#------------------------------------------------------------------------------ #$Date: 2014-03-12 08:54:25 +0200 (Wed, 12 Mar 2014) $ #$Revision: 105515 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/11/21/7112102.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7112102 loop_ _publ_author_name 'Yan Li' 'Kartik Chandra Mondal' 'Peter Stollberg' 'Hongping Zhu' 'Herbert W. Roesky' 'Regine Herbst-Irmer' 'Dietmar Stalke' 'Heike Fliegl' _publ_section_title ; Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond ; _journal_name_full Chem.Commun. _journal_page_first 3356 _journal_volume 50 _journal_year 2014 _chemical_formula_moiety '2(C36 H44 Cl2 Ge2 N4), 3(C7 H8)' _chemical_formula_sum 'C93 H112 Cl4 Ge4 N8' _chemical_formula_weight 1774.06 _chemical_name_systematic ; ? ; _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2013 _cell_angle_alpha 98.61(2) _cell_angle_beta 102.61(2) _cell_angle_gamma 113.07(3) _cell_formula_units_Z 1 _cell_length_a 12.692(2) _cell_length_b 12.839(2) _cell_length_c 15.409(3) _cell_measurement_reflns_used 9752 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 20.726 _cell_measurement_theta_min 2.246 _cell_volume 2175.6(9) _computing_cell_refinement 'SAINT V7.68A' _computing_data_collection 'APEX2 v2012.2' _computing_data_reduction 'SAINT V7.68A' _computing_molecular_graphics 'XP Version 5.1' _computing_publication_material 'XSHELL in SHELXTL-97' _computing_structure_refinement 'SHELXL-2012 (Sheldrick, 2012)' _computing_structure_solution 'SHELXS-2012 (Sheldrick, 2012)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_device_type 'Bruker Smart APEX II Quazar' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type AgK\a _diffrn_radiation_wavelength 0.56086 _diffrn_reflns_av_R_equivalents 0.0476 _diffrn_reflns_av_unetI/netI 0.0299 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 64131 _diffrn_reflns_theta_full 19.665 _diffrn_reflns_theta_max 20.835 _diffrn_reflns_theta_min 1.445 _diffrn_source 'INCOATEC Ag Microsource' _exptl_absorpt_coefficient_mu 0.814 _exptl_absorpt_correction_T_max 0.8618 _exptl_absorpt_correction_T_min 0.7689 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS-2012/1 _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.354 _exptl_crystal_description block _exptl_crystal_F_000 922 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.552 _refine_diff_density_min -0.382 _refine_diff_density_rms 0.058 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.051 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 539 _refine_ls_number_reflns 9244 _refine_ls_number_restraints 227 _refine_ls_restrained_S_all 1.051 _refine_ls_R_factor_all 0.0323 _refine_ls_R_factor_gt 0.0258 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0237P)^2^+1.3017P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0608 _refine_ls_wR_factor_ref 0.0639 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8098 _reflns_number_total 9244 _reflns_threshold_expression 'I > 2\s(I)' _[local]_cod_data_source_file c4cc00251b2.cif _[local]_cod_data_source_block p-1_a _cod_original_cell_volume 2175.6(8) _cod_database_code 7112102 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _diffrn_reflns_laue_measured_fraction_max 0.995 _diffrn_reflns_laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_point_group_measured_fraction_full 1.000 _shelxl_version_number 