35.647 1 0 2 15 568.617 62.8204 1 0 -2 15 513.028 76.0138 1 0 2 -15 490.555 63.9721 1 0 -2 -15 511.002 51.5904 1 0 -2 16 1344.79 116.41 1 0 2 16 1348.80 101.101 1 0 2 -16 1249.84 68.104 1 0 -2 -16 1270.29 86.3498 1 0 2 17 129.02 29.6646 1 0 -2 17 113.40 34.8825 1 0 2 -17 147.68 47.5895 1 0 -2 -17 133.774 25.4452 1 0 -2 18 941.095 126.698 1 0 2 18 1081.10 112.514 1 0 -2 -18 974.999 96.9534 1 0 2 -18 995.878 73.8016 1 0 -2 19 1990.77 127.399 1 0 2 19 2307.54 120.065 1 0 -2 -19 1918.54 147.688 1 0 2 -19 1890.75 171.661 1 0 2 20 17.2698 34.1141 1 0 -2 20-15.9319 39.1418 1 0 -2 -20 37.4307 28.3097 1 0 2 -20-6.66236 20.6123 1 0 2 21 81.3675 58.857 1 0 -2 21 106.458 39.8838 1 0 2 -21 119.605 56.213 1 0 -2 -21 98.0746 49.1004 1 0 3 0128476.0 8006.77 1 0 -3 0128075.0 7969.03 1 0 -3 1 1346.57 45.1151 1 0 3 1 1313.14 35.4992 1 0 3 -1 1309.28 42.9869 1 0 -3 -1 1314.46 28.4098 1 0 3 242817.70 1671.71 1 0 -3 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4821.26 180.744 1 -3 8 -3 4902.26 169.764 1 3 -8 4 299.261 26.2733 1 3 8 4 263.773 26.2203 1 -3 8 -4 262.998 34.828 1 3 -8 5 1659.32 97.0001 1 3 8 5 1549.02 59.6217 1 -3 8 -5 1609.32 84.2567 1 3 -8 6 6421.14 226.859 1 3 8 6 6570.33 218.251 1 3 8 6 6195.37 191.565 1 -3 8 -6 6160.30 247.512 1 3 -8 7 4862.96 227.852 1 3 8 7 4857.40 158.623 1 3 8 7 4603.73 144.485 1 -3 8 -7 4598.75 197.497 1 3 -8 8 1016.90 94.2613 1 3 8 8 944.158 53.0596 1 3 8 8 983.944 47.0457 1 -3 8 -8 1002.60 76.4677 1 3 -8 9 5000.86 266.009 1 3 8 9 4719.81 153.469 1 3 8 9 5113.56 169.198 1 -3 8 -9 4714.11 224.827 1 3 -8 10 2361.79 169.931 1 3 8 10 2229.82 80.4235 1 3 8 10 2274.83 86.3335 1 -3 8 -10 2107.81 139.944 1 3 -8 11 1098.49 124.271 1 3 8 11 1157.43 55.8251 1 3 8 11 1166.46 53.0319 1 -3 8 -11 1052.98 67.4237 1 3 -8 12 841.798 118.462 1 3 8 12 862.029 46.3143 1 3 8 12 913.017 62.0353 1 -3 8 -12 854.699 62.9306 1 3 -8 13 47.8065 44.9702 1 -3 8 -13 19.2599 36.3892 1 3 -8 14 45.3877 43.0846 1 -3 8 -14-5.12769 34.0998 1 3 -8 15 288.363 58.029 1 -3 8 -15 291.475 78.5878 1 3 9 -15 2820.45 165.298 1 -3 -9 15 3009.84 161.572 1 3 9 -14 1103.65 137.219 1 -3 -9 14 1191.32 135.505 1 3 9 -13-11.6177 22.0389 1 -3 -9 13 46.8797 35.056 1 3 9 -12 1428.26 140.68 1 -3 -9 12 1587.00 135.422 1 3 9 -11 360.257 73.3832 1 -3 -9 11 335.494 43.1675 1 3 9 -10 1308.98 117.864 1 -3 -9 10 1267.85 116.396 1 3 9 -9 97.9984 47.2975 1 -3 -9 9 96.1636 27.4658 1 3 9 -8 116.479 29.1903 1 -3 -9 8 145.70 43.2608 1 3 9 -7 5303.25 257.866 1 -3 -9 7 5423.46 244.73 1 3 9 -6 182.723 50.2217 1 -3 -9 6 226.258 28.3721 1 3 9 -5 697.674 70.7011 1 -3 -9 5 719.337 42.5459 1 3 9 -4 4517.07 201.924 1 -3 -9 4 4813.08 193.035 1 3 9 -3 404.393 50.8059 1 -3 -9 3 465.119 47.1698 1 3 9 -2 1004.61 69.2691 1 -3 -9 2 1061.86 44.3674 1 3 -9 -1 1079.95 30.9118 1 3 9 -1 1180.37 67.6079 1 -3 9 1 1049.73 33.6781 1 -3 -9 1 1236.32 64.463 1 3 -9 0 6685.32 189.037 1 3 9 0 6362.49 233.499 1 -3 9 0 6211.26 188.092 1 -3 -9 0 7195.81 248.985 1 3 -9 1 951.926 42.9769 1 3 9 1 938.966 53.5973 1 -3 9 -1 929.893 44.3633 1 -3 -9 -1 933.354 63.5882 1 3 -9 2 478.231 35.5461 1 3 9 2 440.561 35.1727 1 -3 9 -2 421.456 34.622 1 3 -9 3 4096.14 152.811 1 3 9 3 3893.51 150.792 1 -3 9 -3 3938.13 122.305 1 3 -9 4 511.14 49.5365 1 3 9 4 448.282 32.6523 1 -3 9 -4 497.26 44.5447 1 3 -9 5 421.174 52.5856 1 3 9 5 416.085 37.7092 1 -3 9 -5 444.718 44.9766 1 3 -9 6 8736.49 315.693 1 3 9 6 8156.32 284.368 1 3 9 6 8639.12 315.01 1 -3 9 -6 8214.52 295.276 1 3 -9 7 4849.11 232.428 1 3 9 7 4625.29 167.263 1 3 9 7 4439.42 153.395 1 -3 9 -7 4628.92 168.317 1 3 -9 8 664.968 82.5542 1 3 9 8 628.901 33.9181 1 3 9 8 670.975 32.0873 1 -3 9 -8 702.819 46.3429 1 3 -9 9 3485.94 149.447 1 3 9 9 3149.80 98.1242 1 3 9 9 3067.48 100.696 1 -3 9 -9 3171.18 133.761 1 3 -9 10 2428.56 124.354 1 -3 9 -10 2208.60 106.031 1 3 -9 11 849.279 72.7457 1 -3 9 -11 838.799 92.0684 1 3 -9 12 337.954 50.6087 1 -3 9 -12 219.215 66.1884 1 3 -9 13 40.911 30.1752 1 -3 9 -13 13.7396 39.7836 1 3 -9 14 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900.751 71.4353 1 8 0 5 13.4245 25.6634 1 8 0 6 108.167 26.148 1 8 0 7 9.49724 32.6537 1 8 0 814265.50 678.472 1 8 0 9 19.5239 22.5068 1 8 0 10 4222.40 177.671 1 8 0 11-20.9613 22.0301 1 8 0 12 3266.25 154.811 1 8 0 13-10.4664 23.8615 1 8 0 14 6456.43 312.989 1 8 0 15-3.13235 36.8239 1 8 0 16 55.7881 53.3607 1 8 0 17-2.32526 37.4044 1 8 0 18 1372.20 177.698 1 8 1 -21-7.02475 22.1714 1 8 -1 -21-14.2959 31.4156 1 -8 -1 21 5.90864 31.2534 1 -8 1 21 5.9661 27.1879 1 8 1 -20 1596.21 105.276 1 8 -1 -20 1551.02 135.637 1 -8 -1 20 1706.53 136.911 1 -8 1 20 1808.65 126.288 1 8 1 -19 16.1493 36.1907 1 8 -1 -19 11.7417 31.3788 1 -8 -1 19-12.7283 30.7113 1 -8 1 19 24.535 26.9142 1 8 1 -18 252.553 71.615 1 8 -1 -18 248.947 62.2242 1 -8 1 18 312.598 53.2284 1 -8 -1 18 328.145 60.8046 1 8 1 -17 1006.62 128.459 1 8 -1 -17 1085.54 107.948 1 -8 1 17 1180.78 90.8703 1 -8 -1 17 1019.60 107.243 1 8 1 -16 1983.89 107.245 1 8 -1 -16 1973.99 139.279 1 -8 -1 16 2259.51 95.6416 1 -8 1 16 2105.40 86.4511 1 8 1 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485.318 44.0754 1 -9 -2 9 577.763 38.4023 1 9 2 -8 5756.13 220.275 1 9 -2 -8 5713.60 185.47 1 -9 -2 8 5926.55 196.51 1 -9 2 8 5995.65 219.573 1 9 2 -7 6308.29 298.735 1 9 -2 -7 6286.66 204.473 1 -9 -2 7 6481.41 217.75 1 -9 2 7 7176.59 233.045 1 9 2 -6 2950.66 121.213 1 9 -2 -6 2887.86 131.145 1 -9 -2 6 3073.71 110.396 1 9 -2 -543382.90 2103.04 1 9 2 -544447.40 2253.37 1 -9 -2 546586.60 2202.33 1 9 2 -4 1207.13 64.2165 1 9 -2 -4 1189.69 71.4341 1 -9 -2 4 1237.78 84.9902 1 9 -2 -3 8623.89 319.648 1 9 2 -3 9325.78 376.028 1 -9 -2 310776.10 378.721 1 9 2 -2 645.019 40.3444 1 9 -2 -2 578.186 50.1248 1 9 2 -1 1457.78 87.9396 1 9 -2 -1 1575.27 83.4962 1 9 2 012363.20 429.178 1 9 -2 012551.30 517.152 1 9 2 1 402.782 57.4375 1 9 -2 1 574.92 61.8628 1 9 2 2 3045.40 111.427 1 9 -2 2 3493.71 124.997 1 9 2 3 105.018 22.7413 1 9 -2 3 83.5828 37.3048 1 9 -2 4 93.7019 35.4178 1 9 2 4 38.6921 37.928 1 9 2 5 275.639 37.4947 1 9 -2 5 185.094 56.9819 1 9 2 6 2265.03 159.804 1 9 -2 6 2404.47 163.001 1 9 2 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0 2798.06 124.673 1 9 6 1 1094.25 93.8942 1 9 -6 1 1178.50 79.0154 1 9 6 2 619.653 74.6931 1 9 -6 2 771.625 45.0975 1 9 6 3 1919.76 119.58 1 9 -6 3 2158.99 121.932 1 9 6 4 973.429 87.6911 1 9 -6 4 1213.64 62.7422 1 9 6 5 5081.76 237.139 1 9 -6 5 5869.25 271.849 1 9 6 6 1148.44 98.1051 1 9 -6 6 1410.97 117.661 1 9 6 7 127.075 49.5251 1 9 6 7 63.5884 39.7193 1 9 -6 7 91.5942 50.242 1 9 6 8 1417.46 110.656 1 9 6 8 1485.81 134.173 1 9 -6 8 1565.37 139.927 1 9 6 9 39.2589 32.09 1 9 6 9 13.4682 16.9481 1 9 -6 9-19.2155 21.8471 1 9 6 10 789.058 92.7077 1 9 6 10 897.891 68.1881 1 9 -6 10 984.355 117.072 1 9 6 11 1323.81 125.217 1 9 6 11 1210.35 114.031 1 9 -6 11 1277.19 93.4286 1 -9 6 -11 1034.39 75.9267 1 9 6 12 1975.45 161.511 1 9 6 12 1409.28 145.244 1 9 -6 12 1982.73 187.587 1 -9 6 -12 1757.60 108.351 1 9 6 13 333.536 83.5961 1 9 6 13 237.154 47.5117 1 9 -6 13 342.57 62.2882 1 -9 6 -13 360.361 49.9658 1 9 6 14 2493.24 215.962 1 9 -6 14 3188.39 283.857 1 9 6 14 3306.96 179.644 1 -9 6 -14 3025.77 168.671 1 9 7 -16 18.7496 69.6222 1 -9 -7 16 85.3563 32.4155 1 9 7 -15 174.963 78.487 1 -9 -7 15 112.741 58.7393 1 9 7 -14 1072.05 148.81 1 -9 -7 14 1056.70 117.346 1 9 7 -13 3580.79 268.445 1 -9 -7 13 3449.73 161.977 1 9 7 -12 6632.97 318.90 1 -9 -7 12 7037.05 355.39 1 9 7 -11 1168.58 99.1871 1 -9 -7 11 1315.99 81.0104 1 9 7 -1010227.20 452.377 1 -9 -7 1010606.60 501.00 1 9 7 -9 917.177 80.7496 1 -9 -7 9 930.51 65.1336 1 9 7 -8 2719.91 202.248 1 -9 -7 8 2663.21 119.108 1 9 7 -7 28.6002 47.1336 1 -9 -7 7 66.7566 36.7638 1 9 7 -6 128.016 58.8989 1 9 -7 -6 170.809 14.4493 1 9 -7 -6 141.226 10.5971 1 -9 -7 6 153.969 46.601 1 9 7 -5 2521.64 174.347 1 9 -7 -5 2428.12 64.8616 1 9 -7 -5 2313.88 61.4687 1 -9 -7 5 2751.90 149.449 1 9 7 -4 8.10326 37.285 1 9 -7 -4 30.9834 10.8843 1 9 -7 -4 12.2176 14.7127 1 -9 -7 4 35.8202 30.2189 1 9 7 -3 4583.36 243.056 1 9 -7 -3 4613.99 145.804 1 9 -7 -3 4578.61 143.955 1 -9 -7 3 5116.24 241.164 1 9 7 -2 222.454 54.8993 1 9 -7 -2 210.231 25.5695 1 9 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10 -6 -9 619.642 31.5637 1 -10 -6 9 600.668 51.7711 1 10 6 -8 6121.11 347.81 1 10 -6 -8 5889.28 174.704 1 10 -6 -8 5965.54 185.001 1 -10 -6 8 6366.32 299.158 1 10 6 -7 7859.85 411.946 1 10 -6 -7 7349.36 247.013 1 10 -6 -7 7730.97 271.845 1 -10 -6 7 8253.24 376.886 1 10 6 -6 1642.65 149.10 1 10 -6 -6 1496.00 57.3447 1 10 -6 -6 1582.43 84.2446 1 -10 -6 6 1699.38 127.097 1 10 -6 -525924.80 1082.72 1 10 -6 -525252.90 1031.86 1 10 6 -524428.70 1235.99 1 -10 -6 526184.40 1236.63 1 10 6 -4 1850.33 156.302 1 10 -6 -4 2016.61 91.2807 1 10 -6 -4 2031.92 101.343 1 -10 -6 4 2004.03 137.193 1 10 6 -3 5307.14 271.493 1 10 -6 -3 5831.94 209.852 1 10 -6 -3 5287.27 189.378 1 -10 -6 3 4168.84 247.917 1 10 6 -2 1848.58 135.057 1 10 -6 -2 2141.11 97.1909 1 10 -6 -2 1723.16 82.0862 1 -10 -6 2 1399.75 166.596 1 10 -6 -1-2.21966 11.4309 1 10 -6 -1 8.96305 11.5376 1 10 6 -1-4.12745 