#------------------------------------------------------------------------------ #$Date: 2020-10-06 13:00:51 +0300 (Tue, 06 Oct 2020) $ #$Revision: 257720 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/05/96/7059673.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7059673 loop_ _publ_author_name 'Dinda, Soumitra' 'Sultana, Tamanna' 'Sultana, Suhana' 'Patra, Sarat Chandra' 'Mitra, Arup Kumar' 'Roy, Subhadip' 'Pramanik, Kausikisankar' 'Ganguly, Sanjib' _publ_section_title ; Ruthenocycles of benzothiazolyl and pyridyl hydrazones with ancillary PAHs: synthesis, structure, electrochemistry and antimicrobial activity ; _journal_issue 26 _journal_name_full 'New Journal of Chemistry' _journal_page_first 11022 _journal_page_last 11034 _journal_paper_doi 10.1039/D0NJ01447H _journal_volume 44 _journal_year 2020 _chemical_formula_moiety 'C59 H44 Cl N3 O P2 Ru' _chemical_formula_sum 'C59 H44 Cl N3 O P2 Ru' _chemical_formula_weight 1009.491 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_Int_Tables_number 2 _audit_creation_date 2020-04-14 _audit_creation_method ; Olex2 1.3-dev (compiled 2020.03.26 svn.re84ffbc8 for OlexSys, GUI svn.r5830) ; _audit_update_record ; 2020-04-19 deposited with the CCDC. 2020-05-22 downloaded from the CCDC. ; _cell_angle_alpha 107.300(2) _cell_angle_beta 93.585(2) _cell_angle_gamma 103.021(2) _cell_formula_units_Z 2 _cell_length_a 10.4963(8) _cell_length_b 13.4855(11) _cell_length_c 18.0538(14) _cell_measurement_reflns_used 1260 _cell_measurement_temperature 273(2) _cell_measurement_theta_max 27.109 _cell_measurement_theta_min 2.011 _cell_volume 2354.0(3) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Olex2 1.3-dev (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-dev (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _diffrn_ambient_temperature 273.15 _diffrn_measured_fraction_theta_full 0.9978 _diffrn_measured_fraction_theta_max 0.9939 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0331 _diffrn_reflns_av_unetI/netI 0.0189 _diffrn_reflns_Laue_measured_fraction_full 0.9978 _diffrn_reflns_Laue_measured_fraction_max 0.9939 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 81824 _diffrn_reflns_point_group_measured_fraction_full 0.9978 _diffrn_reflns_point_group_measured_fraction_max 0.9939 _diffrn_reflns_theta_full 25.2417 _diffrn_reflns_theta_max 27.11 _diffrn_reflns_theta_min 2.01 _exptl_absorpt_coefficient_mu 0.504 _exptl_absorpt_correction_T_max 0.904 _exptl_absorpt_correction_T_min 0.834 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour orange _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 1.424 _exptl_crystal_description prism _exptl_crystal_F_000 1034.581 _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.3930 _refine_diff_density_min -0.5882 _refine_diff_density_rms 0.0542 _refine_ls_d_res_high 0.7799 _refine_ls_d_res_low 10.1268 _refine_ls_goodness_of_fit_ref 1.1048 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 146 _refine_ls_number_parameters 745 _refine_ls_number_reflns 10344 _refine_ls_number_restraints 6 _refine_ls_restrained_S_all 1.1044 _refine_ls_R_factor_all 0.0374 _refine_ls_R_factor_gt 0.0298 _refine_ls_shift/su_max 0.0006 _refine_ls_shift/su_mean 0.0000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0341P)^2^+1.1853P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0735 _refine_ls_wR_factor_ref 0.0829 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 13 _reflns_limit_h_min -13 _reflns_limit_k_max 16 _reflns_limit_k_min -17 _reflns_limit_l_max 23 _reflns_limit_l_min 0 _reflns_number_gt 9001 _reflns_number_total 10344 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL 3a.res in P-1 CELL 0.71073 10.4963 13.4855 18.0538 107.3 93.585 103.021 ZERR 2 0.0008 0.0011 0.0014 0.002 0.002 0.002 LATT 1 SFAC C H Cl N O P Ru UNIT 118 88 2 6 2 4 2 SADI 0.001 O2 C76 O1 C23 SADI 0.001 Ru1 Cl2 Ru1 Cl1 SADI 0.001 Ru1 C76 Ru1 C23 RIGU 0.001 0.001 L.S. 6 PLAN 5 TEMP 0 CONF BOND $H MORE -1 fmap 2 acta OMIT 1 0 1 OMIT 0 -1 2 OMIT -1 -1 1 OMIT -1 0 2 OMIT 0 -2 2 OMIT -1 1 0 WGHT 0.03409 1.185312 FVAR 0.520346 REM REM REM REM > REM REM > REM > REM REM C1 1 1.15624 0.49739 0.69327 11.00000 0.04188 0.08058 0.05935 = 0.04374 0.01403 0.01432 AFIX 43 H1 2 1.16257 0.51398 0.64696 11.00000 -1.20000 AFIX 0 C2 1 1.26705 0.52418 0.74618 11.00000 0.03355 0.15740 0.09877 = 0.08334 0.00701 0.00123 AFIX 43 H2 2 1.34810 0.55886 0.73620 11.00000 -1.20000 AFIX 0 C3 1 1.25717 0.49907 0.81475 11.00000 0.03293 0.22130 0.09940 = 0.10484 -0.01498 -0.01058 AFIX 43 H3 2 1.33207 0.51799 0.85139 11.00000 -1.20000 AFIX 0 C4 1 1.13898 0.44687 0.82953 11.00000 0.03580 0.15857 0.07071 = 0.07856 -0.00424 0.00348 AFIX 43 H4 2 1.13181 0.42896 0.87530 11.00000 -1.20000 AFIX 0 C5 1 1.02994 0.42164 0.77333 11.00000 0.03152 0.06395 0.04501 = 0.02991 0.00103 0.00910 C6 1 0.74442 0.30952 0.83536 11.00000 0.03767 0.08837 0.07993 = 0.05911 0.00373 0.00573 AFIX 43 H6 2 0.68522 0.31313 0.79630 11.00000 -1.20000 AFIX 0 C7 1 0.69333 0.26724 0.89558 11.00000 0.04775 0.08093 0.07588 = 0.05037 0.00774 0.00196 C8 1 0.77960 0.25466 0.95234 11.00000 0.05966 0.11476 0.08793 = 0.07030 0.00545 0.00265 AFIX 43 H8 2 0.87003 0.27419 0.95098 11.00000 -1.20000 AFIX 0 C9 1 0.73490 0.21447 1.00980 11.00000 0.08552 0.12988 0.08330 = 0.07167 0.00256 0.00061 AFIX 43 H9 2 0.79525 0.20729 1.04658 11.00000 -1.20000 AFIX 0 C10 1 0.60052 0.18417 1.01403 11.00000 0.09092 0.09196 0.06838 = 0.04273 0.02128 0.00003 C11 1 0.55192 0.14145 1.07360 11.00000 0.13439 0.13052 0.07735 = 0.05748 0.03073 -0.00595 AFIX 43 H11 2 0.61099 0.13357 1.11072 11.00000 -1.20000 AFIX 0 C12 1 0.42199 0.11281 1.07615 11.00000 0.14979 0.11271 0.08422 = 0.03995 0.05854 -0.01113 AFIX 43 H12 2 0.39293 0.08425 1.11491 11.00000 -1.20000 AFIX 0 C13 1 0.32804 0.12417 1.02271 11.00000 0.10279 0.06560 0.09137 = 0.00463 0.06041 -0.01251 C14 1 0.19178 0.10051 1.02533 11.00000 0.12736 0.07802 0.13175 = -0.00083 0.09189 -0.01830 AFIX 43 H14 2 0.15965 0.07339 1.06415 11.00000 -1.20000 AFIX 0 C15 1 0.10460 0.11561 0.97338 11.00000 0.08414 0.07879 0.16849 = -0.00109 0.07860 -0.01425 AFIX 43 H15 2 0.01518 0.09981 0.97819 11.00000 -1.20000 AFIX 0 C16 1 0.14578 0.15378 0.91380 11.00000 0.06453 0.07731 0.17196 = 0.01153 0.04941 -0.00327 AFIX 43 H16 2 0.08507 0.16362 0.87861 11.00000 -1.20000 AFIX 0 C17 1 0.28189 0.17777 0.90704 11.00000 0.05885 0.06374 0.12095 = 0.01155 0.04095 -0.00553 C18 1 0.32903 0.21876 0.84610 11.00000 0.04855 0.09982 0.12618 = 0.04309 0.01541 0.00636 AFIX 43 H18 2 0.26900 0.22590 0.80913 11.00000 -1.20000 AFIX 0 C19 1 0.45985 0.24703 0.84202 11.00000 0.04601 0.09716 0.09958 = 0.04893 0.01385 0.00255 AFIX 43 H19 2 0.48808 0.27347 0.80214 11.00000 -1.20000 AFIX 0 C20 1 0.55591 0.23729 0.89745 11.00000 0.04990 0.07350 0.07637 = 0.03933 0.01662 0.00134 C21 1 0.51062 0.19480 0.95818 11.00000 0.06959 0.06020 0.07270 = 0.02244 0.02851 -0.00261 C22 1 0.37328 0.16527 0.96146 11.00000 0.07520 0.05588 0.08552 = 0.00949 0.03999 -0.00787 C24 1 0.66562 0.60279 0.69229 11.00000 0.03643 0.04652 0.03741 = 0.01862 0.00307 0.01496 C25 1 0.64593 0.70202 0.73076 11.00000 0.06244 0.05154 0.05776 = 0.00667 -0.01272 0.02222 AFIX 43 H25 2 0.70153 0.74626 0.77634 11.00000 -1.20000 AFIX 0 C26 1 0.54407 0.73635 0.70210 11.00000 0.07142 0.05625 0.07836 = 0.01500 -0.00384 0.03399 AFIX 43 H26 2 0.53187 0.80348 0.72831 11.00000 -1.20000 AFIX 0 C27 1 0.46115 0.67130 0.63501 11.00000 0.04668 0.06932 0.06382 = 0.03361 0.00603 0.02612 AFIX 43 H27 2 0.39318 0.69454 0.61559 11.00000 -1.20000 AFIX 0 C28 1 0.47853 0.57286 0.59702 11.00000 0.04363 0.06577 0.04114 = 0.02198 -0.00033 0.01924 AFIX 43 H28 2 0.42157 0.52853 0.55199 11.00000 -1.20000 AFIX 0 C29 1 0.58090 0.53813 0.62507 11.00000 0.04393 0.05307 0.03858 = 0.01619 0.00189 0.01883 AFIX 43 H29 2 0.59249 0.47093 0.59845 11.00000 -1.20000 AFIX 0 C30 1 0.76786 0.57054 0.83168 11.00000 0.04005 0.05347 0.03523 = 0.01736 0.00320 0.00799 C31 1 0.86952 0.58464 0.89023 11.00000 0.04151 0.06594 0.04062 = 0.02267 0.00096 0.00801 AFIX 43 H31 2 0.95644 0.59707 0.88003 11.00000 -1.20000 AFIX 0 C32 1 0.84262 0.58036 0.96320 11.00000 0.05716 0.09053 0.04018 = 0.02865 -0.00572 0.00472 AFIX 43 H32 2 0.91126 0.58963 1.00179 11.00000 -1.20000 AFIX 0 C33 1 0.71520 0.56249 0.97886 11.00000 0.06458 0.12689 0.04278 = 0.03996 0.00804 0.00725 AFIX 43 H33 2 0.69737 0.56049 1.02829 11.00000 -1.20000 AFIX 0 C34 1 0.61344 0.54748 0.92166 11.00000 0.04743 0.14537 0.05668 = 0.04780 0.01447 0.01221 AFIX 43 H34 2 0.52678 0.53449 0.93229 11.00000 -1.20000 AFIX 0 C35 1 0.63944 0.55162 0.84849 11.00000 0.04113 0.10251 0.04670 = 0.03348 0.00280 0.01183 AFIX 43 H35 2 0.57007 0.54162 0.81013 11.00000 -1.20000 AFIX 0 C36 1 0.94249 0.67443 0.74379 11.00000 0.03858 0.04262 0.04230 = 0.01914 -0.00152 0.00758 C37 1 0.98158 0.76188 0.81181 11.00000 0.06315 0.04794 0.04849 = 0.01583 -0.00260 0.00578 AFIX 43 H37 2 0.93538 0.76380 0.85431 11.00000 -1.20000 AFIX 0 C38 1 1.08834 0.84599 0.81698 11.00000 0.08182 0.04959 0.06620 = 0.01987 -0.01829 -0.00811 AFIX 43 H38 2 1.11360 0.90426 0.86283 11.00000 -1.20000 AFIX 0 C39 1 1.15752 0.84402 0.75464 11.00000 0.06500 0.06582 0.09021 = 0.04547 -0.01478 -0.01269 AFIX 43 H39 2 1.23048 0.90023 0.75870 11.00000 -1.20000 AFIX 0 C40 1 1.11885 0.75892 0.68626 11.00000 0.05528 0.07549 0.07484 = 0.04769 0.01079 0.00750 AFIX 43 H40 2 1.16470 0.75825 0.64374 11.00000 -1.20000 AFIX 0 C41 1 1.01137 0.67396 0.68062 11.00000 0.04674 0.05380 0.05023 = 0.02636 0.00541 0.00971 AFIX 43 H41 2 0.98547 0.61652 0.63429 11.00000 -1.20000 AFIX 0 PART 3 Cl1 3 0.82500 0.42434 0.54147 10.75000 0.08357 0.05257 0.03883 = 0.02014 0.00555 0.02816 PART 0 N1 4 1.03936 0.44804 0.70656 11.00000 0.03347 0.05173 0.03995 = 0.02351 0.00258 0.01084 N2 4 0.90262 0.37428 0.77242 11.00000 0.03192 0.05578 0.04601 = 0.03065 -0.00087 0.00580 N3 4 0.86902 0.34223 0.83414 11.00000 0.03904 0.06398 0.05719 = 0.03865 0.00269 0.00569 P1 6 0.80121 0.56010 0.73220 11.00000 0.03125 0.04063 0.03125 = 0.01484 0.00002 0.00853 P2 6 0.86941 0.21777 0.59442 11.00000 0.04114 0.03657 0.04761 = 0.01891 -0.00221 0.01058 Ru1 7 0.83201 0.38749 0.66482 11.00000 0.03139 0.03840 0.03713 = 0.01837 -0.00263 0.00751 PART 1 AFIX 66 C42 1 0.75733 0.13998 0.49858 10.60000 0.04700 0.03487 0.04590 = 0.01232 -0.00519 0.00366 C43 1 0.62631 0.14385 0.48895 10.60000 0.04388 0.06696 0.06217 = 0.01244 -0.00293 0.01262 AFIX 43 H43 2 0.59416 0.18966 0.52839 10.60000 -1.20000 AFIX 0 AFIX 65 C44 1 0.54334 0.07925 0.42037 10.60000 0.04416 0.08249 0.06406 = 0.01201 -0.01294 -0.00058 AFIX 43 H44 2 0.45568 0.08184 0.41393 10.60000 -1.20000 AFIX 0 AFIX 65 C45 1 0.59139 0.01078 0.36142 10.60000 0.06758 0.06611 0.06812 = 0.01604 -0.01876 0.00343 AFIX 43 H45 2 0.53587 -0.03244 0.31554 10.60000 -1.20000 AFIX 0 AFIX 65 C47 1 0.72241 0.00691 0.37106 10.60000 0.07930 0.05288 0.05851 = 0.00387 -0.00322 0.01678 AFIX 43 H47 2 0.75456 -0.03891 0.33162 10.60000 -1.20000 AFIX 0 AFIX 65 C46 1 0.80538 0.07150 0.43964 10.60000 0.05191 0.05691 0.06659 = 0.01361 -0.00497 0.01635 AFIX 43 H46 2 0.89304 0.06891 0.44608 10.60000 -1.20000 AFIX 0 PART 2 AFIX 66 C48 1 1.03675 0.23403 0.55767 10.40000 0.02645 0.03985 0.07295 = 0.02500 0.00384 0.01142 C64 1 1.15327 0.27766 0.60987 10.40000 0.03751 0.04795 0.07570 = 0.01718 0.00327 0.01786 AFIX 43 H64 2 1.15055 0.29405 0.66347 10.40000 -1.20000 AFIX 0 AFIX 65 C63 1 1.27386 0.29678 0.58198 10.40000 0.03384 0.06034 0.12291 = 0.02887 0.00807 0.01681 AFIX 43 H63 2 1.35182 0.32597 0.61691 10.40000 -1.20000 AFIX 0 AFIX 65 C62 1 1.27793 0.27228 0.50188 10.40000 0.04186 0.06276 0.13500 = 0.04878 0.04021 0.01581 AFIX 43 H62 2 1.35861 0.28507 0.48322 10.40000 -1.20000 AFIX 0 AFIX 65 C61 1 1.16141 0.22865 0.44968 10.40000 0.08563 0.08536 0.10389 = 0.04843 0.05103 0.02861 AFIX 43 H61 2 1.16413 0.21226 0.39608 10.40000 -1.20000 AFIX 0 AFIX 65 C60 1 1.04082 0.20953 0.47757 10.40000 0.05392 0.06035 0.07230 = 0.03199 0.02106 0.01636 AFIX 43 H60 2 0.96286 0.18034 0.44264 10.40000 -1.20000 AFIX 0 AFIX 66 C54 1 0.88293 0.13091 0.65417 10.40000 0.04947 0.03056 0.03958 = 0.01761 0.00248 0.01278 C55 1 0.77123 0.10517 0.68910 10.40000 0.05324 0.03698 0.04736 = 0.01683 0.00152 0.00431 AFIX 43 H55 2 0.69972 0.13307 0.68204 10.40000 -1.20000 AFIX 0 AFIX 65 C58 1 0.76639 0.03774 0.73458 10.40000 0.08366 0.05677 0.06053 = 0.03029 0.01712 -0.00007 AFIX 43 H58 2 0.69165 0.02052 0.75795 10.40000 -1.20000 AFIX 0 AFIX 65 C56 1 0.87326 -0.00396 0.74513 10.40000 0.09433 0.05967 0.07577 = 0.04485 -0.00540 0.01067 AFIX 43 H56 2 0.87003 -0.04907 0.77556 10.40000 -1.20000 AFIX 0 AFIX 65 C57 1 0.98497 0.02178 0.71021 10.40000 0.09290 0.07909 0.09295 = 0.05449 -0.00556 0.03681 AFIX 43 H57 2 1.05648 -0.00612 0.71727 10.40000 -1.20000 AFIX 0 AFIX 65 C59 1 0.98981 0.08921 0.66473 10.40000 0.06143 0.06724 0.07460 = 0.03923 0.00145 0.02763 AFIX 43 H59 2 1.06455 0.10643 0.64136 10.40000 -1.20000 AFIX 0 PART 1 AFIX 66 C70 1 0.83940 0.11464 0.64683 10.40000 0.04242 0.04848 0.07234 = 0.02848 0.00590 0.01816 C71 1 0.89750 0.02949 0.62257 10.40000 0.10426 0.08095 0.10130 = 0.05988 0.05422 0.05895 AFIX 43 H71 2 0.94336 0.02238 0.57964 10.40000 -1.20000 AFIX 0 AFIX 65 C72 1 0.88704 -0.04503 0.66248 10.40000 0.10928 0.08252 0.14516 = 0.07349 0.05065 0.06307 AFIX 43 H72 2 0.92591 -0.10201 0.64625 10.40000 -1.20000 AFIX 0 AFIX 65 C73 1 0.81849 -0.03440 0.72665 10.40000 0.08318 0.06860 0.11133 = 0.06267 0.01160 0.02107 AFIX 43 H73 2 0.81150 -0.08426 0.75335 10.40000 -1.20000 AFIX 0 AFIX 65 CXE 1 0.76040 0.05075 0.75090 10.40000 0.10889 0.05365 0.06475 = 0.03292 0.01349 0.01295 AFIX 43 HXE 2 0.71454 0.05786 0.79383 10.40000 -1.20000 AFIX 0 AFIX 65 CXF 1 0.77086 0.12528 0.71099 10.40000 0.06961 0.04357 0.03944 = 0.01204 0.00640 0.00727 AFIX 43 HXF 2 0.73199 0.18225 0.72722 10.40000 -1.20000 AFIX 0 PART 2 AFIX 66 C74 1 0.75920 0.13082 0.51171 10.40000 0.02675 0.04408 0.05083 = 0.02401 0.00252 0.00871 C67 1 0.76658 0.02516 0.48038 10.40000 0.04288 0.04092 0.06476 = 0.00782 -0.00496 0.01686 AFIX 43 H67 2 0.83017 0.00090 0.50310 10.40000 -1.20000 AFIX 0 AFIX 65 C66 1 0.67893 -0.04423 0.41508 10.40000 0.06296 0.04159 0.07214 = 0.00102 -0.01160 0.01243 AFIX 43 H66 2 0.68387 -0.11492 0.39412 10.40000 -1.20000 AFIX 0 AFIX 65 C65 1 0.58388 -0.00796 0.38112 10.40000 0.06081 0.04346 0.07007 = 0.00027 -0.02591 0.00210 AFIX 43 H65 2 0.52523 -0.05439 0.33744 10.40000 -1.20000 AFIX 0 AFIX 65 C69 1 0.57650 0.09769 0.41245 10.40000 0.04397 0.05051 0.06994 = 0.02978 -0.01012 0.00826 AFIX 43 H69 2 0.51291 0.12196 0.38973 10.40000 -1.20000 AFIX 0 AFIX 65 C68 1 0.66416 0.16709 0.47774 10.40000 0.04595 0.03675 0.04263 = 0.01649 -0.00593 0.00859 AFIX 43 H68 2 0.65921 0.23778 0.49870 10.40000 -1.20000 AFIX 0 PART 1 AFIX 66 C75 1 1.02404 0.23653 0.57217 10.40000 0.03787 0.03974 0.05161 = 0.01617 0.00485 0.01061 C50 1 1.05354 0.27494 0.51019 10.40000 0.04073 0.05652 0.07042 = 0.02747 0.00809 0.01809 AFIX 43 H50 2 0.98654 0.28438 0.47883 10.40000 -1.20000 AFIX 0 AFIX 65 C51 1 1.18319 0.29922 0.49508 10.40000 0.06085 0.07317 0.10240 = 0.05477 0.02938 0.01481 AFIX 43 H51 2 1.20293 0.32492 0.45361 10.40000 -1.20000 AFIX 0 AFIX 65 C49 1 1.28333 0.28510 0.54196 10.40000 0.03622 0.06678 0.08802 = 0.02990 0.01021 0.01207 AFIX 43 H49 2 1.37007 0.30135 0.53185 10.40000 -1.20000 AFIX 0 AFIX 65 C53 1 1.25383 0.24670 0.60394 10.40000 0.03295 0.09637 0.11030 = 0.05814 0.00016 0.01337 AFIX 43 H53 2 1.32083 0.23725 0.63531 10.40000 -1.20000 AFIX 0 AFIX 65 C52 1 1.12418 0.22241 0.61905 10.40000 0.03767 0.08268 0.07960 = 0.04363 0.00627 0.01960 AFIX 43 H52 2 1.10444 0.19671 0.66052 10.40000 -1.20000 AFIX 0 PART 3 AFIX 66 C77 1 0.77431 0.00923 0.60095 10.20000 0.05385 AFIX 43 H77 2 0.71608 -0.00490 0.55589 10.20000 -1.20000 AFIX 0 AFIX 65 C78 1 0.77096 -0.06926 0.63675 10.20000 0.06874 AFIX 43 H78 2 0.71048 -0.13590 0.61564 10.20000 -1.20000 AFIX 0 AFIX 65 C79 1 0.85800 -0.04814 0.70410 10.20000 0.07061 AFIX 43 H79 2 0.85575 -0.10065 0.72805 10.20000 -1.20000 AFIX 0 AFIX 65 CXD 1 0.94839 0.05147 0.73565 10.20000 0.07318 AFIX 43 HXD 2 1.00663 0.06560 0.78072 10.20000 -1.20000 AFIX 0 AFIX 65 C1A 1 0.95175 0.12996 0.69986 10.20000 0.05707 AFIX 43 H1A 2 1.01223 0.19660 0.72097 10.20000 -1.20000 AFIX 0 AFIX 65 C1B 1 0.86471 0.10884 0.63251 10.20000 0.04054 AFIX 0 PART 4 O2 5 0.81534 0.42955 0.51277 10.25000 0.06964 0.07313 0.05042 = 0.03599 0.01436 0.02660 C76 1 0.81543 0.41207 0.57148 10.25000 0.04909 0.04181 0.04665 = 0.01871 0.01712 0.01919 Cl2 3 0.59889 0.31425 0.66308 10.25000 0.02851 0.05796 0.06582 = 0.02804 -0.00242 0.00621 PART 3 O1 5 0.54697 0.28929 0.65775 10.75000 0.03624 0.09351 0.10806 = 0.05029 -0.01636 -0.00551 C23 1 0.65667 0.32640 0.65685 10.75000 0.04821 0.05205 0.05467 = 0.02654 -0.00429 0.01355 AFIX 66 C80 1 1.25434 0.19983 0.55039 10.20000 0.06274 AFIX 43 H80 2 1.31529 0.16445 0.56233 10.20000 -1.20000 AFIX 0 AFIX 65 C81 1 1.12953 0.17988 0.57317 10.20000 0.05138 AFIX 43 H81 2 1.10697 0.13115 0.60035 10.20000 -1.20000 AFIX 0 AFIX 65 C82 1 1.03844 0.23277 0.55533 10.20000 0.03634 C1C 1 1.07216 0.30561 0.51470 10.20000 0.03598 AFIX 43 H1C 2 1.01121 0.34099 0.50277 10.20000 -1.20000 AFIX 0 AFIX 65 C1D 1 1.19697 0.32555 0.49192 10.20000 0.04032 AFIX 43 H1D 2 1.21952 0.37429 0.46474 10.20000 -1.20000 AFIX 0 AFIX 65 C1E 1 1.28806 0.27267 0.50977 10.20000 0.07886 AFIX 43 H1E 2 1.37157 0.28601 0.49453 10.20000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.833333 0.488889 0.7 11 0.05 0.39 Q2 1 0.861111 0.288889 0.633333 11 0.05 0.39 REM The information below was added by Olex2. REM REM R1 = 0.0298 for 9001 Fo > 4sig(Fo) and 0.0374 for all 10344 data REM 745 parameters refined using 6 restraints REM Highest difference peak 0.3930, deepest hole -0.5882 REM Mean Shift 0.0000, Max Shift 0.0006. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0374 REM R1_gt = 0.0298 REM wR_ref = 0.0829 REM GOOF = 1.1048 REM Shift_max = 0.0006 REM Shift_mean = 0.0000 REM Reflections_all = 10344 REM Reflections_gt = 9001 REM Parameters = 745 REM Hole = -0.5882 REM Peak = 0.3930 REM Flack = n/a ; _cod_data_source_file d0nj01447h2.cif _cod_data_source_block 3a _cod_depositor_comments ;Adding full bibliography for 7059673--7059676.cif. Adding full bibliography for 7059673--7059676.cif. ; _cod_database_code 7059673 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2. Restrained distances O2-C76 \\sim O1-C23 with sigma of 0.001 Ru1-Cl2 \\sim Ru1-Cl1 with sigma of 0.001 Ru1-C76 \\sim Ru1-C23 with sigma of 0.001 3. Rigid body (RIGU) restrains All non-hydrogen atoms with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 4. Others Fixed Sof: Cl1(0.75) C42(0.6) C43(0.6) H43(0.6) C44(0.6) H44(0.6) C45(0.6) H45(0.6) C47(0.6) H47(0.6) C46(0.6) H46(0.6) C48(0.4) C64(0.4) H64(0.4) C63(0.4) H63(0.4) C62(0.4) H62(0.4) C61(0.4) H61(0.4) C60(0.4) H60(0.4) C54(0.4) C55(0.4) H55(0.4) C58(0.4) H58(0.4) C56(0.4) H56(0.4) C57(0.4) H57(0.4) C59(0.4) H59(0.4) C70(0.4) C71(0.4) H71(0.4) C72(0.4) H72(0.4) C73(0.4) H73(0.4) CXE(0.4) HXE(0.4) CXF(0.4) HXF(0.4) C74(0.4) C67(0.4) H67(0.4) C66(0.4) H66(0.4) C65(0.4) H65(0.4) C69(0.4) H69(0.4) C68(0.4) H68(0.4) C75(0.4) C50(0.4) H50(0.4) C51(0.4) H51(0.4) C49(0.4) H49(0.4) C53(0.4) H53(0.4) C52(0.4) H52(0.4) C77(0.2) H77(0.2) C78(0.2) H78(0.2) C79(0.2) H79(0.2) CXD(0.2) HXD(0.2) C1A(0.2) H1A(0.2) C1B(0.2) O2(0.25) C76(0.25) Cl2(0.25) O1(0.75) C23(0.75) C80(0.2) H80(0.2) C81(0.2) H81(0.2) C82(0.2) C1C(0.2) H1C(0.2) C1D(0.2) H1D(0.2) C1E(0.2) H1E(0.2) 5.a Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C3(H3), C4(H4), C6(H6), C8(H8), C9(H9), C11(H11), C12(H12), C14(H14), C15(H15), C16(H16), C18(H18), C19(H19), C25(H25), C26(H26), C27(H27), C28(H28), C29(H29), C31(H31), C32(H32), C33(H33), C34(H34), C35(H35), C37(H37), C38(H38), C39(H39), C40(H40), C41(H41), C43(H43), C44(H44), C45(H45), C47(H47), C46(H46), C64(H64), C63(H63), C62(H62), C61(H61), C60(H60), C55(H55), C58(H58), C56(H56), C57(H57), C59(H59), C71(H71), C72(H72), C73(H73), CXE(HXE), CXF(HXF), C67(H67), C66(H66), C65(H65), C69(H69), C68(H68), C50(H50), C51(H51), C49(H49), C53(H53), C52(H52), C77(H77), C78(H78), C79(H79), CXD(HXD), C1A(H1A), C80(H80), C81(H81), C1C(H1C), C1D(H1D), C1E(H1E) 5.b Fitted hexagon refined as free rotating group: C42(C43,C44,C45,C47,C46), C48(C64,C63,C62,C61,C60), C54(C55,C58,C56,C57,C59), C70(C71,C72,C73,CXE,CXF), C74(C67,C66,C65,C69,C68), C75(C50,C51,C49,C53,C52), C77(C78,C79,CXD,C1A,C1B), C80(C81,C82,C1C,C1D,C1E) ; _iucr_refine_fcf_details ; data_3a_CCDC1 _computing_structure_refinement 'olex2.refine 1.3-dev (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 _cell_length_a 10.4963(8) _cell_length_b 13.4855(11) _cell_length_c 18.0538(14) _cell_angle_alpha 107.300(2) _cell_angle_beta 93.585(2) _cell_angle_gamma 103.021(2) _cell_volume 2354.0(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -13 0 1 41.214 26.161 5.135 86.076 o -13 0 2 56.182 52.410 5.862 59.182 o -13 0 3 18.695 0.576 5.775 125.543 o -13 0 4 7.008 2.276 4.756 209.448 o -13 0 5 198.369 194.739 8.815 17.091 o -13 1 1 1.173 -10.149 3.544 451.883 o -13 1 2 115.124 100.884 6.807 31.852 o -13 1 3 252.604 266.866 9.100 13.110 o -13 1 4 58.733 55.085 5.249 61.202 o -13 1 5 163.395 134.503 7.449 22.977 o -13 1 6 368.208 381.189 10.795 8.471 o -13 1 7 7.365 -2.585 10.711 50.545 o -13 2 1 220.699 175.774 9.746 15.706 o -13 2 2 0.414 -1.352 3.924 387.610 o -13 2 3 265.278 260.416 9.541 12.582 o -13 2 4 182.530 191.487 8.810 18.056 o -13 2 5 2.716 -4.791 3.265 475.670 o -13 2 6 167.288 160.443 7.601 21.383 o -13 2 7 16.684 2.847 3.366 236.127 o -13 3 1 348.180 324.775 10.865 9.288 o -13 3 2 219.753 206.360 8.187 16.204 o -13 3 3 13.458 11.143 3.693 211.121 o -13 3 4 161.414 145.583 7.663 22.395 o -13 3 5 20.890 10.155 4.156 159.767 o -13 3 6 31.360 22.558 4.019 119.996 o -13 3 7 26.800 8.917 3.705 156.519 o -13 4 1 91.168 79.430 6.932 38.009 o -13 4 2 249.836 232.855 9.727 13.443 o -13 4 3 5.529 1.965 4.397 248.709 o -13 4 4 106.161 87.198 6.656 34.977 o -13 4 5 48.840 53.251 5.581 65.026 o -13 4 6 0.730 -9.312 3.515 471.298 o -13 5 1 64.751 59.055 5.758 54.295 o -13 5 2 66.673 58.135 6.347 50.498 o -13 5 3 0.444 -7.499 3.972 377.800 o -13 5 4 40.044 35.039 5.383 80.003 o -13 5 5 41.052 37.023 5.240 79.807 o -13 5 6 40.344 35.447 5.632 76.803 o -13 6 1 13.812 -0.087 4.518 193.906 o -13 6 2 43.094 40.466 5.758 71.471 o -13 6 3 71.501 60.901 6.489 47.596 o -13 6 4 99.086 99.556 7.654 32.473 o -13 6 5 1.439 -1.883 4.294 311.230 o -13 7 1 151.799 132.877 11.033 19.116 o -13 7 2 50.722 62.540 7.618 48.252 o -13 7 3 62.658 57.283 6.591 50.829 o -12 -4 3 208.735 184.196 12.752 13.631 o -12 -4 4 196.516 176.630 8.816 17.679 o -12 -4 5 21.549 13.437 5.909 105.671 o -12 -4 6 421.838 429.467 13.246 6.864 o -12 -3 1 332.264 300.829 10.928 9.810 o -12 -3 2 114.977 104.181 6.217 32.926 o -12 -3 3 16.829 19.723 4.001 162.646 o -12 -3 4 277.797 290.688 10.403 11.389 o -12 -3 5 15.989 28.407 4.647 132.689 o -12 -3 6 67.396 64.351 5.967 51.036 o -12 -3 7 62.802 55.437 5.911 55.050 o -12 -3 8 0.238 3.136 4.272 309.682 o -12 -3 9 42.571 36.675 5.872 72.092 o -12 -2 1 125.730 105.238 6.338 30.851 o -12 -2 2 216.765 209.579 11.052 14.184 o -12 -2 3 38.214 31.984 4.158 98.858 o -12 -2 4 37.632 37.049 4.277 94.774 o -12 -2 5 39.379 44.877 4.670 83.903 o -12 -2 6 4.064 3.314 3.236 405.964 o -12 -2 7 27.556 3.128 3.453 172.300 o -12 -2 8 71.818 70.529 5.632 49.845 o -12 -2 9 16.926 7.806 3.829 194.407 o -12 -2 10 145.155 145.843 8.915 22.051 o -12 -1 1 0.163 -4.224 3.097 627.088 o -12 -1 2 135.461 119.895 6.865 27.543 o -12 -1 3 55.214 62.268 5.134 61.902 o -12 -1 4 7.349 -0.547 2.886 430.319 o -12 -1 5 74.077 81.828 5.922 45.901 o -12 -1 6 63.045 51.262 5.098 60.867 o -12 -1 7 4.002 -9.270 2.838 542.779 o -12 -1 8 172.029 171.637 8.253 19.902 o -12 -1 9 237.746 258.822 9.365 13.619 o -12 -1 10 1.368 -3.158 3.590 436.254 o -12 -1 11 201.087 197.775 9.109 16.628 o -12 0 1 32.465 30.896 4.938 96.072 o -12 0 2 57.512 59.897 5.793 57.155 o -12 0 3 108.312 123.631 7.137 30.421 o -12 0 4 50.282 46.444 4.635 73.997 o -12 0 5 54.083 42.701 5.961 62.137 o -12 0 6 410.749 407.517 10.326 7.741 o -12 0 7 166.875 181.226 7.792 20.420 o -12 0 8 71.673 64.304 5.543 51.499 o -12 0 9 327.063 348.356 10.191 9.678 o -12 0 10 141.090 137.756 7.755 24.491 o -12 0 11 40.986 27.886 4.770 89.989 o -12 1 1 113.529 109.575 6.771 31.497 o -12 1 2 4.593 0.030 3.426 395.919 o -12 1 3 291.862 310.059 9.185 11.272 o -12 1 4 500.640 557.136 11.796 5.703 o -12 1 5 41.835 48.368 4.468 81.932 o -12 1 6 189.342 164.145 7.895 19.355 o -12 1 7 287.446 308.972 13.181 9.769 o -12 1 8 18.547 13.339 3.585 184.069 o -12 1 9 145.314 135.258 7.456 24.643 o -12 1 10 91.989 90.238 6.234 38.836 o -12 1 11 8.428 -0.482 3.513 320.050 o -12 2 1 447.745 438.044 10.815 6.977 o -12 2 2 200.211 195.572 10.117 15.882 o -12 2 3 9.277 11.516 3.595 244.541 o -12 2 4 309.750 314.622 9.446 10.673 o -12 2 5 183.518 195.325 8.571 18.111 o -12 2 6 1.670 -3.353 2.992 593.354 o -12 2 7 106.435 104.577 6.368 34.047 o -12 2 8 105.712 92.757 5.736 36.928 o -12 2 9 0.453 -5.729 3.718 429.657 o -12 2 10 24.624 14.392 3.954 147.548 o -12 2 11 19.242 23.924 3.903 150.872 o -12 3 1 111.932 122.351 10.267 23.650 o -12 3 2 592.310 564.233 13.530 4.802 o -12 3 3 436.880 439.932 10.758 7.106 o -12 3 4 25.597 14.620 5.357 110.281 o -12 3 5 115.376 104.791 6.502 32.178 o -12 3 6 12.486 10.872 3.709 216.998 o -12 3 7 27.813 12.774 3.438 154.484 o -12 3 8 89.617 72.311 5.420 44.504 o -12 3 9 29.721 22.416 3.808 127.740 o -12 3 10 31.332 15.306 4.170 124.410 o -12 3 11 123.652 109.053 7.272 29.009 o -12 4 1 126.394 116.135 6.479 29.682 o -12 4 2 133.814 130.930 10.330 21.406 o -12 4 3 285.547 328.735 10.400 10.724 o -12 4 4 0.607 -2.159 2.827 719.546 o -12 4 5 11.641 13.544 3.280 239.121 o -12 4 6 4.704 5.559 3.209 375.265 o -12 4 7 0.169 -7.078 3.310 549.655 o -12 4 8 86.312 82.161 5.718 42.993 o -12 4 9 113.697 109.876 6.556 31.918 o -12 4 10 1.000 6.967 3.864 329.753 o -12 5 1 80.911 91.169 7.907 35.692 o -12 5 2 26.677 20.521 3.615 141.856 o -12 5 3 89.717 83.607 5.672 42.019 o -12 5 4 2.062 2.050 4.416 277.731 o -12 5 5 0.599 -2.759 3.758 417.489 o -12 5 6 21.037 11.818 3.345 185.484 o -12 5 7 52.188 50.457 5.591 63.789 o -12 5 8 0.030 -10.025 3.099 633.118 o -12 5 9 136.224 124.093 8.048 25.209 o -12 5 10 132.708 125.069 9.405 23.222 o -12 6 1 88.933 84.968 7.001 37.667 o -12 6 2 10.925 3.806 3.659 258.102 o -12 6 3 53.468 49.031 6.424 57.472 o -12 6 4 166.216 149.531 9.472 19.649 o -12 6 5 102.889 112.355 7.806 30.516 o -12 6 6 16.865 3.909 3.365 231.046 o -12 6 7 275.535 285.838 10.200 11.604 o -12 6 8 146.019 150.493 10.020 20.277 o -12 6 9 22.741 19.056 6.384 91.230 o -12 7 1 144.222 122.006 9.169 22.740 o -12 7 2 226.312 205.125 9.829 14.779 o -12 7 3 11.755 7.343 3.848 224.716 o -12 7 4 267.241 247.711 10.217 12.375 o -12 7 5 462.549 517.025 19.216 5.046 o -12 7 6 26.490 47.896 6.181 76.775 o -12 7 7 122.046 104.778 10.048 23.944 o -12 7 8 198.124 157.387 11.463 15.636 o -12 8 1 19.936 9.645 4.408 155.032 o -12 8 2 436.052 430.625 13.417 6.668 o -12 8 3 285.390 293.022 11.579 10.659 o -12 8 4 19.231 17.694 4.994 128.200 o -12 8 5 286.704 325.659 15.534 8.695 o -12 8 6 51.615 62.973 8.137 44.990 o -12 8 7 0.088 -9.418 3.931 392.547 o -12 9 1 35.081 38.891 6.339 71.857 o -12 9 2 249.372 275.850 14.467 10.280 o -12 9 3 430.564 490.598 21.937 4.870 o -12 9 4 40.333 31.962 6.112 72.985 o -12 9 5 17.528 8.428 7.625 80.640 o -12 10 1 243.171 217.901 12.899 11.981 o -12 10 2 3.814 -4.853 6.579 131.598 o -12 10 3 94.842 77.798 8.321 33.092 o -11 -6 2 0.802 -13.990 4.154 340.692 o -11 -6 3 23.344 17.564 5.089 117.600 o -11 -6 4 1.911 -10.134 3.412 463.186 o -11 -6 5 37.648 29.591 4.637 94.680 o -11 -6 6 138.287 123.573 7.409 26.080 o -11 -6 7 131.912 139.088 8.039 24.896 o -11 -6 8 47.579 37.718 4.559 80.646 o -11 -6 9 369.322 407.357 12.493 7.829 o -11 -5 1 48.474 38.873 5.388 71.629 o -11 -5 2 20.022 9.213 4.850 140.747 o -11 -5 3 69.582 73.517 5.856 49.082 o -11 -5 4 296.901 324.057 10.150 10.608 o -11 -5 5 100.949 84.054 6.846 35.761 o -11 -5 6 266.858 238.053 13.671 10.715 o -11 -5 7 508.087 516.756 14.924 5.384 o -11 -5 8 105.717 102.486 6.294 34.552 o -11 -5 9 338.854 381.377 12.082 8.592 o -11 -5 10 88.300 80.253 6.107 41.372 o -11 -5 11 6.155 2.811 3.783 300.018 o -11 -4 1 325.893 332.508 17.711 7.363 o -11 -4 2 398.078 389.484 11.616 7.764 o -11 -4 3 1.050 3.141 3.380 451.540 o -11 -4 4 702.987 747.604 15.935 3.577 o -11 -4 5 596.661 617.744 18.170 4.148 o -11 -4 6 25.014 29.579 4.147 123.189 o -11 -4 7 395.286 415.819 14.325 7.006 o -11 -4 8 78.235 69.639 5.420 48.632 o -11 -4 9 9.045 14.677 4.515 182.063 o -11 -4 10 121.717 125.364 7.109 28.502 o -11 -4 11 39.390 42.179 4.689 85.034 o -11 -4 12 8.530 13.122 4.509 188.254 o -11 -3 1 395.740 390.483 11.692 7.772 o -11 -3 2 659.566 655.132 13.822 4.133 o -11 -3 3 133.601 127.523 7.674 25.936 o -11 -3 4 260.681 274.224 12.045 11.261 o -11 -3 5 359.328 356.269 9.963 9.053 o -11 -3 6 8.232 10.244 3.294 283.483 o -11 -3 7 91.532 96.414 6.721 36.783 o -11 -3 8 51.315 56.392 5.925 60.218 o -11 -3 9 4.184 -4.910 3.123 466.421 o -11 -3 10 2.983 -9.700 3.098 509.506 o -11 -3 11 72.517 94.977 6.443 42.383 o -11 -3 12 41.231 33.842 5.217 81.346 o -11 -3 13 0.781 -5.675 3.162 573.931 o -11 -2 1 9.193 6.148 4.474 204.593 o -11 -2 2 236.743 249.724 8.675 14.221 o -11 -2 3 196.377 198.659 7.741 17.989 o -11 -2 4 0.752 -3.011 2.879 686.053 o -11 -2 5 31.032 30.592 3.882 115.454 o -11 -2 6 5.723 -1.915 2.491 567.126 o -11 -2 7 1.869 1.299 2.723 647.857 o -11 -2 8 144.489 131.023 6.520 26.354 o -11 -2 9 83.912 82.213 4.907 46.538 o -11 -2 10 92.017 86.088 5.935 40.259 o -11 -2 11 92.610 76.210 6.137 40.687 o -11 -2 12 248.681 273.507 9.460 12.944 o -11 -2 13 27.094 27.546 4.437 115.329 o -11 -2 14 39.531 23.559 4.656 95.841 o -11 -1 1 326.200 320.761 9.068 10.346 o -11 -1 2 17.513 11.120 3.214 211.338 o -11 -1 3 22.916 24.636 3.649 145.799 o -11 -1 4 2.636 -6.247 2.100 938.338 o -11 -1 5 0.019 -6.023 2.483 986.064 o -11 -1 6 49.100 53.966 4.305 74.639 o -11 -1 7 182.828 187.150 7.168 19.705 o -11 -1 8 0.237 -3.086 2.831 742.862 o -11 -1 9 323.924 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571.060 600.733 18.438 4.289 o 10 -1 11 38.548 14.003 6.772 73.489 o 10 -1 12 76.035 71.184 7.900 38.804 o 10 0 0 473.152 478.646 12.360 6.231 o 10 0 1 382.252 372.842 8.965 8.746 o 10 0 2 107.549 99.608 5.924 35.385 o 10 0 3 87.264 93.524 8.142 33.579 o 10 0 4 1006.680 995.265 21.649 2.156 o 10 0 5 97.886 125.121 8.850 27.902 o 10 0 6 448.058 447.564 18.393 5.528 o 10 0 7 535.466 543.057 16.395 4.903 o 10 0 8 214.108 208.174 11.073 14.293 o 10 0 9 16.996 10.754 5.203 135.381 o 10 0 10 257.374 261.061 12.994 11.018 o 10 0 11 85.508 101.585 9.090 30.482 o 10 1 0 0.088 -1.675 2.544 931.592 o 10 1 1 367.238 374.041 8.815 9.037 o 10 1 2 642.066 605.332 12.690 4.453 o 10 1 3 52.375 46.121 6.534 57.904 o 10 1 4 436.657 429.251 13.977 6.559 o 10 1 5 456.692 509.174 18.827 5.174 o 10 1 6 3.517 -0.280 3.935 333.625 o 10 1 7 193.849 181.655 10.355 16.293 o 10 1 8 69.266 75.266 9.371 34.199 o 10 1 9 55.244 52.054 7.821 47.312 o 10 1 10 26.298 21.562 6.808 79.813 o 10 2 0 963.762 974.434 15.193 2.472 o 10 2 1 43.265 40.539 3.843 90.875 o 10 2 2 421.327 381.995 9.323 7.972 o 10 2 3 591.888 584.496 15.399 4.549 o 10 2 4 11.830 4.145 4.671 185.201 o 10 2 5 138.392 142.249 8.503 23.391 o 10 2 6 37.003 24.796 5.738 83.221 o 10 2 7 0.389 -11.367 3.688 438.122 o 10 2 8 3.908 -4.221 8.209 86.450 o 10 2 9 92.755 101.189 16.951 14.819 o 10 3 0 878.009 844.121 15.087 2.864 o 10 3 1 228.579 214.482 8.084 15.667 o 10 3 2 45.866 42.847 4.607 79.416 o 10 3 3 160.734 172.514 7.621 21.400 o 10 3 4 45.750 36.279 5.476 73.794 o 10 3 5 0.084 -10.788 4.272 332.640 o 10 3 6 8.171 -6.337 4.780 207.720 o 10 3 7 41.032 37.151 6.767 64.332 o 10 3 8 2.545 8.473 4.993 201.010 o 10 4 0 285.880 283.763 19.756 7.406 o 10 4 1 151.036 137.942 9.399 21.219 o 10 4 2 0.616 -1.479 3.844 399.334 o 10 4 3 3.548 -3.843 4.382 276.856 o 10 4 4 53.415 52.389 7.295 51.041 o 10 4 5 13.146 10.702 7.387 87.850 o 10 4 6 39.009 32.676 6.418 70.446 o 10 4 7 348.165 384.939 16.448 7.180 o 10 5 0 0.005 -3.841 4.090 364.206 o 10 5 1 41.214 27.015 5.695 78.916 o 10 5 2 160.750 154.301 11.587 17.338 o 10 5 3 33.728 30.257 6.556 73.581 o 10 5 4 195.107 187.367 12.155 14.543 o 10 5 5 260.887 264.692 14.054 10.362 o 10 6 0 94.355 93.488 8.132 32.431 o 10 6 1 14.049 7.517 4.802 163.400 o 10 6 2 255.568 241.205 13.614 10.967 o 10 6 3 100.362 101.827 9.797 26.807 o 10 7 0 269.679 257.156 12.695 10.925 o 10 7 1 20.201 22.133 7.584 73.667 o 11 -12 0 8.489 20.326 7.030 94.712 o 11 -12 1 3.370 0.783 6.910 120.145 o 11 -12 2 38.389 42.350 6.601 65.896 o 11 -12 3 143.511 162.674 15.965 13.287 o 11 -12 4 153.938 164.871 9.417 20.025 o 11 -12 5 32.987 50.339 7.724 56.758 o 11 -12 6 349.450 404.253 21.610 5.749 o 11 -12 7 113.509 105.653 9.266 26.314 o 11 -11 0 83.936 105.098 9.495 29.351 o 11 -11 1 351.472 370.416 13.891 7.958 o 11 -11 2 25.513 26.576 4.893 110.048 o 11 -11 3 290.077 335.836 12.622 9.680 o 11 -11 4 528.746 575.006 19.512 4.449 o 11 -11 5 12.552 15.225 5.285 138.260 o 11 -11 6 184.508 207.261 12.034 14.671 o 11 -11 7 261.901 243.810 16.117 9.535 o 11 -11 8 12.933 -3.905 4.963 174.439 o 11 -11 9 82.115 89.925 10.419 28.044 o 11 -10 0 1.823 1.117 5.065 221.268 o 11 -10 1 517.548 544.512 15.076 5.193 o 11 -10 2 314.366 313.652 11.924 9.685 o 11 -10 3 107.587 97.005 8.648 28.921 o 11 -10 4 543.138 630.986 18.018 4.403 o 11 -10 5 256.978 295.647 13.764 10.260 o 11 -10 6 25.701 22.470 5.433 102.587 o 11 -10 7 59.014 54.922 7.231 48.953 o 11 -10 8 77.585 54.201 8.775 36.848 o 11 -10 9 4.141 -5.699 7.329 106.931 o 11 -10 10 76.453 65.124 9.409 33.704 o 11 -9 0 214.380 187.925 9.564 15.861 o 11 -9 1 32.984 50.397 5.835 74.529 o 11 -9 2 427.113 502.921 15.623 5.986 o 11 -9 3 6.563 13.046 4.857 179.116 o 11 -9 4 46.849 46.005 6.485 61.080 o 11 -9 5 55.497 58.233 6.959 51.218 o 11 -9 6 84.835 97.936 8.348 32.999 o 11 -9 7 1.983 -6.958 4.680 259.656 o 11 -9 8 145.631 128.866 9.620 21.662 o 11 -9 9 54.512 49.360 8.178 45.924 o 11 -9 10 74.558 66.639 9.347 34.116 o 11 -9 11 427.001 434.935 19.194 5.580 o 11 -8 0 231.534 221.001 10.205 14.014 o 11 -8 1 59.001 59.755 7.876 44.696 o 11 -8 2 157.915 169.186 9.831 19.125 o 11 -8 3 11.755 11.299 4.662 170.950 o 11 -8 4 15.899 13.203 4.358 164.547 o 11 -8 5 16.555 9.326 4.643 158.051 o 11 -8 6 254.298 227.023 11.209 12.535 o 11 -8 7 147.127 119.631 9.063 22.757 o 11 -8 8 252.637 258.039 14.205 10.533 o 11 -8 9 623.790 649.308 20.305 3.747 o 11 -8 10 74.933 68.277 8.369 37.530 o 11 -8 11 258.334 314.581 15.195 9.397 o 11 -7 0 69.127 49.515 7.209 46.624 o 11 -7 1 195.283 196.212 11.326 15.063 o 11 -7 2 21.152 18.535 5.023 122.508 o 11 -7 3 243.415 287.028 12.017 11.553 o 11 -7 4 210.374 215.929 12.176 13.478 o 11 -7 5 24.024 14.324 4.929 123.249 o 11 -7 6 446.515 466.261 20.451 5.104 o 11 -7 7 1028.310 1043.130 25.990 1.940 o 11 -7 8 2.962 16.702 6.642 114.713 o 11 -7 9 804.566 760.810 21.843 2.849 o 11 -7 10 387.965 420.078 16.593 6.535 o 11 -7 11 0.362 -11.788 5.836 177.434 o 11 -7 12 356.900 364.736 39.334 2.870 o 11 -6 0 3.311 -0.417 3.656 381.183 o 11 -6 1 442.503 449.935 14.142 6.364 o 11 -6 2 101.160 95.627 8.072 31.357 o 11 -6 3 398.211 436.247 13.264 7.093 o 11 -6 4 1352.230 1381.640 24.442 1.395 o 11 -6 5 216.532 217.717 10.332 14.559 o 11 -6 6 328.159 332.528 14.477 8.388 o 11 -6 7 1382.460 1397.440 29.417 1.284 o 11 -6 8 315.696 324.400 14.710 8.559 o 11 -6 9 87.926 106.782 10.248 26.844 o 11 -6 10 207.487 194.426 12.668 13.566 o 11 -6 11 20.776 37.714 7.289 71.475 o 11 -6 12 58.123 61.201 14.002 22.551 o 11 -5 0 5.628 0.462 4.466 247.762 o 11 -5 1 691.016 677.768 19.560 3.494 o 11 -5 2 1007.150 985.577 21.080 2.183 o 11 -5 3 7.019 2.535 3.662 304.751 o 11 -5 4 955.112 1018.060 19.407 2.308 o 11 -5 5 476.929 530.124 17.090 5.241 o 11 -5 6 7.427 9.783 4.736 188.999 o 11 -5 7 121.059 111.882 10.794 22.359 o 11 -5 8 104.983 107.507 9.828 25.929 o 11 -5 9 11.463 -0.915 4.751 192.238 o 11 -5 10 102.984 104.297 10.097 25.717 o 11 -5 11 23.704 24.679 6.274 88.942 o 11 -4 0 786.461 775.736 21.321 2.909 o 11 -4 1 23.046 29.070 4.529 119.626 o 11 -4 2 600.917 630.291 10.960 4.771 o 11 -4 3 297.815 308.792 10.144 10.769 o 11 -4 4 80.120 68.418 6.090 45.418 o 11 -4 5 278.843 280.608 12.568 10.509 o 11 -4 6 49.757 50.188 6.979 55.025 o 11 -4 7 6.020 -2.283 6.166 142.387 o 11 -4 8 0.372 -10.554 3.561 469.624 o 11 -4 9 170.599 231.095 12.923 13.996 o 11 -4 10 18.538 -3.854 7.371 88.127 o 11 -4 11 88.402 89.486 10.736 26.538 o 11 -3 0 1086.310 1081.420 17.172 2.067 o 11 -3 1 118.280 109.112 7.589 29.076 o 11 -3 2 62.260 48.640 6.528 53.039 o 11 -3 3 170.350 194.461 10.929 16.566 o 11 -3 4 18.067 11.759 3.814 180.474 o 11 -3 5 88.917 78.215 6.631 39.673 o 11 -3 6 34.757 36.169 5.246 86.171 o 11 -3 7 71.625 68.762 6.618 45.693 o 11 -3 8 17.036 17.939 4.527 147.228 o 11 -3 9 279.565 294.563 12.178 10.512 o 11 -3 10 173.713 183.793 11.894 15.715 o 11 -3 11 195.236 204.425 13.213 13.384 o 11 -2 0 140.726 137.430 6.378 26.630 o 11 -2 1 106.530 89.659 6.424 35.286 o 11 -2 2 14.206 7.738 3.631 220.504 o 11 -2 3 1.752 -8.861 3.246 511.089 o 11 -2 4 69.052 79.949 6.893 43.589 o 11 -2 5 0.542 -4.155 3.414 504.443 o 11 -2 6 107.968 94.896 7.585 31.605 o 11 -2 7 294.069 297.741 12.751 9.926 o 11 -2 8 83.263 75.174 7.964 36.607 o 11 -2 9 249.394 238.545 14.146 10.851 o 11 -2 10 587.137 635.922 21.413 3.816 o 11 -1 0 11.101 4.412 3.334 280.546 o 11 -1 1 9.354 3.099 4.261 227.073 o 11 -1 2 185.599 173.744 8.928 18.280 o 11 -1 3 38.242 24.268 4.735 95.904 o 11 -1 4 265.338 263.022 12.157 11.229 o 11 -1 5 330.136 351.263 14.975 8.060 o 11 -1 6 2.667 -2.213 5.835 168.531 o 11 -1 7 362.671 323.018 15.966 7.514 o 11 -1 8 422.716 436.852 16.375 6.174 o 11 -1 9 6.693 8.269 5.347 163.807 o 11 -1 10 332.611 333.776 16.572 7.635 o 11 0 0 56.451 66.018 6.198 53.814 o 11 0 1 33.763 30.213 3.805 112.170 o 11 0 2 622.999 623.403 17.564 4.067 o 11 0 3 192.249 167.499 10.455 16.616 o 11 0 4 218.252 211.428 12.757 12.885 o 11 0 5 604.331 596.937 17.846 4.195 o 11 0 6 143.371 127.056 10.983 19.900 o 11 0 7 97.287 75.085 8.216 33.222 o 11 0 8 323.027 305.443 13.524 9.018 o 11 0 9 212.447 219.117 13.312 12.560 o 11 1 0 457.643 454.879 15.376 5.974 o 11 1 1 31.185 34.352 5.504 87.414 o 11 1 2 423.261 415.093 14.278 6.713 o 11 1 3 454.830 458.968 15.340 5.987 o 11 1 4 0.216 -1.969 3.905 395.288 o 11 1 5 246.533 232.724 11.624 12.439 o 11 1 6 313.004 326.240 13.063 9.178 o 11 1 7 30.356 24.178 7.078 72.061 o 11 1 8 0.175 -6.180 12.076 41.748 o 11 2 0 322.943 296.058 9.289 10.635 o 11 2 1 422.167 401.002 10.390 7.615 o 11 2 2 1.064 -1.041 3.353 504.397 o 11 2 3 247.826 226.841 9.152 13.957 o 11 2 4 108.183 104.854 8.046 29.729 o 11 2 5 5.035 -3.117 8.220 85.163 o 11 2 6 71.892 50.749 8.181 40.989 o 11 2 7 34.787 32.836 7.424 62.870 o 11 3 0 103.156 89.465 5.755 37.786 o 11 3 1 301.546 254.763 8.764 11.931 o 11 3 2 44.356 38.325 6.973 60.393 o 11 3 3 13.189 9.907 5.698 129.722 o 11 3 4 47.996 54.325 7.645 50.464 o 11 3 5 5.501 1.481 5.421 177.466 o 11 4 0 0.323 -3.944 6.286 153.217 o 11 4 1 43.308 14.177 7.889 58.948 o 11 4 2 24.061 33.786 7.323 70.158 o 11 4 3 59.975 69.376 8.649 39.512 o 11 4 4 8.374 17.207 6.689 104.507 o 11 5 0 8.447 -3.356 8.129 83.727 o 11 5 1 3.009 10.784 5.864 148.431 o 12 -11 1 148.574 115.970 28.069 6.262 o 12 -11 2 184.592 185.632 13.964 13.425 o 12 -11 3 0.281 1.108 15.512 25.257 o 12 -10 0 376.388 418.353 16.098 6.779 o 12 -10 1 1.795 -5.065 4.206 318.818 o 12 -10 2 489.395 543.862 15.769 5.301 o 12 -10 3 277.004 274.180 14.012 9.956 o 12 -10 4 6.926 3.221 4.719 209.744 o 12 -10 5 234.060 255.055 12.791 11.790 o 12 -10 6 240.414 247.237 16.235 9.834 o 12 -9 0 514.843 548.544 15.364 5.159 o 12 -9 1 156.339 148.689 9.413 20.424 o 12 -9 2 183.289 205.406 17.059 10.897 o 12 -9 3 319.906 334.362 16.182 7.922 o 12 -9 4 25.195 29.219 6.276 85.034 o 12 -9 5 4.259 -5.551 5.864 161.405 o 12 -9 6 23.171 3.609 5.823 112.932 o 12 -9 7 25.788 37.734 7.848 62.245 o 12 -8 0 222.869 228.642 10.583 13.940 o 12 -8 1 198.315 181.611 10.653 15.823 o 12 -8 2 8.341 4.077 4.644 204.325 o 12 -8 3 81.191 86.944 8.223 34.991 o 12 -8 4 10.779 18.932 5.367 135.382 o 12 -8 5 4.033 -3.378 4.348 275.773 o 12 -8 6 2.829 6.191 5.101 198.397 o 12 -8 7 164.158 184.214 13.061 14.973 o 12 -8 8 99.384 105.177 10.637 24.856 o 12 -7 0 1.632 -6.509 3.646 417.792 o 12 -7 1 10.562 13.728 5.016 155.914 o 12 -7 2 0.463 -7.629 3.745 423.544 o 12 -7 3 29.611 30.469 5.574 90.214 o 12 -7 4 129.688 128.113 9.486 23.218 o 12 -7 5 146.451 126.892 10.264 20.730 o 12 -7 6 1.727 3.606 6.915 120.396 o 12 -7 7 350.225 314.800 14.205 8.280 o 12 -7 8 465.692 483.849 17.762 5.377 o 12 -6 0 19.025 2.666 4.141 182.186 o 12 -6 1 3.978 -2.241 3.866 336.800 o 12 -6 2 163.900 161.766 10.274 18.470 o 12 -6 3 134.718 111.913 8.151 25.835 o 12 -6 4 124.629 122.980 8.854 25.041 o 12 -6 5 463.983 442.146 16.349 5.798 o 12 -6 6 194.637 213.493 12.219 14.029 o 12 -6 7 86.089 75.302 8.147 35.416 o 12 -6 8 422.137 411.305 16.411 6.289 o 12 -6 9 129.694 123.915 10.725 21.350 o 12 -5 0 259.397 261.304 14.890 10.015 o 12 -5 1 48.922 46.181 5.840 65.046 o 12 -5 2 317.840 336.078 11.586 9.520 o 12 -5 3 644.016 666.575 13.780 4.187 o 12 -5 4 0.482 -4.197 4.446 302.426 o 12 -5 5 393.650 394.482 15.960 6.756 o 12 -5 6 473.379 472.435 16.849 5.517 o 12 -5 7 24.383 11.560 5.524 111.174 o 12 -5 8 88.106 79.213 9.965 29.207 o 12 -5 9 251.941 294.905 57.800 1.630 o 12 -4 0 652.776 588.395 12.690 4.440 o 12 -4 1 323.726 313.848 10.062 10.150 o 12 -4 2 75.137 91.511 5.874 44.294 o 12 -4 3 529.041 572.968 17.989 4.647 o 12 -4 4 136.291 135.748 11.695 19.065 o 12 -4 5 58.618 41.085 7.172 51.987 o 12 -4 6 120.480 116.566 9.627 24.334 o 12 -4 7 35.242 30.659 7.570 61.817 o 12 -4 8 14.173 9.413 8.809 65.737 o 12 -3 0 72.997 65.538 4.921 53.658 o 12 -3 1 379.241 392.863 20.553 5.812 o 12 -3 2 32.829 19.483 5.660 91.493 o 12 -3 3 37.615 29.776 5.419 84.317 o 12 -3 4 63.052 61.499 6.376 51.074 o 12 -3 5 2.872 -0.810 4.395 282.207 o 12 -3 6 5.606 4.237 6.992 110.750 o 12 -3 7 31.351 15.703 6.221 86.468 o 12 -3 8 239.328 245.827 13.453 11.390 o 12 -2 0 113.692 103.259 6.494 32.601 o 12 -2 1 42.732 37.754 5.208 78.366 o 12 -2 2 31.513 24.980 4.862 102.573 o 12 -2 3 3.682 -4.960 4.652 248.125 o 12 -2 4 26.510 23.134 7.510 69.861 o 12 -2 5 98.986 96.272 7.662 32.740 o 12 -2 6 106.235 118.743 8.681 27.652 o 12 -2 7 0.341 -2.664 4.020 370.862 o 12 -1 0 43.288 40.192 4.866 80.352 o 12 -1 1 8.352 -1.236 5.033 190.643 o 12 -1 2 46.606 47.387 5.944 65.219 o 12 -1 3 60.983 46.900 5.910 57.859 o 12 -1 4 0.703 -10.630 3.434 493.506 o 12 -1 5 158.232 148.532 9.637 20.013 o 12 -1 6 352.561 392.314 13.599 7.873 o 12 0 0 48.133 32.131 5.523 73.106 o 12 0 1 77.616 76.602 8.969 34.047 o 12 0 2 35.891 28.741 5.091 91.038 o 12 0 3 353.311 347.017 13.706 8.153 o 12 0 4 74.411 69.718 7.591 40.589 o 12 0 5 12.523 7.376 7.460 88.835 o 12 1 0 138.730 104.785 7.301 27.304 o 12 1 1 413.783 404.781 12.362 7.291 o 12 1 2 111.171 154.416 14.422 16.243 o 12 1 3 258.338 285.137 24.307 6.152 o 12 1 4 362.799 392.895 16.408 6.983 o 12 2 0 14.303 6.319 4.152 195.361 o 12 2 1 543.284 492.623 13.791 5.364 o 12 2 2 371.001 390.498 20.187 5.971 o 12 2 3 0.036 1.873 10.381 56.151 o 12 3 0 126.170 140.706 10.624 21.151 o 12 3 1 61.932 63.263 15.706 18.743 o 13 -8 0 4.765 10.031 7.364 98.280 o 13 -8 1 111.581 142.689 18.281 12.286 o 13 -7 0 9.463 8.526 5.771 137.729 o 13 -7 1 6.497 1.807 5.582 164.529 o 13 -7 2 1.084 -2.421 5.109 226.023 o 13 -7 3 2.827 2.292 4.845 228.950 o 13 -6 0 0.240 1.868 4.955 239.155 o 13 -6 1 1.775 -5.124 5.320 205.156 o 13 -6 2 3.966 3.609 5.138 196.724 o 13 -6 3 262.288 300.880 16.907 8.706 o 13 -6 4 79.403 80.871 8.624 34.528 o 13 -5 0 38.528 29.106 5.255 85.807 o 13 -5 1 231.044 183.433 11.581 13.757 o 13 -5 2 19.069 19.706 5.969 103.444 o 13 -5 3 286.091 332.695 15.751 8.567 o 13 -5 4 424.669 427.044 16.151 6.247 o 13 -4 0 17.049 9.303 4.450 163.865 o 13 -4 1 621.170 627.317 21.800 3.659 o 13 -4 2 246.998 225.846 15.989 10.040 o 13 -4 3 22.067 23.808 5.705 101.597 o 13 -4 4 203.203 209.841 16.484 10.800 o 13 -3 0 156.124 178.735 15.273 13.295 o 13 -3 1 143.595 144.840 11.614 18.484 o 13 -3 2 339.366 347.907 14.524 8.097 o 13 -3 3 11.169 7.437 5.478 145.481 o 13 -2 0 299.726 247.834 16.128 8.863 o 13 -2 1 39.777 35.642 5.652 76.969 o 13 -2 2 10.974 -3.053 6.166 130.332 o 13 -1 0 63.570 45.779 6.091 55.761 o 13 -1 1 40.364 22.007 5.274 87.346 o ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_disorder_group C1 C 1.1562(2) 0.4974(2) 0.69327(15) 0.0557(6) Uani 1.000000 . U . H1 H 1.1626(2) 0.5140(2) 0.64696(15) 0.0668(7) Uiso 1.000000 R . . C2 C 1.2670(3) 0.5242(3) 0.7462(2) 0.0910(11) Uani 1.000000 . U . H2 H 1.3481(3) 0.5589(3) 0.7362(2) 0.1092(14) Uiso 1.000000 R . . C3 C 1.2572(3) 0.4991(4) 0.8148(2) 0.1141(16) Uani 1.000000 . U . H3 H 1.3321(3) 0.5180(4) 0.8514(2) 0.1369(19) Uiso 1.000000 R . . C4 C 1.1390(2) 0.4469(3) 0.82953(17) 0.0830(10) Uani 1.000000 . U . H4 H 1.1318(2) 0.4290(3) 0.87530(17) 0.0996(13) Uiso 1.000000 R . . C5 C 1.02994(19) 0.42164(19) 0.77333(12) 0.0447(5) Uani 1.000000 . U . C6 C 0.7444(2) 0.3095(2) 0.83536(17) 0.0633(7) Uani 1.000000 . U . H6 H 0.6852(2) 0.3131(2) 0.79630(17) 0.0760(8) Uiso 1.000000 R . . C7 C 0.6933(2) 0.2672(2) 0.89558(17) 0.0649(7) Uani 1.000000 . U . C8 C 0.7796(3) 0.2547(3) 0.95234(19) 0.0824(10) Uani 1.000000 . U . H8 H 0.8700(3) 0.2742(3) 0.95098(19) 0.0989(11) Uiso 1.000000 R . . C9 C 0.7349(4) 0.2145(3) 1.0098(2) 0.0960(12) Uani 1.000000 . U . H9 H 0.7952(4) 0.2073(3) 1.0466(2) 0.1152(14) Uiso 1.000000 R . . C10 C 0.6005(4) 0.1842(3) 1.01403(19) 0.0834(9) Uani 1.000000 . U . C11 C 0.5519(5) 0.1414(3) 1.0736(2) 0.1146(15) Uani 1.000000 . U . H11 H 0.6110(5) 0.1336(3) 1.1107(2) 0.1375(18) Uiso 1.000000 R . . C12 C 0.4220(5) 0.1128(3) 1.0762(2) 0.1193(16) Uani 1.000000 . U . H12 H 0.3929(5) 0.0843(3) 1.1149(2) 0.1431(19) Uiso 1.000000 R . . C13 C 0.3280(4) 0.1242(3) 1.0227(2) 0.0948(13) Uani 1.000000 . U . C14 C 0.1918(5) 0.1005(3) 1.0253(3) 0.1243(19) Uani 1.000000 . U . H14 H 0.1597(5) 0.0734(3) 1.0641(3) 0.149(2) Uiso 1.000000 R . . C15 C 0.1046(4) 0.1156(3) 0.9734(3) 0.1229(19) Uani 1.000000 . U . H15 H 0.0152(4) 0.0998(3) 0.9782(3) 0.147(2) Uiso 1.000000 R . . C16 C 0.1458(3) 0.1538(3) 0.9138(3) 0.1132(16) Uani 1.000000 . U . H16 H 0.0851(3) 0.1636(3) 0.8786(3) 0.1358(19) Uiso 1.000000 R . . C17 C 0.2819(3) 0.1778(2) 0.9070(2) 0.0876(11) Uani 1.000000 . U . C18 C 0.3290(3) 0.2188(3) 0.8461(2) 0.0919(10) Uani 1.000000 . U . H18 H 0.2690(3) 0.2259(3) 0.8091(2) 0.1103(13) Uiso 1.000000 R . . C19 C 0.4598(3) 0.2470(3) 0.8420(2) 0.0795(9) Uani 1.000000 . U . H19 H 0.4881(3) 0.2735(3) 0.8021(2) 0.0953(10) Uiso 1.000000 R . . C20 C 0.5559(3) 0.2373(2) 0.89745(17) 0.0652(7) Uani 1.000000 . U . C21 C 0.5106(3) 0.1948(2) 0.95818(18) 0.0696(8) Uani 1.000000 . U . C22 C 0.3733(3) 0.1653(2) 0.9615(2) 0.0780(9) Uani 1.000000 . U . C24 C 0.66562(19) 0.60279(16) 0.69229(11) 0.0383(4) Uani 1.000000 . U . C25 C 0.6459(3) 0.7020(2) 0.73076(15) 0.0594(6) Uani 1.000000 . U . H25 H 0.7015(3) 0.7463(2) 0.77634(15) 0.0713(7) Uiso 1.000000 R . . C26 C 0.5441(3) 0.7363(2) 0.70210(17) 0.0678(7) Uani 1.000000 . U . H26 H 0.5319(3) 0.8035(2) 0.72831(17) 0.0814(9) Uiso 1.000000 R . . C27 C 0.4611(2) 0.6713(2) 0.63501(15) 0.0553(6) Uani 1.000000 . U . H27 H 0.3932(2) 0.6945(2) 0.61559(15) 0.0664(7) Uiso 1.000000 R . . C28 C 0.4785(2) 0.5729(2) 0.59702(13) 0.0485(5) Uani 1.000000 . U . H28 H 0.4216(2) 0.5285(2) 0.55199(13) 0.0582(6) Uiso 1.000000 R . . C29 C 0.5809(2) 0.53813(18) 0.62507(12) 0.0439(5) Uani 1.000000 . U . H29 H 0.5925(2) 0.47093(18) 0.59845(12) 0.0527(6) Uiso 1.000000 R . . C30 C 0.7679(2) 0.57054(18) 0.83168(12) 0.0430(4) Uani 1.000000 . U . C31 C 0.8695(2) 0.58464(19) 0.89023(12) 0.0493(5) Uani 1.000000 . U . H31 H 0.9564(2) 0.59707(19) 0.88003(12) 0.0591(6) Uiso 1.000000 R . . C32 C 0.8426(3) 0.5804(2) 0.96320(14) 0.0638(7) Uani 1.000000 . U . H32 H 0.9113(3) 0.5896(2) 1.00179(14) 0.0766(8) Uiso 1.000000 R . . C33 C 0.7152(3) 0.5625(3) 0.97886(15) 0.0781(9) Uani 1.000000 . U . H33 H 0.6974(3) 0.5605(3) 1.02829(15) 0.0937(11) Uiso 1.000000 R . . C34 C 0.6134(3) 0.5475(3) 0.92166(16) 0.0814(10) Uani 1.000000 . U . H34 H 0.5268(3) 0.5345(3) 0.93229(16) 0.0977(12) Uiso 1.000000 R . . C35 C 0.6394(2) 0.5516(2) 0.84849(14) 0.0625(7) Uani 1.000000 . U . H35 H 0.5701(2) 0.5416(2) 0.81013(14) 0.0750(8) Uiso 1.000000 R . . C36 C 0.9425(2) 0.67443(16) 0.74379(12) 0.0407(4) Uani 1.000000 . U . C37 C 0.9816(3) 0.76188(19) 0.81181(14) 0.0550(6) Uani 1.000000 . U . H37 H 0.9354(3) 0.76380(19) 0.85431(14) 0.0660(7) Uiso 1.000000 R . . C38 C 1.0883(3) 0.8460(2) 0.81698(17) 0.0711(8) Uani 1.000000 . U . H38 H 1.1136(3) 0.9043(2) 0.86283(17) 0.0853(9) Uiso 1.000000 R . . C39 C 1.1575(3) 0.8440(2) 0.75464(19) 0.0752(8) Uani 1.000000 . U . H39 H 1.2305(3) 0.9002(2) 0.75870(19) 0.0902(10) Uiso 1.000000 R . . C40 C 1.1188(3) 0.7589(2) 0.68626(17) 0.0647(7) Uani 1.000000 . U . H40 H 1.1647(3) 0.7583(2) 0.64374(17) 0.0776(8) Uiso 1.000000 R . . C41 C 1.0114(2) 0.67396(19) 0.68062(14) 0.0486(5) Uani 1.000000 . U . H41 H 0.9855(2) 0.61652(19) 0.63429(14) 0.0584(6) Uiso 1.000000 R . . Cl1 Cl 0.82500(17) 0.42434(11) 0.54147(6) 0.0554(3) Uani 0.750000 D U 3 N1 N 1.03936(16) 0.44804(14) 0.70656(10) 0.0398(4) Uani 1.000000 . U . N2 N 0.90262(16) 0.37428(15) 0.77242(10) 0.0425(4) Uani 1.000000 . U . N3 N 0.86902(17) 0.34223(16) 0.83414(11) 0.0505(5) Uani 1.000000 . U . P1 P 0.80121(5) 0.56010(4) 0.73220(3) 0.03393(11) Uani 1.000000 . U . P2 P 0.86941(5) 0.21777(4) 0.59442(3) 0.04081(12) Uani 1.000000 . U . Ru1 Ru 0.832013(14) 0.387487(12) 0.664824(9) 0.03479(6) Uani 1.000000 D U . C42 C 0.7573(4) 0.1400(3) 0.49858(19) 0.0444(14) Uani 0.600000 . U 1 C43 C 0.6263(4) 0.1438(3) 0.4890(3) 0.0603(17) Uani 0.600000 G U 1 H43 H 0.5942(4) 0.1897(3) 0.5284(3) 0.072(2) Uiso 0.600000 R . 1 C44 C 0.5433(3) 0.0793(4) 0.4204(3) 0.070(2) Uani 0.600000 G U 1 H44 H 0.4557(3) 0.0818(4) 0.4139(3) 0.084(2) Uiso 0.600000 R . 1 C45 C 0.5914(3) 0.0108(4) 0.3614(2) 0.0721(19) Uani 0.600000 G U 1 H45 H 0.5359(3) -0.0324(4) 0.3155(2) 0.087(2) Uiso 0.600000 R . 1 C47 C 0.7224(4) 0.0069(3) 0.37106(17) 0.0673(12) Uani 0.600000 G U 1 H47 H 0.7546(4) -0.0389(3) 0.33162(17) 0.0808(14) Uiso 0.600000 R . 1 C46 C 0.8054(3) 0.0715(3) 0.43964(19) 0.0601(10) Uani 0.600000 G U 1 H46 H 0.8930(3) 0.0689(3) 0.44608(19) 0.0721(12) Uiso 0.600000 R . 1 C48 C 1.0367(3) 0.2340(4) 0.5577(3) 0.044(15) Uani 0.400000 . U 2 C64 C 1.1533(4) 0.2777(4) 0.6099(3) 0.0534(15) Uani 0.400000 G U 2 H64 H 1.1505(4) 0.2940(4) 0.6635(3) 0.0640(18) Uiso 0.400000 R . 2 C63 C 1.2739(3) 0.2968(4) 0.5820(4) 0.072(3) Uani 0.400000 G U 2 H63 H 1.3518(3) 0.3260(4) 0.6169(4) 0.086(4) Uiso 0.400000 R . 2 C62 C 1.2779(4) 0.2723(4) 0.5019(4) 0.074(5) Uani 0.400000 G U 2 H62 H 1.3586(4) 0.2851(4) 0.4832(4) 0.089(6) Uiso 0.400000 R . 2 C61 C 1.1614(6) 0.2287(5) 0.4497(3) 0.085(3) Uani 0.400000 G U 2 H61 H 1.1641(6) 0.2123(5) 0.3961(3) 0.102(3) Uiso 0.400000 R . 2 C60 C 1.0408(4) 0.2095(4) 0.4776(3) 0.0589(16) Uani 0.400000 G U 2 H60 H 0.9629(4) 0.1803(4) 0.4426(3) 0.071(2) Uiso 0.400000 R . 2 C54 C 0.8829(6) 0.1309(5) 0.6542(4) 0.0382(19) Uani 0.400000 . U 2 C55 C 0.7712(6) 0.1052(8) 0.6891(6) 0.047(2) Uani 0.400000 G U 2 H55 H 0.6997(6) 0.1331(8) 0.6820(6) 0.056(2) Uiso 0.400000 R . 2 C58 C 0.7664(6) 0.0377(8) 0.7346(5) 0.067(3) Uani 0.400000 G U 2 H58 H 0.6916(6) 0.0205(8) 0.7579(5) 0.081(4) Uiso 0.400000 R . 2 C56 C 0.8733(7) -0.0040(6) 0.7451(4) 0.074(3) Uani 0.400000 G U 2 H56 H 0.8700(7) -0.0491(6) 0.7756(4) 0.088(3) Uiso 0.400000 R . 2 C57 C 0.9850(6) 0.0218(5) 0.7102(4) 0.081(2) Uani 0.400000 G U 2 H57 H 1.0565(6) -0.0061(5) 0.7173(4) 0.097(3) Uiso 0.400000 R . 2 C59 C 0.9898(5) 0.0892(4) 0.6647(3) 0.0625(17) Uani 0.400000 G U 2 H59 H 1.0645(5) 0.1064(4) 0.6414(3) 0.075(2) Uiso 0.400000 R . 2 C70 C 0.8394(8) 0.1146(5) 0.6468(5) 0.051(3) Uani 0.400000 . U 1 C71 C 0.8975(7) 0.0295(5) 0.6226(4) 0.081(2) Uani 0.400000 G U 1 H71 H 0.9434(7) 0.0224(5) 0.5796(4) 0.097(3) Uiso 0.400000 R . 1 C72 C 0.8870(7) -0.0450(5) 0.6625(4) 0.096(3) Uani 0.400000 G U 1 H72 H 0.9259(7) -0.1020(5) 0.6463(4) 0.115(4) Uiso 0.400000 R . 1 C73 C 0.8185(7) -0.0344(7) 0.7266(4) 0.080(3) Uani 0.400000 G U 1 H73 H 0.8115(7) -0.0843(7) 0.7534(4) 0.096(4) Uiso 0.400000 R . 1 CXE C 0.7604(8) 0.0508(8) 0.7509(4) 0.074(4) Uani 0.400000 G U 1 HXE H 0.7145(8) 0.0579(8) 0.7938(4) 0.089(4) Uiso 0.400000 R . 1 CXF C 0.7709(9) 0.1253(7) 0.7110(5) 0.052(3) Uani 0.400000 G U 1 HXF H 0.7320(9) 0.1822(7) 0.7272(5) 0.063(3) Uiso 0.400000 R . 1 C74 C 0.7592(5) 0.1308(3) 0.5117(3) 0.039(2) Uani 0.400000 . U 2 C67 C 0.7666(4) 0.0252(3) 0.4804(3) 0.0511(13) Uani 0.400000 G U 2 H67 H 0.8302(4) 0.0009(3) 0.5031(3) 0.0613(16) Uiso 0.400000 R . 2 C66 C 0.6789(5) -0.0442(3) 0.4151(3) 0.0639(17) Uani 0.400000 G U 2 H66 H 0.6839(5) -0.1149(3) 0.3941(3) 0.077(2) Uiso 0.400000 R . 2 C65 C 0.5839(5) -0.0080(5) 0.3811(4) 0.066(3) Uani 0.400000 G U 2 H65 H 0.5252(5) -0.0544(5) 0.3374(4) 0.079(3) Uiso 0.400000 R . 2 C69 C 0.5765(5) 0.0977(5) 0.4125(5) 0.054(2) Uani 0.400000 G U 2 H69 H 0.5129(5) 0.1220(5) 0.3897(5) 0.065(2) Uiso 0.400000 R . 2 C68 C 0.6642(6) 0.1671(3) 0.4777(4) 0.0418(16) Uani 0.400000 G U 2 H68 H 0.6592(6) 0.2378(3) 0.4987(4) 0.050(2) Uiso 0.400000 R . 2 C75 C 1.0240(4) 0.2365(6) 0.5722(4) 0.043(4) Uani 0.400000 . U 1 C50 C 1.0535(5) 0.2749(6) 0.5102(4) 0.0533(19) Uani 0.400000 G U 1 H50 H 0.9865(5) 0.2844(6) 0.4788(4) 0.064(2) Uiso 0.400000 R . 1 C51 C 1.1832(6) 0.2992(6) 0.4951(4) 0.072(3) Uani 0.400000 G U 1 H51 H 1.2029(6) 0.3249(6) 0.4536(4) 0.087(3) Uiso 0.400000 R . 1 C49 C 1.2833(4) 0.2851(7) 0.5420(4) 0.063(3) Uani 0.400000 G U 1 H49 H 1.3701(4) 0.3013(7) 0.5319(4) 0.075(4) Uiso 0.400000 R . 1 C53 C 1.2538(4) 0.2467(6) 0.6039(4) 0.075(2) Uani 0.400000 G U 1 H53 H 1.3208(4) 0.2372(6) 0.6353(4) 0.090(3) Uiso 0.400000 R . 1 C52 C 1.1242(5) 0.2224(5) 0.6190(3) 0.0620(18) Uani 0.400000 G U 1 H52 H 1.1044(5) 0.1967(5) 0.6605(3) 0.074(2) Uiso 0.400000 R . 1 C77 C 0.7743(9) 0.0092(7) 0.6010(5) 0.054(3) Uiso 0.200000 . U 3 H77 H 0.7161(9) -0.0049(7) 0.5559(5) 0.065(3) Uiso 0.200000 R . 3 C78 C 0.7710(9) -0.0693(6) 0.6367(6) 0.069(4) Uiso 0.200000 G U 3 H78 H 0.7105(9) -0.1359(6) 0.6156(6) 0.082(4) Uiso 0.200000 R . 3 C79 C 0.8580(11) -0.0481(8) 0.7041(6) 0.071(6) Uiso 0.200000 G U 3 H79 H 0.8558(11) -0.1007(8) 0.7280(6) 0.085(7) Uiso 0.200000 R . 3 CXD C 0.9484(10) 0.0515(9) 0.7357(5) 0.073(5) Uiso 0.200000 G U 3 HXD H 1.0066(10) 0.0656(9) 0.7807(5) 0.088(6) Uiso 0.200000 R . 3 C1A C 0.9517(9) 0.1300(7) 0.6999(6) 0.057(3) Uiso 0.200000 G U 3 H1A H 1.0122(9) 0.1966(7) 0.7210(6) 0.068(4) Uiso 0.200000 R . 3 C1B C 0.8647(10) 0.1088(6) 0.6325(6) 0.041(5) Uiso 0.200000 G U 3 O2 O 0.8153(14) 0.4296(12) 0.5128(5) 0.059(3) Uani 0.250000 D U 4 C76 C 0.8154(13) 0.4121(12) 0.5715(4) 0.043(3) Uani 0.250000 D U 4 Cl2 Cl 0.59889(18) 0.3143(3) 0.6631(2) 0.0501(7) Uani 0.250000 D U 4 O1 O 0.5470(2) 0.2893(4) 0.6578(3) 0.0801(12) Uani 0.750000 D U 3 C23 C 0.65667(19) 0.3264(4) 0.6568(3) 0.0499(10) Uani 0.750000 D U 3 C80 C 1.2543(9) 0.1998(8) 0.5504(7) 0.063(3) Uiso 0.200000 . U 3 H80 H 1.3153(9) 0.1644(8) 0.5623(7) 0.075(4) Uiso 0.200000 R . 3 C81 C 1.1295(9) 0.1799(7) 0.5732(6) 0.051(3) Uiso 0.200000 G U 3 H81 H 1.1070(9) 0.1312(7) 0.6003(6) 0.062(3) Uiso 0.200000 R . 3 C82 C 1.0384(8) 0.2328(9) 0.5553(7) 0.04(2) Uiso 0.200000 G U 3 C1C C 1.0722(10) 0.3056(9) 0.5147(8) 0.036(4) Uiso 0.200000 G U 3 H1C H 1.0112(10) 0.3410(9) 0.5028(8) 0.043(4) Uiso 0.200000 R . 3 C1D C 1.1970(12) 0.3256(9) 0.4919(7) 0.040(3) Uiso 0.200000 G U 3 H1D H 1.2195(12) 0.3743(9) 0.4647(7) 0.048(4) Uiso 0.200000 R . 3 C1E C 1.2881(9) 0.2727(10) 0.5098(7) 0.079(11) Uiso 0.200000 G U 3 H1E H 1.3716(9) 0.2860(10) 0.4945(7) 0.095(14) Uiso 0.200000 R . 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.0419(11) 0.0806(17) 0.0594(14) 0.0143(11) 0.0140(10) 0.0437(13) C2 0.0336(12) 0.157(3) 0.099(2) 0.0012(16) 0.0070(13) 0.083(2) C3 0.0329(13) 0.221(5) 0.099(2) -0.0106(19) -0.0150(14) 0.105(3) C4 0.0358(12) 0.159(3) 0.0707(17) 0.0035(15) -0.0042(11) 0.079(2) C5 0.0315(9) 0.0640(14) 0.0450(11) 0.0091(9) 0.0010(8) 0.0299(10) C6 0.0377(11) 0.0884(19) 0.0799(17) 0.0057(12) 0.0037(11) 0.0591(16) C7 0.0477(13) 0.0809(18) 0.0759(17) 0.0020(12) 0.0077(12) 0.0504(15) C8 0.0597(16) 0.115(3) 0.088(2) 0.0027(16) 0.0054(15) 0.070(2) C9 0.086(2) 0.130(3) 0.083(2) 0.001(2) 0.0026(18) 0.072(2) C10 0.091(2) 0.092(2) 0.0684(18) 0.0000(18) 0.0213(17) 0.0427(17) C11 0.134(4) 0.131(3) 0.077(2) -0.006(3) 0.031(2) 0.057(2) C12 0.150(4) 0.113(3) 0.084(3) -0.011(3) 0.059(3) 0.040(2) C13 0.103(3) 0.0656(19) 0.091(2) -0.0125(18) 0.060(2) 0.0046(17) C14 0.127(4) 0.078(2) 0.132(4) -0.018(3) 0.092(3) -0.001(3) C15 0.084(3) 0.079(2) 0.168(5) -0.014(2) 0.079(3) -0.001(3) C16 0.065(2) 0.077(2) 0.172(4) -0.0033(17) 0.049(2) 0.012(2) C17 0.0589(17) 0.0637(18) 0.121(3) -0.0055(14) 0.0410(19) 0.0116(18) C18 0.0485(15) 0.100(2) 0.126(3) 0.0064(16) 0.0154(17) 0.043(2) C19 0.0460(14) 0.097(2) 0.100(2) 0.0026(14) 0.0139(14) 0.0489(19) C20 0.0499(13) 0.0735(17) 0.0764(17) 0.0013(12) 0.0166(12) 0.0393(14) C21 0.0696(17) 0.0602(16) 0.0727(18) -0.0026(13) 0.0285(14) 0.0224(14) C22 0.0752(19) 0.0559(16) 0.086(2) -0.0079(14) 0.0400(17) 0.0095(15) C24 0.0364(9) 0.0465(11) 0.0374(10) 0.0150(8) 0.0031(8) 0.0186(8) C25 0.0624(15) 0.0515(13) 0.0578(14) 0.0222(12) -0.0127(11) 0.0067(11) C26 0.0714(17) 0.0563(15) 0.0784(18) 0.0340(13) -0.0038(14) 0.0150(13) C27 0.0467(12) 0.0693(16) 0.0638(15) 0.0261(11) 0.0060(11) 0.0336(13) C28 0.0436(11) 0.0658(14) 0.0411(11) 0.0192(10) -0.0003(9) 0.0220(10) C29 0.0439(11) 0.0531(12) 0.0386(10) 0.0188(9) 0.0019(8) 0.0162(9) C30 0.0400(10) 0.0535(12) 0.0352(10) 0.0080(9) 0.0032(8) 0.0174(9) C31 0.0415(11) 0.0659(14) 0.0406(11) 0.0080(10) 0.0010(9) 0.0227(10) C32 0.0572(14) 0.0905(19) 0.0402(12) 0.0047(13) -0.0057(10) 0.0287(13) C33 0.0646(17) 0.127(3) 0.0428(13) 0.0073(17) 0.0080(12) 0.0400(16) C34 0.0474(14) 0.145(3) 0.0567(16) 0.0122(16) 0.0145(12) 0.0478(18) C35 0.0411(12) 0.103(2) 0.0467(13) 0.0118(13) 0.0028(10) 0.0335(13) C36 0.0386(10) 0.0426(11) 0.0423(10) 0.0076(8) -0.0015(8) 0.0191(9) C37 0.0631(15) 0.0479(13) 0.0485(13) 0.0058(11) -0.0026(11) 0.0158(10) C38 0.0818(19) 0.0496(14) 0.0662(17) -0.0081(13) -0.0183(14) 0.0199(13) C39 0.0650(17) 0.0658(17) 0.090(2) -0.0127(13) -0.0148(15) 0.0455(16) C40 0.0553(14) 0.0755(18) 0.0748(18) 0.0075(13) 0.0108(13) 0.0477(15) C41 0.0467(12) 0.0538(13) 0.0502(12) 0.0097(10) 0.0054(9) 0.0264(10) Cl1 0.0836(7) 0.0526(6) 0.0388(10) 0.0282(5) 0.0056(8) 0.0201(7) N1 0.0335(8) 0.0517(10) 0.0400(9) 0.0108(7) 0.0026(7) 0.0235(8) N2 0.0319(8) 0.0558(10) 0.0460(9) 0.0058(7) -0.0009(7) 0.0307(8) N3 0.0390(9) 0.0640(12) 0.0572(11) 0.0057(8) 0.0027(8) 0.0386(10) P1 0.0312(2) 0.0406(3) 0.0312(2) 0.00853(19) 0.00002(18) 0.0148(2) P2 0.0411(3) 0.0366(3) 0.0476(3) 0.0106(2) -0.0022(2) 0.0189(2) Ru1 0.03139(8) 0.03840(9) 0.03713(9) 0.00751(6) -0.00263(6) 0.01837(7) C42 0.047(3) 0.035(3) 0.046(2) 0.004(2) -0.005(2) 0.012(2) C43 0.044(3) 0.067(3) 0.062(3) 0.013(3) -0.003(2) 0.012(3) C44 0.044(3) 0.082(4) 0.064(4) -0.001(3) -0.013(2) 0.012(3) C45 0.068(4) 0.066(4) 0.068(4) 0.003(3) -0.019(3) 0.016(3) C47 0.079(3) 0.053(2) 0.059(3) 0.017(2) -0.003(2) 0.004(2) C46 0.052(2) 0.057(2) 0.067(3) 0.0163(19) -0.005(2) 0.014(2) C48 0.026(11) 0.040(15) 0.07(2) 0.011(5) 0.004(5) 0.025(9) C64 0.038(3) 0.048(3) 0.076(4) 0.018(3) 0.003(3) 0.017(3) C63 0.034(4) 0.060(5) 0.123(10) 0.017(3) 0.008(4) 0.029(6) C62 0.042(5) 0.063(6) 0.135(12) 0.016(4) 0.040(5) 0.049(6) C61 0.086(6) 0.085(6) 0.104(7) 0.029(5) 0.051(5) 0.048(5) C60 0.054(4) 0.060(4) 0.072(5) 0.016(3) 0.021(3) 0.032(4) C54 0.049(5) 0.031(3) 0.040(4) 0.013(3) 0.002(3) 0.018(3) C55 0.053(4) 0.037(4) 0.047(6) 0.004(3) 0.002(4) 0.017(4) C58 0.084(8) 0.057(6) 0.061(5) -0.000(5) 0.017(5) 0.030(4) C56 0.094(8) 0.060(5) 0.076(5) 0.011(5) -0.005(5) 0.045(5) C57 0.093(6) 0.079(5) 0.093(6) 0.037(5) -0.006(5) 0.054(5) C59 0.061(4) 0.067(4) 0.075(4) 0.028(3) 0.001(3) 0.039(4) C70 0.042(5) 0.048(5) 0.072(5) 0.018(4) 0.006(4) 0.028(4) C71 0.104(6) 0.081(5) 0.101(6) 0.059(5) 0.054(5) 0.060(5) C72 0.109(7) 0.083(6) 0.145(9) 0.063(5) 0.051(7) 0.073(6) C73 0.083(7) 0.069(7) 0.111(8) 0.021(6) 0.012(6) 0.063(6) CXE 0.109(9) 0.054(6) 0.065(6) 0.013(6) 0.013(5) 0.033(5) CXF 0.070(5) 0.044(5) 0.039(5) 0.007(4) 0.006(3) 0.012(4) C74 0.027(4) 0.044(4) 0.051(4) 0.009(3) 0.003(3) 0.024(3) C67 0.043(3) 0.041(3) 0.065(4) 0.017(2) -0.005(3) 0.008(3) C66 0.063(4) 0.042(3) 0.072(4) 0.012(3) -0.012(3) 0.001(3) C65 0.061(5) 0.043(4) 0.070(5) 0.002(3) -0.026(4) 0.000(4) C69 0.044(4) 0.051(4) 0.070(5) 0.008(3) -0.010(4) 0.030(4) C68 0.046(4) 0.037(3) 0.043(3) 0.009(3) -0.006(3) 0.016(3) C75 0.038(4) 0.040(5) 0.052(7) 0.011(3) 0.005(3) 0.016(4) C50 0.041(3) 0.057(6) 0.070(5) 0.018(4) 0.008(3) 0.027(5) C51 0.061(5) 0.073(6) 0.102(7) 0.015(4) 0.029(4) 0.055(5) C49 0.036(4) 0.067(5) 0.088(9) 0.012(4) 0.010(4) 0.030(5) C53 0.033(3) 0.096(6) 0.110(7) 0.013(4) 0.000(3) 0.058(6) C52 0.038(3) 0.083(5) 0.080(5) 0.020(3) 0.006(3) 0.044(4) O2 0.070(5) 0.073(5) 0.050(7) 0.027(4) 0.014(6) 0.036(6) C76 0.049(5) 0.042(5) 0.047(8) 0.019(4) 0.017(6) 0.019(6) Cl2 0.029(2) 0.058(2) 0.0658(17) 0.006(2) -0.002(2) 0.0280(15) O1 0.036(2) 0.094(3) 0.108(2) -0.0055(18) -0.016(2) 0.050(2) C23 0.048(3) 0.052(2) 0.055(2) 0.014(2) -0.004(2) 0.0265(16) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source Ru -1.23940 0.83517 19.26740 12.91820 4.86337 1.56756 0.80852 8.43467 24.79970 94.29280 5.37873983383 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Cl 0.14873 0.16029 11.46040 7.19640 6.25560 1.64550 0.01040 1.16620 18.51940 47.77840 -9.55739974976 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' P 0.10434 0.09671 6.43450 4.17910 1.78000 1.49080 1.90670 27.15700 0.52600 68.16450 1.11489999294 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u -1 0 0 2132.89 49 -1 0 0 2206.88 49.1 -2 0 0 2820.82 60.99 -2 0 0 2649.93 61.99 -2 0 0 2731.53 60.09 -2 0 0 2725.03 62.39 2 0 0 2757.22 62.09 2 0 0 2811.12 62.39 2 0 0 2653.63 60.79 -3 0 0 5238.48 120.19 -3 0 0 5391.86 119.89 -3 0 0 5337.87 120.89 -3 0 0 5280.07 117.29 3 0 0 5492.45 117.49 3 0 0 5569.84 119.19 3 0 0 5447.16 120.79 3 0 0 5339.27 119.59 3 0 0 5317.37 118.79 3 0 0 5330.57 120.29 -4 0 0 675.73 18.5 -4 0 0 679.43 20.9 -4 0 0 671.83 17.7 -4 0 0 690.33 18.9 -4 0 0 678.63 18.3 -4 0 0 712.33 20.7 -4 0 0 666.93 21.5 4 0 0 692.93 17.5 4 0 0 692.03 19.1 4 0 0 697.73 19.2 4 0 0 678.63 20.9 4 0 0 682.73 18.3 4 0 0 691.23 19.6 4 0 0 714.63 18 4 0 0 692.93 21.4 4 0 0 698.93 19.8 4 0 0 689.23 18 4 0 0 714.63 20.5 -5 0 0 337.47 10.7 -5 0 0 350.26 11.7 -5 0 0 366.26 12.3 -5 0 0 344.17 14.2 -5 0 0 348.27 14.9 -5 0 0 351.56 11.8 -5 0 0 346.77 15.9 5 0 0 378.66 13.2 5 0 0 345.17 10.6 5 0 0 350.76 12.3 5 0 0 354.26 11.2 5 0 0 345.67 11 5 0 0 357.06 12.5 5 0 0 364.76 13.7 5 0 0 378.16 13.4 -6 0 0 888.01 23.4 -6 0 0 901.21 28.8 -6 0 0 907.91 25.5 -6 0 0 936.31 30.1 -6 0 0 866.01 24.9 -6 0 0 952.3 28.6 6 0 0 905.51 25.6 6 0 0 932.91 24 6 0 0 898.41 27 6 0 0 904.21 23.3 6 0 0 917.21 26.2 6 0 0 931.71 24.9 6 0 0 899.01 24.2 -7 0 0 489.15 21.2 -7 0 0 520.95 15.5 -7 0 0 563.34 20.8 -7 0 0 508.35 17.4 -7 0 0 513.45 20.7 7 0 0 509.95 16.2 7 0 0 508.55 15.1 7 0 0 589.54 28.1 7 0 0 537.65 18.6 7 0 0 530.25 15.8 7 0 0 534.55 17.9 7 0 0 525.65 16.9 -8 0 0 14.7 3.7 -8 0 0 15.4 3.4 -8 0 0 11 4.1 -8 0 0 14.5 4.1 8 0 0 10.4 2.8 8 0 0 12.4 2.5 8 0 0 10.1 2.6 8 0 0 13.8 2.2 8 0 0 10.5 2.5 -9 0 0 140.29 11.1 -9 0 0 141.99 11.2 -9 0 0 132.39 8.4 -9 0 0 144.19 12 9 0 0 135.99 9.3 9 0 0 132.49 6.3 9 0 0 138.69 7 9 0 0 140.99 8.2 9 0 0 135.99 7.7 -10 0 0 121.39 11.4 -10 0 0 140.69 9.3 -10 0 0 108.69 10.3 10 0 0 129.99 8.5 10 0 0 123.99 6.4 10 0 0 117.79 7.5 10 0 0 130.59 9.9 10 0 0 136.39 6.7 10 0 0 148.99 9.8 -11 0 0 22.1 5.9 -11 0 0 22.9 4.4 -11 0 0 6 3.8 11 0 0 18.6 4.3 11 0 0 15 3.5 11 0 0 19.9 4.5 11 0 0 19.9 5.1 -12 0 0 12.8 4.8 -12 0 0 9.8 4.8 -12 0 0 9.3 3.9 12 0 0 9.2 3.6 12 0 0 6.2 3.4 12 0 0 10.7 4.5 12 0 0 4.9 3.5 13 -1 0 11.2 4.1 13 -1 0 15 4.4 13 -1 0 2 3.1 13 -1 0 22.6 5.6 -13 1 0 12.2 4.4 -13 1 0 13.4 5.6 -13 1 0 14.4 5.2 12 -1 0 16.7 6.4 12 -1 0 14.5 3.7 12 -1 0 15.1 4.7 12 -1 0 10.9 4.2 12 -1 0 8.7 2.2 -12 1 0 9.7 4.3 -12 1 0 7 3.5 -12 1 0 8.4 5.4 11 -1 0 -0.7 1.1 11 -1 0 2.6 2.2 11 -1 0 5.2 2.7 11 -1 0 -1.4 2.4 -11 1 0 3.2 3.5 -11 1 0 1.4 1.9 10 -1 0 63.29 5.8 10 -1 0 66.89 4.9 10 -1 0 61.59 6.8 10 -1 0 73.19 6.8 10 -1 0 67.49 5.2 -10 1 0 75.39 9 -10 1 0 67.99 8.6 -10 1 0 67.49 6.5 9 -1 0 247.78 12.7 9 -1 0 245.28 12 9 -1 0 259.37 11.1 9 -1 0 244.18 10 9 -1 0 239.38 9.4 9 -1 0 229.58 9.8 -9 1 0 240.38 12.2 -9 1 0 248.38 14.8 -9 1 0 252.67 14.9 -9 1 0 247.98 9.8 8 -1 0 31.5 3.5 8 -1 0 46.4 4.2 8 -1 0 40.8 4.3 8 -1 0 34.1 3.2 8 -1 0 44.1 4.6 8 -1 0 44.7 5 -8 1 0 49.8 5.2 -8 1 0 44 6.7 -8 1 0 40.5 5.3 -8 1 0 46.5 3.8 7 -1 0 12.7 2.8 7 -1 0 21.1 2.5 7 -1 0 17.7 3 7 -1 0 16.8 3 7 -1 0 16 2.6 7 -1 0 17.7 2.3 7 -1 0 16.6 2.5 -7 1 0 21.6 4.5 -7 1 0 20.7 3.7 -7 1 0 19.3 4.3 -7 1 0 20 2.5 6 -1 0 180.08 7 6 -1 0 181.18 7.5 6 -1 0 168.38 7.5 6 -1 0 170.08 9.5 6 -1 0 192.58 7.4 6 -1 0 174.08 8.5 -6 1 0 184.88 10.1 -6 1 0 174.18 9.2 -6 1 0 183.18 7.5 -6 1 0 173.58 9.9 -6 1 0 183.88 10.8 5 -1 0 11.9 1.9 5 -1 0 17.9 3.5 5 -1 0 18.5 3.3 5 -1 0 12.1 2.3 4 -1 0 3063.59 74.59 4 -1 0 3233.28 71.39 4 -1 0 3111.99 72.39 4 -1 0 3183.18 70.59 4 -1 0 3205.98 72.69 4 -1 0 3315.57 74.69 4 -1 0 3229.18 71.29 -4 1 0 3247.97 71.69 -4 1 0 3111.09 71.29 -4 1 0 3104.49 74.39 -4 1 0 3144.79 74.29 -4 1 0 3141.69 74.59 -4 1 0 3239.38 75.69 3 -1 0 664.13 18.7 3 -1 0 667.03 17.3 3 -1 0 649.43 18.5 3 -1 0 675.63 16.6 3 -1 0 660.73 16.2 3 -1 0 654.43 17.1 3 -1 0 640.14 18.5 3 -1 0 669.03 15.8 3 -1 0 668.03 16.2 3 -1 0 642.94 16.9 3 -1 0 671.93 19.1 -3 1 0 634.34 18.5 -3 1 0 617.54 18 -3 1 0 672.53 16.4 -3 1 0 667.43 16.7 -3 1 0 661.93 16.4 -3 1 0 652.43 18.5 -3 1 0 655.73 17.2 2 -1 0 56.89 3.2 2 -1 0 59.69 2 2 -1 0 54.69 2.6 2 -1 0 63.29 3.3 2 -1 0 56.29 2.2 2 -1 0 55.99 2.6 2 -1 0 45.9 3.1 -2 1 0 58.19 3.3 -2 1 0 60.89 2.7 -2 1 0 60.39 2.2 -2 1 0 58.69 2.3 -2 1 0 54.99 3.2 -2 1 0 59.39 3.2 1 -1 0 -0.1 0.2 -1 -1 0 6 0.8 -1 -1 0 6.3 1 -1 -1 0 5.9 0.4 -1 -1 0 6.1 0.8 -1 -1 0 7.1 0.7 -1 -1 0 6.9 1.1 -1 -1 0 5.3 1 1 1 0 6.5 0.6 1 1 0 6.2 0.8 1 1 0 5.8 0.7 -2 -1 0 3336.97 72.49 -2 -1 0 3298.77 70.69 -2 -1 0 3062.99 73.39 -2 -1 0 3174.88 73.29 -2 -1 0 3266.17 70.99 2 1 0 2973.1 70.99 2 1 0 3460.95 71.09 2 1 0 3324.97 72.79 2 1 0 3151.98 73.29 2 1 0 3342.77 70.79 2 1 0 3098.29 71.99 2 1 0 3342.87 73.39 -3 -1 0 1446.46 34.9 -3 -1 0 1389.36 33.5 -3 -1 0 1292.27 35.2 -3 -1 0 1441.46 34.6 -3 -1 0 1375.36 32.3 -3 -1 0 1388.06 32.3 -3 -1 0 1377.66 33.4 -3 -1 0 1418.96 36.1 3 1 0 1391.06 34.4 3 1 0 1329.47 35.1 3 1 0 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90.59 7 -6 -3 0 92.39 4.5 -6 -3 0 94.89 9.1 -6 -3 0 82.19 7.8 6 3 0 104.19 6.5 6 3 0 93.99 4.6 6 3 0 92.69 6.5 6 3 0 93.29 4.8 6 3 0 97.59 5.5 6 3 0 95.59 6.4 -7 -3 0 322.87 17.4 -7 -3 0 309.77 10.6 -7 -3 0 345.37 17.1 -7 -3 0 326.27 15 7 3 0 316.47 13.2 7 3 0 313.97 10.7 7 3 0 306.97 13.1 7 3 0 324.97 10.8 7 3 0 311.67 14 7 3 0 312.37 12.2 7 3 0 313.97 12 -8 -3 0 1.4 2.8 -8 -3 0 4.7 3.5 -8 -3 0 3.9 1.7 -8 -3 0 8.6 3.6 8 3 0 5.3 1.8 8 3 0 2.3 1.5 8 3 0 3 2 8 3 0 3.9 2.4 8 3 0 6.5 2.6 8 3 0 4.1 2.5 -9 -3 0 26.9 6.6 -9 -3 0 10.9 3.8 -9 -3 0 19.3 5.5 9 3 0 13.9 3 9 3 0 11.5 3.4 9 3 0 12.9 3.7 9 3 0 13.8 3.3 9 3 0 10.2 3.5 9 3 0 10.8 2.2 9 3 0 19.4 2.9 -10 -3 0 236.78 17.4 -10 -3 0 249.78 18.4 -10 -3 0 224.98 9.8 -10 -3 0 221.28 14.7 10 3 0 233.28 14.1 10 3 0 238.08 10.1 10 3 0 210.08 8.9 10 3 0 223.28 12.3 10 3 0 248.58 14.8 -11 -3 0 35.3 8.5 -11 -3 0 28 6.7 -11 -3 0 27.2 3.9 -11 -3 0 27.1 7.4 11 3 0 21.3 3.1 11 3 0 27.2 6.1 11 3 0 24.5 5.4 11 3 0 20.7 3.4 11 3 0 18.7 5 -12 -3 0 36.3 7.2 -12 -3 0 41.7 8.1 -12 -3 0 39.1 9.1 12 3 0 24.7 5.2 12 3 0 36.9 8 12 3 0 48.9 6.8 13 -4 0 -1.2 2 13 -4 0 5.8 3.2 13 -4 0 2.1 3.1 13 -4 0 -3 2.6 -13 4 0 6.4 2.9 -13 4 0 8 4.5 -13 4 0 5.4 4.7 -13 4 0 2.2 4.1 12 -4 0 148.39 7.6 12 -4 0 163.28 11.6 12 -4 0 166.88 9.1 12 -4 0 154.28 9.5 12 -4 0 180.88 11.7 -12 4 0 155.48 9.1 -12 4 0 158.68 13.3 -12 4 0 159.18 12.7 -12 4 0 154.68 13.4 11 -4 0 194.18 12.4 11 -4 0 224.78 13 11 -4 0 193.88 10.2 11 -4 0 217.18 7.8 -11 4 0 201.18 10.5 -11 4 0 214.38 15.1 -11 4 0 251.07 18 -11 4 0 195.98 13.7 10 -4 0 74.69 7 10 -4 0 67.49 5.7 10 -4 0 60.79 3.7 10 -4 0 67.09 6.3 10 -4 0 74.19 4.1 -10 4 0 70.79 8.2 -10 4 0 64.79 6.1 -10 4 0 63.79 8.2 -10 4 0 85.69 8.8 9 -4 0 121.69 4.9 9 -4 0 126.79 8.2 9 -4 0 130.29 8.6 9 -4 0 126.39 6.9 9 -4 0 124.89 5.3 -9 4 0 122.89 7.9 -9 4 0 120.89 9.9 -9 4 0 132.59 10.6 -9 4 0 125.59 10.1 8 -4 0 214.98 10.7 8 -4 0 206.78 10.2 8 -4 0 211.38 7.1 8 -4 0 222.28 8.9 8 -4 0 209.98 6.6 -8 4 0 217.58 12.6 -8 4 0 195.68 10.1 -8 4 0 215.48 12.4 -8 4 0 226.38 13 7 -4 0 44 3.5 7 -4 0 42.7 2.2 7 -4 0 39.3 2.4 7 -4 0 39.6 4.4 7 -4 0 47.1 4.4 7 -4 0 47.2 4.6 7 -4 0 41.4 4.1 -7 4 0 38.2 3.3 -7 4 0 53.89 5.9 -7 4 0 43.4 5.1 -7 4 0 48.4 5.6 -7 4 0 42.2 5.2 6 -4 0 1272.67 33.8 6 -4 0 1337.87 34.1 6 -4 0 1238.98 33.5 6 -4 0 1243.38 29.1 6 -4 0 1298.77 33.7 6 -4 0 1282.07 29 6 -4 0 1264.67 31.1 -6 4 0 1336.77 37.3 -6 4 0 1299.07 37.7 -6 4 0 1299.17 36.3 -6 4 0 1323.77 34.4 5 -4 0 1117.39 25.1 5 -4 0 1127.19 29.2 5 -4 0 1138.49 26.8 5 -4 0 1106.49 29.6 5 -4 0 1118.49 29.3 -5 4 0 1146.69 30.1 -5 4 0 1106.19 26.8 -5 4 0 1123.19 32.9 -5 4 0 1103.29 31.8 4 -4 0 317.57 12.1 4 -4 0 321.97 13.7 4 -4 0 329.37 12.2 4 -4 0 327.77 10.8 4 -4 0 327.47 8 4 -4 0 315.17 11.4 4 -4 0 316.27 8.9 4 -4 0 333.07 12.7 -4 4 0 319.17 11.7 -4 4 0 328.67 10.7 -4 4 0 325.37 8.4 -4 4 0 312.87 8.8 -4 4 0 329.87 12.4 -4 4 0 325.37 18 -4 4 0 313.07 10.7 3 -4 0 1013.1 31.1 3 -4 0 1107.79 27.5 3 -4 0 1107.99 28.4 3 -4 0 1089.39 29 3 -4 0 1121.29 25.2 3 -4 0 1128.79 25.4 -3 4 0 1115.89 27.4 -3 4 0 1091.79 28.9 -3 4 0 1116.59 29.1 -3 4 0 1079.89 30.5 -3 4 0 1114.19 25.1 -3 4 0 1095.99 28.6 -3 4 0 1132.69 25.5 2 -4 0 1279.37 29.8 2 -4 0 1261.97 30.3 2 -4 0 1231.18 32 2 -4 0 1282.67 29.1 2 -4 0 1282.47 31.5 2 -4 0 1243.18 31 2 -4 0 1236.98 33 2 -4 0 1235.38 28.7 -2 4 0 1263.47 30.7 -2 4 0 1127.69 34.9 -2 4 0 1295.47 30.2 -2 4 0 1292.47 30.4 -2 4 0 1270.67 29.3 -2 4 0 1221.98 32 -2 4 0 1299.47 28.5 1 -4 0 1534.45 37.7 1 -4 0 1594.64 36.6 1 -4 0 1574.64 37.2 1 -4 0 1612.84 37.2 1 -4 0 1598.84 37.3 1 -4 0 1593.84 39.4 1 -4 0 1617.34 38.4 -1 4 0 1675.83 36.9 -1 4 0 1516.75 39.2 -1 4 0 1673.13 37.1 -1 4 0 1582.24 37.3 -1 4 0 1654.83 40 -1 4 0 1620.94 36.6 -1 4 0 1618.84 37.6 -1 4 0 1637.14 38.1 0 -4 0 218.18 6.4 0 -4 0 217.78 8.2 0 -4 0 221.98 7.7 0 -4 0 215.08 7.8 0 -4 0 233.68 7.9 0 -4 0 237.98 8.1 0 4 0 210.08 7.7 0 4 0 215.28 6.3 0 4 0 219.28 8.2 0 4 0 231.48 8.1 0 4 0 224.48 9.7 0 4 0 234.08 8 -1 -4 0 176.78 5.3 -1 -4 0 163.18 7.1 -1 -4 0 165.88 5 -1 -4 0 163.98 6.9 -1 -4 0 169.58 6.5 -1 -4 0 164.58 7 -1 -4 0 164.38 7.4 1 4 0 152.38 5.6 1 4 0 164.58 5.1 1 4 0 159.38 7 1 4 0 164.08 6.7 1 4 0 162.78 6.8 1 4 0 155.98 6.3 1 4 0 159.88 7.1 1 4 0 162.78 6.8 -2 -4 0 11 2.5 -2 -4 0 14.3 2.6 -2 -4 0 11.9 1.7 -2 -4 0 13.6 1.7 -2 -4 0 14.6 2.7 -2 -4 0 15.4 2.6 2 4 0 15 1.9 2 4 0 13 2.4 2 4 0 18 2.7 2 4 0 12.7 1.4 2 4 0 16 2.2 2 4 0 13.8 1.2 2 4 0 15.8 1.9 2 4 0 15.2 2.7 -3 -4 0 794.42 21.2 -3 -4 0 834.02 23.9 -3 -4 0 816.22 21.7 -3 -4 0 790.32 24.7 -3 -4 0 791.92 24.3 3 4 0 796.22 20.2 3 4 0 786.82 22.7 3 4 0 803.32 21.2 3 4 0 773.52 22.1 3 4 0 786.32 23 -4 -4 0 958.4 26 -4 -4 0 944.21 29 -4 -4 0 931.01 29.3 -4 -4 0 939.91 27.7 -4 -4 0 919.51 24.5 4 4 0 902.31 21.6 4 4 0 889.11 24 4 4 0 904.31 25.6 4 4 0 956.2 24.3 4 4 0 925.61 26.4 -5 -4 0 2.1 1.2 -5 -4 0 5.5 2.4 -5 -4 0 2.6 1.9 -5 -4 0 2.4 2.6 -5 -4 0 -1.2 1.8 5 4 0 1.6 1.2 5 4 0 5.4 2.2 5 4 0 2.9 1.2 5 4 0 4.8 1.9 5 4 0 2.4 1.6 5 4 0 2.8 0.7 5 4 0 2.9 1.2 -6 -4 0 151.38 12.8 -6 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0 76.49 9.7 -12 5 0 77.59 7 11 -5 0 2.3 2.8 11 -5 0 -1.5 2.2 -11 5 0 -0.2 3.2 -11 5 0 -0.9 2.1 -11 5 0 3.6 6.3 10 -5 0 10.5 3.2 10 -5 0 21.2 4.5 10 -5 0 21.4 3.8 -10 5 0 9.8 4.5 -10 5 0 19.8 5.2 -10 5 0 20.2 4.2 9 -5 0 65.69 6.1 9 -5 0 85.89 5.5 9 -5 0 80.99 6.9 -9 5 0 74.69 8.6 -9 5 0 94.69 9.2 -9 5 0 74.89 6.5 8 -5 0 2.8 1.8 8 -5 0 -2.4 1 7 -5 0 385.56 11.9 7 -5 0 361.96 13 7 -5 0 403.76 14.8 -7 5 0 398.86 17.8 -7 5 0 381.96 12.1 -7 5 0 387.76 15 6 -5 0 1571.24 39.8 6 -5 0 1595.94 42.7 6 -5 0 1512.75 36.4 6 -5 0 1509.35 39.4 -6 5 0 1536.85 40.8 -6 5 0 1600.14 43.2 -6 5 0 1557.24 44.2 -6 5 0 1517.15 36.6 5 -5 0 27.1 3.9 5 -5 0 33.6 3.5 5 -5 0 35.6 3.2 5 -5 0 32.9 1.6 5 -5 0 29.7 2.6 -5 5 0 32.7 5.6 -5 5 0 31.5 2.2 -5 5 0 23.5 3.9 -5 5 0 33.8 5.7 -5 5 0 34 1.9 4 -5 0 891.01 26.2 4 -5 0 912.01 21.6 4 -5 0 897.11 25.1 4 -5 0 927.21 21.1 -4 5 0 901.71 21.3 -4 5 0 887.21 27.7 -4 5 0 897.11 24.1 -4 5 0 878.61 21.5 -4 5 0 921.41 26 -4 5 0 905.01 25.9 3 -5 0 586.44 20.1 3 -5 0 617.54 18.2 3 -5 0 563.84 19.8 3 -5 0 615.24 17.5 3 -5 0 591.04 16.9 3 -5 0 605.24 14.9 3 -5 0 594.64 16.6 3 -5 0 599.24 15.2 -3 5 0 597.24 17.8 -3 5 0 596.14 15.5 -3 5 0 604.94 20.1 -3 5 0 602.74 19 -3 5 0 611.44 16.8 -3 5 0 600.84 14.6 -3 5 0 607.64 17 2 -5 0 50.09 4 2 -5 0 43.3 3.4 2 -5 0 51.49 4 2 -5 0 48.1 3 2 -5 0 50.09 3 2 -5 0 50.99 3.4 2 -5 0 45.4 4.6 2 -5 0 46.1 2.7 -2 5 0 50.09 2.6 -2 5 0 46.1 3.1 -2 5 0 46.2 4.6 -2 5 0 45.9 3.1 -2 5 0 48.3 3.9 -2 5 0 45.3 4.5 1 -5 0 4154.48 94.09 1 -5 0 4128.39 91.49 1 -5 0 4028.6 92.49 1 -5 0 4021 90.69 1 -5 0 4082.39 91.99 1 -5 0 4061.59 93.19 1 -5 0 4318.67 92.09 -1 5 0 4125.99 94.39 -1 5 0 3875.71 93.89 -1 5 0 4180.98 90.69 -1 5 0 3894.01 96.59 -1 5 0 4245.28 94.59 -1 5 0 4345.57 91.49 -1 5 0 4179.18 94.29 0 -5 0 1390.56 34.9 0 -5 0 1377.66 33.4 0 -5 0 1335.17 31.4 0 -5 0 1222.88 38.8 0 -5 0 1428.16 34.2 0 -5 0 1399.36 31.8 0 -5 0 1348.27 34.1 0 5 0 1218.18 35.1 0 5 0 1437.46 33.9 0 5 0 1331.07 34.2 0 5 0 1448.26 34.1 0 5 0 1398.26 34.1 0 5 0 1397.46 31.4 0 5 0 1399.16 35 -1 -5 0 2.1 1.2 -1 -5 0 2.7 1.1 -1 -5 0 2.3 0.8 -1 -5 0 1.8 0.7 -1 -5 0 0.5 0.7 -1 -5 0 -0.4 1.1 -1 -5 0 0.5 1.2 1 5 0 2.7 1.4 1 5 0 0.9 0.5 1 5 0 1.4 0.8 1 5 0 1.9 1.2 1 5 0 0.9 0.9 1 5 0 0.3 0.7 1 5 0 1.9 1.3 1 5 0 1.7 1.3 -2 -5 0 594.64 15.8 -2 -5 0 592.74 17.1 -2 -5 0 545.85 19 -2 -5 0 583.44 13.7 -2 -5 0 605.24 18.8 -2 -5 0 584.94 18.8 2 5 0 588.14 17.4 2 5 0 567.74 17.6 2 5 0 591.34 18.1 2 5 0 581.04 18.6 2 5 0 582.04 14.9 2 5 0 575.14 14.4 2 5 0 584.94 17.3 -3 -5 0 1609.04 39.7 -3 -5 0 1636.04 43.5 -3 -5 0 1653.33 44.2 -3 -5 0 1638.14 42.7 -3 -5 0 1616.54 39.6 3 5 0 1582.54 39.9 3 5 0 1631.04 37.9 3 5 0 1599.04 40.7 3 5 0 1612.44 41.6 -4 -5 0 73.29 4.7 -4 -5 0 69.69 5.2 -4 -5 0 80.09 6.5 -4 -5 0 77.29 6.9 -4 -5 0 65.99 6.6 4 5 0 73.89 5.1 4 5 0 71.39 5.7 4 5 0 68.89 4.2 4 5 0 68.89 5.1 -5 -5 0 62.49 6.4 -5 -5 0 55.59 5.1 -5 -5 0 52.69 6.7 -5 -5 0 56.89 6.4 -5 -5 0 49.7 5.6 5 5 0 63.99 4.3 5 5 0 49.2 4.4 5 5 0 63.29 5.6 5 5 0 57.59 5.1 5 5 0 54.99 4.2 -6 -5 0 189.98 13 -6 -5 0 202.98 10.6 -6 -5 0 190.78 12.4 6 5 0 201.48 10.7 6 5 0 193.28 10.1 6 5 0 188.58 8.4 -7 -5 0 6.3 3.2 -7 -5 0 -0.8 2.2 -7 -5 0 2.6 3.2 7 5 0 2.7 2.2 7 5 0 3.6 2 7 5 0 0.3 1.4 -8 -5 0 50.09 9 -8 -5 0 64.59 9.8 -8 -5 0 51.19 8.1 8 5 0 66.79 5.2 8 5 0 66.19 6.4 8 5 0 61.99 6.7 8 5 0 59.99 6.7 -9 -5 0 76.19 16.1 -9 -5 0 77.59 8.2 -9 -5 0 72.29 10.8 9 5 0 72.19 5.4 9 5 0 69.29 12 9 5 0 77.79 7.5 -10 -5 0 -1.6 3.3 -10 -5 0 1.7 4.1 -10 -5 0 -0.8 3 10 5 0 -3.4 2.7 10 5 0 -2.1 2.1 10 5 0 0.8 2.3 -11 -5 0 -7.6 3.9 -11 -5 0 6.7 4.7 11 5 0 0.3 2.7 11 5 0 -4.7 2.8 11 5 0 1.8 2.7 13 -6 0 1.2 2.9 13 -6 0 -1.2 2.5 13 -6 0 -5.1 2.7 -13 6 0 6.1 4.1 -13 6 0 0.5 4 -13 6 0 4.9 3.8 12 -6 0 3.2 2.7 12 -6 0 -1.8 2.7 12 -6 0 -2.4 2.1 -12 6 0 2.6 2.6 -12 6 0 2.7 3.6 -12 6 0 1.6 3.8 11 -6 0 -0.4 2.1 11 -6 0 1.2 2.4 11 -6 0 0.2 2 -11 6 0 0 2.3 -11 6 0 -4.1 3.1 -11 6 0 2.3 3.6 10 -6 0 89.29 6 10 -6 0 111.49 8.4 10 -6 0 84.79 7.6 -10 6 0 93.39 7.8 -10 6 0 88.29 9.7 -10 6 0 92.69 10.1 9 -6 0 17.2 3 9 -6 0 13.5 3.6 9 -6 0 18 3.7 -9 6 0 16.3 5 -9 6 0 16.2 4.9 -9 6 0 14.7 3.6 8 -6 0 1.5 1.6 8 -6 0 0.5 1.7 8 -6 0 0.3 1.4 8 -6 0 -1.1 1.1 -8 6 0 0.5 1.1 -8 6 0 0.4 2.6 -8 6 0 7 3.3 -8 6 0 2.1 1.9 7 -6 0 215.98 10.3 7 -6 0 214.98 10.1 7 -6 0 206.08 7.8 -7 6 0 214.28 11 -7 6 0 215.88 7.9 -7 6 0 213.78 12.1 -7 6 0 208.18 13 6 -6 0 530.85 17.2 6 -6 0 537.35 17.5 -6 6 0 542.05 19.8 -6 6 0 493.75 18.5 -6 6 0 514.85 14.2 -6 6 0 537.55 21.5 5 -6 0 74.49 5 5 -6 0 68.69 2.9 5 -6 0 67.69 5.2 5 -6 0 71.99 3.6 -5 6 0 69.29 3.3 -5 6 0 57.69 5.6 -5 6 0 53.99 6.2 -5 6 0 77.29 6 -5 6 0 67.19 3.2 4 -6 0 333.87 9.6 4 -6 0 344.87 9.8 4 -6 0 327.27 11.6 4 -6 0 346.17 12 4 -6 0 352.66 12.5 -4 6 0 348.97 14 -4 6 0 339.67 10.2 -4 6 0 343.77 9.3 -4 6 0 359.46 13.3 -4 6 0 347.07 15.1 3 -6 0 409.76 13 3 -6 0 383.96 11 3 -6 0 385.06 13.6 3 -6 0 384.36 11.3 3 -6 0 397.86 13.4 3 -6 0 382.26 15.6 3 -6 0 383.36 12.1 -3 6 0 382.66 11.7 -3 6 0 404.06 13.3 -3 6 0 402.96 15.7 -3 6 0 389.96 12.8 -3 6 0 378.16 14.8 -3 6 0 398.56 10.6 2 -6 0 484.45 15.4 2 -6 0 478.95 15.7 2 -6 0 484.55 14 2 -6 0 488.25 14.8 2 -6 0 450.05 16.7 2 -6 0 487.05 13.7 2 -6 0 489.75 17.1 2 -6 0 474.65 13.6 -2 6 0 454.85 16.8 -2 6 0 481.95 14.2 -2 6 0 483.05 14.2 -2 6 0 504.85 15.2 -2 6 0 462.25 16.7 -2 6 0 478.75 12.9 -2 6 0 479.25 14.4 1 -6 0 3529.75 76.09 1 -6 0 3095.89 77.39 1 -6 0 3092.19 75.19 1 -6 0 3164.88 73.79 1 -6 0 3210.88 76.79 1 -6 0 3285.77 75.09 1 -6 0 3182.48 72.79 1 -6 0 3138.79 71.99 -1 6 0 3210.18 73.89 -1 6 0 3215.58 76.39 -1 6 0 3327.97 73.09 -1 6 0 3225.78 73.79 -1 6 0 3162.98 75.79 -1 