15.6438 1 10 6 0 1561.22 81.9287 1 10 -6 0 1570.76 95.4542 1 10 6 1 1325.15 72.8945 1 10 -6 1 1546.32 96.8428 1 10 6 2 4140.40 165.268 1 10 -6 2 4696.03 171.941 1 10 -6 3 776.123 75.1481 1 10 6 3 652.174 50.4053 1 10 6 4 152.956 48.1348 1 10 -6 4 234.646 50.2622 1 10 6 5 2135.25 140.495 1 10 -6 5 2439.58 114.838 1 10 6 6 1232.70 109.243 1 10 -6 6 1632.28 130.52 1 10 6 7 282.023 63.3042 1 10 6 7 385.863 80.1301 1 10 -6 7 415.355 49.0696 1 10 6 8 1974.56 102.403 1 10 6 8 2119.53 120.803 1 10 -6 8 2283.40 171.559 1 10 6 9 105.384 52.685 1 10 6 9 91.2116 45.4242 1 10 -6 9 82.3243 56.041 1 10 6 10 258.905 38.4327 1 10 6 10 210.833 70.5896 1 10 -6 10 262.652 48.917 1 10 6 11 246.171 48.336 1 10 6 11 257.912 62.9097 1 10 -6 11 258.311 86.1757 1 10 6 12 176.026 72.3911 1 10 6 12 152.44 37.4848 1 10 -6 12 213.326 51.4559 1 10 6 13 426.302 97.4267 1 10 6 13 303.035 87.2654 1 10 -6 13 472.666 114.225 1 10 7 -15 188.593 95.7851 1 -10 -7 15 285.476 69.2984 1 10 7 -14 2189.31 147.821 1 -10 -7 14 2107.35 116.793 1 10 7 -13-3.88621 25.40 1 -10 -7 13 5.48784 19.2288 1 10 7 -12-13.9033 29.2091 1 -10 -7 12-11.6514 35.4552 1 10 7 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5212.40 339.485 1 -10 -8 8 5539.48 294.766 1 10 8 -7 7774.70 448.875 1 -10 -8 7 8069.94 333.334 1 10 8 -6 461.656 60.0033 1 -10 -8 6 427.419 50.295 1 10 8 -5 5953.96 271.534 1 -10 -8 5 6528.67 263.295 1 10 8 -4 119.407 32.8543 1 10 -8 -4 79.1424 13.5225 1 10 -8 -4 68.1172 13.6371 1 -10 -8 4 104.488 31.09 1 10 8 -3 4439.04 195.516 1 10 -8 -3 4292.51 136.573 1 10 -8 -3 4411.97 157.027 1 -10 -8 3 3883.87 199.907 1 10 8 -2 32.5577 36.6883 1 10 -8 -2 7.57614 15.5912 1 10 -8 -2 19.7012 14.8592 1 -10 -8 2 33.707 29.454 1 10 8 -1 17.2987 39.6557 1 10 -8 -1 42.5917 20.1444 1 10 -8 -1 22.455 20.0863 1 10 8 0 5446.53 292.352 1 10 -8 0 5785.85 230.454 1 10 8 1 59.9616 41.5305 1 10 -8 1 47.9104 29.3751 1 10 8 2 1589.01 131.797 1 10 -8 2 1809.52 110.924 1 10 8 3-6.95804 16.9179 1 10 -8 3 23.7558 23.7015 1 10 8 4 116.965 28.9519 1 10 -8 4 138.742 47.2918 1 10 8 5-3.20855 30.6842 1 10 -8 5 31.603 32.9236 1 10 8 6 469.533 77.0764 1 10 -8 6 631.436 88.2162 1 10 8 7 1526.82 142.524 1 10 8 7 1089.87 116.219 1 10 -8 7 1363.13 90.9056 1 10 8 8 2324.95 164.869 1 10 8 8 2491.61 197.111 1 10 -8 8 2356.58 200.953 1 10 8 9 243.429 75.3965 1 10 8 9 225.499 63.1732 1 10 -8 9 289.20 83.8801 1 10 8 10 107.74 32.7896 1 10 8 10 98.9451 40.0248 1 10 -8 10 166.76 44.3878 1 10 9 -11 1189.44 111.257 1 -10 -9 11 1164.00 85.276 1 10 9 -10 2124.55 225.624 1 -10 -9 10 2219.42 177.489 1 10 9 -9 825.491 140.893 1 -10 -9 9 885.542 110.239 1 10 9 -8 2389.51 225.113 1 -10 -9 8 2633.00 135.66 1 10 9 -7 6263.01 303.795 1 -10 -9 7 7010.53 368.734 1 10 9 -6 89.5155 36.0606 1 -10 -9 6 27.4634 47.5582 1 10 9 -5 1037.78 133.133 1 -10 -9 5 1168.42 114.54 1 10 9 -4 139.806 63.8452 1 -10 -9 4 138.309 57.8787 1 10 9 -3 2263.71 173.076 1 -10 -9 3 1877.20 181.425 1 10 9 -2 357.523 49.4884 1 10 9 -1 140.263 35.6374 1 10 9 0 4293.39 252.058 1 10 -9 0 4223.91 168.712 1 10 9 1 68.0787 48.0814 1 10 -9 1 88.9941 30.7881 1 10 9 2 1.94071 37.1243 1 10 -9 2 36.5181 27.0144 1 10 9 3-2.07708 30.8863 1 10 -9 3-11.2049 25.523 1 10 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87.6386 1 11 1 -19 4948.76 344.829 1 11 -1 -19 4888.69 304.926 1 -11 -1 19 5340.43 296.789 1 -11 1 19 5566.96 231.977 1 11 1 -18 122.329 66.4664 1 11 -1 -18 93.4951 57.6582 1 -11 -1 18 137.93 33.7842 1 -11 1 18 131.875 48.6048 1 11 1 -17 1716.25 163.342 1 11 -1 -17 1650.99 142.242 1 -11 -1 17 1734.12 92.803 1 -11 1 17 1971.85 123.654 1 11 1 -16 14.2362 39.6132 1 11 -1 -16 37.5675 33.8231 1 -11 -1 16 13.1177 29.4068 1 -11 1 16 10.9792 16.3495 1 11 1 -15 1427.19 144.07 1 11 -1 -15 1537.19 87.135 1 -11 -1 15 1535.81 111.70 1 -11 1 15 1785.90 105.845 1 11 1 -14 372.518 48.1848 1 11 -1 -14 325.918 68.8288 1 -11 -1 14 271.053 58.6408 1 -11 1 14 352.431 51.6584 1 11 1 -13 9039.16 375.925 1 11 -1 -13 9140.03 425.183 1 -11 -1 13 9418.24 405.677 1 -11 1 13 9635.72 397.562 1 11 1 -12 204.537 66.7966 1 11 -1 -12 261.452 34.5221 1 -11 -1 12 236.951 50.0606 1 -11 1 12 219.798 29.0309 1 11 1 -11 493.725 85.277 1 11 -1 -11 573.196 73.0158 1 -11 -1 11 560.173 41.5415 1 -11 1 11 579.913 38.0352 1 11 1 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11 -2 10 485.138 60.643 1 11 2 11 318.64 83.1114 1 11 -2 11 263.356 85.0946 1 11 2 12 791.359 127.748 1 11 -2 12 707.424 127.68 1 11 2 13 152.679 72.9707 1 11 -2 13 120.542 73.3238 1 11 2 14 130.856 65.4876 1 11 -2 14 60.7874 67.3871 1 11 2 15 72.8475 62.8133 1 11 -2 15 64.4907 39.2216 1 11 3 -18 740.509 133.49 1 11 -3 -18 640.795 83.4161 1 -11 -3 18 729.069 100.791 1 -11 3 18 810.548 77.0164 1 11 -3 -17 1888.41 129.292 1 11 3 -17 1947.32 195.742 1 -11 -3 17 1949.88 152.236 1 -11 3 17 2107.53 116.443 1 11 3 -16 371.654 95.0919 1 11 -3 -16 411.948 58.4742 1 -11 -3 16 383.509 44.8778 1 -11 3 16 381.56 49.4481 1 11 3 -15 266.496 77.9936 1 11 -3 -15 258.744 48.0166 1 -11 -3 15 288.301 36.5419 1 -11 3 15 159.095 38.9704 1 11 3 -14 1364.94 151.799 1 11 -3 -14 1399.95 96.4342 1 -11 -3 14 1288.29 113.719 1 -11 3 14 1410.07 80.1891 1 11 3 -13 1282.54 148.334 1 11 -3 -13 1309.30 94.7355 1 -11 -3 13 1364.53 75.129 1 -11 3 13 1369.67 86.2103 1 11 3 -12 296.625 79.4976 1 11 -3 -12 240.435 29.1993 1 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996.934 99.1997 1 11 -3 1 1159.83 105.286 1 11 -3 1 1096.65 79.1826 1 11 3 2 1816.58 131.128 1 11 -3 2 2137.09 138.667 1 11 3 3 1828.08 126.90 1 11 -3 3 2099.66 138.789 1 11 3 4 1821.52 126.197 1 11 -3 4 2041.05 139.70 1 11 3 5 9525.78 399.673 1 11 3 5 7540.21 377.197 1 11 -3 5 8707.35 424.41 1 11 3 6 3514.81 165.176 1 11 3 6 2504.21 130.811 1 11 -3 6 2793.26 195.455 1 11 3 7 8212.68 356.40 1 11 -3 7 7342.79 390.897 1 11 3 8 1285.84 122.117 1 11 3 8 628.921 115.517 1 11 -3 8 1221.52 124.558 1 11 -3 9 1849.72 166.14 1 11 3 9 1942.37 162.114 1 11 3 10 75.4829 46.7543 1 11 -3 10 30.1566 30.5746 1 11 3 11 90.5106 56.8846 1 11 -3 11 62.426 35.4773 1 11 3 12 1817.29 186.157 1 11 -3 12 1881.46 194.262 1 11 3 13 14.3377 30.7861 1 11 -3 13 39.8943 52.3651 1 11 3 14 63.0987 39.9739 1 11 -3 14 105.359 41.8784 1 11 4 -17 1841.74 204.828 1 11 -4 -17 1751.25 109.676 1 -11 -4 17 2155.31 159.797 1 -11 4 17 2189.72 117.125 1 11 4 -16 227.417 89.6158 1 11 -4 -16 254.394 44.3795 1 -11 -4 16 240.562 64.7986 1 -11 4 16 319.931 45.3636 1 11 4 -15 87.9938 62.8958 1 11 -4 -15 84.2309 31.809 1 -11 -4 15 89.3637 28.776 1 -11 4 15 99.6792 31.1719 1 11 4 -14 615.62 112.284 1 11 -4 -14 611.067 56.4841 1 -11 -4 14 592.555 82.6359 1 -11 4 14 557.545 64.1058 1 11 4 -13-25.0384 34.0992 1 11 -4 -13 4.18163 10.6498 1 -11 -4 13-1.51083 15.4185 1 11 4 -12 431.32 92.1726 1 11 -4 -12 395.203 47.1066 1 -11 -4 12 393.291 66.91 1 11 4 -11 2117.11 174.447 1 11 -4 -11 2010.84 98.9374 1 -11 -4 11 1981.63 94.9553 1 11 4 -10 787.278 108.888 1 11 -4 -10 822.027 58.1167 1 -11 -4 10 813.767 82.5238 1 11 4 -9 1256.58 127.65 1 11 -4 -9 1267.94 70.2696 1 -11 -4 9 1245.17 99.4539 1 11 4 -810510.70 502.714 1 11 -4 -810045.60 377.899 1 -11 -4 810657.50 400.136 1 11 4 -7 4908.90 206.619 1 11 -4 -7 4806.87 153.086 1 -11 -4 7 5148.73 189.86 1 11 4 -6 3270.51 148.02 1 11 -4 -6 3384.87 140.529 1 -11 -4 6 3329.04 175.094 1 11 4 -5 1319.06 115.14 1 11 -4 -5 1233.30 75.0173 1 -11 -4 5 1240.82 105.516 1 11 4 -4 467.327 73.0386 1 11 -4 -4 471.505 47.2093 1 -11 -4 4 364.598 78.9535 1 11 4 -3 36.4858 36.0165 1 11 -4 -3 26.8104 28.5165 1 11 -4 -3 50.6265 24.1206 1 -11 -4 3 29.456 29.5309 1 11 4 -2 222.958 55.3683 1 11 -4 -2 212.969 24.7162 1 11 -4 -2 303.853 47.0431 1 11 4 -1 869.963 62.0255 1 11 -4 -1 1036.78 86.8859 1 11 -4 -1 881.215 78.2004 1 11 4 028977.00 1338.40 1 11 -4 034873.40 1662.37 1 11 -4 027852.20 1441.51 1 11 4 1 109.299 28.107 1 11 -4 1 163.222 47.9734 1 11 4 2 2076.82 92.3483 1 11 -4 2 2456.28 142.065 1 11 4 3 867.501 57.1814 1 11 -4 3 929.903 90.5378 1 11 4 4 1453.90 79.3214 1 11 -4 4 1580.93 120.898 1 11 4 5 3705.21 209.766 1 11 -4 5 3983.53 229.525 1 11 4 6 5460.86 310.248 1 11 4 6 4056.15 241.658 1 11 -4 6 4547.88 266.858 1 11 4 7 3373.30 212.374 1 11 4 7 4311.62 269.175 1 11 -4 7 4185.23 193.132 1 11 4 8 2391.44 179.287 1 11 4 8 1705.22 105.279 1 11 -4 8 2386.57 125.916 1 11 4 9 586.071 101.053 1 11 -4 9 637.531 102.712 1 11 4 9 656.403 62.997 1 11 4 10 657.884 77.4964 1 11 4 10 1284.91 84.3677 1 11 -4 10 1171.86 129.645 1 11 4 11 435.389 89.466 1 11 4 11 6.83124 102.777 1 11 -4 11 409.414 59.0893 1 11 4 12 1875.63 183.745 1 11 -4 12 1704.92 129.325 1 11 4 13 162.016 77.0829 1 11 -4 13 176.579 85.2904 1 11 -4 14 82.0174 71.069 1 11 4 14 80.4105 65.1507 1 11 5 -17 1074.21 109.904 1 -11 -5 17 1202.14 126.269 1 11 5 -16 802.503 88.912 1 -11 -5 16 804.089 68.082 1 11 5 -15-0.02554 31.1903 1 -11 -5 15 33.0326 22.943 1 11 5 -14 1058.04 93.7153 1 11 -5 -14 915.722 54.5768 1 -11 -5 14 1078.30 105.814 1 11 5 -13 810.299 79.9152 1 11 -5 -13 701.969 48.6211 1 -11 -5 13 813.284 59.9165 1 11 5 -12 246.537 52.085 1 11 -5 -12 294.773 33.1469 1 -11 -5 12 286.347 61.3856 1 11 5 -11 3052.42 159.285 1 11 -5 -11 2930.42 134.491 1 -11 -5 11 3012.95 127.539 1 11 5 -10 53.7067 27.8662 1 11 -5 -10 9.87816 17.9286 1 -11 -5 10 53.806 32.4865 1 11 5 -9 1644.25 103.288 1 11 -5 -9 1651.50 72.9407 1 -11 -5 9 1672.86 82.198 1 11 5 -8 3733.89 176.325 1 11 -5 -8 3762.58 137.553 1 -11 -5 8 4114.14 160.078 1 11 5 -7 4188.13 186.445 1 11 -5 -7 4144.28 151.331 1 -11 -5 7 4637.43 222.967 1 11 5 -6 109.292 30.5549 1 11 -5 -6 117.986 27.759 1 11 -5 -6 34.7182 24.8123 1 -11 -5 6 70.9027 40.6664 1 11 5 -5 861.885 65.9394 1 11 -5 -5 826.484 63.8239 1 11 -5 -5 863.942 58.2579 1 -11 -5 5 1010.67 93.4265 1 11 5 -4 1329.58 119.631 1 11 -5 -4 1331.46 73.1792 1 11 -5 -4 1401.17 82.8876 1 -11 -5 4 1188.08 127.283 1 11 5 -3 322.633 69.601 1 11 -5 -3 414.116 49.1449 1 11 -5 -3 381.344 42.2325 1 -11 -5 3 358.509 90.8352 1 11 5 -2 1193.73 109.292 1 11 -5 -2 1155.84 73.8211 1 11 -5 -2 1342.24 86.2351 1 11 -5 -1 883.723 50.816 1 11 -5 -1 1007.99 84.9165 1 11 5 -1 828.101 99.2421 1 11 5 026181.80 1264.91 1 11 -5 030389.40 1407.12 1 11 -5 022399.10 1241.92 1 11 5 1 27.7375 30.5963 1 11 -5 1-5.30078 29.0706 1 11 5 2 3223.51 182.072 1 11 -5 2 3741.96 150.99 1 11 -5 3 547.094 71.7709 1 11 5 3 424.363 64.751 1 11 5 4 665.371 79.6668 1 11 -5 4 886.168 93.4953 1 11 5 5 627.922 51.0623 1 11 -5 5 601.194 94.3645 1 11 5 6 3765.74 180.094 1 11 5 6 2843.60 139.919 1 11 -5 6 3324.00 161.769 1 11 5 7 4052.38 196.854 1 11 5 7 3243.85 212.966 1 11 -5 7 3872.24 246.943 1 11 5 8 1894.73 148.328 1 11 5 8 2295.47 179.655 1 11 -5 8 2182.03 180.802 1 11 5 9 426.399 83.813 1 11 5 9 364.549 44.8368 1 11 -5 9 411.344 56.1044 1 11 5 10 920.535 119.345 1 11 -5 10 710.081 79.5395 1 11 5 10 956.623 97.1531 1 11 5 11 475.059 55.4479 1 11 5 11 187.713 48.6846 1 11 -5 11 298.473 95.1078 1 11 5 12 1263.42 101.008 1 11 5 12 860.319 130.848 1 11 -5 12 1218.56 110.076 1 11 5 13 453.392 93.8048 1 11 5 13 39.4118 95.732 1 11 -5 13 447.113 106.20 1 11 6 -15-3.03016 43.6718 1 -11 -6 15-3.73594 31.2887 1 11 6 -14 188.014 87.0716 1 -11 -6 14 229.765 62.4072 1 11 6 -13 2882.50 238.073 1 -11 -6 13 2694.87 132.034 1 11 6 -12 450.373 63.3577 1 -11 -6 12 435.058 74.7301 1 11 6 -11 2357.37 137.442 1 -11 -6 11 2378.53 114.448 1 11 6 -10 443.764 60.6285 1 11 -6 -10 373.144 26.8824 1 11 -6 -10 467.838 29.9006 1 -11 -6 10 453.897 70.3125 1 11 6 -9 624.778 64.2219 1 11 -6 -9 537.702 31.3137 1 11 -6 -9 520.489 35.5224 1 -11 -6 9 558.174 75.9656 1 11 6 -8 2236.83 128.036 1 11 -6 -8 2100.81 75.3478 1 11 -6 -8 2210.96 85.1634 1 -11 -6 8 2357.18 109.634 1 11 6 -7 5037.27 228.047 1 11 -6 -7 5137.55 178.445 1 11 -6 -7 4859.97 160.785 1 -11 -6 7 5391.56 265.322 1 11 6 -6 171.369 39.0167 1 11 -6 -6 144.45 25.0115 1 11 -6 -6 140.051 27.2919 1 -11 -6 6 152.714 51.1249 1 11 6 -5 1714.02 102.853 1 11 -6 -5 1915.80 83.1105 1 11 -6 -5 1935.21 90.1487 1 -11 -6 5 1786.82 129.564 1 11 6 -4 449.41 53.5179 1 11 -6 -4 526.595 47.9103 1 11 -6 -4 533.564 43.7825 1 -11 -6 4 401.417 78.1823 1 11 6 -3 849.103 65.5359 1 11 -6 -3 930.469 64.8164 1 11 -6 -3 803.285 57.2006 1 -11 -6 3 870.172 112.289 1 11 6 -2 2287.07 115.136 1 11 -6 -2 2636.79 125.478 1 11 -6 -2 2179.39 106.591 1 11 6 -1 672.168 59.8653 1 11 -6 -1 812.432 73.0644 1 11 -6 -1 659.015 42.6637 1 11 6 019419.30 830.174 1 11 -6 023063.80 935.378 1 11 -6 015098.50 825.745 1 11 6 1 9.66269 22.6638 1 11 -6 1 72.3709 34.1472 1 11 6 2 3926.72 167.677 1 11 -6 2 4871.13 237.009 1 11 6 3 70.0182 48.3187 1 11 -6 3 157.285 31.1538 1 11 6 4 850.20 93.6659 1 11 -6 4 1066.08 104.886 1 11 6 5 493.757 74.4083 1 11 -6 5 507.709 83.7223 1 11 6 6 464.116 60.2206 1 11 6 6 422.264 73.0809 1 11 -6 6 467.971 55.0407 1 11 6 7 1474.92 98.2881 1 11 6 7 1157.56 78.3375 1 11 -6 7 1293.38 137.828 1 11 6 8 42.5491 40.0139 1 11 6 8 49.958 46.9768 1 11 -6 8 32.729 29.1028 1 11 6 9 619.411 58.8381 1 11 -6 9 692.097 110.673 1 11 6 9 757.526 106.254 1 11 6 10 277.91 71.6357 1 11 6 10 421.923 86.0893 1 11 -6 10 314.122 92.7609 1 11 6 11 1077.49 95.1058 1 11 6 11 908.466 116.993 1 11 -6 11 1104.97 102.168 1 11 6 12 1712.65 124.895 1 11 6 12 1462.86 151.546 1 11 -6 12 1746.38 203.257 1 11 7 -14 184.154 85.3274 1 -11 -7 14 133.085 38.1363 1 11 7 -13 3787.09 306.089 1 -11 -7 13 4013.57 241.524 1 11 7 -12 126.443 73.0582 1 -11 -7 12 99.1727 32.5112 1 11 7 -11 1765.28 181.913 1 -11 -7 11 1639.28 135.329 1 11 7 -10 2.0233 51.4173 1 -11 -7 10 37.931 23.4493 1 11 7 -9 863.063 86.5673 1 -11 -7 9 1010.20 99.0443 1 11 7 -8 152.541 42.6129 1 -11 -7 8 135.257 33.6182 1 11 7 -7 2918.95 156.751 1 -11 -7 7 3104.47 137.422 1 11 7 -6 460.078 56.7696 1 11 -7 -6 382.57 27.1877 1 11 -7 -6 387.007 28.0241 1 -11 -7 6 489.981 73.2822 1 11 7 -5 3763.84 181.23 1 11 -7 -5 3934.94 134.092 1 11 -7 -5 3867.20 133.824 1 -11 -7 5 4146.61 237.676 1 11 7 -4 68.7811 40.3249 1 11 -7 -4 6.10925 16.876 1 11 -7 -4 29.5206 17.3136 1 -11 -7 4-1.26198 42.9418 1 11 7 -3 2158.20 175.204 1 11 -7 -3 2234.93 99.1143 1 11 -7 -3 2397.12 106.444 1 -11 -7 3 2150.68 215.823 1 11 7 -2 6879.23 366.693 1 11 -7 -2 6388.04 257.083 1 11 -7 -2 7544.83 294.868 1 11 7 -1 465.396 87.1646 1 11 -7 -1 566.602 59.2678 1 11 -7 -1 450.94 54.4432 1 11 7 0 6233.94 329.039 1 11 -7 0 7576.60 307.919 1 11 -7 0 4842.16 296.136 1 11 7 1 199.219 60.3503 1 11 -7 1 214.118 53.3011 1 11 7 2 7879.43 397.742 1 11 -7 2 8694.42 337.308 1 11 7 3 1.31332 15.0153 1 11 -7 3-3.07999 22.4459 1 11 7 4 106.592 29.4337 1 11 -7 4 106.609 29.8176 1 11 7 5 171.192 56.4195 1 11 -7 5 214.371 61.1149 1 11 7 6 450.45 57.765 1 11 7 6 328.554 73.2776 1 11 -7 6 394.938 51.8446 1 11 7 7 106.092 33.3317 1 11 7 7 37.3436 27.491 1 11 -7 7 38.7781 52.7098 1 11 7 8 213.902 64.0442 1 11 7 8 262.461 48.9296 1 11 -7 8 233.456 48.0295 1 11 7 9 7.72745 41.4442 1 11 7 9 14.992 34.5506 1 11 -7 9 14.4322 44.3858 1 11 7 10 1517.74 147.178 1 11 7 10 1847.47 176.407 1 11 -7 10 1714.68 128.065 1 11 8 -12 870.345 154.489 1 -11 -8 12 880.195 72.5738 1 11 8 -11 592.046 127.989 1 -11 -8 11 647.713 95.657 1 11 8 -10 130.075 79.1523 1 -11 -8 10 158.389 57.3811 1 11 8 -9 716.09 79.5094 1 -11 -8 9 687.653 62.7284 1 11 8 -8 250.759 52.7652 1 -11 -8 8 226.724 65.5332 1 11 8 -7 1495.76 110.023 1 -11 -8 7 1613.17 135.516 1 11 8 -6 454.20 107.567 1 -11 -8 6 614.896 57.4407 1 11 8 -5 4346.48 278.726 1 -11 -8 5 4347.93 198.753 1 11 8 -4 154.308 60.5491 1 -11 -8 4 109.861 40.2967 1 11 8 -3 3095.42 213.504 1 11 -8 -3 2974.52 110.196 1 11 -8 -3 2906.17 111.166 1 -11 -8 3 2502.66 256.421 1 11 8 -2 7456.62 324.538 1 11 -8 -2 7436.16 279.721 1 11 -8 -2 7364.34 285.141 1 11 8 -1 957.928 76.6707 1 11 -8 -1 966.642 68.626 1 11 -8 -1 914.419 64.643 1 11 8 0 3768.30 172.441 1 11 -8 0 4043.71 173.268 1 11 -8 0 3021.64 176.201 1 11 8 1 433.804 84.5499 1 11 -8 1 541.225 62.5952 1 11 8 2 3644.51 229.69 1 11 -8 2 4214.27 209.508 1 11 8 3 343.595 71.3188 1 11 -8 3 371.328 41.0994 1 11 8 4 66.3607 28.7349 1 11 -8 4 84.9605 44.3102 1 11 8 5 1821.23 150.871 1 11 -8 5 1957.93 157.709 1 11 8 6 45.9883 31.3461 1 11 8 6 34.2208 41.6584 1 11 -8 6 36.6133 28.6324 1 11 8 7 81.5673 34.6589 1 11 8 7 42.5811 28.0675 1 11 -8 7 40.8214 53.2177 1 11 8 8 124.456 61.0155 1 11 8 8 137.651 74.1972 1 11 -8 8 278.102 74.4151 1 11 9 -9 1343.25 118.524 1 -11 -9 9 1540.22 143.137 1 11 9 -8 1091.86 106.161 1 -11 -9 8 1319.27 89.3682 1 11 9 -7 350.276 108.593 1 -11 -9 7 497.725 85.5191 1 11 9 -6 641.288 125.082 1 -11 -9 6 701.119 100.058 1 11 9 -5 3530.91 259.351 1 -11 -9 5 3765.41 248.941 1 11 9 -4 196.208 47.2177 1 -11 -9 4 263.456 80.3132 1 11 9 -3 2189.37 125.931 1 -11 -9 3 1642.74 143.505 1 11 9 -2 5273.61 323.93 1 11 9 -1 135.596 63.5633 1 11 9 0 480.04 86.0725 1 11 -9 0 373.906 45.1036 1 11 -9 0 419.745 46.3033 1 11 9 1 227.295 42.9187 1 11 -9 1 225.522 45.6845 1 11 9 2 3961.65 255.154 1 11 -9 2 4137.65 210.149 1 11 9 3 209.357 69.3419 1 11 -9 3 255.34 59.1902 1 11 9 4 120.139 59.5474 1 11 -9 4 177.693 56.3342 1 11 9 5 1371.08 138.409 1 11 -9 5 1554.44 97.5215 1 11 10 -2 4306.47 222.135 1 11 10 -1 284.243 84.4919 1 12 0 -18 1131.04 145.592 1 -12 0 18 1249.76 112.98 1 12 0 -17 7.11835 33.5595 1 -12 0 17-4.10486 15.4379 1 12 0 -16 179.082 40.0485 1 -12 0 16 169.493 48.2103 1 12 0 -15 34.7031 25.9963 1 -12 0 15 27.21 20.3816 1 12 0 -14 5605.72 317.734 1 -12 0 14 5839.61 278.561 1 12 0 -13 -28.728 33.6624 1 -12 0 13 1.36389 16.2496 1 12 0 -1212344.50 514.347 1 -12 0 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4420.83 234.30 1 -12 2 13 4500.23 200.975 1 12 2 -12 6931.07 387.647 1 12 -2 -12 6878.04 322.582 1 -12 -2 12 7135.89 273.307 1 -12 2 12 7016.32 258.403 1 12 2 -11 33.2971 24.7926 1 12 -2 -11 13.4497 17.9154 1 -12 -2 11-0.51688 30.0022 1 -12 2 11 19.7531 29.5881 1 12 2 -10 4166.31 181.262 1 12 -2 -10 4187.15 197.763 1 -12 -2 10 4461.97 205.981 1 -12 2 10 3273.23 208.862 1 12 -2 -9 220.03 46.5425 1 12 2 -9 224.288 62.9893 1 -12 -2 9 193.253 30.4635 1 12 2 -811283.00 532.845 1 12 -2 -810934.20 409.882 1 -12 -2 811896.90 444.712 1 12 2 -7 4407.61 183.502 1 12 -2 -7 4270.84 200.966 1 -12 -2 7 4658.76 181.453 1 12 2 -6 2822.25 130.458 1 12 -2 -6 2743.80 147.341 1 -12 -2 6 3356.33 144.716 1 12 2 -5 1064.11 