6 0 3245.18 74.69 -1 6 0 3232.78 71.89 0 -6 0 1155.18 29.2 0 -6 0 1104.39 29 0 -6 0 1040.4 29.7 0 -6 0 1071.29 26 0 -6 0 1100.59 28.1 0 -6 0 1092.29 26.4 0 -6 0 1104.99 29 0 -6 0 1079.19 31.3 0 6 0 1091.29 25.9 0 6 0 1080.19 28.8 0 6 0 1097.79 28.5 0 6 0 1075.19 29.3 0 6 0 1154.78 30.5 -1 -6 0 359.66 10.2 -1 -6 0 361.36 10.4 -1 -6 0 344.67 13.1 -1 -6 0 403.86 13.4 -1 -6 0 362.76 14 1 6 0 374.36 13.4 1 6 0 370.86 13.2 1 6 0 354.06 11.4 1 6 0 355.36 10 1 6 0 359.46 13.2 -2 -6 0 1479.65 40.3 -2 -6 0 1437.96 39.2 -2 -6 0 1448.06 35 -2 -6 0 1448.85 33 -2 -6 0 1493.05 39.3 2 6 0 1467.55 37.4 2 6 0 1505.35 38.6 2 6 0 1481.45 34 2 6 0 1441.86 34.1 2 6 0 1468.35 37.9 -3 -6 0 906.01 24.6 -3 -6 0 928.21 28.2 -3 -6 0 921.01 28.8 -3 -6 0 928.01 29.5 3 6 0 915.01 26.1 3 6 0 933.01 26.4 3 6 0 966.6 27.6 3 6 0 935.11 23.2 -4 -6 0 437.86 17.7 -4 -6 0 429.86 18.4 -4 -6 0 445.06 21.2 -4 -6 0 456.85 15.2 4 6 0 463.05 16.2 4 6 0 446.66 14 4 6 0 424.56 15 4 6 0 433.36 16.6 -5 -6 0 768.12 26 -5 -6 0 734.63 27.6 -5 -6 0 701.33 26.7 5 6 0 714.23 23.8 5 6 0 702.23 21.5 5 6 0 674.73 19.8 5 6 0 718.93 23.1 -6 -6 0 156.68 12.4 -6 -6 0 175.18 12.6 -6 -6 0 170.58 9.7 -6 -6 0 162.88 11.1 6 6 0 172.98 8.6 6 6 0 169.38 9.8 6 6 0 181.28 10.6 -7 -6 0 30.9 6.7 -7 -6 0 38.6 6 -7 -6 0 39.6 7.3 7 6 0 45.5 5.4 7 6 0 43.5 4.5 7 6 0 49 6.1 -8 -6 0 224.18 18.9 -8 -6 0 272.97 18.5 -8 -6 0 255.97 17.1 8 6 0 248.68 13.7 8 6 0 242.88 13.2 8 6 0 236.38 10.9 -9 -6 0 1 4 -9 -6 0 4.7 5.1 -9 -6 0 3.9 3.2 9 6 0 5.7 3 9 6 0 5 3.1 9 6 0 0.8 3.4 -10 -6 0 31 8.3 -10 -6 0 31.5 6.6 -10 -6 0 31.2 8.6 10 6 0 24.2 5.2 10 6 0 22.4 5.6 10 6 0 20.6 4.2 10 6 0 24 5.8 13 -7 0 -2 2.7 13 -7 0 10.2 3.3 13 -7 0 -2 2.4 13 -7 0 2.4 2.6 -13 7 0 5.5 3.8 -13 7 0 5.9 3.5 -13 7 0 -1.1 3.5 12 -7 0 -3.7 2.2 12 -7 0 -5.3 2 12 -7 0 -1.1 2.4 12 -7 0 -2.3 2.7 -12 7 0 0.6 2.9 -12 7 0 1.9 3.6 -12 7 0 1.2 4 11 -7 0 8.9 2.9 11 -7 0 14.7 4 11 -7 0 14.2 4.1 -11 7 0 19.9 7.3 -11 7 0 6.7 4 -11 7 0 19.8 4.9 10 -7 0 58.89 6.3 10 -7 0 55.79 4.8 10 -7 0 50.89 6.2 -10 7 0 61.89 8 -10 7 0 50.99 8.3 -10 7 0 46.3 5.9 9 -7 0 85.09 5.5 9 -7 0 93.09 7.6 9 -7 0 94.89 7.3 -9 7 0 83.49 8.6 -9 7 0 99.89 8.7 -9 7 0 82.99 9.5 8 -7 0 39.7 3.7 8 -7 0 35.4 4.4 8 -7 0 37.5 3.6 8 -7 0 37.9 4.8 -8 7 0 30.6 2.9 -8 7 0 37.4 6.7 -8 7 0 28.6 5.9 -8 7 0 43 5.4 7 -7 0 10.6 2 7 -7 0 7.4 2.6 7 -7 0 9.4 2.5 -7 7 0 10.8 4.3 -7 7 0 8.8 3.1 -7 7 0 9.7 1.7 -7 7 0 6.3 2.8 6 -7 0 15.9 3.3 6 -7 0 14.3 3.2 6 -7 0 12.4 1.3 6 -7 0 11.7 2.4 6 -7 0 13 1.9 -6 7 0 13.5 6.5 -6 7 0 14.6 3.9 -6 7 0 14.9 1.4 -6 7 0 14.1 1.6 -6 7 0 9.7 3.3 5 -7 0 149.49 7.6 5 -7 0 143.09 5.4 5 -7 0 148.99 5.4 5 -7 0 143.49 8 5 -7 0 153.48 7.6 -5 7 0 142.69 10.2 -5 7 0 161.78 9 -5 7 0 142.89 5.1 -5 7 0 135.59 8.9 -5 7 0 141.79 5.7 4 -7 0 284.77 11 4 -7 0 269.57 8.6 4 -7 0 277.77 10.4 4 -7 0 293.87 11.7 4 -7 0 289.07 9.1 -4 7 0 277.07 8.1 -4 7 0 261.97 9.3 -4 7 0 287.27 13.2 -4 7 0 260.97 13.4 -4 7 0 275.97 11.4 3 -7 0 -0.7 0.5 3 -7 0 1 1.7 3 -7 0 -0.4 0.6 3 -7 0 0.8 0.8 3 -7 0 1.4 1.1 -3 7 0 -1.6 1.6 -3 7 0 0.9 1.6 -3 7 0 -0.9 0.7 -3 7 0 0.7 1 -3 7 0 -0.4 0.9 2 -7 0 310.37 12 2 -7 0 325.47 12.5 2 -7 0 315.17 10.2 2 -7 0 313.87 11.7 2 -7 0 325.57 11.1 2 -7 0 298.37 13 -2 7 0 302.07 13.9 -2 7 0 321.37 13.9 -2 7 0 323.47 9.9 -2 7 0 314.87 11.1 1 -7 0 232.38 8.4 1 -7 0 218.18 10 1 -7 0 224.88 9.8 1 -7 0 224.58 10.3 1 -7 0 246.38 9.5 1 -7 0 228.78 9.3 -1 7 0 230.88 9.4 -1 7 0 229.78 7.7 -1 7 0 216.68 10.9 -1 7 0 227.88 10.4 -1 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33.2 4.9 -6 -7 0 33.5 6.7 -6 -7 0 26.3 6.6 6 7 0 26.9 4.4 6 7 0 27.1 5.1 6 7 0 22.6 4.2 -7 -7 0 248.68 16.9 -7 -7 0 233.68 12.3 -7 -7 0 229.68 15.5 7 7 0 227.48 11.2 7 7 0 243.68 13.6 7 7 0 225.88 12.6 -8 -7 0 127.79 12.7 -8 -7 0 116.49 12.8 8 7 0 123.79 10.3 8 7 0 111.79 9.1 -9 -7 0 25.3 6.4 -9 -7 0 14.3 4.4 -9 -7 0 6.5 5 9 7 0 11.3 3.6 9 7 0 7.3 3.4 9 7 0 12.8 4.9 -10 -7 0 82.79 11.4 -10 -7 0 73.49 9.1 -10 -7 0 55.29 9.7 10 7 0 67.59 8.1 10 7 0 69.39 8.7 10 7 0 58.09 6.7 10 7 0 83.39 9.1 13 -8 0 3.3 2.3 -13 8 0 1.7 4 12 -8 0 65.19 7.1 12 -8 0 62.69 7.8 12 -8 0 59.59 7.7 12 -8 0 52.89 5.6 -12 8 0 51.59 8.9 -12 8 0 64.29 10.6 -12 8 0 77.09 8.1 11 -8 0 60.79 7.2 11 -8 0 61.09 6.7 11 -8 0 52.39 5 11 -8 0 59.49 12.1 -11 8 0 55.89 8.6 -11 8 0 77.99 7.8 -11 8 0 47.6 8.9 10 -8 0 5 2.4 10 -8 0 3.5 3.1 10 -8 0 3.5 2.3 10 -8 0 1.5 1.8 -10 8 0 2.6 3.2 -10 8 0 0.1 2.9 -10 8 0 3.7 3.1 9 -8 0 1.4 2.6 9 -8 0 5.3 2.5 9 -8 0 3.8 2 9 -8 0 4.2 2.4 9 -8 0 4.7 1.9 -9 8 0 4.2 3.8 -9 8 0 7.7 3.5 -9 8 0 3.9 2.8 -9 8 0 2.4 1.6 8 -8 0 75.49 6.8 8 -8 0 68.39 4.4 8 -8 0 65.79 4.8 8 -8 0 69.39 6.1 8 -8 0 76.79 6.5 -8 8 0 62.39 7 -8 8 0 69.19 6.9 -8 8 0 73.59 8.2 -8 8 0 66.09 4 7 -8 0 0.6 1.5 7 -8 0 -0.2 1.4 7 -8 0 0.6 1.1 7 -8 0 -0.2 2.1 -7 8 0 -0.3 1.9 -7 8 0 1.2 0.7 -7 8 0 0 2 6 -8 0 65.19 5.3 6 -8 0 52.59 5.8 6 -8 0 54.39 3 6 -8 0 58.49 3.3 6 -8 0 55.89 5.5 -6 8 0 58.69 6.4 -6 8 0 61.09 7.4 -6 8 0 60.39 3 -6 8 0 53.29 3.3 5 -8 0 9.8 3.2 5 -8 0 11.9 1.7 5 -8 0 11.3 1.7 5 -8 0 10.8 2.7 5 -8 0 7 2 -5 8 0 8.9 3.2 -5 8 0 12.1 2.2 -5 8 0 12.1 1.6 -5 8 0 8.9 2.8 -5 8 0 7.8 3.4 4 -8 0 0.2 0.8 4 -8 0 -0.4 0.7 4 -8 0 0.1 2 4 -8 0 0.5 1.2 4 -8 0 0.5 0.9 -4 8 0 -1.3 1.7 -4 8 0 4 1.6 -4 8 0 2.7 1.5 -4 8 0 1.3 0.9 -4 8 0 -0.5 2 3 -8 0 73.19 6 3 -8 0 75.09 5.6 3 -8 0 74.19 4.6 3 -8 0 79.19 5.7 3 -8 0 71.69 4.5 -3 8 0 76.09 7.1 -3 8 0 73.49 5 -3 8 0 74.49 5 -3 8 0 72.69 6.7 -3 8 0 69.99 3.9 2 -8 0 134.29 6.9 2 -8 0 124.89 6.5 2 -8 0 130.09 7.9 2 -8 0 140.79 6.2 2 -8 0 129.19 7.5 -2 8 0 137.49 9.3 -2 8 0 124.09 8.3 -2 8 0 141.69 7.1 -2 8 0 131.69 6 1 -8 0 10 2.6 1 -8 0 5.9 2.3 1 -8 0 10.5 2.4 1 -8 0 8.1 1.9 1 -8 0 10.9 2.7 1 -8 0 7.1 1.5 -1 8 0 13 2.7 -1 8 0 8.3 1.9 -1 8 0 11 3.5 -1 8 0 10.7 2.9 0 -8 0 17.2 3.6 0 -8 0 11 2.6 0 -8 0 16.9 2.2 0 -8 0 17.1 3.4 0 -8 0 13.3 2.1 0 -8 0 14.6 3.1 0 8 0 11.7 3.3 0 8 0 16.4 1.7 0 8 0 17.6 3.3 0 8 0 15.1 3 0 8 0 14.5 2.5 -1 -8 0 225.58 7.8 -1 -8 0 235.18 12 -1 -8 0 235.28 8.2 -1 -8 0 238.48 7.9 -1 -8 0 214.58 10.8 -1 -8 0 234.28 11.4 1 8 0 225.48 7.6 1 8 0 242.88 11.9 1 8 0 248.18 10.2 1 8 0 239.98 9.3 1 8 0 245.38 11.2 -2 -8 0 18.5 3.9 -2 -8 0 12.8 1.4 -2 -8 0 13.3 3.5 -2 -8 0 12.2 2 2 8 0 10.6 1.6 2 8 0 12.1 3.2 2 8 0 14.3 2.1 2 8 0 14.1 3.3 2 8 0 11.4 2.7 -3 -8 0 174.38 11 -3 -8 0 170.98 10.6 -3 -8 0 158.68 10.9 -3 -8 0 166.38 7.6 3 8 0 160.48 6.4 3 8 0 171.08 10 3 8 0 171.38 9.1 3 8 0 172.48 9.8 -4 -8 0 310.47 11.9 -4 -8 0 296.07 16.3 -4 -8 0 302.37 15.1 -4 -8 0 326.47 16.5 4 8 0 276.17 9.9 4 8 0 315.87 14.6 4 8 0 305.47 13.4 4 8 0 292.87 13.5 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0 23.8 8.3 1 -9 0 27.6 4.9 1 -9 0 28.3 3.6 1 -9 0 33.6 3.1 1 -9 0 29 4.7 1 -9 0 30 2.7 -1 9 0 28.1 7.6 -1 9 0 32.8 3.9 -1 9 0 26.8 4.5 0 -9 0 15.3 3.2 0 -9 0 14.9 3.8 0 -9 0 15.5 3.4 0 -9 0 17.7 3 0 -9 0 15.8 2.3 0 -9 0 16.1 2 0 9 0 19.3 2 0 9 0 24 3.9 0 9 0 15.7 3.3 0 9 0 18.3 3 -1 -9 0 49.7 5.4 -1 -9 0 45 3.1 -1 -9 0 45.2 3.3 -1 -9 0 42.8 5.5 1 9 0 47.4 4 1 9 0 50.69 4.5 1 9 0 45.8 6.8 1 9 0 44.1 2.8 1 9 0 44.8 4.9 -2 -9 0 237.28 12.7 -2 -9 0 238.28 13.5 -2 -9 0 231.38 7.3 -2 -9 0 249.68 14.8 2 9 0 248.78 13.2 2 9 0 231.68 12 2 9 0 244.98 12.8 2 9 0 236.78 7.9 2 9 0 233.78 8.2 -3 -9 0 13.4 3.9 -3 -9 0 24.9 5.1 -3 -9 0 15.6 2.6 -3 -9 0 16.2 4.8 3 9 0 23.2 4 3 9 0 17.7 4.2 3 9 0 27.1 5.1 3 9 0 18.8 2 -4 -9 0 93.29 8.7 -4 -9 0 95.89 9 -4 -9 0 92.59 9.4 -4 -9 0 93.99 6.2 4 9 0 74.99 7.2 4 9 0 92.29 8.2 4 9 0 100.59 7.3 4 9 0 83.69 4.7 -5 -9 0 5.9 3.8 -5 -9 0 0.7 2.4 -5 -9 0 -1.3 2.8 5 9 0 -0.5 2.6 5 9 0 2.7 2.7 5 9 0 1.7 2 5 9 0 -2.1 1.2 -6 -9 0 71.09 11.2 -6 -9 0 73.49 6.3 -6 -9 0 68.29 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380.76 20.1 -7 10 0 368.66 16.6 -7 10 0 345.97 11.2 -7 10 0 345.87 10.2 -7 10 0 360.36 11.6 6 -10 0 402.96 17.1 6 -10 0 399.46 15.3 6 -10 0 391.46 12.6 6 -10 0 423.26 16.5 -6 10 0 383.86 16.4 -6 10 0 396.46 20.3 -6 10 0 379.16 18.8 -6 10 0 378.66 13.1 -6 10 0 399.66 11.1 5 -10 0 8.4 3.6 5 -10 0 11.1 2.5 5 -10 0 11.9 2.3 5 -10 0 8.5 2.6 5 -10 0 8.9 2.7 -5 10 0 8.5 1.6 -5 10 0 8.2 3.6 -5 10 0 13.4 3.3 -5 10 0 7 4.1 4 -10 0 129.99 9.3 4 -10 0 134.29 7.3 4 -10 0 136.09 6.6 4 -10 0 144.09 8.9 -4 10 0 143.89 6.1 -4 10 0 138.29 10.5 -4 10 0 134.19 7.8 -4 10 0 143.69 11 3 -10 0 143.69 9.5 3 -10 0 147.99 7.5 3 -10 0 156.58 9.2 3 -10 0 149.09 7.3 -3 10 0 148.69 10.3 -3 10 0 137.89 10.9 -3 10 0 144.29 6.6 -3 10 0 146.59 8.4 2 -10 0 5.4 1.6 2 -10 0 7.7 2.3 2 -10 0 7.3 3 2 -10 0 6.4 2.7 2 -10 0 9.6 3.5 -2 10 0 7.6 3.2 -2 10 0 9.1 2.7 -2 10 0 6.7 2.8 1 -10 0 41.2 3.4 1 -10 0 52.89 5.1 1 -10 0 48 4.2 1 -10 0 41.5 5.1 1 -10 0 45.2 5.9 -1 10 0 42.3 4.8 -1 10 0 41.3 6.7 -1 10 0 48 4.1 -1 10 0 49.6 5.3 0 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4 278.77 13.6 -9 -4 4 274.27 17.9 8 4 -4 173.38 8.8 8 4 -4 177.78 8.7 8 4 -4 159.28 10.1 8 4 -4 171.48 10.3 8 4 -4 175.98 10.2 -8 -4 4 168.58 11.4 -8 -4 4 163.08 12.6 -8 -4 4 183.88 10 -8 -4 4 169.58 11.8 7 4 -4 9.5 2.2 7 4 -4 13.6 3.5 7 4 -4 7.5 2.8 7 4 -4 11.2 3.1 7 4 -4 10.8 2.5 -7 -4 4 11.7 2.6 -7 -4 4 6.8 3.1 -7 -4 4 7.1 3.3 -7 -4 4 6.9 4.2 6 4 -4 256.07 11.8 6 4 -4 233.78 9.8 6 4 -4 213.08 9.7 6 4 -4 213.68 9 -6 -4 4 225.78 10.1 -6 -4 4 228.18 12.2 -6 -4 4 224.68 13.1 5 4 -4 736.43 22.5 5 4 -4 755.42 22.8 5 4 -4 760.42 20.8 5 4 -4 722.03 23.4 5 4 -4 743.03 22 -5 -4 4 720.13 20.9 -5 -4 4 800.82 26.2 -5 -4 4 775.92 24.5 -5 -4 4 768.62 24.9 4 4 -4 571.64 18.9 4 4 -4 589.24 17.6 4 4 -4 573.64 15 4 4 -4 581.04 19.1 4 4 -4 553.14 16.4 4 4 -4 578.04 16.3 4 4 -4 572.44 16.5 4 4 -4 564.84 17.9 -4 -4 4 568.24 18.6 -4 -4 4 556.24 20.1 -4 -4 4 565.04 19.9 -4 -4 4 579.54 19.6 -4 -4 4 557.94 15.8 -4 -4 4 595.84 19 3 4 -4 445.36 13.9 3 4 -4 462.95 11.5 3 4 -4 447.86 16.6 3 4 -4 449.66 14.3 3 4 -4 440.96 12.5 3 4 -4 452.75 13.4 3 4 -4 445.66 15.2 3 4 -4 425.06 14.7 3 4 -4 447.96 14.5 3 4 -4 466.05 16.9 3 4 -4 433.76 14.9 -3 -4 4 443.26 13.3 -3 -4 4 462.85 14.8 -3 -4 4 442.26 11.8 -3 -4 4 450.85 14.8 -3 -4 4 450.85 15.8 -3 -4 4 449.86 16.5 2 4 -4 193.18 6.9 2 4 -4 190.98 8.3 2 4 -4 189.98 5.8 2 4 -4 199.28 8.4 2 4 -4 192.38 7.8 2 4 -4 201.98 8.6 2 4 -4 199.58 6.9 2 4 -4 197.28 5.3 2 4 -4 193.58 8.3 2 4 -4 191.48 9 -2 -4 4 195.58 7.6 -2 -4 4 194.08 9.3 -2 -4 4 202.98 8.2 -2 -4 4 200.48 7.2 1 4 -4 743.43 21.5 1 4 -4 756.62 21 1 4 -4 760.12 20.5 1 4 -4 760.52 18.3 1 4 -4 752.52 19.4 1 4 -4 748.23 16.9 1 4 -4 779.42 20.7 1 4 -4 721.73 20.1 -1 -4 4 754.92 20.5 -1 -4 4 763.62 21.1 -1 -4 4 759.22 21.9 -1 -4 4 777.02 18.9 -1 -4 4 754.72 19.5 -1 -4 4 746.63 20.7 0 4 -4 23.7 2.4 0 4 -4 28.5 2.6 0 4 -4 24.2 1.7 0 4 -4 27.8 2.5 0 4 -4 24.9 2.3 0 4 -4 23.9 1.5 0 4 -4 26.4 2.7 0 4 -4 25.4 2.4 0 -4 4 21 2.3 0 -4 4 26.7 1.5 0 -4 4 26 1.8 0 -4 4 25.8 2.3 0 -4 4 22.3 2.5 0 -4 4 26.1 2.2 -1 4 -4 3358.26 75.69 -1 4 -4 3549.04 79.29 -1 4 -4 3490.45 77.69 -1 4 -4 3404.26 77.79 -1 4 -4 3342.27 77.39 -1 4 -4 3667.03 77.69 1 -4 4 3362.56 77.89 1 -4 4 3382.46 76.79 1 -4 4 3536.75 78.19 -2 4 -4 227.28 9.8 -2 4 -4 233.28 7.8 -2 4 -4 234.08 7.4 -2 4 -4 213.58 7.7 -2 4 -4 230.28 8.1 -2 4 -4 224.28 8.8 -2 4 -4 226.18 7.1 2 -4 4 231.08 9 2 -4 4 230.58 8.1 2 -4 4 221.58 8.3 2 -4 4 225.28 7.6 2 -4 4 223.58 7.9 2 -4 4 231.68 8.3 2 -4 4 226.48 7.4 2 -4 4 227.58 7.1 -3 4 -4 179.68 5.5 -3 4 -4 163.58 9.1 -3 4 -4 167.58 6.4 -3 4 -4 173.78 8.4 -3 4 -4 176.78 6.8 -3 4 -4 170.68 7.1 -3 4 -4 173.38 7.5 3 -4 4 165.48 8 3 -4 4 171.78 6.4 3 -4 4 171.88 7.7 3 -4 4 175.48 7.2 3 -4 4 171.28 5.5 3 -4 4 186.58 6.3 3 -4 4 175.58 6.9 -4 4 -4 41.3 4.5 -4 4 -4 47.7 4.2 -4 4 -4 42.7 3.4 -4 4 -4 47 2 -4 4 -4 45.8 5.3 -4 4 -4 53.19 4.4 -4 4 -4 46.3 3.1 4 -4 4 44.9 2.1 4 -4 4 46.5 3.7 4 -4 4 44.5 2.7 4 -4 4 49.4 4.3 4 -4 4 41.6 4.3 4 -4 4 47.6 3.5 4 -4 4 40.4 4 4 -4 4 45 3.3 -5 4 -4 928.81 24 -5 4 -4 942.11 30.6 -5 4 -4 907.91 24.3 -5 4 -4 947.61 29.1 -5 4 -4 920.61 27.6 5 -4 4 908.51 25.8 5 -4 4 946.81 24.6 5 -4 4 936.61 25.2 5 -4 4 930.81 22.8 -6 4 -4 143.49 6.1 -6 4 -4 132.49 9.4 -6 4 -4 144.89 9 -6 4 -4 141.79 10.3 6 -4 4 154.38 8.1 6 -4 4 145.19 5.4 6 -4 4 142.89 7.4 6 -4 4 152.78 7.1 6 -4 4 136.09 4.6 -7 4 -4 56.29 6.9 -7 4 -4 61.59 11.4 -7 4 -4 67.19 7.5 -7 4 -4 62.69 3.9 7 -4 4 60.69 3.3 7 -4 4 61.49 5.4 7 -4 4 65.09 3 7 -4 4 63.19 4.8 7 -4 4 60.99 3 -8 4 -4 89.69 4.7 -8 4 -4 102.49 9.4 -8 4 -4 85.79 14.5 -8 4 -4 93.29 8.5 8 -4 4 82.39 4 8 -4 4 93.89 4.1 8 -4 4 89.89 6.8 8 -4 4 86.49 7 8 -4 4 88.69 4.1 -9 4 -4 141.39 11.5 -9 4 -4 146.09 11.9 -9 4 -4 141.89 6 -9 4 -4 157.88 11.6 9 -4 4 141.39 5.8 9 -4 4 136.69 5.6 9 -4 4 144.89 9.7 9 -4 4 147.59 8.5 9 -4 4 157.08 9.5 9 -4 4 142.99 5.3 -10 4 -4 182.88 14.4 -10 4 -4 192.18 13.6 -10 4 -4 199.78 13.7 10 -4 4 191.38 6.5 10 -4 4 185.68 6 10 -4 4 189.98 7.2 10 -4 4 207.38 10.5 10 -4 4 193.18 7 10 -4 4 206.38 12.2 10 -4 4 195.88 11.3 -11 4 -4 18 5.6 -11 4 -4 19.1 5.4 -11 4 -4 18.8 6 11 -4 4 14.9 2.7 11 -4 4 17.2 4.8 11 -4 4 25.1 4.9 11 -4 4 19.8 4.4 -12 4 -4 39.2 7.2 -12 4 -4 35.2 7.6 -12 4 -4 35.2 8.1 12 -4 4 39.6 6.9 12 -4 4 34.1 6.1 -13 4 -4 53.49 8.9 -13 4 -4 46.9 8.9 -13 4 -4 29 7.6 13 -4 4 60.19 7 13 -4 4 69.99 7.7 13 -4 4 59.09 7.5 12 3 -4 89.19 8.4 12 3 -4 76.49 6.2 12 3 -4 69.29 6.6 12 3 -4 71.89 8.3 12 3 -4 79.19 8.4 12 3 -4 80.29 8.5 -12 -3 4 85.29 10.3 -12 -3 4 83.19 16.6 -12 -3 4 85.59 11.7 11 3 -4 72.89 7.3 11 3 -4 56.19 6 11 3 -4 66.59 6 11 3 -4 59.89 6.4 11 3 -4 83.19 7.7 11 3 -4 79.09 7.8 11 3 -4 88.49 9 -11 -3 4 74.89 8.2 -11 -3 4 87.19 11.2 -11 -3 4 101.69 10.4 -11 -3 4 71.29 6.7 10 3 -4 67.29 7.1 10 3 -4 57.19 5.9 10 3 -4 68.39 7.4 10 3 -4 64.29 7.1 10 3 -4 68.99 5.8 -10 -3 4 71.09 6.2 -10 -3 4 85.89 8.2 -10 -3 4 78.69 9 -10 -3 4 81.69 10.3 9 3 -4 283.07 12.4 9 3 -4 269.97 13.9 9 3 -4 265.57 13.3 9 3 -4 260.17 13 9 3 -4 256.77 11.6 -9 -3 4 256.17 17.1 -9 -3 4 256.47 13.6 -9 -3 4 277.37 15.8 -9 -3 4 270.27 12.1 8 3 -4 37 4.6 8 3 -4 36.5 4.2 8 3 -4 37.9 5 8 3 -4 25.2 4.5 8 3 -4 41.9 4.2 -8 -3 4 37.2 7.6 -8 -3 4 40.6 6.9 -8 -3 4 42.8 4.6 -8 -3 4 36.1 5.4 -8 -3 4 41.3 6.7 7 3 -4 201.08 10.1 7 3 -4 200.98 9.3 7 3 -4 199.48 10.4 7 3 -4 192.38 9.2 -7 -3 4 195.68 11.5 -7 -3 4 207.68 10.3 -7 -3 4 200.08 9.3 -7 -3 4 203.18 11.8 -7 -3 4 194.68 12.8 6 3 -4 351.76 13 6 3 -4 354.86 13.6 6 3 -4 353.36 14.2 6 3 -4 365.76 15.4 6 3 -4 347.47 13 -6 -3 4 345.07 14.8 -6 -3 4 353.16 15.8 -6 -3 4 330.17 13 -6 -3 4 351.76 16.3 -6 -3 4 338.27 15 -6 -3 4 350.16 14.2 5 3 -4 276.97 11.2 5 3 -4 276.37 11.8 5 3 -4 305.37 11.2 5 3 -4 288.07 10.5 5 3 -4 272.57 11.1 5 3 -4 324.77 14.1 5 3 -4 291.77 10.8 5 3 -4 272.97 12 -5 -3 4 298.37 13.4 -5 -3 4 281.17 10.6 -5 -3 4 291.37 13.6 -5 -3 4 281.87 10.3 -5 -3 4 278.27 12.5 -5 -3 4 278.97 12.2 4 3 -4 33.7 3.6 4 3 -4 33.7 2.9 4 3 -4 30.4 3 4 3 -4 31.3 3.4 4 3 -4 31.9 3.4 4 3 -4 33 3.5 4 3 -4 29.6 2.6 4 3 -4 30.7 3.1 4 3 -4 32.7 2.9 -4 -3 4 29.9 3.2 -4 -3 4 30.6 2.8 -4 -3 4 34.6 4.2 -4 -3 4 32.5 3.5 -4 -3 4 31.6 3.8 -4 -3 4 36.6 4.2 3 3 -4 1450.35 37.7 3 3 -4 1442.06 36.9 3 3 -4 1411.76 36.6 3 3 -4 1482.55 35.1 3 3 -4 1470.15 35.4 3 3 -4 1467.35 35.6 3 3 -4 1375.56 38.5 3 3 -4 1446.66 34.5 3 3 -4 1430.36 33.2 3 3 -4 1466.25 37 3 3 -4 1448.66 35.9 -3 -3 4 1427.86 37.1 -3 -3 4 1443.46 38 -3 -3 4 1424.16 37.1 -3 -3 4 1441.36 36.5 -3 -3 4 1403.06 33.6 -3 -3 4 1463.45 35.1 -3 -3 4 1447.66 35.9 2 3 -4 24.2 1.7 2 3 -4 18.4 2.2 2 3 -4 25.8 1.5 2 3 -4 23.8 2.4 2 3 -4 24.9 2.7 2 3 -4 25.7 2.7 2 3 -4 26.1 2.1 2 3 -4 24.3 2.5 2 3 -4 26 2.9 2 3 -4 23.8 2.1 -2 -3 4 19.4 2.5 -2 -3 4 22.7 2.8 -2 -3 4 24.4 2.2 -2 -3 4 25.2 2.2 -2 -3 4 27.8 2.6 1 3 -4 164.88 4.8 1 3 -4 167.98 6 1 3 -4 156.28 8.4 1 3 -4 162.28 4.7 1 3 -4 162.78 6.3 1 3 -4 171.38 6.6 1 3 -4 170.38 7.1 1 3 -4 160.18 6.8 -1 -3 4 154.88 7.4 -1 -3 4 164.28 6.1 -1 -3 4 163.08 5.1 -1 -3 4 159.88 6.4 -1 -3 4 164.28 4.6 -1 -3 4 168.08 6.7 0 3 -4 2564.44 56.59 0 3 -4 2469.65 57.59 0 3 -4 2509.65 55.39 0 3 -4 2507.95 56.79 0 3 -4 2475.05 56.69 0 3 -4 2485.85 54.29 0 3 -4 2506.35 56.89 0 -3 4 2514.55 55.19 0 -3 4 2577.44 56.89 0 -3 4 2435.86 56.69 0 -3 4 2478.35 56.99 0 -3 4 2525.35 54.49 0 -3 4 2566.94 57.19 0 -3 4 2413.36 57.59 -1 3 -4 192.88 5.4 -1 3 -4 188.98 6.6 -1 3 -4 187.88 6.7 -1 3 -4 197.58 6.7 -1 3 -4 186.28 7.2 -1 3 -4 188.18 6.3 -1 3 -4 189.38 6.4 1 -3 4 185.88 6.7 1 -3 4 186.58 6.8 1 -3 4 186.98 6.3 1 -3 4 194.48 6.5 1 -3 4 182.88 5.3 1 -3 4 179.98 5.9 1 -3 4 176.98 6.5 1 -3 4 185.58 6.7 -2 3 -4 634.14 18.7 -2 3 -4 630.84 17.1 -2 3 -4 627.54 16 -2 3 -4 638.24 16.8 -2 3 -4 648.64 16.1 -2 3 -4 665.33 16.7 -2 3 -4 625.34 18.1 2 -3 4 625.04 15.9 2 -3 4 655.63 17.8 2 -3 4 628.94 17.3 2 -3 4 629.54 15.9 2 -3 4 607.84 17.4 2 -3 4 628.74 16.1 -3 3 -4 55.19 4 -3 3 -4 48.8 4.5 -3 3 -4 52.89 2.9 -3 3 -4 51.59 4.3 -3 3 -4 52.29 2.6 -3 3 -4 50.99 4 -3 3 -4 53.59 3.1 3 -3 4 54.59 2.7 3 -3 4 58.39 4.2 3 -3 4 52.19 3.1 3 -3 4 57.69 2.7 3 -3 4 54.89 3.5 3 -3 4 49.1 3.4 3 -3 4 58.19 4.3 -4 3 -4 39 5.6 -4 3 -4 33.9 3.7 -4 3 -4 32.1 4 -4 3 -4 36.2 2.6 -4 3 -4 36.1 2.8 -4 3 -4 35 2 -4 3 -4 33.4 3.1 4 -3 4 34.3 2.2 4 -3 4 40.4 4 4 -3 4 34.3 2.8 4 -3 4 36.1 3.8 4 -3 4 32.9 1.9 4 -3 4 33 2.8 4 -3 4 32.4 3.6 4 -3 4 40.3 3.5 -5 3 -4 6.4 2.3 -5 3 -4 4.3 2.4 -5 3 -4 3.2 1.9 -5 3 -4 5.7 1.1 5 -3 4 2 1.3 5 -3 4 2.6 1.1 5 -3 4 5.6 0.9 5 -3 4 3.5 1.3 5 -3 4 3.2 1 5 -3 4 2.1 1.8 -6 3 -4 65.19 3.2 -6 3 -4 70.39 6.8 -6 3 -4 64.09 6.8 -6 3 -4 66.79 3.4 -6 3 -4 69.69 6.2 6 -3 4 61.79 4.7 6 -3 4 67.49 4.6 6 -3 4 68.09 5.4 6 -3 4 61.99 3.4 6 -3 4 72.19 2.9 -7 3 -4 31.4 2.2 -7 3 -4 44.2 7.1 -7 3 -4 22.1 6 -7 3 -4 23.8 5.1 -7 3 -4 31 2.5 7 -3 4 32.8 3.6 7 -3 4 26.3 4.2 7 -3 4 28.1 1.8 7 -3 4 27.5 2.8 7 -3 4 31.2 2.8 -8 3 -4 4.1 0.9 -8 3 -4 0.6 2.6 -8 3 -4 3.5 3.7 -8 3 -4 5.4 3.3 -8 3 -4 0.4 1.1 8 -3 4 3.2 0.8 8 -3 4 5.1 1.6 8 -3 4 2.3 2.1 8 -3 4 3.5 2.2 8 -3 4 -1.3 1.6 8 -3 4 3.8 1.8 8 -3 4 2.4 0.9 -9 3 -4 93.29 10.1 -9 3 -4 119.69 9.8 -9 3 -4 111.19 10.1 9 -3 4 100.39 6.9 9 -3 4 96.49 5.5 9 -3 4 100.59 7.8 9 -3 4 105.39 7.2 9 -3 4 109.29 8.4 -10 3 -4 59.79 7.1 -10 3 -4 42.1 8 -10 3 -4 45 7.8 10 -3 4 51.59 4.4 10 -3 4 59.89 6.7 10 -3 4 62.59 4.8 10 -3 4 51.29 6 10 -3 4 52.59 5.7 -11 3 -4 0.9 3.1 -11 3 -4 6.4 3.8 -11 3 -4 5.4 4.1 11 -3 4 -0.8 1.8 11 -3 4 5.9 2.6 11 -3 4 2.5 3 11 -3 4 5.2 2.7 -12 3 -4 10.6 4.6 -12 3 -4 15.3 6.3 -12 3 -4 18.1 6.1 12 -3 4 15.4 3.2 12 -3 4 17.2 4.7 12 -3 4 19.9 4.9 12 -3 4 19.3 4.4 12 2 -4 9.5 4.3 12 2 -4 10.9 3.8 12 2 -4 15.8 3.6 12 2 -4 7.6 2.7 12 2 -4 10.6 4.4 12 2 -4 12.3 3.8 12 2 -4 7.4 3.4 -12 -2 4 5.3 4 -12 -2 4 8.8 8.8 -12 -2 4 11.1 3.5 -12 -2 4 7.4 4.8 11 2 -4 0.4 1.9 11 2 -4 -3.7 1.6 11 2 -4 1.8 2.7 11 2 -4 -2.6 2.4 11 2 -4 -2.3 2.4 11 2 -4 -4.4 1.6 11 2 -4 2.6 2.6 -11 -2 4 0.1 3.5 -11 -2 4 4.2 3.5 -11 -2 4 -1.1 2 -11 -2 4 3.1 4.2 10 2 -4 114.89 8.5 10 2 -4 111.59 7.9 10 2 -4 115.79 9.2 10 2 -4 118.09 8.6 10 2 -4 107.89 10.5 10 2 -4 111.39 8.3 -10 -2 4 116.69 9.3 -10 -2 4 123.09 11.9 -10 -2 4 106.29 10.2 -10 -2 4 113.29 8 9 2 -4 8.3 3 9 2 -4 7.9 2.1 9 2 -4 6.8 2.5 9 2 -4 4 2.5 9 2 -4 5.9 2.5 9 2 -4 9.9 3.5 -9 -2 4 11.7 4.7 -9 -2 4 7.2 3.6 -9 -2 4 9.3 4 -9 -2 4 7.8 2.8 8 2 -4 2.4 1.5 8 2 -4 2.5 2.2 8 2 -4 3.3 1.9 8 2 -4 2.8 2 8 2 -4 4 2.5 -8 -2 4 3.7 2.3 -8 -2 4 3.1 1.7 -8 -2 4 1.9 2.5 -8 -2 4 0.3 2.5 -8 -2 4 1.1 2.8 7 2 -4 391.26 15 7 2 -4 358.46 13.9 7 2 -4 372.36 14 7 2 -4 368.46 14.6 7 2 -4 376.76 14.2 -7 -2 4 378.86 16.4 -7 -2 4 377.16 15.8 -7 -2 4 365.46 17.5 -7 -2 4 370.16 14 -7 -2 4 359.76 14.8 -7 -2 4 378.36 14.3 6 2 -4 385.86 14 6 2 -4 373.16 13.7 6 2 -4 388.66 14.5 6 2 -4 382.46 13.8 6 2 -4 370.46 13.9 6 2 -4 385.96 13.8 -6 -2 4 379.96 13.7 -6 -2 4 360.46 14.8 -6 -2 4 378.76 15.7 -6 -2 4 379.76 14.1 -6 -2 4 410.06 17.1 -6 -2 4 359.46 13.9 -6 -2 4 402.76 15.8 5 