103.164 1 12 -2 -5 1140.16 58.2305 1 -12 -2 5 1092.50 87.7001 1 12 2 -4 6843.53 318.444 1 12 -2 -4 6978.78 293.651 1 12 2 -3 741.973 51.1282 1 12 -2 -3 695.806 46.4058 1 12 2 -2 10.6422 18.4947 1 12 -2 -2 19.8891 26.4617 1 12 2 -1 837.407 95.2625 1 12 -2 -1 984.878 55.0391 1 12 2 0 5661.26 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396.598 47.0608 1 -12 3 17 403.17 56.3348 1 12 3 -16 76.6942 35.74 1 12 -3 -16 25.6006 36.0905 1 -12 -3 16 77.4327 25.9998 1 -12 3 16 2.58128 30.1429 1 12 3 -15 1488.94 114.515 1 12 -3 -15 1663.25 113.448 1 -12 -3 15 1572.71 128.304 1 -12 3 15 1532.84 104.739 1 12 3 -14 2874.53 239.184 1 12 -3 -14 3029.11 168.101 1 -12 -3 14 2941.80 137.983 1 -12 3 14 3191.04 159.497 1 12 3 -13 6364.27 375.101 1 12 -3 -13 6368.04 284.513 1 -12 -3 13 6492.92 308.273 1 -12 3 13 5503.51 280.284 1 12 3 -12 6688.12 377.218 1 12 -3 -12 6688.31 286.211 1 -12 -3 12 6715.74 255.854 1 -12 3 12 4827.77 288.211 1 12 3 -11 62.4397 43.9653 1 12 -3 -11 32.6458 27.2851 1 -12 -3 11-6.91918 31.1217 1 12 -3 -10 926.777 74.2488 1 12 3 -10 937.51 114.433 1 -12 -3 10 948.62 58.4022 1 12 3 -9 169.169 62.3955 1 12 -3 -9 183.891 25.3316 1 -12 -3 9 163.97 47.4876 1 12 3 -8 359.312 46.021 1 12 -3 -8 335.133 47.858 1 -12 -3 8 244.066 58.5071 1 12 3 -7 7306.85 292.231 1 12 -3 -7 6893.06 286.833 1 -12 -3 7 7922.30 340.80 1 12 3 -6 5603.47 287.07 1 12 -3 -6 5455.71 236.308 1 -12 -3 6 5891.00 281.669 1 12 3 -5 1666.46 131.722 1 12 -3 -5 1815.67 101.956 1 -12 -3 5 1775.41 140.38 1 12 3 -4 3279.97 188.917 1 12 -3 -4 3315.94 120.558 1 12 3 -3 1201.81 69.1701 1 12 -3 -3 1239.83 85.2056 1 12 3 -2 683.935 50.2294 1 12 -3 -2 643.351 44.1701 1 12 3 -1 1560.15 82.8069 1 12 -3 -1 2152.24 133.304 1 12 -3 -1 1733.23 106.433 1 12 3 0 2486.39 113.508 1 12 -3 0 2482.94 107.837 1 12 -3 0 3039.32 168.756 1 12 3 1 141.635 28.3318 1 12 -3 1 126.86 48.346 1 12 -3 1 126.954 31.6999 1 12 3 2 193.466 30.621 1 12 -3 2 205.324 53.8757 1 12 3 3 447.117 43.0222 1 12 -3 3 457.561 73.2214 1 12 3 4-5.89045 15.5526 1 12 -3 4 12.7745 28.2806 1 12 3 5 8455.87 368.729 1 12 3 5 6292.18 338.272 1 12 -3 5 7238.31 389.723 1 12 3 6 491.602 63.3614 1 12 3 6 285.964 73.953 1 12 -3 6 495.26 87.3207 1 12 3 7 2022.44 121.167 1 12 3 7 3023.12 152.265 1 12 -3 7 2606.95 187.617 1 12 3 8 691.254 100.485 1 12 3 8 231.347 91.9781 1 12 -3 8 611.153 57.8458 1 12 3 9 546.90 93.5796 1 12 3 9 147.005 89.388 1 12 -3 9 532.627 55.6802 1 12 -3 10 2140.85 137.749 1 12 3 10 2075.74 190.442 1 12 3 11 498.995 87.9483 1 12 3 11 18.1883 60.6253 1 12 -3 11 510.361 90.4211 1 12 3 12 3660.50 292.328 1 12 -3 12 3481.36 304.002 1 12 3 13 282.838 96.4182 1 12 -3 13 273.789 63.3233 1 12 4 -17 456.572 71.6197 1 12 -4 -17 391.823 54.5921 1 -12 -4 17 598.542 83.3088 1 -12 4 17 214.733 72.431 1 12 4 -16 310.91 61.1576 1 12 -4 -16 261.75 50.8837 1 -12 4 16 223.749 61.3843 1 -12 -4 16 325.806 43.9393 1 12 4 -15 1547.56 122.471 1 12 -4 -15 1544.10 100.62 1 -12 -4 15 1607.08 137.824 1 12 4 -14 1704.73 120.734 1 12 -4 -14 1613.78 100.701 1 -12 -4 14 1624.69 137.634 1 12 4 -13 6608.75 311.064 1 12 -4 -13 6500.65 272.865 1 -12 -4 13 6631.84 272.818 1 12 4 -12 3047.01 165.771 1 12 -4 -12 2912.81 141.527 1 -12 -4 12 3000.71 181.895 1 12 4 -11 174.381 44.0607 1 12 -4 -11 213.391 38.8252 1 -12 -4 11 167.95 32.4913 1 12 4 -10 671.588 69.3278 1 12 -4 -10 725.18 59.0863 1 -12 -4 10 749.687 53.1191 1 12 4 -9 38.2062 23.4305 1 12 -4 -9-4.36799 20.0578 1 -12 -4 9 2.40828 28.0264 1 12 4 -8 40.871 25.4966 1 12 -4 -8 3.82908 22.6993 1 -12 -4 8 35.0806 31.909 1 12 4 -7 7142.84 373.195 1 12 -4 -7 7500.54 298.315 1 -12 -4 7 7775.22 292.202 1 12 4 -6 1664.13 139.104 1 12 -4 -6 1661.43 94.5365 1 -12 -4 6 1661.79 87.4367 1 12 4 -5 943.545 98.1152 1 12 -4 -5 847.886 67.2436 1 -12 -4 5 881.623 67.8069 1 12 4 -4 1301.11 114.369 1 12 -4 -4 1483.30 67.6789 1 12 -4 -4 1315.42 58.9309 1 -12 -4 4 1158.37 94.9487 1 12 4 -3 1503.19 121.086 1 12 -4 -3 1677.31 108.564 1 12 -4 -3 1489.22 92.3555 1 12 4 -2 3219.19 136.271 1 12 -4 -2 3324.47 158.608 1 12 -4 -2 3792.38 183.084 1 12 4 -1 1698.07 85.6181 1 12 -4 -1 1881.07 121.837 1 12 -4 -1 1646.28 74.6967 1 12 4 0 180.467 32.0274 1 12 -4 0 226.052 51.1038 1 12 -4 0 213.337 46.4279 1 12 4 1 47.4231 22.8589 1 12 -4 1 148.201 39.2548 1 12 -4 1 17.7084 46.4703 1 12 4 2 194.727 33.367 1 12 -4 2 283.224 55.0611 1 12 4 3 756.243 88.5946 1 12 -4 3 888.301 91.7324 1 12 -4 4 827.621 99.3009 1 12 4 4 701.252 93.5949 1 12 4 5 7273.28 382.925 1 12 -4 5 8508.27 433.095 1 12 4 6 112.27 62.8273 1 12 4 6 71.573 28.8419 1 12 -4 6 79.1794 32.8614 1 12 4 7 3893.22 248.956 1 12 4 7 5401.92 317.705 1 12 -4 7 4713.52 218.403 1 12 4 8 144.831 40.2472 1 12 4 8 111.666 50.9123 1 12 -4 8 159.23 61.8311 1 12 4 9 849.844 77.0473 1 12 4 9 684.295 66.3502 1 12 -4 9 814.277 112.173 1 12 4 10 1403.85 152.733 1 12 4 10 1941.65 122.922 1 12 -4 10 1834.13 127.965 1 12 4 11 776.154 128.165 1 12 4 11 183.81 121.72 1 12 -4 11 929.633 86.7751 1 12 4 12 1304.97 155.609 1 12 4 12 694.558 94.8851 1 12 -4 12 1342.18 164.382 1 12 4 13 290.482 82.5039 1 12 4 13-28.3658 81.5505 1 12 -4 13 259.295 89.4554 1 12 5 -16 260.50 104.709 1 -12 -5 16 288.598 45.7929 1 12 5 -15 500.796 122.072 1 -12 -5 15 521.847 89.0091 1 12 5 -14 571.897 122.675 1 -12 -5 14 573.564 88.2959 1 12 5 -13 4698.68 326.129 1 12 -5 -13 4217.39 168.116 1 -12 -5 13 4547.65 195.289 1 12 5 -12 1506.85 172.388 1 12 -5 -12 1554.35 80.6765 1 -12 -5 12 1668.80 130.973 1 12 5 -11 656.70 107.168 1 12 -5 -11 558.12 48.0806 1 -12 -5 11 600.269 50.0054 1 12 5 -10 53.2788 51.3327 1 12 -5 -10 46.0418 22.488 1 -12 -5 10 52.5855 37.9356 1 12 5 -9 15.201 41.2211 1 12 -5 -9 10.4857 18.1162 1 -12 -5 9 31.5925 31.0517 1 12 5 -8 448.598 90.5095 1 12 -5 -8 427.65 43.2983 1 -12 -5 8 483.059 46.154 1 12 5 -7 4446.06 272.516 1 12 -5 -7 4641.41 183.553 1 -12 -5 7 4518.32 184.47 1 12 5 -6 4096.95 245.949 1 12 -5 -6 4265.58 185.365 1 12 -5 -6 4078.08 137.784 1 -12 -5 6 3873.31 231.91 1 12 5 -5 555.778 88.7552 1 12 -5 -5 649.04 60.6688 1 12 -5 -5 568.761 52.4167 1 -12 -5 5 534.533 94.3883 1 12 5 -4 532.879 77.2965 1 12 -5 -4 432.17 32.0005 1 12 -5 -4 485.752 55.0175 1 -12 -5 4 328.808 97.1265 1 12 5 -3 1448.12 132.276 1 12 -5 -3 1837.88 108.764 1 12 -5 -3 1597.37 92.5275 1 12 5 -2 6987.77 351.051 1 12 -5 -2 7984.74 340.431 1 12 -5 -2 7008.46 294.317 1 12 5 -1 1625.32 134.435 1 12 -5 -1 1650.47 104.312 1 12 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4892.87 220.75 1 12 6 -1 828.839 68.286 1 12 -6 -1 1010.84 57.3242 1 12 -6 -1 847.01 71.8022 1 12 6 0 1610.81 92.2096 1 12 -6 0 1981.96 120.526 1 12 -6 0 1301.58 117.689 1 12 6 1 56.2684 25.6199 1 12 -6 1 118.021 38.1931 1 12 -6 1 18.1301 27.6816 1 12 6 2 100.71 30.1992 1 12 -6 2 135.799 30.7563 1 12 6 3 1366.19 126.183 1 12 -6 3 1729.80 134.208 1 12 6 4 2731.27 191.046 1 12 -6 4 3216.52 215.385 1 12 6 5 6500.26 359.287 1 12 -6 5 7809.15 339.559 1 12 6 6 2053.61 131.922 1 12 6 6 1656.26 101.64 1 12 -6 6 1951.05 175.618 1 12 6 7 5227.26 253.025 1 12 6 7 3873.87 264.988 1 12 -6 7 4860.19 236.745 1 12 6 8 154.948 63.6683 1 12 -6 8 86.5486 63.9244 1 12 6 8 88.939 32.6013 1 12 6 9 402.86 95.7157 1 12 6 9 359.356 81.0355 1 12 -6 9 472.733 99.9899 1 12 6 10 474.952 106.102 1 12 6 10 434.089 88.2139 1 12 -6 10 428.577 71.1852 1 12 7 -13 1310.86 124.14 1 -12 -7 13 1342.95 135.279 1 12 7 -12 119.639 45.7555 1 -12 -7 12 64.5265 32.3143 1 12 7 -11 1488.59 120.861 1 -12 -7 11 1582.53 135.282 1 12 7 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2783.42 133.601 1 12 7 4 2462.82 186.812 1 12 -7 4 3083.68 208.842 1 12 7 5 2884.96 217.039 1 12 -7 5 3696.94 185.251 1 12 7 6 978.931 90.1268 1 12 7 6 771.15 113.768 1 12 -7 6 1010.22 133.296 1 12 7 7 3885.08 209.866 1 12 7 7 3163.00 234.308 1 12 -7 7 3803.71 207.539 1 12 7 8 338.822 82.4541 1 12 7 8 434.691 96.1853 1 12 -7 8 441.007 106.694 1 12 7 9-9.39366 44.34 1 12 7 9-14.4246 23.8927 1 12 -7 9-3.54204 30.1253 1 12 8 -10 17.7538 36.7551 1 -12 -8 10 58.7323 44.594 1 12 8 -9 213.166 87.8811 1 -12 -8 9 205.884 41.6876 1 12 8 -8 2999.81 258.632 1 -12 -8 8 3298.95 212.977 1 12 8 -7 35.9788 54.0238 1 -12 -8 7 33.5655 42.2843 1 12 8 -6 80.6035 37.8396 1 -12 -8 6 73.3606 33.024 1 12 8 -5 450.208 57.9807 1 -12 -8 5 327.497 60.0254 1 12 8 -4 603.891 65.7314 1 -12 -8 4 450.327 124.416 1 12 8 -3 15.55 42.7553 1 12 -8 -3 19.8766 16.1535 1 12 -8 -3 22.3806 17.5194 1 12 8 -2 2553.77 199.768 1 12 -8 -2 2681.87 121.841 1 12 -8 -2 2603.63 122.03 1 12 8 -1 31.9701 47.8094 1 12 -8 -1 42.3307 28.3025 1 12 -8 -1 48.3761 26.1348 1 12 8 0 2765.83 146.662 1 12 -8 0 3211.50 158.696 1 12 -8 0 2407.23 146.675 1 12 8 1 355.938 46.0579 1 12 -8 1 383.682 59.034 1 12 -8 1 4.82764 70.1609 1 12 8 2 1520.10 143.801 1 12 -8 2 1670.76 92.9044 1 12 8 3 2213.12 185.574 1 12 -8 3 2672.30 182.264 1 12 8 4 1799.79 114.36 1 12 -8 4 2156.17 171.773 1 12 8 5 1765.88 168.116 1 12 -8 5 2169.85 130.908 1 12 8 6 524.798 70.076 1 12 8 6 381.411 90.7691 1 12 -8 6 484.64 107.71 1 12 9 -7-2.05822 30.7034 1 -12 -9 7-28.6012 42.3475 1 12 9 -6 111.655 43.1792 1 -12 -9 6 80.0875 61.2411 1 12 9 -5 1859.55 179.072 1 -12 -9 5 1390.01 174.184 1 12 9 -4 423.754 88.4618 1 -12 -9 4 206.368 66.1626 1 12 9 -3 162.566 70.9942 1 12 9 -2 1327.90 100.618 1 12 9 -1 35.1374 48.6459 1 12 9 0 1290.21 147.178 1 12 9 1 1191.02 128.446 1 12 -9 1 1041.46 83.1646 1 12 -9 1 670.071 93.5678 1 12 9 2 2376.46 138.813 1 12 -9 2 2463.39 157.601 1 12 9 3 1633.49 161.037 1 12 -9 3 1688.77 99.282 1 13 0 -17-10.0379 43.5751 1 -13 0 17 30.2283 33.3433 1 13 0 -16 0.07977 32.2652 1 -13 0 16-0.70993 25.0353 1 13 0 -15 2181.19 184.623 1 -13 0 15 2353.70 154.698 1 13 0 -14-1.12713 18.4105 1 -13 0 14 2.2732 23.2411 1 13 0 -13 3055.95 215.611 1 -13 0 13 3321.31 177.673 1 13 0 -12 25.3248 32.0553 1 -13 0 12-10.1624 15.6056 1 13 0 -11 451.454 51.7151 1 -13 0 11 513.832 70.7668 1 13 0 -10 12.6971 20.8693 1 -13 0 10 6.88391 29.5244 1 13 0 -9 1896.63 147.704 1 -13 0 9 2025.11 111.94 1 13 0 -8 36.9793 24.5186 1 -13 0 8 26.5049 32.9567 1 13 0 -730219.50 1487.76 1 13 0 -6 21.6785 33.8769 1 13 0 -5 1671.48 80.6787 1 13 0 -4-16.6145 28.4388 1 13 0 -3 922.635 88.3855 1 13 0 -2 242.088 54.5123 1 13 0 -112017.50 475.616 1 13 0 0 24.8074 20.1091 1 13 0 1 1370.33 71.7112 1 13 0 2-14.2536 21.9032 1 13 0 2 20.1926 15.9321 1 13 0 3 152.161 29.971 1 13 0 3 124.125 60.366 1 13 0 4 51.8358 42.3983 1 13 0 4-9.12315 38.4293 1 13 0 5 2069.16 168.929 1 13 0 5 1217.28 168.118 1 13 0 6-23.1262 45.5912 1 13 0 6 51.2065 30.2748 1 13 0 7 949.431 118.103 1 13 0 8-8.97287 37.1298 1 13 0 9 580.333 101.145 1 13 0 10 43.1221 52.2407 1 13 0 11 402.206 103.116 1 13 0 12 70.2879 64.1337 1 13 0 13 655.106 132.011 1 13 1 -17 122.64 64.0479 1 13 -1 -17 65.4596 33.6667 1 -13 -1 17 125.978 46.3943 1 -13 1 17 50.028 43.4606 1 13 1 -16 9.36379 54.597 1 13 -1 -16 0.51804 47.1089 1 -13 -1 16 56.4911 24.1931 1 -13 1 16 54.8029 36.4794 1 13 1 -15 1564.36 110.882 1 13 -1 -15 1596.70 146.802 1 -13 -1 15 1592.45 127.561 1 -13 1 15 1623.77 118.563 1 13 -1 -14 41.3229 46.0476 1 13 1 -14 62.2267 33.2989 1 -13 -1 14 50.0544 25.3044 1 -13 1 14 53.4555 36.3775 1 13 1 -13 2711.50 208.455 1 13 -1 -13 2520.27 129.66 1 -13 1 13 2871.70 152.887 1 -13 -1 13 2964.06 171.455 1 13 -1 -12 248.899 63.9754 1 13 1 -12 301.876 73.7214 1 -13 -1 12 269.746 35.8685 1 -13 1 12 220.468 34.8022 1 13 1 -11 376.669 81.189 1 13 -1 -11 400.742 70.6078 1 -13 -1 11 438.306 63.835 1 -13 1 11 287.169 70.426 1 13 1 -10 358.189 47.8408 1 13 -1 -10 331.436 66.2837 1 -13 -1 10 317.215 60.5495 1 -13 1 10 336.902 67.3848 1 13 1 -9 2147.36 112.604 1 13 -1 -9 2016.14 144.706 1 -13 -1 9 2172.29 105.10 1 13 1 -8 1087.72 122.623 1 13 -1 -8 1207.59 73.1509 1 -13 -1 8 1155.25 88.7218 1 13 1 -726507.30 1282.72 1 13 -1 -726038.00 1228.79 1 -13 -1 724419.10 1219.80 1 13 1 -6 74.5847 28.8248 1 13 -1 -6 98.776 25.7664 1 13 1 -5 1731.57 123.197 1 13 -1 -5 1814.94 115.982 1 13 1 -4 369.502 59.0682 1 13 -1 -4 352.347 36.3117 1 13 1 -3 881.649 88.4733 1 13 -1 -3 886.912 54.1822 1 13 1 -2 461.73 43.2389 1 13 -1 -2 337.723 63.31 1 13 1 -1 8670.93 337.282 1 13 -1 -1 9048.25 400.359 1 13 1 0 150.943 29.6341 1 13 -1 0 149.591 46.8469 1 13 1 1 1368.08 74.7339 1 13 -1 1 1433.56 73.1354 1 13 -1 1 1620.61 94.1886 1 13 1 2 113.03 25.0011 1 13 -1 2 115.758 51.8821 1 13 -1 2 77.1545 25.9619 1 13 1 3 25.0757 42.1494 1 13 1 3 276.356 31.0691 1 13 -1 3 304.646 65.0017 1 13 -1 3 224.892 38.8211 1 13 1 4 1355.44 136.497 1 13 1 4 884.512 104.198 1 13 -1 4 1231.23 129.322 1 13 -1 5 1582.70 151.439 1 13 1 5 1630.25 159.921 1 13 1 5 1190.28 140.25 1 13 1 6 425.787 77.6422 1 13 1 6 151.768 44.3657 1 13 -1 6 371.911 76.4109 1 13 1 7 1063.51 114.318 1 13 1 7 552.005 77.697 1 13 -1 7 922.246 109.27 1 13 1 8 300.077 76.85 1 13 -1 8 239.115 74.0052 1 13 1 9 570.917 105.986 1 13 -1 9 639.061 102.10 1 13 1 10 120.112 62.3637 1 13 -1 10 37.92 60.1396 1 13 1 11 315.468 95.2977 1 13 -1 11 287.415 93.1012 1 13 -1 12 477.266 113.23 1 13 1 12 543.845 120.244 1 13 1 13 475.545 124.895 1 13 -1 13 577.765 78.0364 1 13 2 -17 74.9346 64.9121 1 13 -2 -17 73.9414 48.7575 1 -13 -2 17 20.4013 45.7098 1 -13 2 17 80.0179 36.7241 1 13 2 -16 177.266 74.4761 1 13 -2 -16 210.101 54.8069 1 -13 2 16 98.391 26.9181 1 -13 -2 16 111.299 52.2973 1 13 2 -15 436.376 69.309 1 13 -2 -15 462.242 51.9073 1 -13 -2 15 482.158 50.8414 1 -13 2 15 555.648 65.2736 1 13 2 -14 1220.68 97.6066 1 13 -2 -14 1184.25 114.717 1 -13 -2 14 1282.02 110.327 1 -13 2 14 1086.53 68.5754 1 13 2 -13 1255.87 100.512 1 13 -2 -13 1278.87 115.295 1 -13 -2 13 1411.13 80.222 1 -13 2 13 1085.35 113.63 1 13 -2 -12 1628.54 129.425 1 13 2 -12 1752.41 164.038 1 -13 -2 12 1899.88 130.393 1 -13 2 12 1599.52 129.874 1 13 2 -11 254.364 75.1528 1 13 -2 -11 205.575 55.326 1 -13 -2 11 254.545 35.1575 1 13 -2 -10 1936.97 134.235 1 13 2 -10 1982.51 171.77 1 -13 -2 10 2178.41 136.728 1 13 2 -9 2173.38 177.064 1 13 -2 -9 2249.00 142.979 1 -13 -2 9 2390.53 152.439 1 13 2 -8 2061.15 117.884 1 13 -2 -8 2076.14 138.176 1 -13 -2 8 2274.60 164.168 1 13 2 -717710.80 764.28 1 13 -2 -717996.50 803.075 1 -13 -2 717967.00 807.058 1 13 2 -6 259.929 65.4639 1 13 -2 -6 155.128 52.4177 1 -13 -2 6 384.558 54.2956 1 13 2 -5 2087.65 146.276 1 13 -2 -5 2279.97 93.427 1 13 2 -4 1868.71 130.915 1 13 -2 -4 2080.21 119.984 1 13 2 -3 682.819 54.0399 1 13 -2 -3 718.319 72.2446 1 13 2 -2 6167.16 245.52 1 13 -2 -2 6386.46 236.79 1 13 2 -1 6342.17 251.326 1 13 -2 -1 6600.15 297.283 1 13 2 0 519.409 48.9483 1 13 -2 0 802.029 59.0999 1 13 -2 0 546.71 70.1108 1 13 -2 1 1997.33 100.027 1 13 -2 1 1486.76 117.677 1 13 2 1 1549.11 80.8656 1 13 2 2 130.966 30.007 1 13 -2 2 171.956 53.7308 1 13 -2 2 200.312 35.7231 1 13 2 3 280.326 36.3767 1 13 -2 3 335.42 43.3555 1 13 -2 3 74.0804 76.8338 1 13 2 4 3132.08 164.072 1 13 2 4 2237.98 162.671 1 13 -2 4 2738.00 142.046 1 13 2 5 884.101 104.968 1 13 2 5 1164.38 95.5392 1 13 -2 5 1233.09 87.5374 1 13 2 6 316.49 50.5705 1 13 2 6 170.604 40.5506 1 13 -2 6 335.69 46.5024 1 13 2 7 532.92 60.7489 1 13 2 7 219.078 85.8014 1 13 -2 7 476.46 56.8375 1 13 2 8 254.598 93.9731 1 13 -2 8 638.369 94.0378 1 13 2 8 658.703 66.517 1 13 2 9 426.844 55.0399 1 13 2 9 16.5893 89.6142 1 13 -2 9 283.492 80.5103 1 13 2 10 173.307 41.0786 1 13 2 10-7.17636 42.5933 1 13 -2 10 67.2373 61.1321 1 13 2 11 240.409 59.2516 1 13 -2 11 294.281 90.4534 1 13 2 12 1151.66 106.193 1 13 -2 12 970.998 101.648 1 13 -2 13 434.009 72.8372 1 13 3 -16 68.8589 82.1361 1 13 -3 -16 151.521 51.4645 1 -13 -3 16 155.923 57.7102 1 -13 3 16 160.339 54.6782 1 13 3 -15 31.4409 61.721 1 13 -3 -15 42.2069 39.197 1 -13 -3 15 76.5642 43.482 1 -13 3 15 29.3665 40.2343 1 13 3 -14 386.67 102.684 1 13 -3 -14 592.715 66.7953 1 -13 -3 14 340.131 48.1925 1 -13 3 14 131.995 78.0917 1 13 3 -13 426.293 100.518 1 13 -3 -13 410.197 41.5521 1 -13 -3 13 379.442 75.1318 1 13 3 -12 2930.66 158.106 1 13 -3 -12 2746.41 162.685 1 -13 -3 12 3069.85 135.993 1 13 3 -11 160.435 42.7563 1 13 -3 -11 104.906 43.3909 1 -13 -3 11 207.544 50.9315 1 13 3 -10 1995.91 119.582 1 13 -3 -10 1982.37 123.20 1 -13 -3 10 2143.35 141.292 1 13 3 -9 3345.06 163.129 1 13 -3 -9 3210.58 167.765 1 -13 -3 9 3335.68 145.323 1 13 3 -8 4677.13 288.803 1 13 -3 -8 4881.82 230.715 1 -13 -3 8 5069.04 275.257 1 13 3 -710185.10 515.164 1 13 -3 -710054.90 438.927 1 -13 -3 710614.70 548.266 1 13 3 -6 703.609 96.8859 1 13 -3 -6 709.591 74.3413 1 -13 -3 6 907.338 109.838 1 13 3 -5 2283.67 156.259 1 13 -3 -5 2366.24 96.1062 1 13 3 -4 689.14 85.216 1 13 -3 -4 730.821 69.3913 1 13 3 -3 488.656 47.4532 1 13 -3 -3 555.569 40.7565 1 13 -3 -213066.20 572.529 1 13 -3 -215522.20 607.02 1 13 3 -211420.70 472.982 1 13 3 -1 4234.08 182.641 1 13 -3 -1 5357.98 267.475 1 13 -3 -1 4301.85 217.671 1 13 3 0 830.887 58.1208 1 13 -3 0 704.871 50.4137 1 13 -3 0 794.129 94.8788 1 13 3 1 1947.55 95.9011 1 13 -3 1 2513.31 151.98 1 13 -3 1 1777.53 129.908 1 13 -3 2 27.9859 39.7569 1 13 -3 2 24.0505 38.9025 1 13 3 2 64.0956 35.9578 1 13 3 3 446.457 76.2579 1 13 -3 3 615.615 85.2973 1 13 3 4 5058.34 279.723 1 13 -3 4 5999.57 329.87 1 13 3 5 522.408 55.212 1 13 -3 5 627.866 102.135 1 13 3 5 696.277 76.293 1 13 3 6 1073.69 132.718 1 13 3 6 848.087 66.1289 1 13 -3 6 870.842 116.692 1 13 3 7 239.744 74.2336 1 13 3 7 129.834 54.0481 1 13 -3 7 202.474 41.0318 1 13 3 8 1056.81 130.136 1 13 3 8 754.79 68.3148 1 13 -3 8 1059.33 78.7107 1 13 3 9-8.61036 39.9377 1 13 -3 9-27.0022 24.9925 1 13 3 9 38.5178 44.2889 1 13 3 10 188.073 78.3612 1 13 3 10 110.627 47.2448 1 13 -3 10 269.339 74.983 1 13 3 11 5.24736 55.7294 1 13 3 11 -2.6498 53.8481 1 13 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4 -4 112.633 52.2252 1 13 -4 -4 161.584 28.8069 1 13 -4 -4 137.686 38.4832 1 13 4 -3 19.1494 37.317 1 13 -4 -3 46.2524 20.5445 1 13 -4 -3 14.5309 27.5698 1 13 -4 -2 4479.24 209.757 1 13 -4 -2 5232.25 198.055 1 13 4 -2 3950.61 172.493 1 13 4 -1 712.622 90.3432 1 13 -4 -1 785.89 76.3686 1 13 -4 -1 1080.41 94.607 1 13 4 0 759.184 83.7527 1 13 -4 0 747.786 88.0092 1 13 -4 0 696.396 71.658 1 13 4 1 1452.25 118.413 1 13 -4 1 1118.14 119.518 1 13 -4 1 1611.32 123.213 1 13 4 2-2.01396 32.9266 1 13 -4 2 42.0083 33.2059 1 13 -4 2 3.05091 39.3841 1 13 4 3 1347.99 123.34 1 13 -4 3 