2 -4 3.6 1.8 5 2 -4 3.2 1 5 2 -4 3.2 1.4 5 2 -4 4.5 1.8 5 2 -4 3.8 1.8 -5 -2 4 1.8 1.9 -5 -2 4 5.3 2.2 -5 -2 4 2.5 1.5 -5 -2 4 3.3 1.6 -5 -2 4 5.4 1.7 -5 -2 4 4.4 1.8 4 2 -4 297.67 10.5 4 2 -4 298.77 9.5 4 2 -4 282.77 11.1 4 2 -4 296.07 10.5 4 2 -4 289.37 11.6 4 2 -4 296.37 11.4 4 2 -4 295.67 11.4 4 2 -4 312.27 11.6 4 2 -4 293.77 11.7 4 2 -4 299.77 10.9 4 2 -4 308.87 11 -4 -2 4 288.17 11 -4 -2 4 309.27 11.4 -4 -2 4 302.27 10.3 -4 -2 4 300.87 10.5 -4 -2 4 309.37 11.8 -4 -2 4 304.47 12.2 -4 -2 4 300.47 12.2 3 2 -4 1984.8 47.8 3 2 -4 1909.81 46.8 3 2 -4 1980.3 46.2 3 2 -4 1939.21 44.5 3 2 -4 2009.7 45.9 3 2 -4 1989.4 46.9 3 2 -4 1920.41 46.3 3 2 -4 1938.41 46.6 -3 -2 4 1952.8 46.3 -3 -2 4 2048.1 51.09 -3 -2 4 1980.7 47.5 -3 -2 4 1980.6 46.2 -3 -2 4 1945.21 47.2 -3 -2 4 1838.12 49.2 -3 -2 4 1895.41 45.1 -3 -2 4 1956.4 48.1 2 2 -4 30.6 2.6 2 2 -4 36.1 2.6 2 2 -4 41.3 2.2 2 2 -4 39.4 2.3 2 2 -4 32.6 2.5 2 2 -4 37.6 3.2 2 2 -4 39.7 2.5 2 2 -4 37.7 2.7 2 2 -4 37.1 3.1 -2 -2 4 33.6 3.8 -2 -2 4 35.5 2.7 -2 -2 4 38.5 2.7 -2 -2 4 41.3 2.5 -2 -2 4 36.4 2.9 -2 -2 4 36 2 -2 -2 4 36.4 2.9 1 2 -4 2623.34 59.89 1 2 -4 2605.14 59.29 1 2 -4 2633.04 58.79 1 2 -4 2623.34 57.29 1 2 -4 2633.24 56.49 1 2 -4 2549.34 59.79 1 2 -4 2591.04 58.59 1 2 -4 2638.04 57.99 -1 -2 4 2593.44 57.29 -1 -2 4 2593.14 59.49 -1 -2 4 2581.64 58.99 -1 -2 4 2589.14 59.49 -1 -2 4 2609.14 58.89 -1 -2 4 2598.74 58.19 -1 -2 4 2524.05 59.89 -1 -2 4 2558.84 56.39 0 2 -4 2.6 0.8 0 2 -4 2 0.9 0 2 -4 1.2 0.7 0 2 -4 2.6 0.8 0 2 -4 1.9 0.3 0 2 -4 3.1 0.8 0 2 -4 1.6 0.6 0 2 -4 1.8 0.9 0 -2 4 1.8 0.6 0 -2 4 2.1 0.6 0 -2 4 1.9 0.7 0 -2 4 2.1 0.2 0 -2 4 3.2 1.1 0 -2 4 2.3 0.8 0 -2 4 4.4 1 0 -2 4 1.2 0.9 -1 2 -4 2152.48 48.5 -1 2 -4 2090.09 49.3 -1 2 -4 2261.27 49.1 -1 2 -4 2170.28 49.5 -1 2 -4 2155.38 48.5 -1 2 -4 2145.29 49.1 -1 2 -4 2188.58 48.9 -1 2 -4 2173.58 48.6 1 -2 4 2198.68 49.2 1 -2 4 2145.19 48.7 1 -2 4 2150.48 49.3 1 -2 4 2202.18 48.7 1 -2 4 2104.29 48.5 1 -2 4 2119.49 49.2 1 -2 4 2151.28 49 -2 2 -4 2371.26 52.69 -2 2 -4 2354.66 55.89 -2 2 -4 2480.95 53.59 -2 2 -4 2314.67 55.59 -2 2 -4 2391.86 55.29 -2 2 -4 2400.36 54.29 -2 2 -4 2422.66 53.99 2 -2 4 2384.56 55.19 2 -2 4 2347.57 55.19 2 -2 4 2401.56 53.79 2 -2 4 2404.86 54.39 2 -2 4 2461.25 52.99 2 -2 4 2331.97 54.19 2 -2 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174.38 8.1 5 1 -4 169.78 8.3 5 1 -4 171.28 8.8 5 1 -4 190.18 7.7 5 1 -4 185.58 8.5 5 1 -4 186.38 10 5 1 -4 182.08 9.1 -5 -1 4 194.38 10.5 -5 -1 4 181.38 8.7 -5 -1 4 179.88 9.4 -5 -1 4 167.08 8.3 -5 -1 4 177.28 8.2 4 1 -4 52.89 4 4 1 -4 58.49 4.7 4 1 -4 50.99 4.1 4 1 -4 50.79 3.2 4 1 -4 49.3 4 4 1 -4 51.79 4 4 1 -4 45.7 5.6 4 1 -4 50.19 4 4 1 -4 54.49 4.1 4 1 -4 56.69 4 4 1 -4 56.29 3.4 -4 -1 4 47.6 4 -4 -1 4 51.19 4 -4 -1 4 49 4.3 -4 -1 4 47.1 3.8 -4 -1 4 51.19 3.7 -4 -1 4 51.09 4.2 -4 -1 4 55.29 4 3 1 -4 306.77 10.4 3 1 -4 309.97 10.2 3 1 -4 316.47 10.4 3 1 -4 320.27 10.4 3 1 -4 318.67 11.1 3 1 -4 299.07 10.8 3 1 -4 308.57 10.4 3 1 -4 312.37 9 3 1 -4 314.37 10.3 3 1 -4 335.67 11.5 3 1 -4 323.27 9.5 -3 -1 4 305.17 10.4 -3 -1 4 303.07 10.7 -3 -1 4 319.37 10 -3 -1 4 294.67 11 -3 -1 4 309.77 11.1 -3 -1 4 306.77 10.5 -3 -1 4 307.27 10.1 2 1 -4 107.69 4.9 2 1 -4 118.19 4.6 2 1 -4 108.09 4.6 2 1 -4 97.99 4.1 2 1 -4 101.79 4.1 2 1 -4 102.69 5.2 2 1 -4 103.49 5.3 2 1 -4 105.79 3.6 2 1 -4 108.79 4.9 2 1 -4 100.29 4.2 -2 -1 4 105.69 4.1 -2 -1 4 110.89 5 -2 -1 4 101.99 4.4 -2 -1 4 106.99 4.1 -2 -1 4 100.39 5.3 -2 -1 4 112.99 4.9 1 1 -4 1915.91 41 1 1 -4 1904.41 43.5 1 1 -4 1894.01 44.3 1 1 -4 1815.22 43.3 1 1 -4 1854.11 41.6 1 1 -4 1944.51 42.7 1 1 -4 1915.61 42.5 1 1 -4 1821.92 43.9 -1 -1 4 1907.91 42.4 -1 -1 4 1878.81 44.2 -1 -1 4 1880.01 42.8 -1 -1 4 1823.12 41.7 -1 -1 4 1887.11 43.5 -1 -1 4 1890.71 44.2 -1 -1 4 1846.72 41 0 1 -4 223.88 6.7 0 1 -4 209.88 5.8 0 1 -4 212.58 7 0 1 -4 210.18 7.2 0 1 -4 210.48 6.6 0 1 -4 210.58 7.2 0 -1 4 208.68 5.6 0 -1 4 208.58 6.6 0 -1 4 209.48 6.5 0 -1 4 225.38 5.8 0 -1 4 213.38 7 0 -1 4 216.88 7.2 0 -1 4 206.18 7.3 -1 1 -4 352.36 10.5 -1 1 -4 357.56 9.6 -1 1 -4 375.56 10.4 -1 1 -4 359.66 9.6 -1 1 -4 362.86 10.1 -1 1 -4 366.06 9.9 -1 1 -4 354.76 10.4 -1 1 -4 353.86 9.9 1 -1 4 348.77 10 1 -1 4 361.36 10.3 1 -1 4 349.37 9.5 1 -1 4 356.06 10.1 1 -1 4 346.67 10.1 1 -1 4 351.36 10.4 1 -1 4 371.96 9.8 -2 1 -4 260.27 8 -2 1 -4 242.48 6.5 -2 1 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29.3 -7 1 -4 787.42 28.7 -7 1 -4 807.32 26 7 -1 4 801.32 27.3 7 -1 4 806.82 25.6 -8 1 -4 919.41 29 -8 1 -4 888.01 32.5 -8 1 -4 879.61 32.5 8 -1 4 898.91 28.9 8 -1 4 891.71 25.1 8 -1 4 955.7 27.4 -9 1 -4 27.4 5.1 -9 1 -4 28.5 6.3 -9 1 -4 33.5 6.9 9 -1 4 18.9 4 9 -1 4 29.5 5.7 9 -1 4 30.5 4.2 -10 1 -4 265.67 17.1 -10 1 -4 296.87 18.4 -10 1 -4 262.17 17.7 10 -1 4 283.07 15.1 10 -1 4 266.67 13.2 10 -1 4 275.37 11.8 -11 1 -4 68.59 7.2 -11 1 -4 69.09 10.8 -11 1 -4 65.59 11.2 11 -1 4 71.09 7.1 11 -1 4 74.99 6.9 11 -1 4 72.89 8 -12 1 -4 -3.4 2.6 -12 1 -4 -4.2 2.4 -12 1 -4 0.3 4 12 -1 4 -4.9 2.5 12 -1 4 0 2.4 12 -1 4 -5.9 2 12 -1 4 -0.4 2.3 13 0 -4 3.9 2.9 13 0 -4 -4.6 2.1 13 0 -4 2.7 2.8 13 0 -4 -3.3 2.7 13 0 -4 7.1 3 13 0 -4 -1 2.6 -13 0 4 3.2 3 -13 0 4 4.2 4.1 -13 0 4 -3.4 3.3 12 0 -4 11.9 3.6 12 0 -4 17.3 4.4 12 0 -4 8.1 3 12 0 -4 10.6 3.7 12 0 -4 14.7 4 12 0 -4 10.7 3.9 12 0 -4 16.7 5.3 -12 0 4 10.6 4.6 -12 0 4 12.2 3.8 -12 0 4 14.4 4.9 11 0 -4 21 4.4 11 0 -4 14.4 3.8 11 0 -4 19.7 4.8 11 0 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358.76 15.2 3 -9 5 366.56 13.5 3 -9 5 355.16 12.7 3 -9 5 362.16 13.5 -4 9 -5 122.99 8.9 -4 9 -5 113.69 7.5 -4 9 -5 119.69 6.1 -4 9 -5 116.89 5.6 4 -9 5 118.49 6.9 4 -9 5 118.79 6.6 4 -9 5 130.29 8.7 -5 9 -5 67.99 7 -5 9 -5 70.59 3.8 -5 9 -5 63.89 6.1 -5 9 -5 68.39 3.5 -5 9 -5 56.69 8.8 5 -9 5 78.69 5.4 5 -9 5 70.59 6.7 5 -9 5 61.39 4.8 -6 9 -5 191.98 13.5 -6 9 -5 225.88 12.4 -6 9 -5 215.28 15.4 6 -9 5 211.78 9.6 6 -9 5 216.28 11.8 6 -9 5 202.38 9.8 -7 9 -5 16.9 4.1 -7 9 -5 10.3 4.8 -7 9 -5 14.3 4.1 7 -9 5 14.9 3.3 7 -9 5 13.7 3 7 -9 5 19.9 4.3 -8 9 -5 64.79 10.7 -8 9 -5 89.59 7.6 -8 9 -5 106.69 9.7 8 -9 5 79.49 7.8 8 -9 5 87.59 6.5 8 -9 5 85.79 6.6 -9 9 -5 3.7 4.7 -9 9 -5 1.5 3 -9 9 -5 -0.6 2.2 9 -9 5 0.9 2.1 9 -9 5 -0.9 2.8 9 -9 5 -2.4 1.6 -10 9 -5 12.9 8.4 -10 9 -5 24.8 4.5 10 -9 5 21.4 4.8 10 -9 5 20.9 4.3 10 -9 5 24.8 5.6 -11 9 -5 19.6 4.1 -11 9 -5 13.7 5.3 -11 9 -5 10.8 6 11 -9 5 16.5 4.3 11 -9 5 14.6 4.1 11 -9 5 15.1 4.7 -12 9 -5 1.2 3.6 -12 9 -5 2.8 3.3 -12 9 -5 -5.8 4 12 -9 5 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17.7 -5 -8 5 387.26 18.5 4 8 -5 339.37 11.9 4 8 -5 331.57 15.3 4 8 -5 358.86 11.9 4 8 -5 335.47 14.1 -4 -8 5 333.07 16.9 -4 -8 5 351.06 16.6 -4 -8 5 327.17 11.6 -4 -8 5 359.56 15.8 3 8 -5 4.1 2.3 3 8 -5 4.6 1.9 3 8 -5 5.8 2.1 -3 -8 5 5.3 2.3 -3 -8 5 6.9 1.7 -3 -8 5 1.8 1.9 -3 -8 5 2.2 2.5 2 8 -5 592.14 18.2 2 8 -5 617.64 20.9 2 8 -5 616.64 18.9 2 8 -5 594.04 19.9 -2 -8 5 604.24 21.8 -2 -8 5 620.64 19.9 -2 -8 5 575.34 17.5 -2 -8 5 584.94 21.6 1 8 -5 172.68 7.4 1 8 -5 171.88 9 1 8 -5 179.08 9.1 1 8 -5 164.38 9 -1 -8 5 163.98 9.6 -1 -8 5 183.48 7.8 -1 -8 5 171.28 8.2 -1 -8 5 170.98 9.9 0 8 -5 35.5 4.4 0 8 -5 33.6 3.9 0 8 -5 34.6 3.8 0 8 -5 32.2 2.9 0 -8 5 32.5 4.3 0 -8 5 38.9 3.7 0 -8 5 32.6 4.3 -1 8 -5 1027.1 29.2 -1 8 -5 983.5 30.6 -1 8 -5 1002.9 24.8 -1 8 -5 1021.8 27.9 -1 8 -5 998 25.7 1 -8 5 1042.5 26.8 1 -8 5 1029.7 25 1 -8 5 1013.7 28.8 1 -8 5 994.1 29.6 -2 8 -5 1870.91 46.3 -2 8 -5 1919.11 46.7 -2 8 -5 2008.7 52.79 -2 8 -5 1899.41 45.6 -2 8 -5 1998.4 49.5 -2 8 -5 1909.61 48 2 -8 5 1848.92 47.7 2 -8 5 1802.62 48.9 2 -8 5 2060.39 46.6 -3 8 -5 20.2 3.5 -3 8 -5 17.3 4.9 -3 8 -5 18.9 2.6 -3 8 -5 16.1 3.4 -3 8 -5 15.5 2.5 3 -8 5 14.6 3.6 3 -8 5 16.1 2.9 3 -8 5 17.9 2.7 3 -8 5 20.3 3.2 -4 8 -5 840.52 21.5 -4 8 -5 824.52 30.6 -4 8 -5 843.92 22.2 -4 8 -5 890.21 26.8 -4 8 -5 864.11 26.3 4 -8 5 846.52 25.9 4 -8 5 853.51 23.6 4 -8 5 833.32 23.7 -5 8 -5 270.67 8.1 -5 8 -5 282.37 13.5 -5 8 -5 267.47 19.6 -5 8 -5 278.57 7.8 -5 8 -5 276.27 13.2 5 -8 5 318.97 19.6 5 -8 5 283.07 11.1 5 -8 5 312.77 11.4 -6 8 -5 60.79 9.5 -6 8 -5 73.59 7.2 -6 8 -5 71.99 7.2 6 -8 5 76.29 6.7 6 -8 5 71.29 5.4 6 -8 5 83.19 5.6 -7 8 -5 520.75 25.4 -7 8 -5 502.45 21.8 -7 8 -5 517.35 19.2 7 -8 5 528.95 17.5 7 -8 5 534.75 18.2 7 -8 5 511.15 19.5 -8 8 -5 205.08 10.9 -8 8 -5 209.58 16 -8 8 -5 208.78 13.7 8 -8 5 207.78 11.8 8 -8 5 205.38 10.4 8 -8 5 200.18 10.1 -9 8 -5 0.5 3.8 -9 8 -5 1.1 2.8 -9 8 -5 5.6 2.7 9 -8 5 2.4 2.4 9 -8 5 6.5 2.7 9 -8 5 0.8 2.5 -10 8 -5 67.19 6 -10 8 -5 56.19 9.3 -10 8 -5 68.89 11.1 10 -8 5 66.89 6.6 10 -8 5 61.89 6.4 10 -8 5 73.79 8.9 -11 8 -5 5.3 2.5 -11 8 -5 -3.2 3.1 -11 8 -5 1.5 4.9 11 -8 5 4.8 3.1 11 -8 5 1.5 3.1 11 -8 5 4.1 2.9 -12 8 -5 0.4 3.8 -12 8 -5 -1.3 4.6 -12 8 -5 -0.4 2.7 12 -8 5 -0.8 2.9 12 -8 5 3 2.3 12 -8 5 -6.4 2.5 10 7 -5 2.8 3.2 10 7 -5 4 2.6 10 7 -5 -0.7 3.2 10 7 -5 2.7 1.8 10 7 -5 7.2 3.9 10 7 -5 2.7 2 -10 -7 5 8.4 4.4 -10 -7 5 7.5 5.5 -10 -7 5 0.5 3 9 7 -5 -1.2 1.4 9 7 -5 0.1 1.2 9 7 -5 -2.7 2.2 9 7 -5 2.5 2.9 9 7 -5 1.5 2.4 -9 -7 5 6.4 3.9 -9 -7 5 4.1 4.2 -9 -7 5 2.8 4.4 -9 -7 5 -0.4 1.9 8 7 -5 86.79 8.3 8 7 -5 90.99 5.2 8 7 -5 89.89 8.6 8 7 -5 80.49 6.5 8 7 -5 90.69 5.4 8 7 -5 83.29 7.1 -8 -7 5 80.09 10.1 -8 -7 5 81.59 6.1 -8 -7 5 76.29 8.7 -8 -7 5 92.79 9.5 7 7 -5 20.4 4.1 7 7 -5 17.6 3.2 7 7 -5 17.2 2.5 7 7 -5 10.5 3.3 7 7 -5 20.2 3 7 7 -5 19.4 4.4 -7 -7 5 33.6 6.7 -7 -7 5 24.1 6.3 -7 -7 5 23.8 5.6 6 7 -5 60.99 6.1 6 7 -5 50.89 4.3 6 7 -5 57.99 3.5 6 7 -5 50.39 3.7 6 7 -5 58.79 6.4 6 7 -5 50.79 5.2 6 7 -5 50.19 3.7 -6 -7 5 50.39 10.8 -6 -7 5 45.4 7 -6 -7 5 59.39 9.2 -6 -7 5 49 3.7 5 7 -5 233.68 11.7 5 7 -5 241.28 15.9 5 7 -5 217.88 12.1 5 7 -5 235.68 8.7 5 7 -5 221.98 9.1 5 7 -5 223.08 7.6 5 7 -5 226.58 7.2 -5 -7 5 238.78 12.8 -5 -7 5 233.58 13.9 -5 -7 5 219.58 7.5 -5 -7 5 231.58 13.2 4 7 -5 90.49 5.2 4 7 -5 93.29 5 4 7 -5 92.19 6.4 4 7 -5 93.99 3.4 4 7 -5 94.69 7.2 4 7 -5 88.89 3.1 -4 -7 5 92.69 7.3 -4 -7 5 78.89 9.2 -4 -7 5 87.79 5.1 -4 -7 5 80.89 7.5 3 7 -5 163.28 7.7 3 7 -5 162.18 9.2 3 7 -5 169.98 7.2 3 7 -5 161.38 8.5 -3 -7 5 164.98 10.2 -3 -7 5 169.78 10.2 -3 -7 5 163.68 8.8 -3 -7 5 160.28 7.2 2 7 -5 1219.28 31.4 2 7 -5 1273.67 33.8 2 7 -5 1263.97 32 2 7 -5 1255.97 34.8 -2 -7 5 1235.28 35.8 -2 -7 5 1249.07 35.6 -2 -7 5 1247.38 33.1 -2 -7 5 1217.28 31.5 1 7 -5 734.33 22.6 1 7 -5 740.43 22.1 1 7 -5 727.93 19.7 1 7 -5 709.73 21.4 -1 -7 5 711.33 23.1 -1 -7 5 743.23 20.6 -1 -7 5 772.82 23.7 -1 -7 5 759.72 20.8 0 7 -5 1207.58 32 0 7 -5 1175.08 28.9 0 7 -5 1182.08 26.9 0 -7 5 1191.18 33.7 0 -7 5 1214.18 29.9 0 -7 5 1214.38 26.6 0 -7 5 1215.88 30.8 0 -7 5 1172.68 32.7 0 -7 5 1172.68 32.5 0 -7 5 1150.28 26.4 -1 7 -5 1287.27 35.1 -1 7 -5 1216.78 32.1 -1 7 -5 1218.08 30.1 -1 7 -5 1264.47 33.1 -1 7 -5 1190.48 33 -1 7 -5 1240.78 30 1 -7 5 1259.07 29.8 1 -7 5 1209.78 32.7 1 -7 5 1220.28 33.6 1 -7 5 1388.56 35.2 1 -7 5 1227.38 30.6 1 -7 5 1185.38 33.5 -2 7 -5 488.15 14.2 -2 7 -5 496.75 15.8 -2 7 -5 534.95 19.4 -2 7 -5 494.45 15.4 -2 7 -5 493.25 15.1 -2 7 -5 526.25 16.9 -2 7 -5 513.95 15.7 2 -7 5 488.25 16.9 2 -7 5 488.55 14.5 2 -7 5 523.85 15.4 2 -7 5 504.55 16 -3 7 -5 1200.08 29.8 -3 7 -5 1188.08 30.2 -3 7 -5 1197.28 32.2 -3 7 -5 1186.68 29 -3 7 -5 1176.68 29.5 -3 7 -5 1173.78 36.1 -3 7 -5 1150.28 31.9 3 -7 5 1176.18 30.5 3 -7 5 1166.88 29.6 3 -7 5 1148.79 31.3 3 -7 5 1177.98 31.3 3 -7 5 1174.88 32.2 -4 7 -5 1283.47 35.9 -4 7 -5 1285.37 30.6 -4 7 -5 1299.87 30.1 -4 7 -5 1280.97 34.8 -4 7 -5 1220.78 39.4 4 -7 5 1285.27 32.4 4 -7 5 1286.27 34.7 4 -7 5 1268.07 32.8 -5 7 -5 58.09 5.8 -5 7 -5 64.29 7.9 -5 7 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5 6.9 3.7 10 6 -5 -2.9 1.3 10 6 -5 -2.7 1.6 10 6 -5 -1.7 2.3 10 6 -5 -2.5 2.5 10 6 -5 -0.7 1.4 -10 -6 5 -3.7 2.2 -10 -6 5 1.6 3.9 -10 -6 5 2.3 4.8 9 6 -5 12.9 3.4 9 6 -5 18.6 4.7 9 6 -5 19.8 3 9 6 -5 17.6 4.8 -9 -6 5 19.6 4 -9 -6 5 6.8 4.5 -9 -6 5 14.5 6.6 8 6 -5 82.39 6.7 8 6 -5 81.89 8 8 6 -5 96.19 8 8 6 -5 84.69 5.5 8 6 -5 85.59 5.3 -8 -6 5 90.79 9 -8 -6 5 88.19 9.2 -8 -6 5 82.59 6.4 -8 -6 5 84.69 10.1 7 6 -5 0.8 1.9 7 6 -5 -2.3 1.6 7 6 -5 4.3 2.4 7 6 -5 2.6 1.2 7 6 -5 0.5 1.5 7 6 -5 0.8 1.1 -7 -6 5 2.1 3.1 -7 -6 5 2.8 3.1 -7 -6 5 3.2 3.3 -7 -6 5 4 1.7 6 6 -5 10 3.1 6 6 -5 10.5 2.2 6 6 -5 13.6 2.1 6 6 -5 14.5 3.4 6 6 -5 17.2 3.2 6 6 -5 12.8 2.8 6 6 -5 17.8 3.2 -6 -6 5 18.7 4.8 -6 -6 5 15.4 4.1 -6 -6 5 15 4.2 -6 -6 5 11 2.2 5 6 -5 198.58 10.8 5 6 -5 201.68 7.8 5 6 -5 182.18 8.8 5 6 -5 201.48 8 5 6 -5 201.98 8.5 5 6 -5 199.68 9.5 -5 -6 5 183.28 7.1 -5 -6 5 181.98 11.2 -5 -6 5 194.18 12.5 -5 -6 5 197.38 10.8 4 6 -5 1.8 1 4 6 -5 0.7 1.5 4 6 -5 0 0.9 4 6 -5 1.7 1.2 4 6 -5 0.6 0.8 4 6 -5 0.5 0.6 4 6 -5 -0.9 1.3 -4 -6 5 0.1 1 -4 -6 5 -0.2 1.3 -4 -6 5 0.8 2 -4 -6 5 0.3 0.6 -4 -6 5 6 2.3 3 6 -5 184.78 5 3 6 -5 188.38 8.8 3 6 -5 185.78 7.9 3 6 -5 194.88 9.8 3 6 -5 181.78 5.2 3 6 -5 194.78 7.5 -3 -6 5 185.28 10.1 -3 -6 5 180.38 10.7 -3 -6 5 188.18 10.2 -3 -6 5 183.38 9 -3 -6 5 183.58 7.9 2 6 -5 281.87 10.9 2 6 -5 261.27 9.1 2 6 -5 256.47 9.3 2 6 -5 263.67 11.4 -2 -6 5 279.77 11.9 -2 -6 5 262.97 12.5 -2 -6 5 273.27 10.2 -2 -6 5 252.57 11.6 -2 -6 5 246.78 10.7 1 6 -5 4 1.5 1 6 -5 6 1.8 1 6 -5 4.8 1.2 1 6 -5 5.8 1.6 -1 -6 5 3 1.2 -1 -6 5 6 2 -1 -6 5 3.4 1.6 -1 -6 5 3.4 1.1 -1 -6 5 5.4 2 0 6 -5 33.2 3.2 0 6 -5 32.3 3.2 0 6 -5 30.7 2.9 0 6 -5 30 2.1 0 6 -5 26.8 3.2 0 6 -5 35.4 3.5 0 6 -5 36.1 3.6 0 6 -5 30.1 1.9 0 -6 5 30.8 3.4 0 -6 5 35.2 2.6 0 -6 5 31.4 1.7 0 -6 5 28.1 3.6 0 -6 5 26.8 3.5 0 -6 5 30.9 2.8 0 -6 5 33.6 3.7 -1 6 -5 147.09 7.9 -1 6 -5 143.69 7 -1 6 -5 135.79 6.4 -1 6 -5 133.89 6.4 -1 6 -5 138.99 5.9 -1 6 -5 138.89 5.1 -1 6 -5 142.39 7 -1 6 -5 142.99 6.9 1 -6 5 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5.3 7 -6 -5 78.19 6.3 -7 6 5 72.39 6 -7 6 5 77.49 7.7 -7 6 5 81.19 7.7 -7 6 5 78.99 7.1 6 -6 -5 5.9 1.9 6 -6 -5 9.1 2.6 6 -6 -5 4.2 1.8 6 -6 -5 4.7 2.4 -6 6 5 5.6 2.1 -6 6 5 8 2.6 -6 6 5 7.7 3.1 -6 6 5 8.1 3.3 5 -6 -5 -0.2 1.3 5 -6 -5 -1.6 1.5 5 -6 -5 -0.4 0.6 5 -6 -5 0.9 1.7 -5 6 5 -1 1.5 -5 6 5 -0.5 1.3 -5 6 5 -0.5 1.4 4 -6 -5 8.2 2.1 4 -6 -5 8.8 2.7 4 -6 -5 7.6 2.2 -4 6 5 7 1.6 -4 6 5 7.1 2.6 -4 6 5 6.9 2.6 -4 6 5 4.8 2.2 3 -6 -5 127.69 7.4 3 -6 -5 115.89 6.2 3 -6 -5 129.99 6.9 -3 6 5 100.99 7.9 -3 6 5 113.39 7.4 -3 6 5 119.79 5.9 -3 6 5 118.89 7.4 2 -6 -5 94.09 6.5 2 -6 -5 93.29 5.7 2 -6 -5 93.79 5.7 -2 6 5 87.79 4.3 -2 6 5 90.29 7.3 -2 6 5 79.79 3.5 -2 6 5 92.69 6.1 -2 6 5 82.69 6.5 -2 6 5 90.89 5.3 1 -6 -5 353.66 13.6 1 -6 -5 349.57 14 1 -6 -5 341.17 12.4 -1 6 5 349.37 11.7 -1 6 5 350.66 12.3 -1 6 5 352.56 14.1 -1 6 5 336.37 14.6 -1 6 5 356.76 12.5 -1 6 5 334.97 10.3 0 -6 -5 2.5 1 0 -6 -5 2.8 1.6 0 -6 -5 3.9 1.8 0 -6 -5 2.2 1.4 0 -6 -5 1.6 1.8 0 6 5 6.4 2.6 0 6 5 2 1.4 0 6 5 1.3 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15.1 2 6 -9 438.66 10.5 -2 -6 9 430.46 11.9 -2 -6 9 422.46 11 -2 -6 9 434.66 15.6 -2 -6 9 426.06 17.7 -2 -6 9 420.56 16.6 1 6 -9 96.69 6.1 1 6 -9 95.19 4.6 1 6 -9 105.99 6.5 -1 -6 9 93.89 6.6 -1 -6 9 94.49 4.3 -1 -6 9 89.89 7 -1 -6 9 100.39 6.3 0 6 -9 429.26 13.5 0 6 -9 449.95 15.2 0 6 -9 446.16 15.5 0 -6 9 423.26 15.6 0 -6 9 438.96 15.1 0 -6 9 415.86 16.3 0 -6 9 444.26 12.9 -1 6 -9 222.78 9.3 -1 6 -9 193.68 9.7 -1 6 -9 195.18 8.8 1 -6 9 210.18 8.1 1 -6 9 214.18 9.6 1 -6 9 218.68 10.2 1 -6 9 198.08 6 1 -6 9 197.38 6.9 1 -6 9 208.98 9.4 -2 6 -9 1.4 1.2 -2 6 -9 2.1 2 -2 6 -9 1.9 1.4 -2 6 -9 2.1 1.4 2 -6 9 2.2 1 2 -6 9 2.3 0.8 2 -6 9 2.2 1.9 2 -6 9 0.3 1.3 2 -6 9 2.6 1.3 -3 6 -9 50.09 3.8 -3 6 -9 54.79 4.2 -3 6 -9 49 5.8 -3 6 -9 49.1 3.8 -3 6 -9 51.79 5.2 -3 6 -9 45.2 4 3 -6 9 47.9 4.3 3 -6 9 45.4 4.5 3 -6 9 48.3 4 3 -6 9 50.39 4.2 3 -6 9 52.99 3.2 3 -6 9 49.5 4.7 -4 6 -9 2 1.3 -4 6 -9 2.4 1.9 -4 6 -9 2.1 1.8 -4 6 -9 3.1 2.3 -4 6 -9 -0.1 1 -4 6 -9 3.2 1.3 4 -6 9 3.5 1.7 4 -6 9 1.6 1 4 -6 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23.7 7.3 -11 6 -9 23.5 8.7 11 -6 9 30.3 5.9 11 -6 9 24.9 6.1 11 -6 9 25.4 6 -12 6 -9 30.1 7.5 -12 6 -9 27.3 7.3 -12 6 -9 39.6 9 12 -6 9 28.7 6.5 12 -6 9 37.2 6.4 12 -6 9 36.2 6.8 11 5 -9 100.39 10 11 5 -9 107.09 10.1 11 5 -9 107.59 9.7 11 5 -9 101.59 8.6 11 5 -9 105.79 9.7 11 5 -9 100.89 7.8 -11 -5 9 109.89 13.1 -11 -5 9 101.19 11.4 -11 -5 9 97.09 10.6 10 5 -9 26.8 4.7 10 5 -9 30.2 6.2 10 5 -9 27.7 5 10 5 -9 22.7 4.8 10 5 -9 28.9 5.8 10 5 -9 26.4 4.2 10 5 -9 24.7 5.5 -10 -5 9 22.1 4.8 -10 -5 9 28.8 7.7 -10 -5 9 25.6 6.3 9 5 -9 198.38 9.7 9 5 -9 209.68 11.4 9 5 -9 196.48 12.2 9 5 -9 200.08 12.1 9 5 -9 196.08 13.1 9 5 -9 186.58 10.1 9 5 -9 195.28 12 -9 -5 9 197.68 14.7 -9 -5 9 211.48 15.4 -9 -5 9 186.28 13.4 -9 -5 9 195.68 12.4 8 5 -9 115.49 9.7 8 5 -9 111.49 6.7 8 5 -9 117.89 7.2 8 5 -9 125.39 8.4 8 5 -9 111.89 8.5 8 5 -9 118.99 9.1 -8 -5 9 98.79 10.5 -8 -5 9 107.69 8.4 -8 -5 9 105.29 9.8 -8 -5 9 107.29 10.4 7 5 -9 84.09 5.4 7 5 -9 89.39 8.2 7 5 -9 79.09 5.5 7 5 -9 86.29 6.8 7 5 -9 75.09 6.9 -7 -5 9 81.89 8.8 -7 -5 9 80.69 6.8 -7 -5 9 82.19 8.8 -7 -5 9 80.19 8.2 6 5 -9 22.1 2.6 6 5 -9 22.5 2.8 6 5 -9 18.6 3.8 6 5 -9 15.4 3.9 6 5 -9 20.2 3.8 -6 -5 9 23.2 5.6 -6 -5 9 22.8 3.8 -6 -5 9 20.2 4.5 -6 -5 9 18.6 4.6 5 5 -9 421.16 12.9 5 5 -9 431.46 17 5 5 -9 415.76 14.9 5 5 -9 429.66 13.4 5 5 -9 427.96 14.6 5 5 -9 449.16 16.1 5 5 -9 430.56 18.4 -5 -5 9 428.56 17.7 -5 -5 9 433.96 19.4 -5 -5 9 428.86 18.3 -5 -5 9 412.96 14.4 4 5 -9 220.98 12.1 4 5 -9 219.18 10 4 5 -9 210.88 10.6 4 5 -9 207.58 7.8 4 5 -9 204.28 7.1 4 5 -9 214.38 7.9 -4 -5 9 209.98 10.6 -4 -5 9 203.18 12.2 -4 -5 9 204.98 8 -4 -5 9 195.48 11.2 3 5 -9 543.75 15.1 3 5 -9 570.94 22.8 3 5 -9 548.05 17.8 3 5 -9 521.75 15.6 3 5 -9 550.14 18.8 3 5 -9 545.55 13.3 3 5 -9 535.55 13.8 -3 -5 9 532.95 18 -3 -5 9 517.55 14.7 -3 -5 9 530.05 19.2 -3 -5 9 533.65 20.6 -3 -5 9 512.05 13.9 2 5 -9 337.87 11.9 2 5 -9 343.57 12.7 2 5 -9 350.76 10.6 2 5 -9 342.47 13.4 -2 -5 9 346.17 14.9 -2 -5 9 326.47 13.5 -2 -5 9 320.07 12.5 -2 -5 9 338.77 10.3 1 5 -9 527.75 16.2 1 5 -9 562.34 17.6 1 5 -9 545.35 15.4 1 5 -9 569.34 18.2 -1 -5 9 536.55 16.9 -1 -5 9 559.44 15.2 -1 -5 9 557.44 19.5 -1 -5 9 531.05 18 0 5 -9 1017.6 27.7 0 5 -9 1002.9 27.5 0 5 -9 976.8 25.8 0 5 -9 986.7 25.8 0 -5 9 964.8 27.5 0 -5 9 978.3 29 0 -5 9 1000.2 26.6 -1 5 -9 331.67 11.8 -1 5 -9 351.96 15.1 -1 5 -9 314.57 10.9 -1 5 -9 327.37 11.8 -1 5 -9 339.17 12.8 -1 5 -9 302.47 12.4 1 -5 9 303.67 12.1 1 -5 9 326.67 13 1 -5 9 325.17 11.7 1 -5 9 349.17 14.1 1 -5 9 327.37 11.1 1 -5 9 316.27 9.4 1 -5 9 322.27 8.4 -2 5 -9 480.05 15.1 -2 5 -9 439.16 13.4 -2 5 -9 446.16 15.3 -2 5 -9 462.15 15.4 -2 5 -9 473.85 15.8 -2 5 -9 481.45 16.9 -2 5 -9 464.25 16.3 2 -5 9 450.25 15.5 2 -5 9 452.45 15.8 2 -5 9 458.65 12.4 2 -5 9 476.65 15.1 2 -5 9 440.26 14.9 2 -5 9 445.46 13.9 -3 5 -9 56.89 4.3 -3 5 -9 60.79 5.7 -3 5 -9 52.89 4.1 -3 5 -9 51.19 5.2 -3 5 -9 53.29 4.1 -3 5 -9 53.59 3.7 3 -5 9 55.09 4.9 3 -5 9 52.89 3.3 3 -5 9 53.19 4.5 3 -5 9 54.59 4 3 -5 9 53.39 5 3 -5 9 53.59 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45.6 7.3 9 7 -14 33.5 6.8 9 7 -14 36.7 7.6 9 7 -14 32.1 6.3 9 7 -14 37.7 4.2 9 7 -14 39.7 4.6 -9 -7 14 38.5 7.6 -9 -7 14 37 7.7 -9 -7 14 40.5 8.9 8 7 -14 101.79 7.3 8 7 -14 113.79 6.2 8 7 -14 109.39 10 8 7 -14 112.29 9.1 8 7 -14 130.79 11.8 -8 -7 14 120.09 11.8 -8 -7 14 128.99 11.6 -8 -7 14 127.09 13.2 7 7 -14 4.3 2.5 7 7 -14 6.7 3.3 7 7 -14 5 2 7 7 -14 3.1 3.1 7 7 -14 5.9 1.6 -7 -7 14 2.8 3.7 -7 -7 14 9.3 5.3 -7 -7 14 2.2 3.5 6 7 -14 312.47 10.3 6 7 -14 320.57 15.5 6 7 -14 317.37 18.2 6 7 -14 329.87 12.4 6 7 -14 332.97 16.9 6 7 -14 330.97 12 -6 -7 14 340.47 18.3 -6 -7 14 313.97 19.4 -6 -7 14 351.06 17.4 5 7 -14 89.19 8.3 5 7 -14 108.29 10.1 5 7 -14 84.39 7.6 5 7 -14 86.79 5.8 -5 -7 14 95.69 8.5 -5 -7 14 94.99 10.1 -5 -7 14 96.69 9.7 4 7 -14 12.7 3.8 4 7 -14 13.9 3.6 4 7 -14 12.7 2.6 -4 -7 14 13.8 4 -4 -7 14 14.6 4.4 -4 -7 14 16.7 3.7 3 7 -14 457.15 15 3 7 -14 481.25 18.7 3 7 -14 444.46 18.9 -3 -7 14 477.65 21.9 -3 -7 14 432.16 19.7 -3 -7 14 464.25 17.8 2 7 -14 481.05 15.8 2 7 -14 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8.4 2.2 -6 7 -14 159.88 12.9 -6 7 -14 151.88 9.9 -6 7 -14 137.79 13.3 -6 7 -14 141.89 7.6 6 -7 14 149.39 10 6 -7 14 147.89 8.1 6 -7 14 148.09 10.6 6 -7 14 151.78 9.4 -7 7 -14 76.49 6.3 -7 7 -14 63.99 5.2 -7 7 -14 72.79 11.2 -7 7 -14 79.49 7.9 -7 7 -14 88.29 10.7 7 -7 14 57.79 8.8 7 -7 14 82.29 6.4 7 -7 14 84.99 6.5 7 -7 14 72.89 7.6 -8 7 -14 7.9 5.7 -8 7 -14 -4.5 4.2 -8 7 -14 9.3 3.9 8 -7 14 1.8 2.5 8 -7 14 0.4 5.3 8 -7 14 5.6 2 8 -7 14 2.2 3.2 -9 7 -14 23.3 7.8 -9 7 -14 23.6 6.9 9 -7 14 37.3 4.1 9 -7 14 35.9 6.8 9 -7 14 21.9 5.6 9 -7 14 24.5 5.9 -10 7 -14 69.19 13 -10 7 -14 66.79 10.7 -10 7 -14 54.59 8.9 10 -7 14 49.5 8.3 10 -7 14 63.59 8.1 10 -7 14 54.89 6.9 9 6 -14 16.1 5.4 9 6 -14 21.6 4 9 6 -14 25.2 4.9 9 6 -14 18.1 3.3 9 6 -14 21.8 6.8 9 6 -14 25.1 5.5 -9 -6 14 28.1 6.3 -9 -6 14 34.2 7.4 -9 -6 14 19 6.5 8 6 -14 0.8 1.7 8 6 -14 2.3 2.5 8 6 -14 6.5 3.5 8 6 -14 6.5 2.2 8 6 -14 4.2 2.5 -8 -6 14 3.7 4.1 -8 -6 14 12.4 7.3 -8 -6 14 5.2 3.9 7 6 -14 23.1 9.7 7 6 -14 28.4 5.1 7 6 -14 25.1 5.7 7 6 -14 27.6 2.7 7 6 -14 22.6 4.2 -7 -6 14 25.7 5.8 -7 -6 14 33.7 10.3 -7 -6 14 28.3 5.8 6 6 -14 456.85 13.5 6 6 -14 446.06 22 6 6 -14 453.45 19.1 6 6 -14 433.46 15.7 6 6 -14 413.86 12.2 6 6 -14 439.46 20.1 -6 -6 14 457.45 21.6 -6 -6 14 433.66 22.3 -6 -6 14 467.65 22.1 5 6 -14 81.49 7.9 5 6 -14 84.89 5.8 5 6 -14 77.59 7.3 5 6 -14 77.19 3.2 -5 -6 14 72.59 8.3 -5 -6 14 77.59 9.1 -5 -6 14 76.29 7 4 6 -14 26.5 4.9 4 6 -14 33.9 3.9 4 6 -14 40.8 6.1 -4 -6 14 34.9 4.8 -4 -6 14 38.6 6.3 -4 -6 14 35.2 6.7 3 6 -14 813.52 23.4 3 6 -14 824.22 26.8 3 6 -14 825.82 27.8 -3 -6 14 767.52 27.6 -3 -6 14 792.32 24.7 -3 -6 14 782.22 29.9 2 6 -14 152.68 9.4 2 6 -14 152.68 8 2 6 -14 169.48 10.2 -2 -6 14 130.59 10.3 -2 -6 14 143.79 8.1 -2 -6 14 143.69 9.7 1 6 -14 194.68 9.4 1 6 -14 186.88 10.5 1 6 -14 186.68 10.6 -1 -6 14 188.98 9.3 -1 -6 14 184.68 10.7 -1 -6 14 186.48 12.1 0 6 -14 731.13 23.9 0 6 -14 739.93 23 0 6 -14 702.33 24.1 0 -6 14 725.93 26.5 0 -6 14 705.73 24.2 0 -6 14 712.73 22 -1 6 -14 91.69 6.9 -1 6 -14 87.89 7.3 -1 6 -14 103.39 7.6 1 -6 14 88.19 7.9 1 -6 14 83.89 7.3 1 -6 14 90.69 6.8 -2 6 -14 754.72 25.9 -2 6 -14 745.73 25.5 -2 6 -14 749.82 23.1 -2 6 -14 663.13 23.5 2 -6 14 764.82 35.1 2 -6 14 735.93 18.5 2 -6 14 745.43 23 2 -6 14 727.53 25 2 -6 14 742.13 19.6 -3 6 -14 753.22 22.5 -3 6 -14 758.12 27.1 -3 6 -14 814.32 23.3 -3 6 -14 766.42 27.4 3 -6 14 764.92 20.4 3 -6 14 757.22 23.8 3 -6 14 720.73 21.7 3 -6 14 746.63 26.1 3 -6 14 738.53 25.5 -4 6 -14 192.68 12.7 -4 6 -14 195.08 12.8 -4 6 -14 183.98 8.6 -4 6 -14 172.08 9.4 4 -6 14 174.78 11 4 -6 14 185.98 11 4 -6 14 179.88 8 4 -6 14 187.28 10.1 -5 6 -14 73.29 6.6 -5 6 -14 73.39 9.3 -5 6 -14 70.79 5 -5 6 -14 79.69 8.9 5 -6 14 74.29 6.8 5 -6 14 69.09 5.2 5 -6 14 78.59 6.7 5 -6 14 79.09 7.7 -6 6 -14 272.17 14.2 -6 6 -14 275.47 10.2 -6 6 -14 262.97 10.8 -6 6 -14 280.47 17.8 -6 6 -14 274.57 17.5 6 -6 14 263.17 13 6 -6 14 289.87 12.2 6 -6 14 260.57 13.1 6 -6 14 287.47 14.8 -7 6 -14 13.4 5.5 -7 6 -14 17 6.1 -7 6 -14 17.7 4.7 -7 6 -14 24.6 2.5 -7 6 -14 11.9 2.3 7 -6 14 13.1 5.2 7 -6 14 20.4 3.9 7 -6 14 15.6 3.2 7 -6 14 17.8 4.5 -8 6 -14 64.09 10.4 -8 6 -14 55.29 10.6 -8 6 -14 65.29 8.1 8 -6 14 64.69 6.4 8 -6 14 55.09 7.7 8 -6 14 69.09 6 8 -6 14 67.49 8.1 -9 6 -14 44.7 9.1 -9 6 -14 52.49 8.9 9 -6 14 55.49 8.5 9 -6 14 46.3 7.3 9 -6 14 71.49 5.7 9 -6 14 68.49 7.9 -10 6 -14 -1.6 5.9 -10 6 -14 10.9 6.6 -10 6 -14 15.6 6.1 10 -6 14 7.3 4.2 10 -6 14 0.3 4.2 10 -6 14 10.5 4.2 10 5 -14 27.4 5.5 10 5 -14 25 3.9 10 5 -14 21.8 5.2 10 5 -14 18.6 5.4 10 5 -14 26.8 4.7 10 5 -14 24.9 5.8 10 5 -14 16.1 5.6 -10 -5 14 19.5 6.7 -10 -5 14 20.1 6.1 -10 -5 14 18.1 5.6 9 5 -14 4.1 2.9 9 5 -14 13.5 5 9 5 -14 3.1 1.9 9 5 -14 6.6 3.9 9 5 -14 5.7 2.4 9 5 -14 1.4 2.8 -9 -5 14 3.6 4.4 -9 -5 14 -2.1 5.1 -9 -5 14 8 3.8 8 5 -14 1.8 1.4 8 5 -14 3.1 1.9 8 5 -14 -2.3 2.3 8 5 -14 6.4 3.2 8 5 -14 -3.9 2.3 8 5 -14 0.2 1.7 -8 -5 14 1.1 3.2 -8 -5 14 4 3.5 -8 -5 14 1.8 3.2 7 5 -14 53.69 5 7 5 -14 49 3.7 7 5 -14 47.8 8 7 5 -14 54.49 6.5 7 5 -14 56.29 7.2 -7 -5 14 55.59 8.7 -7 -5 14 62.09 7.9 -7 -5 14 53.39 7.1 -7 -5 14 51.29 8.7 6 5 -14 257.47 8.8 6 5 -14 297.67 15 6 5 -14 284.07 10.5 6 5 -14 287.87 15.5 -6 -5 14 268.07 15.3 -6 -5 14 281.17 17.3 -6 -5 14 264.97 13.7 -6 -5 14 298.07 16.4 5 5 -14 64.79 3.1 5 5 -14 61.59 7.1 5 5 -14 73.09 3.6 5 5 -14 67.59 5.6 5 5 -14 73.79 7 -5 -5 14 75.39 6.7 -5 -5 14 69.29 7.6 -5 -5 14 69.19 7.7 -5 -5 14 70.99 8.5 4 5 -14 188.38 11 4 5 -14 165.28 11 4 5 -14 169.28 8.7 -4 -5 14 195.88 12.3 -4 -5 14 173.58 11.2 -4 -5 14 172.18 9.2 -4 -5 14 169.38 12.3 3 5 -14 388.06 17.4 3 5 -14 400.76 16.7 3 5 -14 373.96 12.9 3 5 -14 403.76 14.6 -3 -5 14 422.26 18.4 -3 -5 14 411.16 19.4 -3 -5 14 406.76 16.1 -3 -5 14 391.36 17.1 2 5 -14 46.4 5.2 2 5 -14 42.5 4.4 2 5 -14 33.5 3.4 2 5 -14 36.9 5.8 -2 -5 14 47.3 4.1 -2 -5 14 48.7 6.3 -2 -5 14 45.2 5.5 -2 -5 14 53.89 5.9 1 5 -14 639.44 20.3 1 5 -14 601.44 21.5 1 5 -14 602.04 21.8 1 5 -14 566.84 17.2 -1 -5 14 620.94 18.8 -1 -5 14 643.84 22.1 -1 -5 14 637.84 24.3 -1 -5 14 622.34 22.6 0 5 -14 409.96 16.5 0 5 -14 384.46 12.8 0 5 -14 405.96 15.5 0 -5 14 408.56 16.4 0 -5 14 416.76 18.4 -1 5 -14 185.28 9.6 -1 5 -14 158.18 13.6 -1 5 -14 178.68 10.2 -1 5 -14 173.88 6.6 1 -5 14 183.58 8.8 1 -5 14 183.08 10.4 1 -5 14 176.08 6.1 1 -5 14 185.18 11.4 1 -5 14 174.88 5.6 -2 5 -14 316.67 14.6 -2 5 -14 302.27 11.1 -2 5 -14 299.37 14.2 -2 5 -14 299.17 12.3 2 -5 14 292.67 10.2 2 -5 14 286.57 11.9 2 -5 14 280.87 16.5 2 -5 14 298.37 13.9 -3 5 -14 704.03 22.1 -3 5 -14 721.63 21.5 -3 5 -14 709.73 25.3 -3 5 -14 710.43 26 3 -5 14 683.33 28.7 3 -5 14 695.13 21 3 -5 14 712.63 24.4 3 -5 14 718.23 22.2 -4 5 -14 27 6 -4 5 -14 34.2 6.3 -4 5 -14 26.9 3.1 -4 5 -14 29.8 4.8 4 -5 14 29.2 5.4 4 -5 14 30.7 5.7 -5 5 -14 238.38 10.2 -5 5 -14 212.58 14 -5 5 -14 235.58 9.2 -5 5 -14 259.67 15.7 -5 5 -14 252.97 13.1 5 -5 14 238.78 11.7 5 -5 14 257.87 13.3 5 -5 14 241.38 13.1 -6 5 -14 368.16 19.9 -6 5 -14 366.86 17.3 -6 5 -14 328.97 19.2 -6 5 -14 348.17 11.6 6 -5 14 345.37 15.2 6 -5 14 352.46 16.8 6 -5 14 346.07 18.8 -7 5 -14 24.7 8.1 -7 5 -14 28 7.4 -7 5 -14 28.8 6 7 -5 14 34.7 8.4 7 -5 14 29.7 5.5 7 -5 14 24.4 8.6 -8 5 -14 370.06 22.4 -8 5 -14 363.96 19.3 -8 5 -14 350.56 21.6 8 -5 14 344.17 16.7 8 -5 14 356.66 17.8 8 -5 14 343.57 15.6 8 -5 14 340.97 15.7 -9 5 -14 39.1 9.3 -9 5 -14 50.09 10.3 -9 5 -14 47 8.2 9 -5 14 50.59 7.2 9 -5 14 67.49 7 9 -5 14 52.49 8.4 -10 5 -14 0.3 4.2 -10 5 -14 1.7 5.9 -10 5 -14 13.8 4.8 10 -5 14 -1.5 3.3 10 -5 14 5.8 3.3 10 -5 14 4.1 3.5 10 4 -14 45.9 7.6 10 4 -14 37.2 5.7 10 4 -14 37.1 6.8 10 4 -14 46.3 5.9 10 4 -14 39.1 8.5 10 4 -14 36.5 4.4 10 4 -14 35.5 6.4 -10 -4 14 43.5 8 -10 -4 14 49.2 8.6 -10 -4 14 50.09 9.5 9 4 -14 17.6 5.1 9 4 -14 2.7 3.6 9 4 -14 8.5 3.1 9 4 -14 7.8 2.3 9 4 -14 12.1 4.9 9 4 -14 10.8 2.8 -9 -4 14 15.5 4.9 -9 -4 14 4.5 3.6 -9 -4 14 12.8 4.3 -9 -4 14 8.8 4.4 8 4 -14 5 3.5 8 4 -14 3.8 1.4 8 4 -14 0.5 1.9 8 4 -14 0.6 2.4 8 4 -14 -0.3 1.5 -8 -4 14 -2.9 2.4 -8 -4 14 0.4 3.3 -8 -4 14 4.5 3.7 7 4 -14 24.4 4.8 7 4 -14 26.1 3.9 7 4 -14 23.2 3.9 7 4 -14 29.6 2.8 7 4 -14 28.3 5.9 -7 -4 14 33.2 5.5 -7 -4 14 28.3 5.8 -7 -4 14 27 6.5 -7 -4 14 26.9 5.9 6 4 -14 148.19 6.2 6 4 -14 148.59 10.3 6 4 -14 152.28 7.8 6 4 -14 141.89 10.9 6 4 -14 151.98 8.7 -6 -4 14 165.28 12.6 -6 -4 14 143.29 9.1 -6 -4 14 143.89 10.6 -6 -4 14 163.38 12 5 4 -14 2 1.1 5 4 -14 5.2 1.5 5 4 -14 1.6 1.9 5 4 -14 2.2 2.1 5 4 -14 3.7 2.1 5 4 -14 2.8 1.8 -5 -4 14 2.8 3.2 -5 -4 14 1.3 2.2 -5 -4 14 1.2 2.6 4 4 -14 79.59 7.4 4 4 -14 68.99 4.6 4 4 -14 69.59 6.8 4 4 -14 71.79 5.7 4 4 -14 70.09 3 4 4 -14 73.69 3.5 -4 -4 14 71.89 7.8 -4 -4 14 74.19 7.4 -4 -4 14 73.39 5.2 -4 -4 14 75.39 7 3 4 -14 -0.9 1.2 3 4 -14 1.5 1.6 3 4 -14 1.1 1.5 3 4 -14 -0.8 1.2 -3 -4 14 1 1.2 -3 -4 14 1.8 2.2 -3 -4 14 0.1 1.5 -3 -4 14 0.9 1.8 2 4 -14 132.49 5.6 2 4 -14 145.39 9.4 2 4 -14 149.49 9.2 2 4 -14 155.48 8.3 -2 -4 14 133.79 9.6 -2 -4 14 144.59 8.9 -2 -4 14 136.59 7 -2 -4 14 149.29 10.6 1 4 -14 145.59 8 1 4 -14 128.39 5.6 1 4 -14 141.49 9 1 4 -14 145.39 8.9 -1 -4 14 144.29 10.3 -1 -4 14 136.29 6.4 -1 -4 14 122.59 8.8 -1 -4 14 143.59 8.7 0 4 -14 2 1.5 0 4 -14 3.1 1.2 0 4 -14 1.4 1.4 0 4 -14 0.8 1.4 0 4 -14 1.7 1 0 -4 14 2.1 1.8 0 -4 14 -0.2 2 0 -4 14 2.2 0.7 0 -4 14 4.2 1.9 0 -4 14 2 2 -1 4 -14 7.1 1.7 -1 4 -14 6.2 2.2 -1 4 -14 7.8 2.5 -1 4 -14 6.2 2.5 1 -4 14 8.3 2.5 1 -4 14 8.5 3.3 1 -4 14 8 3.2 1 -4 14 7.6 1.7 1 -4 14 6.3 2.9 -2 4 -14 42.9 5.1 -2 4 -14 54.39 4.6 -2 4 -14 55.39 6 -2 4 -14 55.99 4.8 2 -4 14 52.19 4 2 -4 14 52.39 6.2 2 -4 14 43.4 4.5 2 -4 14 46.5 5.7 -3 4 -14 14.4 3.8 -3 4 -14 8.1 2.8 -3 4 -14 7.3 3.4 -3 4 -14 12.6 2.6 3 -4 14 10.8 2.8 3 -4 14 8.9 3.2 3 -4 14 7.8 3.5 -4 4 -14 362.26 17.8 -4 4 -14 352.76 14.5 -4 4 -14 356.36 16.8 -4 4 -14 349.87 12.1 -4 4 -14 368.46 15.8 4 -4 14 343.47 15.8 4 -4 14 340.27 13.6 4 -4 14 355.76 16.3 -5 4 -14 324.47 15.7 -5 4 -14 301.67 11.6 -5 4 -14 293.77 16.9 -5 4 -14 290.37 10 -5 4 -14 315.47 16.6 5 -4 14 306.47 14.9 5 -4 14 299.37 14.7 5 -4 14 303.97 13.2 -6 4 -14 30.4 2.6 -6 4 -14 18.5 2.3 -6 4 -14 14.6 5.1 -6 4 -14 27.1 5.8 -6 4 -14 18.9 5.5 6 -4 14 28.8 4.8 6 -4 14 26.7 5.1 6 -4 14 24.1 5.5 -7 4 -14 490.05 23.9 -7 4 -14 467.85 35.2 -7 4 -14 440.26 21.5 7 -4 14 460.05 19.1 7 -4 14 449.56 18.6 7 -4 14 409.16 27.5 -8 4 -14 341.57 21.1 -8 4 -14 357.26 19.9 -8 4 -14 364.86 22 8 -4 14 374.06 16.5 8 -4 14 361.36 18 8 -4 14 349.47 17 -9 4 -14 0.9 5 -9 4 -14 4 4.3 -9 4 -14 12.7 5.9 9 -4 14 0.7 2.8 9 -4 14 1.9 3.4 9 -4 14 2.9 2.4 10 3 -14 16.9 5.1 10 3 -14 17.3 5.7 10 3 -14 16.6 4.7 10 3 -14 23.8 3.8 10 3 -14 14 4.2 10 3 -14 10.2 3.9 10 3 -14 20.4 4.1 -10 -3 14 18.1 5.4 -10 -3 14 24 6.8 -10 -3 14 24.2 6.1 9 3 -14 15.6 3.8 9 3 -14 18.5 4.9 9 3 -14 19.5 5.5 9 3 -14 10 4.3 9 3 -14 18.2 3.3 9 3 -14 13.5 2.7 -9 -3 14 10.3 3.6 -9 -3 14 13.5 5 -9 -3 14 18.6 5.4 -9 -3 14 18.5 5.3 8 3 -14 119.99 8.3 8 3 -14 108.49 10.2 8 3 -14 128.79 10.4 8 3 -14 111.99 6.4 8 3 -14 103.69 6.7 -8 -3 14 117.29 8.6 -8 -3 14 132.39 12 -8 -3 14 124.89 10.9 -8 -3 14 111.49 9.9 7 3 -14 24.9 3 7 3 -14 33.3 5.9 7 3 -14 26.7 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-4 -3 21 104.59 11.1 -4 -3 21 114.19 10 3 3 -21 11.1 4 3 3 -21 10 4.3 3 3 -21 12.3 4.5 -3 -3 21 14.8 4.4 -3 -3 21 6.6 3.9 -3 -3 21 13.2 4.5 2 3 -21 36.7 7.1 2 3 -21 33.1 6.5 2 3 -21 31 6.1 2 3 -21 33.3 5.4 -2 -3 21 36.1 7.3 -2 -3 21 31.9 7.6 -2 -3 21 33.1 6.1 1 3 -21 184.08 12.7 1 3 -21 189.38 12.9 -1 -3 21 205.58 19.9 -1 -3 21 192.78 15.5 0 3 -21 15.4 4.9 0 3 -21 17.7 5.7 0 3 -21 21.7 3.6 0 3 -21 11.3 4.3 0 -3 21 13 5.4 0 -3 21 20.1 5.1 0 -3 21 16.7 4.8 -1 3 -21 86.29 8.8 -1 3 -21 81.59 8 -1 3 -21 79.39 9.1 -1 3 -21 95.19 7.4 1 -3 21 88.19 8.9 1 -3 21 76.09 8.1 1 -3 21 87.19 10.4 -2 3 -21 108.09 11.2 -2 3 -21 99.89 8.4 -2 3 -21 110.59 10.3 -2 3 -21 116.89 8.8 2 -3 21 109.19 11.5 2 -3 21 99.79 9.9 2 -3 21 87.89 6.3 -3 3 -21 9 4.9 -3 3 -21 6.2 3 -3 3 -21 8.7 4 -3 3 -21 -3 3 3 -3 21 8.9 4.6 3 -3 21 6.1 4.2 -4 3 -21 15.5 4.9 -4 3 -21 0.2 4.4 -4 3 -21 9.7 3.5 -4 3 -21 15.3 5.6 4 -3 21 4.7 3.7 4 -3 21 11.7 4.9 4 -3 21 17.4 5.7 6 2 -21 -2.7 2.8 6 2 -21 3.1 2.5 6 2 -21 -2.2 2.4 -6 -2 21 6 3.6 -6 -2 21 5.3 3.7 -6 -2 21 0.2 2.5 5 2 -21 22.2 5.9 5 2 -21 25.6 5.1 5 2 -21 31.6 6 -5 -2 21 44.4 6.7 -5 -2 21 29.1 6.9 -5 -2 21 23.1 6.7 4 2 -21 20.7 5 4 2 -21 29.7 5.7 4 2 -21 33.2 7.4 -4 -2 21 22 5.9 -4 -2 21 30.2 5.6 -4 -2 21 17.3 5.5 3 2 -21 0.8 2.2 3 2 -21 -3 2.5 3 2 -21 2.4 3 3 2 -21 5.7 2.2 -3 -2 21 1.3 2.6 -3 -2 21 2.8 3.8 -3 -2 21 2 2.8 2 2 -21 48.3 7.9 2 2 -21 57.99 7.7 2 2 -21 61.09 5.1 2 2 -21 44.5 7.2 -2 -2 21 62.59 7.1 -2 -2 21 40.6 8.2 -2 -2 21 46.5 8.3 1 2 -21 81.39 14.7 1 2 -21 93.89 9.1 1 2 -21 89.79 9.1 1 2 -21 93.99 6.9 -1 -2 21 88.29 10.8 -1 -2 21 101.39 9.9 -1 -2 21 67.09 9.2 0 2 -21 3.1 3.1 0 2 -21 4.8 2.4 0 2 -21 -0.6 2.5 0 2 -21 1.5 2.2 0 -2 21 4.8 3 0 -2 21 2.2 3.1 0 -2 21 7.5 4.2 -1 2 -21 116.69 9.5 -1 2 -21 106.59 8.7 -1 2 -21 116.39 10.9 -1 2 -21 126.09 10.6 1 -2 21 118.89 10.1 1 -2 21 150.98 13.4 1 -2 21 127.79 10.5 -2 2 -21 41.7 6.5 -2 2 -21 55.79 7.1 -2 2 -21 41.2 7 -2 2 -21 67.19 8.5 2 -2 21 43 7.4 2 -2 21 48.5 7.1 2 -2 21 59.39 9.8 -3 2 -21 14.6 4.7 -3 2 -21 6 3.7 -3 2 -21 2.1 3 -3 2 -21 4.9 4 3 -2 21 7.2 4.3 3 -2 21 2.8 3.6 3 -2 21 7.7 4.6 6 1 -21 7 3.4 6 1 -21 -2.9 2 6 1 -21 -1.5 2.3 -6 -1 21 -4.1 2.3 -6 -1 21 -2.6 2.9 -6 -1 21 -1.9 2.8 5 1 -21 18.6 4.5 5 1 -21 17.2 4.9 5 1 -21 10.1 4.6 5 1 -21 19.3 3.1 -5 -1 21 8.8 4.6 -5 -1 21 24.2 4.7 -5 -1 21 21.2 6.6 4 1 -21 8.4 4.3 4 1 -21 12.1 2.6 4 1 -21 3.2 3.2 4 1 -21 3.4 2.8 -4 -1 21 5.2 4.4 -4 -1 21 10.5 3.5 -4 -1 21 9.7 4.3 3 1 -21 -2.3 2.7 3 1 -21 -0.7 1.8 3 1 -21 -1.6 2.4 -3 -1 21 4 3.6 -3 -1 21 3.6 2.5 -3 -1 21 -0.7 3.4 2 1 -21 13.4 3.1 2 1 -21 7.7 4.2 2 1 -21 4.8 3.4 2 1 -21 1.5 2.7 -2 -1 21 12.1 5.1 -2 -1 21 7.3 3.1 -2 -1 21 2 3.1 1 1 -21 8.8 3.9 1 1 -21 10.3 3.9 1 1 -21 6.6 3.1 -1 -1 21 11 4.8 -1 -1 21 17.7 5.5 -1 -1 21 13.1 4.1 0 1 -21 6.8 4.4 0 1 -21 11.7 3.5 0 1 -21 11.6 3.9 0 1 -21 7.9 3.9 0 -1 21 9.3 3.6 0 -1 21 4.5 4.1 0 -1 21 5.2 4 -1 1 -21 58.89 7.1 -1 1 -21 55.69 6.7 -1 1 -21 58.09 7.3 -1 1 -21 44.2 7.7 1 -1 21 37 6.9 1 -1 21 73.09 9.6 1 -1 21 41.4 7.1 -2 1 -21 -1.5 2.7 -2 1 -21 4.5 4 -2 1 -21 9.9 4.2 -2 1 -21 2.1 3.4 2 -1 21 1.9 3.2 2 -1 21 5.4 3.2 2 -1 21 0.9 3.6 -3 1 -21 18.7 5.1 -3 1 -21 24.3 4.8 3 -1 21 24.6 4.9 3 -1 21 24 5.9 5 0 -21 -5.6 2.4 5 0 -21 2.8 3.4 5 0 -21 6.9 3.6 -5 0 21 1.6 3.8 -5 0 21 5.1 3.4 -5 0 21 -1.5 2.8 4 0 -21 4.1 2.6 4 0 -21 0.5 2.8 4 0 -21 -1 2.5 4 0 -21 4.7 2 -4 0 21 2.5 3.5 -4 0 21 2.8 3.3 -4 0 21 2.3 3.7 3 0 -21 -1.2 2.3 3 0 -21 -2.4 2.9 3 0 -21 -0.8 2.9 3 0 -21 4.5 2.2 -3 0 21 4.9 2.7 -3 0 21 -1.3 3 -3 0 21 1.5 2.7 2 0 -21 -3.9 2.3 2 0 -21 0.2 2.2 2 0 -21 -4.3 2.7 2 0 -21 3.5 2.6 -2 0 21 -0.4 2.5 -2 0 21 -5.3 2.7 -2 0 21 1.5 2.5 1 0 -21 -2.5 2 1 0 -21 -0.5 1.9 1 0 -21 3.3 2.9 1 0 -21 5.3 2.8 -1 0 21 -4.6 2.4 -1 0 21 0.3 2.8 -1 0 21 1.3 2.7 0 0 -21 0.3 1.8 0 0 -21 3.7 2.5 0 0 -21 1.2 2.7 0 0 -21 0.6 3 0 0 21 0.4 2.8 0 0 21 3.6 3.3 0 0 21 3.5 5.1 -1 0 -21 6.8 3.8 -1 0 -21 -2.2 3.2 -1 0 -21 3.2 3.5 -1 0 -21 7 3.6 1 0 21 3.7 3.8 1 0 21 8.4 3.9 1 0 21 3.6 3.4 -2 0 -21 7 4.2 -2 0 -21 0.8 2.8 -2 0 -21 0.4 3.3 -2 0 -21 -2.1 2.5 2 0 21 -3.2 2.9 2 0 21 -2 2.6 2 0 21 -3.7 3.2 5 -1 -21 14 3.3 -5 1 21 21 5.3 4 -1 -21 38.1 4.8 4 -1 -21 19.2 5.2 4 -1 -21 17.8 4.2 -4 1 21 21.6 4.5 -4 1 21 29.3 6.1 -4 1 21 19.4 5.6 3 -1 -21 9.3 3.9 3 -1 -21 9.9 2.9 3 -1 -21 1.4 2.8 -3 1 21 5.4 4.1 -3 1 21 1 3.2 -3 1 21 8.7 3.6 2 -1 -21 3.2 2.2 2 -1 -21 -1.1 2.2 2 -1 -21 0.3 2.6 -2 1 21 9.2 3.1 -2 1 21 -1.1 3.2 -2 1 21 6.4 4.6 1 -1 -21 3.7 3.3 1 -1 -21 3.2 2.9 1 -1 -21 3.7 3.3 1 -1 -21 2 3.5 -1 1 21 6.8 3.9 -1 1 21 4.2 3.7 -1 1 21 16.5 5.1 0 -1 -21 1.2 3.1 0 -1 -21 -2.2 2.7 0 -1 -21 1.7 3.6 0 -1 -21 -2.2 2.7 0 1 21 4.1 3.4 0 1 21 2.6 3.3 0 1 21 -2.2 3 -1 -1 -21 0.7 2.5 -1 -1 -21 -2 2.6 -1 -1 -21 6 4 1 1 21 1.5 3.2 1 1 21 -6.9 2.6 1 1 21 -3.7 3.2 3 -2 -21 0.3 3.1 3 -2 -21 -0.5 2.6 3 -2 -21 -0.3 2.1 -3 2 21 7.7 4.3 -3 2 21 3.8 2.9 -3 2 21 -1.5 3.1 2 -2 -21 34.6 6.6 2 -2 -21 38.2 6.8 2 -2 -21 30.4 5.4 -2 2 21 36.1 5.9 -2 2 21 24.6 6.8 -2 2 21 32.6 7.4 1 -2 -21 32.4 6.4 1 -2 -21 40.1 7.2 -1 2 21 33.6 7.3 -1 2 21 25.2 6.9 2 9 -22 140.09 10.9 2 9 -22 153.28 11.9 2 9 -22 153.18 12.8 -2 -9 22 159.18 13.1 -2 -9 22 162.68 14.7 -2 -9 22 182.88 10.5 1 9 -22 21.9 5.7 1 9 -22 10.1 4.3 1 9 -22 13.1 4.7 -1 -9 22 7.6 4.4 -1 -9 22 11 3.8 0 9 -22 76.29 9.7 0 9 -22 83.69 8.7 0 -9 22 98.39 7.7 0 -9 22 65.89 10.7 0 -9 22 71.29 8.5 -1 9 -22 156.78 12.8 -1 9 -22 172.38 12.2 -1 9 -22 159.68 13.5 1 -9 22 184.08 11.1 1 -9 22 164.68 14.1 1 -9 22 204.98 14.1 -2 9 -22 25.6 6.5 -2 9 -22 29.5 7.2 -2 9 -22 31 5.6 2 -9 22 26 6.7 2 -9 22 20.8 4.8 2 -9 22 26.8 5.1 3 8 -22 41.5 7.3 3 8 -22 58.39 7.6 3 8 -22 49.4 7 -3 -8 22 59.99 10.5 2 8 -22 33.7 6.3 2 8 -22 38.9 7.5 2 8 -22 43.8 7.5 -2 -8 22 39.5 7 -2 -8 22 45.2 9 1 8 -22 1.3 4.3 1 8 -22 1.8 3.2 1 8 -22 2.7 2.8 -1 -8 22 8.5 2.6 -1 -8 22 0.3 4 0 8 -22 140.59 11.3 0 8 -22 139.69 12 0 8 -22 133.99 10.7 0 -8 22 144.79 11.7 0 -8 22 130.29 13.1 0 -8 22 147.59 9 -1 8 -22 32.5 6.8 -1 8 -22 36.9 6.7 -1 8 -22 40.5 6.5 1 -8 22 35.3 7.6 1 -8 22 29.3 5.7 -2 8 -22 13.1 5.3 -2 8 -22 7.1 4.9 -2 8 -22 11.2 4.9 2 -8 22 9.9 4.7 2 -8 22 13.7 4.3 2 -8 22 14.8 3.9 3 7 -22 16.2 5.1 3 7 -22 5.9 3.5 -3 -7 22 12.2 5 -3 -7 22 17.5 5.5 2 7 -22 14.9 4.8 2 7 -22 16.5 4.8 2 7 -22 12.2 5 -2 -7 22 7.1 4.2 -2 -7 22 9.6 4.4 1 7 -22 6.7 3.8 1 7 -22 5.1 3.3 1 7 -22 0.9 3.4 -1 -7 22 12.1 5.4 -1 -7 22 9.9 4.1 0 7 -22 83.39 9 0 7 -22 90.09 9.3 0 7 -22 72.19 8.1 0 -7 22 70.59 8.6 0 -7 22 55.59 9.7 0 -7 22 93.09 6.3 -1 7 -22 -5.8 2.4 -1 7 -22 -0.1 2.6 -1 7 -22 -3 3.2 1 -7 22 8.4 2.7 1 -7 22 6.3 4.4 1 -7 22 4 2.3 -2 7 -22 49.8 6.5 -2 7 -22 49.1 8.1 -2 7 -22 42.4 7.7 2 -7 22 61.89 7.4 2 -7 22 58.19 9.9 2 -7 22 54.69 6.4 -3 7 -22 150.28 13.2 -3 7 -22 112.29 9 -3 7 -22 120.39 12.1 3 -7 22 142.19 9.9 3 -7 22 165.38 13.7 3 -7 22 122.79 11 4 6 -22 29.4 6.2 4 6 -22 32.7 6.3 4 6 -22 22.4 5.1 -4 -6 22 27.4 6.8 -4 -6 22 24.4 5.6 3 6 -22 8.8 4 3 6 -22 13.3 4.8 3 6 -22 9.7 2.9 -3 -6 22 9.3 4.3 -3 -6 22 11.2 4.9 2 6 -22 1.2 3.2 2 6 -22 -0.2 2.4 2 6 -22 3.7 3.3 -2 -6 22 3.5 4 -2 -6 22 5.6 3.8 1 6 -22 38.8 7 1 6 -22 54.39 7.1 1 6 -22 33.8 6.4 -1 -6 22 32 6.2 -1 -6 22 43.3 9.2 0 6 -22 14.9 4.1 0 6 -22 8.2 3.7 0 6 -22 12.5 4.6 0 -6 22 7 4.8 0 -6 22 9 3.8 -1 6 -22 2.5 3.2 -1 6 -22 -1.9 2.6 -1 6 -22 -3.5 3.3 1 -6 22 8.3 2.6 1 -6 22 5.2 3.9 1 -6 22 3.9 3.6 -2 6 -22 31.9 7.1 -2 6 -22 40.8 7.5 -2 6 -22 28.7 5.4 2 -6 22 46.6 7.4 2 -6 22 31 4.9 2 -6 22 29.4 7.1 -3 6 -22 9.8 3.5 -3 6 -22 10.7 4.1 -3 6 -22 16.1 5.3 3 -6 22 13.2 3.8 3 -6 22 13 4.3 3 -6 22 17.1 5.6 4 5 -22 20.8 5.3 4 5 -22 21.1 4.7 4 5 -22 20.1 4.9 -4 -5 22 20.3 5.7 -4 -5 22 20.4 5.6 -4 -5 22 17.7 4.9 3 5 -22 20.3 5 3 5 -22 17.3 5.2 3 5 -22 26.3 6.1 -3 -5 22 25.3 5.6 -3 -5 22 17.4 5.4 -3 -5 22 15.9 5.3 2 5 -22 74.99 8.6 2 5 -22 68.39 7.8 2 5 -22 74.79 8.5 -2 -5 22 52.29 9.3 -2 -5 22 87.39 9.9 -2 -5 22 84.19 9.1 1 5 -22 25.9 6.1 1 5 -22 23.5 5.6 1 5 -22 31.4 6.6 -1 -5 22 18.6 6 -1 -5 22 32.9 6 0 5 -22 0.5 3.4 0 5 -22 4.7 3.2 0 5 -22 2.7 3.2 0 -5 22 15.6 5.5 0 -5 22 3.8 3.2 -1 5 -22 27.8 6.2 -1 5 -22 26.1 6.3 -1 5 -22 28.7 5.3 1 -5 22 37.2 8.2 1 -5 22 36.6 6.8 -2 5 -22 5.1 4.2 -2 5 -22 -2.2 2.2 -2 5 -22 -2.3 3.4 2 -5 22 -0.3 2.9 2 -5 22 9.2 4.1 2 -5 22 4.1 3.7 -3 5 -22 -3.7 2.8 -3 5 -22 0.2 2.8 -3 5 -22 4.2 3.4 3 -5 22 3 3.3 3 -5 22 3.8 3.9 3 -5 22 -5.3 3 4 4 -22 3.8 3.1 4 4 -22 5.1 2.7 4 4 -22 4.5 2.6 -4 -4 22 3.2 3.9 -4 -4 22 12.4 4.4 3 4 -22 78.89 9.5 3 4 -22 91.49 9.1 3 4 -22 84.59 9 -3 -4 22 86.29 9.5 -3 -4 22 92.59 11.2 -3 -4 22 95.69 10.6 2 4 -22 84.29 8.9 2 4 -22 117.19 10.7 2 4 -22 106.29 10 -2 -4 22 67.29 9 -2 -4 22 101.99 10.4 -2 -4 22 127.59 10.5 1 4 -22 0.4 2.4 1 4 -22 -1 3.5 1 4 -22 -2.5 2.5 -1 -4 22 1.5 3.3 -1 -4 22 0.5 2.5 -1 -4 22 2.3 3.4 0 4 -22 86.59 9.9 0 4 -22 69.39 8.2 0 4 -22 83.99 8.6 0 -4 22 90.69 9 0 -4 22 95.79 9.4 0 -4 22 87.89 10.7 -1 4 -22 74.89 7.8 -1 4 -22 75.69 9.1 -1 4 -22 63.39 9.5 1 -4 22 77.69 8.9 1 -4 22 76.09 10.2 -2 4 -22 7.4 3.4 -2 4 -22 5.7 3.7 -2 4 -22 -2.2 2.8 -2 4 -22 3.2 4 2 -4 22 16 5.7 2 -4 22 6.4 3.8 4 3 -22 12.9 4.9 4 3 -22 19.9 