1472.69 132.801 1 13 4 4 4120.56 186.145 1 13 -4 4 4930.33 282.295 1 13 4 5 48.031 33.2892 1 13 4 5 39.4338 25.148 1 13 -4 5 19.0891 27.7759 1 13 4 6 660.083 111.02 1 13 4 6 489.535 83.1123 1 13 -4 6 556.228 61.8888 1 13 4 7 65.6304 35.924 1 13 4 7 65.5783 27.2166 1 13 -4 7 43.075 51.214 1 13 4 8 1315.07 103.607 1 13 4 8 1091.92 118.327 1 13 -4 8 1310.51 141.201 1 13 4 9 234.142 50.2094 1 13 4 9 154.024 63.7871 1 13 -4 9 232.923 48.5332 1 13 4 10 460.132 109.928 1 13 4 10 729.924 84.5129 1 13 -4 10 726.542 80.3344 1 13 4 11 104.315 41.8631 1 13 4 11 16.5433 35.991 1 13 -4 11 104.483 65.8126 1 13 5 -14 1349.27 130.211 1 -13 -5 14 1504.99 98.3403 1 13 5 -13 264.464 56.8513 1 13 -5 -13 153.834 35.5802 1 -13 -5 13 263.363 65.8106 1 13 5 -12 5134.88 257.512 1 13 -5 -12 4577.85 195.559 1 -13 -5 12 5204.29 287.414 1 13 5 -11-45.0104 42.4565 1 13 -5 -11 9.60501 19.2482 1 -13 -5 11 26.2071 31.0952 1 13 5 -10 1147.53 143.762 1 13 -5 -10 1124.03 73.3717 1 -13 -5 10 1185.99 74.4624 1 13 5 -9 3592.75 254.674 1 13 -5 -9 3467.23 152.01 1 -13 -5 9 3962.32 218.432 1 13 5 -8 3005.18 232.624 1 13 -5 -8 3302.39 152.044 1 -13 -5 8 3225.44 195.816 1 13 5 -7 430.768 92.1045 1 13 -5 -7 478.648 39.2534 1 13 -5 -7 433.701 54.0265 1 -13 -5 7 436.902 53.0341 1 13 5 -6 3101.96 218.809 1 13 -5 -6 3391.88 169.764 1 13 -5 -6 3249.45 154.30 1 -13 -5 6 3436.86 233.445 1 13 5 -5 2366.07 173.663 1 13 -5 -5 2389.04 92.061 1 13 -5 -5 2427.35 137.009 1 -13 -5 5 1773.81 202.931 1 13 5 -4 268.786 65.9009 1 13 -5 -4 301.685 48.9235 1 13 -5 -4 187.536 44.1855 1 13 5 -3 59.5149 43.593 1 13 -5 -3 65.6705 34.389 1 13 -5 -3 29.6101 29.9153 1 13 5 -2 8620.41 443.074 1 13 -5 -2 9347.76 359.206 1 13 -5 -210582.00 462.091 1 13 5 -1 501.77 83.827 1 13 -5 -1 511.385 61.789 1 13 -5 -1 547.108 49.112 1 13 5 0 43.0535 39.0463 1 13 -5 0 52.4538 23.2265 1 13 -5 0 24.2675 33.4453 1 13 5 1 1414.17 121.046 1 13 -5 1 1950.92 127.063 1 13 -5 1 1296.98 84.689 1 13 5 2 266.055 35.4104 1 13 -5 2 278.109 59.7267 1 13 -5 2 107.783 44.2156 1 13 -5 3 1638.06 133.791 1 13 5 3 1290.63 86.5978 1 13 5 4 2998.93 213.719 1 13 -5 4 3709.72 172.007 1 13 5 5-15.6541 30.9064 1 13 5 5 42.3244 38.9466 1 13 -5 5 70.8658 42.9661 1 13 5 6 83.8106 60.9351 1 13 5 6 49.1439 28.5241 1 13 -5 6 98.232 53.5568 1 13 5 7 35.5953 56.9087 1 13 5 7 44.0963 45.0296 1 13 -5 7 57.196 31.6114 1 13 5 8 1037.33 121.534 1 13 -5 8 1300.80 96.5373 1 13 5 8 1268.82 155.994 1 13 5 9 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287.322 1 -14 -3 7 6081.72 428.784 1 14 3 -6 208.848 63.3266 1 14 -3 -6 184.425 48.8127 1 14 -3 -5 631.52 47.615 1 14 3 -5 589.203 87.0966 1 14 3 -4 739.025 96.5666 1 14 -3 -4 881.768 84.3505 1 14 3 -3 72.8111 38.1091 1 14 -3 -3 14.131 27.3972 1 14 -3 -3 35.1393 33.6706 1 14 3 -2 9240.99 469.178 1 14 -3 -211737.10 476.835 1 14 -3 -2 9514.78 387.845 1 14 3 -1 2778.60 201.643 1 14 -3 -1 3597.34 162.611 1 14 -3 -1 2952.25 178.391 1 14 3 0 2917.63 185.217 1 14 -3 0 3561.24 158.035 1 14 -3 0 2822.27 168.555 1 14 3 1 3.03021 30.895 1 14 -3 1 9.56065 21.1074 1 14 -3 1 17.9876 27.4206 1 14 3 2 131.949 48.6938 1 14 -3 2 134.946 34.875 1 14 -3 2 98.0143 48.3543 1 14 -3 3 1348.60 156.177 1 14 -3 3 2308.40 164.204 1 14 3 3 1786.73 99.3502 1 14 3 4 1950.05 112.023 1 14 -3 4 2279.23 185.42 1 14 3 5 309.136 91.1292 1 14 3 5 251.791 67.0899 1 14 -3 5 236.53 80.468 1 14 3 6 1227.48 142.626 1 14 3 6 843.011 103.422 1 14 -3 6 977.075 127.368 1 14 3 7 27.41 24.5271 1 14 -3 7 62.7085 30.5071 1 14 3 7 35.5211 53.9184 1 14 3 8 246.489 86.1789 1 14 3 8 189.104 62.5149 1 14 -3 8 276.867 49.7402 1 14 3 9 1104.71 91.3261 1 14 3 9 1694.06 174.876 1 14 -3 9 1403.87 159.596 1 14 3 10 72.4765 69.6881 1 14 3 10 73.595 55.1652 1 14 -3 10 47.1428 65.5372 1 14 -4 -14 219.853 58.7136 1 14 4 -14 267.387 107.108 1 -14 -4 14 299.73 48.6834 1 14 4 -13 256.621 96.8304 1 14 -4 -13 202.808 53.2478 1 -14 -4 13 271.702 68.1306 1 14 -4 -12 83.8919 38.0271 1 14 4 -12 172.247 67.663 1 -14 -4 12 48.2478 29.467 1 14 4 -11 707.046 127.429 1 14 -4 -11 709.708 48.7214 1 -14 -4 11 737.282 95.5548 1 14 4 -10 312.624 88.3654 1 14 -4 -10 236.799 58.0171 1 -14 -4 10 350.214 44.0849 1 14 4 -9 82.5496 45.9837 1 14 -4 -9 15.7266 29.9132 1 -14 -4 9 4.21571 24.656 1 14 4 -8-46.4481 38.4025 1 14 -4 -8 2.91457 15.9334 1 -14 -4 8-12.9082 33.9348 1 14 4 -7 8656.71 378.851 1 14 -4 -7 9261.08 401.045 1 -14 -4 7 7942.44 466.728 1 14 4 -6 29.8708 22.5376 1 14 -4 -6 11.7322 26.9891 1 -14 -4 6-16.4523 29.405 1 14 4 -5 978.676 73.048 1 14 -4 -5 1054.65 59.4055 1 14 4 -4 2913.26 200.952 1 14 -4 -4 3919.84 204.575 1 14 -4 -4 3202.09 173.107 1 14 4 -3 100.402 52.3009 1 14 -4 -3 121.659 49.4921 1 14 -4 -3 100.249 26.0711 1 14 4 -2 1144.42 122.085 1 14 -4 -2 1530.63 86.8449 1 14 -4 -2 1322.85 106.637 1 14 4 -1 3885.67 236.859 1 14 -4 -1 5081.67 210.18 1 14 -4 0 2789.53 130.902 1 14 -4 0 2235.76 149.18 1 14 4 1 21.3404 35.1143 1 14 -4 1 36.1748 32.5364 1 14 -4 1-8.42459 35.5204 1 14 -4 2 94.374 42.4072 1 14 -4 2 1.22877 43.206 1 14 4 2 40.5335 24.9703 1 14 4 3 1584.62 93.8417 1 14 -4 3 1914.02 150.23 1 14 -4 3 811.669 158.175 1 14 4 4 220.802 67.4212 1 14 -4 4 243.023 46.5539 1 14 4 5 768.479 78.6184 1 14 4 5 485.65 90.5244 1 14 -4 5 621.512 68.3212 1 14 4 6 1622.65 113.833 1 14 4 6 1029.39 83.8847 1 14 -4 6 1371.48 145.712 1 14 4 7 98.9393 42.9943 1 14 4 7 127.368 51.4598 1 14 -4 7 62.1161 61.3826 1 14 4 8 290.474 53.5739 1 14 4 8 192.726 40.3568 1 14 -4 8 211.735 80.3806 1 14 4 9 1963.16 137.551 1 14 4 9 1426.92 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94.6736 1 15 -6 1 692.59 96.2375 1 15 -6 1 545.149 52.749 1 15 6 2 115.294 62.309 1 15 -6 2 187.295 63.868 1 15 -6 2 133.803 56.8665 1 15 6 3 10.514 29.7333 1 15 -6 3 39.72 30.4365 1 15 -6 3 42.4937 30.6455 1 15 6 4 987.62 125.513 1 15 -6 4 1145.60 132.83 1 15 -6 4 572.107 93.248 1 15 7 -5 1232.96 106.052 1 15 7 -4 1124.61 157.068 1 15 -7 -4 1150.81 100.141 1 15 -7 -4 1146.29 67.2729 1 15 7 -3 917.596 141.803 1 15 -7 -3 991.165 100.363 1 15 -7 -3 974.906 95.8054 1 15 7 -2 1718.65 120.96 1 15 -7 -2 1899.82 142.388 1 15 -7 -2 1699.03 130.167 1 15 7 -1 695.579 74.9024 1 15 -7 -1 781.435 91.8199 1 15 -7 -1 744.877 64.2305 1 15 7 0 1159.22 145.329 1 15 -7 0 1443.81 131.013 1 15 -7 0 1183.06 114.57 1 16 0 -13 10.7378 45.5533 1 -16 0 13-28.2812 32.129 1 16 0 -12 9.61205 42.1939 1 16 0 -11 29.4246 48.1966 1 16 0 -10 6045.54 358.364 1 16 0 -9 3.33644 23.0576 1 16 0 -810740.90 465.496 1 16 0 -7-27.1667 43.2933 1 16 0 -6 3301.05 215.171 1 16 0 -5-0.18698 27.4456 1 16 0 -4 747.438 100.455 1 16 0 -3-8.83705 34.0932 1 16 0 -2 924.209 106.188 1 16 0 -1 11.5591 33.2588 1 16 0 0 32.0789 37.8645 1 16 0 1-35.4944 28.6151 1 16 0 1 14.684 34.6269 1 16 0 2 948.847 73.7825 1 16 0 2 1271.90 150.62 1 16 0 3-31.5196 52.736 1 16 0 3-14.1867 39.1054 1 16 0 4 1192.22 148.785 1 16 0 4 757.005 107.318 1 16 0 5 41.6067 53.6265 1 16 0 5 20.3993 24.019 1 16 0 6 3446.09 252.213 1 16 0 6 5148.72 335.272 1 16 0 7 5.30253 34.8364 1 16 0 7 3.91627 28.1496 1 16 0 8 1468.79 119.171 1 16 0 8 555.096 150.762 1 16 1 -13 133.463 70.7719 1 16 -1 -13 104.976 62.5026 1 -16 -1 13 90.4598 41.9729 1 16 -1 -12 61.3302 48.9647 1 16 1 -12 35.6043 55.1812 1 -16 -1 12 11.6158 62.1379 1 16 1 -11 109.679 63.2458 1 16 -1 -11 56.8296 58.0913 1 16 1 -10 8194.29 475.887 1 16 -1 -10 8403.44 372.326 1 16 1 -9 411.685 101.444 1 16 -1 -9 506.677 61.201 1 16 -1 -8 5138.04 297.213 1 16 1 -8 4974.57 310.303 1 16 1 -7 22.358 27.8424 1 16 -1 -7 60.8946 43.3515 1 16 1 -6 4102.95 190.789 1 16 -1 -6 4253.27 250.501 1 16 1 -5 113.811 35.6105 1 16 -1 -5 139.625 33.8831 1 16 1 -4 784.317 67.9814 1 16 -1 -4 747.695 64.8464 1 16 1 -3 762.669 68.617 1 16 -1 -3 810.547 65.9089 1 16 1 -2 330.53 44.6053 1 16 -1 -2 272.331 43.4773 1 16 1 -1-25.7908 34.6928 1 16 -1 -1 25.8195 20.5799 1 16 1 0 363.189 71.1733 1 16 -1 0 439.696 56.9078 1 16 -1 0 293.229 44.1085 1 16 1 1 38.8675 40.90 1 16 -1 1 48.3086 32.4959 1 16 -1 1 30.5849 25.5673 1 16 -1 2 5521.53 336.646 1 16 1 2 5520.91 266.986 1 16 1 2 3893.70 255.501 1 16 -1 2 3836.61 252.531 1 16 1 3 153.208 80.563 1 16 1 3 136.952 37.0951 1 16 -1 3 162.96 77.143 1 16 -1 3 115.369 58.416 1 16 -1 4-1.61888 40.218 1 16 1 4 19.0624 42.4417 1 16 1 4-0.83214 31.0643 1 16 -1 4 1.63001 18.6681 1 16 1 5-14.7108 36.9874 1 16 1 5 7.20124 25.8501 1 16 -1 5 94.6121 35.9847 1 16 -1 5-23.2483 17.9149 1 16 1 6 334.29 93.0177 1 16 1 6 240.93 44.7514 1 16 -1 6 208.779 73.5047 1 16 -1 6 353.36 58.9359 1 16 1 7 233.026 81.3668 1 16 1 7 152.637 56.7659 1 16 -1 7 187.759 51.5195 1 16 -1 7 76.2834 44.4746 1 16 1 8 399.743 62.6214 1 16 1 8 877.35 133.747 1 16 -1 8 650.786 81.2561 1 16 -1 8 231.548 111.074 1 16 2 -12 206.679 50.8476 1 16 -2 -12 155.836 69.6781 1 -16 -2 12 130.60 48.7259 1 16 2 -11 428.767 63.9085 1 16 -2 -11 344.779 86.6537 1 -16 -2 11 176.906 114.592 1 16 -2 -10 5084.84 227.084 1 16 2 -10 4993.48 245.867 1 -16 -2 10 3543.97 258.719 1 16 2 -9 1718.58 183.917 1 16 -2 -9 1883.38 164.483 1 16 2 -8 8100.01 463.145 1 16 -2 -8 8549.50 444.594 1 16 2 -7 172.55 69.0422 1 16 -2 -7 177.993 62.2107 1 16 2 -6 3009.44 219.331 1 16 -2 -6 3206.82 150.164 1 16 2 -5 363.661 83.9322 1 16 -2 -5 464.956 76.0927 1 16 2 -4 683.031 103.513 1 16 -2 -4 679.358 92.4974 1 16 -2 -3 2425.71 176.202 1 16 2 -3 2524.16 184.055 1 16 2 -2 478.267 50.9658 1 16 -2 -2 215.34 54.6937 1 16 -2 -2 468.457 73.8506 1 16 2 -1 63.5251 26.5871 1 16 -2 -1 5.42336 50.2747 1 16 -2 -1 10.23 39.7428 1 16 2 0 58.7098 27.9281 1 16 -2 0 138.489 55.3243 1 16 -2 0 13.157 44.171 1 16 2 1 31.7829 34.5414 1 16 -2 1-10.3568 25.8802 1 16 -2 1 32.8353 34.0883 1 16 2 2 1061.54 123.331 1 16 -2 2 1491.78 105.129 1 16 -2 2 1003.07 120.823 1 16 2 3 500.246 69.0424 1 16 2 3 295.057 48.0481 1 16 -2 3 424.142 97.7229 1 16 -2 3 322.363 49.3188 1 16 2 4 1.02585 38.4304 1 16 -2 4 32.311 40.9744 1 16 -2 4-28.7047 49.7855 1 16 2 4 44.2228 33.0659 1 16 2 5 1115.69 101.493 1 16 2 5 834.40 112.685 1 16 -2 5 816.56 119.978 1 16 -2 5 1116.37 148.992 1 16 2 6 1111.60 80.7715 1 16 -2 6 1421.46 156.872 1 16 -2 6 705.331 89.6496 1 16 2 6 1506.13 165.567 1 16 2 7 192.584 86.8287 1 16 2 7 192.846 63.0049 1 16 -2 7 154.119 51.8827 1 16 -2 7 57.5786 86.4481 1 16 -3 -12 42.6274 28.9472 1 16 3 -12 21.6858 61.6434 1 -16 -3 12 21.6315 55.4772 1 16 3 -11 977.416 138.702 1 16 -3 -11 938.951 109.808 1 -16 -3 11 506.544 83.0658 1 16 3 -10 3314.89 266.307 1 16 -3 -10 3560.48 226.284 1 -16 -3 10 2407.56 292.898 1 16 3 -9 2692.32 234.939 1 16 -3 -9 2862.07 144.584 1 16 3 -8 2698.87 229.699 1 16 -3 -8 2761.01 191.197 1 16 3 -7 136.018 64.1117 1 16 -3 -7 110.059 53.9798 1 16 3 -6 1369.09 144.833 1 16 -3 -6 1527.68 90.0075 1 16 3 -5 885.353 123.232 1 16 -3 -5 1123.19 107.273 1 16 3 -4 84.3949 48.6446 1 16 -3 -4 12.8612 31.0415 1 16 -3 -4 68.69 42.3915 1 16 3 -3 4420.49 280.679 1 16 -3 -3 5513.44 314.269 1 16 -3 -3 4555.93 262.149 1 16 3 -2 54.896 45.6768 1 16 -3 -2 55.864 31.0554 1 16 -3 -2 32.9794 25.6577 1 16 3 -1 205.526 41.0713 1 16 -3 -1 206.949 72.2387 1 16 -3 -1 215.294 36.7858 1 16 3 0 279.906 45.4779 1 16 -3 0 360.312 80.2708 1 16 -3 0 277.268 42.7762 1 16 -3 1 67.8182 53.1053 1 16 -3 1 58.574 26.7575 1 16 3 1 22.5684 46.1003 1 16 3 2 70.7554 55.4739 1 16 -3 2 131.259 65.9162 1 16 -3 2 111.855 51.2687 1 16 3 3 32.2208 67.4842 1 16 3 3 467.944 52.3502 1 16 -3 3 381.063 87.132 1 16 -3 3 518.98 65.056 1 16 3 4 33.0397 68.5502 1 16 3 4 42.5866 30.0445 1 16 -3 4 71.4067 37.4091 1 16 -3 4 57.6038 50.7537 1 16 3 5 1293.00 155.868 1 16 3 5 833.357 111.56 1 16 -3 5 882.566 140.279 1 16 -3 5 687.044 84.0671 1 16 3 6 1148.49 101.58 1 16 3 6 795.24 74.4654 1 16 -3 6 1055.00 142.279 1 16 -3 6 200.326 147.28 1 16 4 -10 705.256 85.3738 1 16 -4 -10 769.086 97.5994 1 -16 -4 10 504.321 132.456 1 16 4 -9 3047.80 178.43 1 16 -4 -9 3465.80 207.661 1 -16 -4 9 2316.23 194.895 1 16 4 -8 3606.70 193.973 1 16 -4 -8 3685.34 225.738 1 16 -4 -7 171.126 54.5504 1 16 4 -7 127.227 42.9145 1 16 4 -6 705.816 74.607 1 16 -4 -6 758.979 62.029 1 16 -4 -6 852.647 70.9847 1 16 4 -5 1265.15 138.712 1 16 -4 -5 1253.20 121.885 1 16 -4 -5 1647.02 141.505 1 16 4 -4 200.116 68.693 1 16 -4 -4 232.358 70.6213 1 16 -4 -4 177.909 60.5444 1 16 4 -3 5072.71 330.899 1 16 -4 -3 6601.49 285.645 1 16 -4 -3 5276.90 235.098 1 16 4 -2 91.6587 58.7597 1 16 -4 -2 137.258 59.1358 1 16 -4 -2 94.1249 30.9113 1 16 4 -1 224.065 46.0524 1 16 -4 -1 113.096 72.1983 1 16 -4 -1 272.146 39.2507 1 16 4 0 23.4031 25.0157 1 16 -4 0 4.09392 41.3589 1 16 -4 0 10.5877 34.0037 1 16 4 1 215.902 69.1567 1 16 -4 1 192.378 38.1438 1 16 -4 1 245.965 47.9091 1 16 4 2 -17.109 34.6877 1 16 -4 2 28.1399 36.6026 1 16 -4 2 0.49151 18.4845 1 16 4 3 985.774 82.1017 1 16 -4 3 1010.30 140.327 1 16 -4 3 792.572 79.3202 1 16 4 4 495.009 75.2554 1 16 4 4 325.988 88.5196 1 16 -4 4 428.431 103.084 1 16 -4 4 166.839 102.407 1 16 4 5 1285.34 168.812 1 16 4 5 975.828 123.582 1 16 -4 5 448.794 140.758 1 16 -4 5 1122.94 98.1986 1 16 5 -8 1298.30 174.646 1 16 -5 -8 1471.43 129.239 1 16 -5 -8 1768.37 143.387 1 16 5 -7 14.0454 29.0208 1 16 -5 -7 26.1689 33.7623 1 16 -5 -7 15.5315 38.4319 1 16 5 -6 45.0905 35.2036 1 16 -5 -6 101.114 46.273 1 16 -5 -6 27.6374 40.8902 1 16 5 -5 1341.18 102.60 1 16 -5 -5 1572.72 138.712 1 16 -5 -5 1407.13 123.944 1 16 5 -4 804.209 129.245 1 16 -5 -4 1155.19 123.338 1 16 -5 -4 928.938 108.309 1 16 5 -3 4304.70 299.442 1 16 -5 -3 4921.94 283.966 1 16 -5 -3 5752.23 254.025 1 16 5 -2 631.433 111.352 1 16 -5 -2 756.733 63.6432 1 16 -5 -2 944.011 114.688 1 16 5 -1 372.336 61.3647 1 16 -5 -1 350.993 76.0717 1 16 -5 -1 638.708 91.0727 1 16 5 0 46.3178 32.455 1 16 -5 0 65.0105 30.662 1 16 -5 0 5.84668 42.3676 1 16 5 1 198.948 70.4724 1 16 -5 1 168.284 70.9999 1 16 -5 1 155.712 57.6551 1 16 5 2 655.228 117.85 1 16 -5 2 849.51 124.679 1 16 -5 2 671.837 98.7525 1 16 5 3 792.734 80.4821 1 16 -5 3 1043.06 131.915 1 16 -5 3 658.292 74.5665 1 16 6 -5 1620.10 126.25 1 16 -6 -5 1685.79 138.88 1 16 -6 -5 1964.91 107.099 1 16 6 -4 1473.41 183.652 1 16 -6 -4 1899.89 154.928 1 16 -6 -4 1832.90 142.903 1 16 6 -3 3456.21 281.474 1 16 -6 -3 4521.91 270.125 1 16 -6 -3 4047.75 241.096 1 16 6 -2 675.274 119.219 1 16 -6 -2 870.33 110.531 1 16 -6 -2 642.291 96.2993 1 16 6 -1 766.044 79.8444 1 16 -6 -1 1123.40 120.978 1 16 -6 -1 864.064 69.044 1 17 0 -11 27.2875 50.7504 1 17 0 -10 17.6889 28.7846 1 17 0 -9 3852.53 197.415 1 17 0 -8-3.18104 21.9163 1 17 0 -7 5.49724 21.8355 1 17 0 -6 1.31653 19.4692 1 17 0 -5 1939.18 171.991 1 17 0 -4 0.46003 33.0534 1 17 0 -311012.90 496.315 1 17 0 -2-0.64631 19.7364 1 17 0 -1 1662.97 104.188 1 17 0 0-3.50373 28.3123 1 17 0 0-11.2369 21.1831 1 17 0 1 68.9267 45.9851 1 17 0 1-26.9859 34.3965 1 17 0 2 21.9079 33.5098 1 17 0 2 12.7956 39.3488 1 17 0 3 245.333 57.9719 1 17 0 3 185.58 44.2355 1 17 0 4 32.5484 36.2637 1 17 0 4 25.9505 43.4792 1 17 0 5 507.557 89.5395 1 17 0 5 583.697 125.377 1 17 1 -11 18.2733 49.283 1 17 -1 -11 22.9628 47.7666 1 17 1 -10 41.4596 62.4597 1 17 -1 -10 91.04 37.033 1 17 1 -9 3494.57 255.882 1 17 -1 -9 3508.81 180.364 1 17 1 -8 10.4116 44.0529 1 17 -1 -8 24.9125 41.2456 1 17 1 -7 17.0947 36.6272 1 17 -1 -7-3.52829 35.1559 1 17 1 -6 53.3838 52.8582 1 17 -1 -6 85.6347 51.6944 1 17 -1 -5 1923.34 160.786 1 17 1 -5 1858.64 169.778 1 17 1 -4 362.918 97.6423 1 17 -1 -4 575.062 95.7999 1 17 1 -310030.40 549.623 1 17 -1 -310408.00 552.201 1 17 -1 -2 62.236 53.3842 1 17 1 -1 1795.90 164.885 1 17 -1 -1 2249.66 140.507 1 17 -1 -1 1815.54 162.129 1 17 1 0 7.71601 24.5975 1 17 -1 0 39.8681 38.1853 1 17 -1 0 32.5629 50.2328 1 17 1 1-29.5551 27.0228 1 17 1 1 20.4762 19.3488 1 17 -1 1 3.81803 41.0418 1 17 -1 1-5.71616 31.7651 1 17 1 2 953.204 155.73 1 17 1 2 757.155 110.976 1 17 -1 2 940.371 95.2805 1 17 -1 2 758.95 74.2715 1 17 1 3 90.7859 45.6956 1 17 1 3 49.3878 53.8469 1 17 -1 3 86.8471 43.5198 1 17 -1 3 88.362 54.6253 1 17 1 4 154.978 51.8214 1 17 1 4 130.305 38.2668 1 17 -1 4 167.765 81.1037 1 17 -1 4 112.123 58.6972 1 17 1 5 187.067 51.6105 1 17 1 5 179.301 58.6259 1 17 -1 5 78.8622 36.6753 1 17 -1 5 237.62 81.6259 1 17 2 -10 438.615 116.184 1 17 -2 -10 567.586 65.6558 1 17 -2 -9 2858.63 212.462 1 17 2 -9 2606.40 225.064 1 17 2 -8 1287.76 147.266 1 17 -2 -8 1216.56 136.885 1 17 2 -7 34.442 46.6025 1 17 -2 -7 21.1599 42.6381 1 17 2 -6 915.683 81.5578 1 17 -2 -6 1066.14 118.916 1 17 2 -5 1649.89 113.529 1 17 -2 -5 1820.04 106.03 1 17 2 -4 1129.04 95.6372 1 17 -2 -4 1308.13 90.4084 1 17 2 -3 6986.56 326.965 1 17 -2 -3 7356.32 325.974 1 17 2 -2 34.6348 30.5413 1 17 -2 -2 85.6648 35.6366 1 17 -2 -2 26.1058 29.1921 1 17 -2 -1 2235.53 133.736 1 17 -2 -1 1686.02 107.285 1 17 2 -1 1676.97 164.997 1 17 2 0 48.2278 40.5309 1 17 -2 0 15.6924 47.9823 1 17 -2 0 7.61953 23.9931 1 17 2 1-1.48885 21.1393 1 17 -2 1 47.4436 42.6318 1 17 -2 1-9.89458 33.9619 1 17 2 2 2043.08 165.455 1 17 2 2 2323.01 137.507 1 17 -2 2 3125.39 245.527 1 17 -2 2 2398.52 192.015 1 17 2 3 63.4071 55.4647 1 17 2 3 -58.116 42.0257 1 17 -2 3 22.3746 31.6897 1 17 -2 3 44.7514 39.4491 1 17 2 4 72.6341 31.9718 1 17 -2 4 36.3646 31.9482 1 17 -2 4 99.2711 42.2717 1 17 2 4 79.654 71.271 1 17 3 -9 733.172 133.832 1 17 -3 -9 773.667 72.9195 1 17 3 -8 116.151 67.9829 1 17 -3 -8 118.047 59.091 1 17 3 -7 34.1226 50.0275 1 17 -3 -7 29.8008 41.5895 1 17 3 -6 617.656 111.297 1 17 -3 -6 648.996 95.8926 1 17 3 -5 1317.45 161.989 1 17 -3 -5 1635.12 99.381 1 17 3 -4 1586.37 182.157 1 17 -3 -4 1777.81 166.624 1 17 -3 -4 2189.11 134.058 1 17 3 -3 3864.45 204.659 1 17 -3 -3 4915.07 309.965 1 17 -3 -3 3938.07 258.888 1 17 -3 -2 48.7011 52.0395 1 17 -3 -2 44.0044 43.1537 1 17 3 -2 27.378 29.7378 1 17 3 -1 1300.95 98.4459 1 17 -3 -1 1816.91 164.444 1 17 -3 -1 1294.82 133.27 1 17 3 0-4.00445 46.5885 1 17 -3 0 72.1101 32.5795 1 17 -3 0 5.80088 43.8876 1 17 3 1 64.5304 47.0863 1 17 -3 1 35.2088 52.8062 1 17 -3 1 12.4899 27.0025 1 17 3 2 3848.49 206.548 1 17 -3 2 3832.71 200.664 1 17 -3 2 5300.57 340.818 1 17 3 3 112.823 50.292 1 17 3 3 79.6774 61.1215 1 17 -3 3 78.6683 58.7749 1 17 -3 3 109.369 75.3452 1 17 4 -7 75.1799 39.9461 1 17 -4 -7 87.7292 52.6032 1 17 -4 -7 104.213 36.2611 1 17 4 -6 1417.41 105.923 1 17 -4 -6 1507.24 140.445 1 17 -4 -6 1799.37 159.073 1 17 4 -5 1095.32 