5.1 4 3 -22 19.6 5 -4 -3 22 15.3 4.9 -4 -3 22 21.3 5.1 -4 -3 22 23.6 6.7 3 3 -22 100.69 10.4 3 3 -22 105.69 9.9 3 3 -22 113.19 10.3 -3 -3 22 105.89 11.3 -3 -3 22 103.59 11.5 -3 -3 22 129.19 10.5 2 3 -22 12.7 4 2 3 -22 11.3 3.7 2 3 -22 11.6 4.4 -2 -3 22 10 4.9 -2 -3 22 22.8 5.6 -2 -3 22 10.1 3.3 1 3 -22 42.8 7.3 1 3 -22 45.8 7.7 1 3 -22 62.79 9.1 -1 -3 22 56.19 8.3 -1 -3 22 50.29 9 -1 -3 22 65.59 7.6 0 3 -22 140.29 11.8 0 3 -22 162.78 13.4 0 3 -22 153.18 12 0 3 -22 129.49 11 0 -3 22 172.88 12 0 -3 22 138.59 11.8 0 -3 22 152.88 13.4 -1 3 -22 16.8 4.6 -1 3 -22 14.1 5 -1 3 -22 20.3 4.3 -1 3 -22 11.7 4.7 1 -3 22 12.5 4.8 1 -3 22 23.4 5.7 1 -3 22 15.8 4.7 -2 3 -22 76.59 7.9 -2 3 -22 88.99 10.2 -2 3 -22 61.49 9.4 -2 3 -22 75.49 7.9 2 -3 22 77.49 9.5 2 -3 22 66.19 8.3 4 2 -22 25.4 6.3 4 2 -22 25.6 5.7 4 2 -22 23.1 4.8 -4 -2 22 24.9 6.9 -4 -2 22 19.6 5.9 -4 -2 22 17.1 5.3 3 2 -22 24.3 6.4 3 2 -22 29.4 6.2 3 2 -22 26.6 5.4 -3 -2 22 33.8 7.7 -3 -2 22 25.3 6.5 -3 -2 22 32 8.9 2 2 -22 3.2 3.1 2 2 -22 -0.5 2.8 2 2 -22 2.6 2.8 -2 -2 22 -0.4 3.7 -2 -2 22 0.9 3.5 1 2 -22 29.7 5.7 1 2 -22 31.8 6.2 1 2 -22 41.5 5.1 1 2 -22 32.7 6.7 -1 -2 22 31.7 6.9 -1 -2 22 38.4 7.6 -1 -2 22 63.79 7.7 0 2 -22 47 7.2 0 2 -22 37.8 6.7 0 2 -22 46 8.1 0 2 -22 47.6 9.1 0 -2 22 46.2 7.5 0 -2 22 66.19 8.4 0 -2 22 64.59 8.9 -1 2 -22 2.9 3.7 -1 2 -22 14.9 4 -1 2 -22 -2.8 3.4 -1 2 -22 7.2 3.3 1 -2 22 10.2 4.2 1 -2 22 10.5 4.3 1 -2 22 12.4 4.9 4 1 -22 19.1 5 4 1 -22 11.5 4.3 -4 -1 22 11.7 4.5 -4 -1 22 7.6 4.6 -4 -1 22 22.7 5 3 1 -22 4.9 3.8 3 1 -22 0.9 3.4 3 1 -22 10.4 4 3 1 -22 12.8 5.1 -3 -1 22 9.5 4.3 -3 -1 22 11.2 3.6 -3 -1 22 8 4.6 2 1 -22 -1.7 2.6 2 1 -22 -5 2.4 2 1 -22 4 2.4 -2 -1 22 -1.9 3 -2 -1 22 -0.5 3.2 -2 -1 22 6.8 3.6 1 1 -22 23.4 4 1 1 -22 11.2 4.8 1 1 -22 5.7 3.9 1 1 -22 8.4 3.6 -1 -1 22 11.1 4.9 -1 -1 22 15 4.3 -1 -1 22 12.1 4.8 0 1 -22 5.2 3.8 0 1 -22 -1.7 2.6 0 1 -22 9.5 3.3 0 1 -22 6.7 3.6 0 -1 22 1.8 3.5 0 -1 22 4.8 3.6 0 -1 22 8.2 4.2 2 0 -22 8.4 4.3 2 0 -22 20.2 3.8 2 0 -22 6.7 3.3 -2 0 22 14.1 5.2 -2 0 22 7.1 5.8 -2 0 22 9.4 4.5 1 0 -22 10.7 3.6 -1 0 22 5.7 3.8 1 6 -23 1.2 2.6 1 6 -23 6.6 3.5 -1 -6 23 8.7 3 -1 -6 23 3.8 3.8 0 6 -23 43.3 7 0 6 -23 36.8 7.8 0 -6 23 34.7 7.2 -2 -5 23 18.3 6.1 1 5 -23 46.9 8.1 1 5 -23 45.5 7.6 1 5 -23 39.5 7 -1 -5 23 37.5 7.2 -1 -5 23 70.89 9.4 0 5 -23 17.4 5.1 0 5 -23 18.8 5 0 -5 23 22.7 4.8 0 -5 23 35.7 7.7 1 4 -23 75.99 9.1 1 4 -23 76.39 8.8 -1 -4 23 90.89 9.5 -1 -4 23 93.39 11 -1 -4 23 63.19 9.4 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 C1 H1 119.32(15) . . ? N1 C1 H1 119.32(12) . . ? N1 C1 C2 121.4(2) . . ? H2 C2 C1 120.46(15) . . ? C3 C2 C1 119.1(2) . . ? C3 C2 H2 120.46(16) . . ? H3 C3 C2 119.53(16) . . ? C4 C3 C2 120.9(2) . . ? C4 C3 H3 119.53(16) . . ? H4 C4 C3 121.40(16) . . ? C5 C4 C3 117.2(2) . . ? C5 C4 H4 121.40(13) . . ? N1 C5 C4 121.79(19) . . ? N2 C5 C4 130.7(2) . . ? N2 C5 N1 107.44(17) . . ? C7 C6 H6 118.93(14) . . ? N3 C6 H6 118.93(13) . . ? N3 C6 C7 122.1(2) . . ? C8 C7 C6 120.3(2) . . ? C20 C7 C6 120.6(2) . . ? C20 C7 C8 119.1(2) . . ? H8 C8 C7 119.04(15) . . ? C9 C8 C7 121.9(3) . . ? C9 C8 H8 119.0(2) . . ? H9 C9 C8 119.5(2) . . ? C10 C9 C8 121.0(3) . . ? C10 C9 H9 119.51(18) . . ? C11 C10 C9 121.7(4) . . ? C21 C10 C9 119.0(3) . . ? C21 C10 C11 119.2(3) . . ? H11 C11 C10 119.8(3) . . ? C12 C11 C10 120.4(4) . . ? C12 C11 H11 119.8(3) . . ? H12 C12 C11 118.7(3) . . ? C13 C12 C11 122.6(3) . . ? C13 C12 H12 118.71(19) . . ? C14 C13 C12 124.7(4) . . ? C22 C13 C12 118.5(3) . . ? C22 C13 C14 116.8(5) . . ? H14 C14 C13 118.7(3) . . ? C15 C14 C13 122.6(4) . . ? C15 C14 H14 118.7(2) . . ? H15 C15 C14 119.3(2) . . ? C16 C15 C14 121.4(4) . . ? C16 C15 H15 119.3(3) . . ? H16 C16 C15 120.6(3) . . ? C17 C16 C15 118.9(5) . . ? C17 C16 H16 120.6(3) . . ? C18 C17 C16 120.6(4) . . ? C22 C17 C16 120.3(4) . . ? C22 C17 C18 119.1(3) . . ? H18 C18 C17 119.7(2) . . ? C19 C18 C17 120.6(4) . . ? C19 C18 H18 119.7(2) . . ? H19 C19 C18 119.1(2) . . ? C20 C19 C18 121.7(3) . . ? C20 C19 H19 119.15(15) . . ? C19 C20 C7 123.3(2) . . ? C21 C20 C7 118.2(3) . . ? C21 C20 C19 118.5(2) . . ? C20 C21 C10 120.8(3) . . ? C22 C21 C10 120.2(3) . . ? C22 C21 C20 119.1(3) . . ? C17 C22 C13 119.9(3) . . ? C21 C22 C13 119.1(4) . . ? C21 C22 C17 121.0(3) . . ? C29 C24 C25 118.57(19) . . ? P1 C24 C25 119.33(16) . . ? P1 C24 C29 122.09(16) . . ? H25 C25 C24 119.68(13) . . ? C26 C25 C24 120.6(2) . . ? C26 C25 H25 119.68(15) . . ? H26 C26 C25 119.98(15) . . ? C27 C26 C25 120.0(2) . . ? C27 C26 H26 119.98(14) . . ? H27 C27 C26 120.04(14) . . ? C28 C27 C26 119.9(2) . . ? C28 C27 H27 120.04(13) . . ? H28 C28 C27 119.81(13) . . ? C29 C28 C27 120.4(2) . . ? C29 C28 H28 119.81(14) . . ? C28 C29 C24 120.4(2) . . ? H29 C29 C24 119.79(12) . . ? H29 C29 C28 119.79(13) . . ? C35 C30 C31 118.34(19) . . ? P1 C30 C31 120.57(16) . . ? P1 C30 C35 120.63(16) . . ? H31 C31 C30 119.66(12) . . ? C32 C31 C30 120.7(2) . . ? C32 C31 H31 119.66(14) . . ? H32 C32 C31 119.95(14) . . ? C33 C32 C31 120.1(2) . . ? C33 C32 H32 119.95(14) . . ? H33 C33 C32 119.96(14) . . ? C34 C33 C32 120.1(2) . . ? C34 C33 H33 119.96(16) . . ? H34 C34 C33 119.90(16) . . ? C35 C34 C33 120.2(2) . . ? C35 C34 H34 119.90(15) . . ? C34 C35 C30 120.6(2) . . ? H35 C35 C30 119.71(13) . . ? H35 C35 C34 119.71(15) . . ? C41 C36 C37 118.8(2) . . ? P1 C36 C37 123.17(17) . . ? P1 C36 C41 118.02(16) . . ? H37 C37 C36 119.70(13) . . ? C38 C37 C36 120.6(2) . . ? C38 C37 H37 119.70(17) . . ? H38 C38 C37 119.87(17) . . ? C39 C38 C37 120.3(3) . . ? C39 C38 H38 119.87(16) . . ? H39 C39 C38 120.01(16) . . ? C40 C39 C38 120.0(2) . . ? C40 C39 H39 120.01(16) . . ? H40 C40 C39 119.97(16) . . ? C41 C40 C39 120.1(3) . . ? C41 C40 H40 119.97(16) . . ? C40 C41 C36 120.3(2) . . ? H41 C41 C36 119.86(13) . . ? H41 C41 C40 119.86(16) . . ? C5 N1 C1 119.60(18) . . ? Ru1 N1 C1 145.98(15) . . ? Ru1 N1 C5 94.39(12) . . ? N3 N2 C5 118.02(16) . . ? Ru1 N2 C5 96.59(12) . . ? Ru1 N2 N3 145.34(13) . . ? N2 N3 C6 115.77(18) . . ? C30 P1 C24 103.11(9) . . ? C36 P1 C24 101.87(9) . . ? C36 P1 C30 104.68(10) . . ? Ru1 P1 C24 118.58(7) . . ? Ru1 P1 C30 111.41(7) . . ? Ru1 P1 C36 115.53(7) . . ? C42 P2 Ru1 116.13(12) . . ? C48 P2 Ru1 111.91(16) . . ? C48 P2 C42 100.02(19) . . ? C54 P2 Ru1 114.4(2) . . ? C54 P2 C42 111.1(3) . . ? C54 P2 C48 101.2(2) . . ? C70 P2 Ru1 114.7(2) . . ? C70 P2 C42 100.3(3) . . ? C70 P2 C48 112.5(3) . . ? C70 P2 C54 13.9(4) . . ? C74 P2 Ru1 120.30(17) . . ? C74 P2 C42 8.3(3) . . ? C74 P2 C48 103.8(2) . . ? C74 P2 C54 103.0(3) . . ? C74 P2 C70 91.9(3) . . ? C75 P2 Ru1 109.5(3) . . ? C75 P2 C42 106.0(3) . . ? C75 P2 C48 6.2(3) . . ? C75 P2 C54 97.6(3) . . ? C75 P2 C70 109.5(3) . . ? C75 P2 C74 109.6(3) . . ? C1B P2 Ru1 125.1(3) . . ? C1B P2 C42 98.3(3) . . ? C1B P2 C48 101.7(4) . . ? C1B P2 C54 13.1(4) . . ? C1B P2 C70 11.7(4) . . ? C1B P2 C74 90.2(4) . . ? C1B P2 C75 99.3(4) . . ? C82 P2 Ru1 112.5(3) . . ? C82 P2 C42 99.1(4) . . ? C82 P2 C48 0.9(4) . . ? C82 P2 C54 101.5(4) . . ? C82 P2 C70 112.6(4) . . ? C82 P2 C74 102.8(4) . . ? C82 P2 C75 7.0(5) . . ? C82 P2 C1B 101.8(5) . . ? N1 Ru1 Cl1 100.28(6) . . y N2 Ru1 Cl1 161.80(6) . . y N2 Ru1 N1 61.57(6) . . y P1 Ru1 Cl1 91.30(3) . . y P1 Ru1 N1 89.28(5) . . y P1 Ru1 N2 89.89(5) . . y P2 Ru1 Cl1 87.00(4) . . y P2 Ru1 N1 89.40(5) . . y P2 Ru1 N2 91.21(5) . . y P2 Ru1 P1 177.634(18) . . y C76 Ru1 Cl1 3.6(4) . . y C76 Ru1 N1 103.9(4) . . y C76 Ru1 N2 165.4(4) . . y C76 Ru1 P1 91.1(5) . . y C76 Ru1 P2 87.3(5) . . y Cl2 Ru1 Cl1 99.57(10) . . y Cl2 Ru1 N1 159.99(10) . . y Cl2 Ru1 N2 98.63(10) . . y Cl2 Ru1 P1 87.72(10) . . y Cl2 Ru1 P2 94.19(10) . . y Cl2 Ru1 C76 95.9(4) . . y C23 Ru1 Cl1 97.08(16) . . y C23 Ru1 N1 162.64(16) . . y C23 Ru1 N2 101.07(16) . . y C23 Ru1 P1 90.76(16) . . y C23 Ru1 P2 91.08(16) . . y C23 Ru1 C76 93.5(5) . . y C23 Ru1 Cl2 3.9(2) . . y C43 C42 P2 121.2 . . ? C46 C42 P2 118.6 . . ? C46 C42 C43 120.0 . . ? H43 C43 C42 120.00(14) . . ? C44 C43 C42 120.0 . . ? C44 C43 H43 120.00(14) . . ? H44 C44 C43 120.00(14) . . ? C45 C44 C43 120.0 . . ? C45 C44 H44 120.00(14) . . ? H45 C45 C44 120.00(14) . . ? C47 C45 C44 120.0 . . ? C47 C45 H45 120.00(14) . . ? H47 C47 C45 120.00(14) . . ? C46 C47 C45 120.0 . . ? C46 C47 H47 120.00(14) . . ? C47 C46 C42 120.0 . . ? H46 C46 C42 120.00(14) . . ? H46 C46 C47 120.00(14) . . ? C64 C48 P2 120.9 . . ? C60 C48 P2 118.9 . . ? C60 C48 C64 120.0 . . ? H64 C64 C48 120.00(16) . . ? C63 C64 C48 120.0 . . ? C63 C64 H64 120.00(16) . . ? H63 C63 C64 120.00(16) . . ? C62 C63 C64 120.0 . . ? C62 C63 H63 120.00(16) . . ? H62 C62 C63 120.00(16) . . ? C61 C62 C63 120.0 . . ? C61 C62 H62 120.00(16) . . ? H61 C61 C62 120.00(16) . . ? C60 C61 C62 120.0 . . ? C60 C61 H61 120.00(16) . . ? C61 C60 C48 120.0 . . ? H60 C60 C48 120.00(16) . . ? H60 C60 C61 120.00(16) . . ? C55 C54 P2 113.7 . . ? C59 C54 P2 126.2 . . ? C59 C54 C55 120.0 . . ? H55 C55 C54 120.0(2) . . ? C58 C55 C54 120.0 . . ? C58 C55 H55 120.0(2) . . ? H58 C58 C55 120.0(2) . . ? C56 C58 C55 120.0 . . ? C56 C58 H58 120.0(2) . . ? H56 C56 C58 120.0(2) . . ? C57 C56 C58 120.0 . . ? C57 C56 H56 120.0(2) . . ? H57 C57 C56 120.0(2) . . ? C59 C57 C56 120.0 . . ? C59 C57 H57 120.0(2) . . ? C57 C59 C54 120.0 . . ? H59 C59 C54 120.0(2) . . ? H59 C59 C57 120.0(2) . . ? C71 C70 P2 117.2 . . ? CXF C70 P2 122.6 . . ? CXF C70 C71 120.0 . . ? H71 C71 C70 120.0(2) . . ? C72 C71 C70 120.0 . . ? C72 C71 H71 120.0(2) . . ? H72 C72 C71 120.0(2) . . ? C73 C72 C71 120.0 . . ? C73 C72 H72 120.0(2) . . ? H73 C73 C72 120.0(2) . . ? CXE C73 C72 120.0 . . ? CXE C73 H73 120.0(2) . . ? HXE CXE C73 120.0(2) . . ? CXF CXE C73 120.0 . . ? CXF CXE HXE 120.0(2) . . ? CXE CXF C70 120.0 . . ? HXF CXF C70 120.0(2) . . ? HXF CXF CXE 120.0(2) . . ? C67 C74 P2 119.8 . . ? C68 C74 P2 120.2 . . ? C68 C74 C67 120.0 . . ? H67 C67 C74 120.00(17) . . ? C66 C67 C74 120.0 . . ? C66 C67 H67 120.00(17) . . ? H66 C66 C67 120.00(17) . . ? C65 C66 C67 120.0 . . ? C65 C66 H66 120.00(17) . . ? H65 C65 C66 120.00(17) . . ? C69 C65 C66 120.0 . . ? C69 C65 H65 120.00(17) . . ? H69 C69 C65 120.00(17) . . ? C68 C69 C65 120.0 . . ? C68 C69 H69 120.00(17) . . ? C69 C68 C74 120.0 . . ? H68 C68 C74 120.00(17) . . ? H68 C68 C69 120.00(17) . . ? C50 C75 P2 119.3 . . ? C52 C75 P2 120.4 . . ? C52 C75 C50 120.0 . . ? H50 C50 C75 120.00(17) . . ? C51 C50 C75 120.0 . . ? C51 C50 H50 120.00(17) . . ? H51 C51 C50 120.00(17) . . ? C49 C51 C50 120.0 . . ? C49 C51 H51 120.00(17) . . ? H49 C49 C51 120.00(17) . . ? C53 C49 C51 120.0 . . ? C53 C49 H49 120.00(17) . . ? H53 C53 C49 120.00(17) . . ? C52 C53 C49 120.0 . . ? C52 C53 H53 120.00(17) . . ? C53 C52 C75 120.0 . . ? H52 C52 C75 120.00(17) . . ? H52 C52 C53 120.00(17) . . ? C78 C77 H77 120.0 . . ? C1B C77 H77 120.0 . . ? C1B C77 C78 120.0 . . ? H78 C78 C77 120.0(3) . . ? C79 C78 C77 120.0 . . ? C79 C78 H78 120.0(3) . . ? H79 C79 C78 120.0(3) . . ? CXD C79 C78 120.0 . . ? CXD C79 H79 120.0(3) . . ? HXD CXD C79 120.0(3) . . ? C1A CXD C79 120.0 . . ? C1A CXD HXD 120.0(3) . . ? H1A C1A CXD 120.0(3) . . ? C1B C1A CXD 120.0 . . ? C1B C1A H1A 120.0(3) . . ? C77 C1B P2 123.2(6) . . ? C1A C1B P2 116.6(6) . . ? C1A C1B C77 120.0 . . ? O2 C76 Ru1 174.7(15) . . ? O1 C23 Ru1 174.9(6) . . ? C81 C80 H80 120.0 . . ? C1E C80 H80 120.0 . . ? C1E C80 C81 120.0 . . ? H81 C81 C80 120.0(3) . . ? C82 C81 C80 120.0 . . ? C82 C81 H81 120.0(3) . . ? C81 C82 P2 121.4(6) . . ? C1C C82 P2 118.4(6) . . ? C1C C82 C81 120.0 . . ? H1C C1C C82 120.0(3) . . ? C1D C1C C82 120.0 . . ? C1D C1C H1C 120.0(3) . . ? H1D C1D C1C 120.0(3) . . ? C1E C1D C1C 120.000000000(16) . . ? C1E C1D H1D 120.0(3) . . ? C1D C1E C80 120.000000000(14) . . ? H1E C1E C80 120.0(3) . . ? H1E C1E C1D 120.0(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 H1 0.9300 . y C1 C2 1.365(4) . y C1 N1 1.330(3) . y C2 H2 0.9300 . y C2 C3 1.381(4) . y C3 H3 0.9300 . y C3 C4 1.366(4) . y C4 H4 0.9300 . y C4 C5 1.389(3) . y C5 N1 1.358(2) . y C5 N2 1.342(2) . y C6 H6 0.9300 . y C6 C7 1.449(3) . y C6 N3 1.286(3) . y C7 C8 1.398(4) . y C7 C20 1.413(3) . y C8 H8 0.9300 . y C8 C9 1.368(4) . y C9 H9 0.9300 . y C9 C10 1.391(5) . y C10 C11 1.433(4) . y C10 C21 1.398(5) . y C11 H11 0.9300 . y C11 C12 1.339(6) . y C12 H12 0.9300 . y C12 C13 1.401(6) . y C13 C14 1.401(6) . y C13 C22 1.438(5) . y C14 H14 0.9300 . y C14 C15 1.360(7) . y C15 H15 0.9300 . y C15 C16 1.377(7) . y C16 H16 0.9300 . y C16 C17 1.413(4) . y C17 C18 1.438(5) . y C17 C22 1.403(5) . y C18 H18 0.9300 . y C18 C19 1.353(4) . y C19 H19 0.9300 . y C19 C20 1.431(4) . y C20 C21 1.440(4) . y C21 C22 1.416(4) . y C24 C25 1.380(3) . y C24 C29 1.382(3) . y C24 P1 1.8340(19) . y C25 H25 0.9300 . y C25 C26 1.386(3) . y C26 H26 0.9300 . y C26 C27 1.373(4) . y C27 H27 0.9300 . y C27 C28 1.360(3) . y C28 H28 0.9300 . y C28 C29 1.389(3) . y C29 H29 0.9300 . y C30 C31 1.393(3) . y C30 C35 1.384(3) . y C30 P1 1.822(2) . y C31 H31 0.9300 . y C31 C32 1.379(3) . y C32 H32 0.9300 . y C32 C33 1.367(4) . y C33 H33 0.9300 . y C33 C34 1.374(4) . y C34 H34 0.9300 . y C34 C35 1.380(3) . y C35 H35 0.9300 . y C36 C37 1.387(3) . y C36 C41 1.387(3) . y C36 P1 1.833(2) . y C37 H37 0.9300 . y C37 C38 1.379(3) . y C38 H38 0.9300 . y C38 C39 1.374(4) . y C39 H39 0.9300 . y C39 C40 1.375(4) . y C40 H40 0.9300 . y C40 C41 1.389(3) . y C41 H41 0.9300 . y Cl1 Ru1 2.4220(9) . y N1 Ru1 2.1447(16) . y N2 N3 1.349(2) . y N2 Ru1 2.1070(16) . y P1 Ru1 2.3889(5) . y P2 Ru1 2.3968(6) . y P2 C42 1.894(3) . y P2 C48 1.906(3) . y P2 C54 1.834(5) . y P2 C70 1.884(6) . y P2 C74 1.753(4) . y P2 C75 1.678(4) . y P2 C1B 1.790(7) . y P2 C82 1.941(8) . y Ru1 C76 1.8171(19) . y Ru1 Cl2 2.4180(17) . y Ru1 C23 1.8165(16) . y C42 C43 1.3900 . y C42 C46 1.3900 . y C43 H43 0.9300 . y C43 C44 1.3900 . y C44 H44 0.9300 . y C44 C45 1.3900 . y C45 H45 0.9300 . y C45 C47 1.3900 . y C47 H47 0.9300 . y C47 C46 1.3900 . y C46 H46 0.9300 . y C48 C64 1.3900 . y C48 C60 1.3900 . y C64 H64 0.9300 . y C64 C63 1.3900 . y C63 H63 0.9300 . y C63 C62 1.3900 . y C62 H62 0.9300 . y C62 C61 1.3900 . y C61 H61 0.9300 . y C61 C60 1.3900 . y C60 H60 0.9300 . y C54 C55 1.3900 . y C54 C59 1.3900 . y C55 H55 0.9300 . y C55 C58 1.3900 . y C58 H58 0.9300 . y C58 C56 1.3900 . y C56 H56 0.9300 . y C56 C57 1.3900 . y C57 H57 0.9300 . y C57 C59 1.3900 . y C59 H59 0.9300 . y C70 C71 1.3900 . y C70 CXF 1.3900 . y C71 H71 0.9300 . y C71 C72 1.3900 . y C72 H72 0.9300 . y C72 C73 1.3900 . y C73 H73 0.9300 . y C73 CXE 1.3900 . y CXE HXE 0.9300 . y CXE CXF 1.3900 . y CXF HXF 0.9300 . y C74 C67 1.3900 . y C74 C68 1.3900 . y C67 H67 0.9300 . y C67 C66 1.3900 . y C66 H66 0.9300 . y C66 C65 1.3900 . y C65 H65 0.9300 . y C65 C69 1.3900 . y C69 H69 0.9300 . y C69 C68 1.3900 . y C68 H68 0.9300 . y C75 C50 1.3900 . y C75 C52 1.3900 . y C50 H50 0.9300 . y C50 C51 1.3900 . y C51 H51 0.9300 . y C51 C49 1.3900 . y C49 H49 0.9300 . y C49 C53 1.3900 . y C53 H53 0.9300 . y C53 C52 1.3900 . y C52 H52 0.9300 . y C77 H77 0.9300 . y C77 C78 1.3900 . y C77 C1B 1.3900 . y C78 H78 0.9300 . y C78 C79 1.3900 . y C79 H79 0.9300 . y C79 CXD 1.3900 . y CXD HXD 0.9300 . y CXD C1A 1.3900 . y C1A H1A 0.9300 . y C1A C1B 1.3900 . y O2 C76 1.152(2) . y O1 C23 1.1507(17) . y C80 H80 0.9300 . y C80 C81 1.3900 . y C80 C1E 1.3900 . y C81 H81 0.9300 . y C81 C82 1.3900 . y C82 C1C 1.3900 . y C1C H1C 0.9300 . y C1C C1D 1.3900 . y C1D H1D 0.9300 . y C1D C1E 1.3900 . y C1E H1E 0.9300 . y loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C1 C2 C3 C4 0.9(5) . . . . ? C1 N1 C5 C4 1.5(3) . . . . ? C1 N1 C5 N2 179.4(2) . . . . ? C2 C3 C4 C5 -0.8(5) . . . . ? C3 C4 C5 N1 -0.4(4) . . . . ? C3 C4 C5 N2 -177.8(3) . . . . ? C4 C5 N1 Ru1 -177.1(3) . . . . ? C4 C5 N2 N3 -1.4(4) . . . . ? C4 C5 N2 Ru1 176.8(3) . . . . ? C5 N2 N3 C6 171.8(2) . . . . ? C6 C7 C8 C9 -179.6(4) . . . . ? C6 C7 C20 C19 -0.5(4) . . . . ? C6 C7 C20 C21 179.4(3) . . . . ? C6 N3 N2 Ru1 -5.1(3) . . . . ? C7 C8 C9 C10 0.0(4) . . . . ? C7 C20 C19 C18 -179.2(3) . . . . ? C7 C20 C21 C10 0.4(4) . . . . ? C7 C20 C21 C22 179.4(3) . . . . ? C8 C9 C10 C11 179.7(4) . . . . ? C8 C9 C10 C21 0.3(5) . . . . ? C9 C10 C11 C12 -179.9(4) . . . . ? C9 C10 C21 C20 -0.5(4) . . . . ? C9 C10 C21 C22 -179.5(3) . . . . ? C10 C11 C12 C13 -1.0(5) . . . . ? C10 C21 C20 C19 -179.7(3) . . . . ? C10 C21 C22 C13 -0.2(4) . . . . ? C10 C21 C22 C17 178.5(3) . . . . ? C11 C12 C13 C14 -176.6(4) . . . . ? C11 C12 C13 C22 1.9(5) . . . . ? C12 C13 C14 C15 178.1(4) . . . . ? C12 C13 C22 C17 -179.9(3) . . . . ? C12 C13 C22 C21 -1.3(4) . . . . ? C13 C14 C15 C16 1.1(5) . . . . ? C13 C22 C17 C16 2.3(3) . . . . ? C13 C22 C17 C18 -179.9(3) . . . . ? C13 C22 C21 C20 -179.2(3) . . . . ? C14 C15 C16 C17 -0.1(5) . . . . ? C15 C16 C17 C18 -179.4(3) . . . . ? C15 C16 C17 C22 -1.6(4) . . . . ? C16 C17 C18 C19 176.5(3) . . . . ? C16 C17 C22 C21 -176.3(3) . . . . ? C17 C18 C19 C20 0.1(4) . . . . ? C17 C22 C21 C20 -0.5(3) . . . . ? C18 C19 C20 C21 0.9(4) . . . . ? C19 C20 C21 C22 -0.7(3) . . . . ? C24 C25 C26 C27 0.3(3) . . . . ? C24 C29 C28 C27 0.5(3) . . . . ? C25 C26 C27 C28 0.4(4) . . . . ? C26 C27 C28 C29 -0.9(3) . . . . ? C30 C31 C32 C33 -0.2(3) . . . . ? C30 C35 C34 C33 0.2(4) . . . . ? C31 C32 C33 C34 0.8(4) . . . . ? C32 C33 C34 C35 -0.8(4) . . . . ? C36 C37 C38 C39 -0.1(3) . . . . ? C36 C41 C40 C39 0.0(3) . . . . ? C37 C38 C39 C40 1.2(3) . . . . ? C38 C39 C40 C41 -1.2(3) . . . . ? P2 C42 C43 C44 -174.74(11) . . . . ? P2 C42 C46 C47 174.88(11) . . . . ? P2 C48 C64 C63 -174.86(12) . . . . ? P2 C48 C60 C61 174.97(12) . . . . ? P2 C54 C55 C58 178.5(2) . . . . ? P2 C54 C59 C57 -178.3(2) . . . . ? P2 C70 C71 C72 175.39(19) . . . . ? P2 C70 CXF CXE -175.14(19) . . . . ? P2 C74 C67 C66 179.63(17) . . . . ? P2 C74 C68 C69 -179.63(17) . . . . ? P2 C75 C50 C51 174.73(19) . . . . ? P2 C75 C52 C53 -174.67(19) . . . . ? P2 C1B C77 C78 -175.8(3) . . . . ? P2 C1B C1A CXD 176.1(3) . . . . ? P2 C82 C81 C80 -174.1(3) . . . . ? P2 C82 C1C C1D 174.3(3) . . . . ? C42 C43 C44 C45 0.0(3) . . . . ? C42 C46 C47 C45 -0.0(3) . . . . ? C43 C44 C45 C47 -0.0(3) . . . . ? C44 C45 C47 C46 0.0(4) . . . . ? C48 C64 C63 C62 0.0(4) . . . . ? C48 C60 C61 C62 -0.0(4) . . . . ? C64 C63 C62 C61 -0.0(4) . . . . ? C63 C62 C61 C60 0.0(4) . . . . ? C54 C55 C58 C56 -0.0(7) . . . . ? C54 C59 C57 C56 0.0(6) . . . . ? C55 C58 C56 C57 0.0(6) . . . . ? C58 C56 C57 C59 -0.0(6) . . . . ? C70 C71 C72 C73 -0.0(7) . . . . ? C70 CXF CXE C73 0.0(7) . . . . ? C71 C72 C73 CXE 0.0(7) . . . . ? C72 C73 CXE CXF -0.0(6) . . . . ? C74 C67 C66 C65 0.0(5) . . . . ? C74 C68 C69 C65 -0.0(4) . . . . ? C67 C66 C65 C69 0.0(4) . . . . ? C66 C65 C69 C68 -0.0(5) . . . . ? C75 C50 C51 C49 -0.0(6) . . . . ? C75 C52 C53 C49 -0.0(6) . . . . ? C50 C51 C49 C53 -0.0(6) . . . . ? C51 C49 C53 C52 0.0(6) . . . . ? C77 C78 C79 CXD -0.0(8) . . . . ? C77 C1B C1A CXD -0.0(9) . . . . ? C78 C79 CXD C1A 0.0(9) . . . . ? C79 CXD C1A C1B -0.0(8) . . . . ? C80 C81 C82 C1C 0.0(8) . . . . ? C80 C1E C1D C1C 0.0(11) . . . . ? C81 C82 C1C C1D -0.0(11) . . . . ? C82 C1C C1D C1E -0.0(10) . . . . ? loop_ _restr_equal_distance_atom_site_label_1 _restr_equal_distance_atom_site_label_2 _restr_equal_distance_site_symmetry_2 _restr_equal_distance_class_id Ru1 Cl1 1 2 Ru1 C76 1 3 Ru1 Cl2 1 2 Ru1 C23 1 3 O2 C76 1 1 O1 C23 1 1 loop_ _restr_equal_distance_class_class_id _restr_equal_distance_class_target_weight_param _restr_equal_distance_class_average _restr_equal_distance_class_esd _restr_equal_distance_class_diff_max 1 0.0010 1.1514 0.0007 0.0007 2 0.0010 2.4200 0.0020 0.0020 3 0.0010 1.8168 0.0003 0.0003