149.98 1 17 -4 -5 1365.66 98.6239 1 17 -4 -5 1133.61 84.417 1 17 4 -4 2596.69 231.853 1 17 -4 -4 3469.74 237.255 1 17 -4 -4 2756.85 203.878 1 17 4 -3 1561.09 174.567 1 17 -4 -3 2191.53 183.78 1 17 -4 -3 1799.54 157.075 1 17 4 -2 45.8729 31.545 1 17 -4 -2 23.0989 30.9772 1 17 -4 -2 41.1345 43.4189 1 17 4 -1 701.889 77.5219 1 17 -4 -1 1052.59 124.269 1 17 -4 -1 738.924 101.985 1 17 4 0 197.545 73.9373 1 17 -4 0 194.28 66.2449 1 17 -4 0 231.986 80.4056 1 17 4 1 120.08 63.8063 1 17 -4 1 76.4454 56.1455 1 17 -4 1 61.99 70.1659 1 18 0 -7-21.9029 28.1331 1 18 0 -6 291.897 51.9586 1 18 0 -5-7.31835 24.6084 1 18 0 -4 3268.90 174.767 1 18 0 -3 43.9692 51.2341 1 18 0 -2-21.0822 42.9857 1 18 0 -1 25.2982 43.9388 1 18 0 0 217.401 53.8224 1 18 0 0 78.3231 67.4444 1 18 0 1-17.6001 58.2527 1 18 0 1 24.6385 27.2989 1 18 1 -7 5.1056 38.3016 1 18 -1 -7-12.8519 37.0045 1 18 1 -6 9.0921 35.1054 1 18 -1 -6-12.5961 34.733 1 18 1 -5 11.0992 33.0597 1 18 -1 -5-10.4894 31.5228 1 18 1 -4 1129.15 139.732 1 18 -1 -4 1095.18 136.247 1 18 1 -3 251.813 80.0021 1 18 -1 -3 323.795 79.1094 1 18 1 -2 34.7437 26.6088 1 18 -1 -2 18.8419 26.2052 1 18 -1 -2 -1.3715 31.7951 1 18 1 -1 39.8473 30.6404 1 18 -1 -1 40.7742 29.3925 1 18 -1 -1 47.8691 37.2289 1 18 1 0 185.932 76.5522 1 18 -1 0 303.888 60.7051 1 18 -1 0 245.018 47.4316 1 18 1 1 31.8534 53.0611 1 18 1 1 79.0475 43.0119 1 18 -1 1 48.7647 65.0121 1 18 -1 1-20.2634 51.2779 1 18 2 -5 52.2111 35.3554 1 18 -2 -5 63.0336 50.812 1 18 2 -4 2213.05 200.193 1 18 -2 -4 2349.43 192.244 1 18 2 -3 1087.57 141.051 1 18 -2 -3 1138.78 134.561 1 18 -2 -3 1169.55 104.54 1 18 2 -2 76.9696 51.4624 1 18 -2 -2 63.0196 59.7864 1 18 -2 -2 19.5182 49.6193 1 18 2 -1 131.215 65.8713 1 18 -2 -1 187.972 77.9673 1 18 -2 -1 136.638 62.9147 1 0 0 0 0.00 0.00 1 ; _shelx_hkl_checksum 30015 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y, -z+1/2' '-x, -y, -z' 'x-1/2, -y, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy I1 I 0.43796(2) 0.02083(2) 0.31199(2) 0.03304(6) Uani 1 1 d . . . I2 I 0.34765(2) 0.05656(2) 0.14350(2) 0.03123(6) Uani 1 1 d . . . I3 I 0.25244(2) 0.07515(2) -0.01409(2) 0.03870(7) Uani 1 1 d . . . I4 I 0.65714(2) -0.03895(2) 0.26514(2) 0.03331(6) Uani 1 1 d . . . N1 N 0.84206(18) 0.2958(2) 0.07078(13) 0.0259(5) Uani 1 1 d . . . H1 H 0.8354 0.2048 0.0714 0.034 Uiso 1 1 calc R U . O1 O 0.93292(17) 0.4695(2) 0.03347(13) 0.0316(5) Uani 1 1 d . . . O2 O 0.56065(18) 0.5680(2) 0.21128(15) 0.0381(6) Uani 1 1 d . . . C1 C 0.9756(2) 0.2348(3) 0.00307(17) 0.0337(7) Uani 1 1 d . . . H1A H 0.9510 0.1414 0.0113 0.051 Uiso 1 1 calc R U . H1B H 0.9741 0.2518 -0.0536 0.051 Uiso 1 1 calc R U . H1C H 1.0413 0.2421 0.0294 0.051 Uiso 1 1 calc R U . C2 C 0.9149(2) 0.3407(3) 0.03706(16) 0.0257(6) Uani 1 1 d . . . C3 C 0.7722(2) 0.3721(3) 0.10656(15) 0.0232(6) Uani 1 1 d . . . C4 C 0.7710(2) 0.5166(3) 0.11376(18) 0.0307(7) Uani 1 1 d . . . C5 C 0.6992(2) 0.5786(3) 0.14960(19) 0.0322(7) Uani 1 1 d . . . C6 C 0.6295(2) 0.4998(3) 0.17766(17) 0.0265(6) Uani 1 1 d . . . C7 C 0.6313(2) 0.3554(3) 0.17048(18) 0.0311(7) Uani 1 1 d . . . C8 C 0.7023(2) 0.2928(3) 0.13523(17) 0.0284(6) Uani 1 1 d . . . N2 N 0.15197(18) 0.6837(2) 0.40990(14) 0.0261(5) Uani 1 1 d . . . H2 H 0.1559 0.7735 0.4008 0.034 Uiso 1 1 calc R U . O3 O 0.06736(16) 0.52199(19) 0.46476(13) 0.0294(5) Uani 1 1 d . . . O4 O 0.44289(17) 0.3965(2) 0.29083(13) 0.0339(5) Uani 1 1 d . . . C9 C 0.0118(3) 0.7579(3) 0.4644(2) 0.0380(8) Uani 1 1 d . . . C10 C 0.0789(2) 0.6467(3) 0.44617(17) 0.0254(6) Uani 1 1 d . . . C11 C 0.2251(2) 0.6020(3) 0.38323(15) 0.0220(5) Uani 1 1 d . . . C12 C 0.2294(2) 0.4580(3) 0.38739(18) 0.0284(6) Uani 1 1 d . . . C13 C 0.3029(2) 0.3892(3) 0.35669(18) 0.0285(6) Uani 1 1 d . . . C14 C 0.3707(2) 0.4623(3) 0.32279(16) 0.0240(6) Uani 1 1 d . . . C15 C 0.3671(2) 0.6066(3) 0.31975(17) 0.0276(6) Uani 1 1 d . . . C16 C 0.2948(2) 0.6750(3) 0.35009(17) 0.0261(6) Uani 1 1 d . . . H1O H 1.0000 0.5000 0.0000 0.10(2) Uiso 1 2 d S . P H2O H 0.529(3) 0.516(4) 0.233(2) 0.044(11) Uiso 1 1 d . . . H3O H 0.0000 0.5000 0.5000 0.08(2) Uiso 1 2 d S . P H4 H 0.821(3) 0.576(3) 0.091(2) 0.041(10) Uiso 1 1 d . . . H4O H 0.441(3) 0.318(4) 0.2924(19) 0.030(10) Uiso 1 1 d . . . H5 H 0.700(2) 0.676(4) 0.1562(17) 0.032(9) Uiso 1 1 d . . . H7 H 0.585(3) 0.303(3) 0.187(2) 0.040(9) Uiso 1 1 d . . . H8 H 0.707(2) 0.185(3) 0.1294(15) 0.017(7) Uiso 1 1 d . . . H9A H 0.039(4) 0.847(5) 0.463(3) 0.086(16) Uiso 1 1 d . . . H9B H -0.048(4) 0.756(5) 0.434(3) 0.10(2) Uiso 1 1 d . . . H9C H -0.004(3) 0.753(5) 0.511(3) 0.078(15) Uiso 1 1 d . . . H12 H 0.179(2) 0.402(3) 0.4097(18) 0.028(8) Uiso 1 1 d . . . H13 H 0.305(2) 0.294(3) 0.3575(17) 0.027(8) Uiso 1 1 d . . . H15 H 0.413(2) 0.658(3) 0.2982(18) 0.033(9) Uiso 1 1 d . . . H16 H 0.293(2) 0.779(3) 0.3527(16) 0.026(8) Uiso 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I1 0.03071(13) 0.02876(11) 0.04194(12) 0.00180(8) 0.01325(9) 0.00049(8) I2 0.02888(12) 0.01830(9) 0.04922(13) -0.00560(7) 0.01506(10) -0.00036(7) I3 0.04319(15) 0.03111(11) 0.04307(13) -0.00468(8) 0.01047(10) -0.00384(9) I4 0.03255(13) 0.03177(11) 0.03606(11) 0.00153(8) 0.00630(9) -0.00416(8) N1 0.0259(14) 0.0218(11) 0.0322(12) 0.0035(9) 0.0121(11) 0.0011(10) O1 0.0292(13) 0.0297(11) 0.0398(11) 0.0004(9) 0.0187(10) -0.0019(9) O2 0.0387(15) 0.0320(12) 0.0500(14) -0.0022(10) 0.0293(12) 0.0017(10) C1 0.0300(18) 0.0390(17) 0.0348(16) 0.0006(13) 0.0139(14) 0.0051(13) C2 0.0237(16) 0.0318(15) 0.0225(13) 0.0021(11) 0.0064(11) 0.0031(12) C3 0.0231(15) 0.0251(13) 0.0232(12) 0.0019(10) 0.0100(11) 0.0037(11) C4 0.0338(18) 0.0266(15) 0.0348(15) -0.0011(12) 0.0162(14) -0.0027(13) C5 0.0345(19) 0.0253(15) 0.0405(16) -0.0038(12) 0.0182(14) -0.0034(12) C6 0.0265(17) 0.0273(14) 0.0280(14) -0.0005(11) 0.0116(12) 0.0006(12) C7 0.0314(18) 0.0305(15) 0.0353(16) 0.0048(12) 0.0183(14) -0.0038(13) C8 0.0311(18) 0.0222(14) 0.0346(15) 0.0036(11) 0.0144(13) -0.0014(12) N2 0.0257(14) 0.0164(10) 0.0393(13) 0.0032(9) 0.0166(11) 0.0003(9) O3 0.0280(12) 0.0228(10) 0.0420(11) 0.0068(8) 0.0210(10) 0.0014(8) O4 0.0344(13) 0.0252(11) 0.0472(13) -0.0041(10) 0.0245(11) -0.0001(10) C9 0.033(2) 0.0281(16) 0.058(2) 0.0055(15) 0.0251(18) 0.0049(14) C10 0.0222(16) 0.0250(14) 0.0307(14) 0.0021(11) 0.0098(12) -0.0009(11) C11 0.0208(14) 0.0206(12) 0.0265(13) -0.0005(10) 0.0099(11) -0.0014(11) C12 0.0287(17) 0.0215(13) 0.0385(16) 0.0030(11) 0.0175(14) -0.0039(12) C13 0.0286(17) 0.0169(13) 0.0433(16) -0.0016(12) 0.0169(13) -0.0020(11) C14 0.0228(16) 0.0243(13) 0.0268(13) -0.0034(10) 0.0105(12) 0.0002(11) C15 0.0294(17) 0.0253(14) 0.0310(14) 0.0017(11) 0.0145(13) -0.0045(12) C16 0.0280(17) 0.0203(13) 0.0325(14) 0.0019(11) 0.0127(12) -0.0011(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle I3 I2 I1 175.845(9) C2 N1 C3 130.1(2) C2 N1 H1 115.0 C3 N1 H1 115.0 C2 O1 H1O 115.9(2) C6 O2 H2O 112(3) C2 C1 H1A 109.5 C2 C1 H1B 109.5 H1A C1 H1B 109.5 C2 C1 H1C 109.5 H1A C1 H1C 109.5 H1B C1 H1C 109.5 O1 C2 N1 121.0(2) O1 C2 C1 120.9(3) N1 C2 C1 118.0(3) C8 C3 C4 119.8(2) C8 C3 N1 115.9(2) C4 C3 N1 124.3(2) C5 C4 C3 118.9(3) C5 C4 H4 121(2) C3 C4 H4 120(2) C6 C5 C4 121.2(3) C6 C5 H5 120.1(19) C4 C5 H5 118.7(19) O2 C6 C5 118.0(2) O2 C6 C7 122.5(3) C5 C6 C7 119.5(3) C8 C7 C6 119.7(3) C8 C7 H7 120(2) C6 C7 H7 120(2) C7 C8 C3 120.8(3) C7 C8 H8 122.4(15) C3 C8 H8 116.8(15) C10 N2 C11 130.5(2) C10 N2 H2 114.7 C11 N2 H2 114.7 C10 O3 H3O 115.5(2) C14 O4 H4O 114(3) C10 C9 H9A 112(3) C10 C9 H9B 115(3) H9A C9 H9B 110(4) C10 C9 H9C 114(3) H9A C9 H9C 104(4) H9B C9 H9C 101(4) O3 C10 N2 120.8(3) O3 C10 C9 121.5(3) N2 C10 C9 117.7(3) C12 C11 C16 119.7(2) C12 C11 N2 124.2(2) C16 C11 N2 116.1(2) C11 C12 C13 118.9(2) C11 C12 H12 121.8(18) C13 C12 H12 119.3(18) C14 C13 C12 121.0(2) C14 C13 H13 119.1(19) C12 C13 H13 120.0(19) O4 C14 C13 122.0(2) O4 C14 C15 118.0(2) C13 C14 C15 120.0(2) C16 C15 C14 119.2(2) C16 C15 H15 119.2(19) C14 C15 H15 121.5(19) C15 C16 C11 121.2(2) C15 C16 H16 121.1(17) C11 C16 H16 117.5(17) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 I1 I2 3.0077(3) . I2 I3 2.8493(3) . I4 I4 2.7509(4) 2_655 N1 C2 1.321(4) . N1 C3 1.434(3) . N1 H1 0.8800 . O1 C2 1.267(3) . O1 H1O 1.210(2) . O2 C6 1.365(3) . O2 H2O 0.80(4) . C1 C2 1.500(4) . C1 H1A 0.9800 . C1 H1B 0.9800 . C1 H1C 0.9800 . C3 C8 1.389(4) . C3 C4 1.396(4) . C4 C5 1.391(4) . C4 H4 1.02(4) . C5 C6 1.382(4) . C5 H5 0.94(3) . C6 C7 1.395(4) . C7 C8 1.379(4) . C7 H7 0.91(4) . C8 H8 1.04(3) . N2 C10 1.325(3) . N2 C11 1.424(3) . N2 H2 0.8800 . O3 C10 1.256(3) . O3 H3O 1.2143(19) . O4 C14 1.377(3) . O4 H4O 0.75(3) . C9 C10 1.492(4) . C9 H9A 0.94(5) . C9 H9B 0.93(6) . C9 H9C 0.86(4) . C11 C12 1.387(4) . C11 C16 1.393(4) . C12 C13 1.395(4) . C12 H12 1.00(3) . C13 C14 1.380(4) . C13 H13 0.91(3) . C14 C15 1.388(4) . C15 C16 1.377(4) . C15 H15 0.94(3) . C16 H16 1.00(3) . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1 H1O O1 1.210(2) 1.210(2) 2.420(4) 180.00(17) 3_765 O2 H2O O4 0.80(4) 2.02(4) 2.822(3) 175(4) . O4 H4O I1 0.75(3) 2.88(3) 3.631(2) 175(3) . N1 H1 I3 0.88 3.07 3.885(2) 155.1 3_655 N2 H2 I2 0.88 2.82 3.699(2) 173.4 2_565