2013-4 _shelx_res_file ; REM Solution 1 R1 0.103, Alpha = 0.0839 in P-1 REM C47 N4 Cl2 Ge2 TITL p-1 in P-1 CELL 0.56086 12.692 12.839 15.409 98.61 102.61 113.07 ZERR 1.00 0.002 0.002 0.003 0.02 0.02 0.03 LATT 1 SFAC C H N CL GE UNIT 93 112 8 4 4 TEMP -173.000 L.S. 10 BOND $H RIGU C1T > C7T SIMU C1T > C7T REM RIGU Ge1 Cl1 Ge2 Cl2 REM DFIX 1.00 C7 H7 C14 H14 rem LIST 6 LIST 4 ACTA CONF FMAP 2 PLAN 20 sadi c6 h6 c24 h24 WGHT 0.023700 1.301700 FVAR 0.31103 GE1 5 0.139183 0.576003 0.424173 11.00000 0.01716 0.01620 = 0.01453 0.00359 0.00752 0.00938 C1 1 0.129963 0.353813 0.469693 11.00000 0.01624 0.02391 = 0.01694 0.00845 0.00641 0.00898 AFIX 43 H1 2 0.098061 0.373674 0.516499 11.00000 -1.20000 AFIX 0 N1 3 0.160159 0.425464 0.414690 11.00000 0.01090 0.01588 = 0.01340 0.00379 0.00284 0.00589 CL1 4 -0.070471 0.465404 0.356077 11.00000 0.01633 0.03102 = 0.02494 0.01011 0.01091 0.01279 GE2 5 0.251015 0.274184 0.065530 11.00000 0.01371 0.01589 = 0.01491 -0.00101 0.00379 0.00727 N2 3 0.194098 0.574781 0.319026 11.00000 0.01373 0.01289 = 0.01403 0.00351 0.00617 0.00801 C2 1 0.144371 0.252365 0.459493 11.00000 0.02075 0.02227 = 0.02457 0.01360 0.00799 0.00962 AFIX 43 H2 2 0.124658 0.203130 0.499509 11.00000 -1.20000 AFIX 0 CL2 4 0.231865 0.120417 0.139563 11.00000 0.02433 0.01650 = 0.02643 0.00048 0.00191 0.01235 C5 1 0.206079 0.400707 0.347703 11.00000 0.00713 0.01520 = 0.01064 0.00175 -0.00064 0.00367 C4 1 0.218946 0.297469 0.332678 11.00000 0.01328 0.01652 = 0.01629 0.00379 0.00389 0.00730 AFIX 43 H4 2 0.248353 0.277783 0.284111 11.00000 -1.20000 AFIX 0 N4 3 0.303497 0.407179 0.164070 11.00000 0.00908 0.01359 = 0.01403 0.00075 0.00342 0.00575 C3 1 0.188493 0.223791 0.389163 11.00000 0.01886 0.01750 = 0.02551 0.00825 0.00579 0.00968 AFIX 43 H3 2 0.197749 0.153415 0.379882 11.00000 -1.20000 AFIX 0 N3 3 0.087980 0.256729 0.076936 11.00000 0.01252 0.01344 = 0.01283 0.00269 0.00062 0.00590 C6 1 0.243696 0.492993 0.295539 11.00000 0.00798 0.01274 = 0.01295 0.00231 0.00262 0.00524 H6 2 0.330122 0.529897 0.316305 11.00000 -1.20000 C16 1 0.446406 0.749815 0.425770 11.00000 0.01597 0.01461 = 0.01625 0.00045 0.00121 0.00648 AFIX 13 H16 2 0.400284 0.669820 0.432877 11.00000 -1.20000 AFIX 0 C7 1 0.244196 0.689417 0.302855 11.00000 0.01609 0.01384 = 0.01202 0.00244 0.00627 0.00817 C17 1 0.557280 0.752714 0.400806 11.00000 0.01926 0.02760 = 0.02880 0.00197 0.00475 0.01123 AFIX 137 H17A 2 0.604051 0.730886 0.447884 11.00000 -1.50000 H17B 2 0.606885 0.831988 0.397675 11.00000 -1.50000 H17C 2 0.532099 0.697128 0.340828 11.00000 -1.50000 AFIX 0 C9 1 0.408641 0.880359 0.330136 11.00000 0.01928 0.01522 = 0.01988 0.00121 0.00386 0.00348 AFIX 43 H9 2 0.491142 0.933681 0.357718 11.00000 -1.20000 AFIX 0 C18 1 0.483437 0.838957 0.517919 11.00000 0.03032 0.02348 = 0.01832 0.00091 0.00144 0.01358 AFIX 137 H18A 2 0.532049 0.820514 0.566369 11.00000 -1.50000 H18B 2 0.411324 0.835362 0.533266 11.00000 -1.50000 H18C 2 0.530624 0.918014 0.513065 11.00000 -1.50000 AFIX 0 C8 1 0.364723 0.771559 0.349813 11.00000 0.01699 0.01545 = 0.01323 0.00139 0.00455 0.00782 C15 1 -0.046202 0.700294 0.217541 11.00000 0.02342 0.03674 = 0.06110 0.00651 0.01185 0.01963 AFIX 137 H15A 2 -0.130626 0.642473 0.191231 11.00000 -1.50000 H15B 2 -0.031699 0.765608 0.188726 11.00000 -1.50000 H15C 2 -0.028107 0.729842 0.284082 11.00000 -1.50000 AFIX 0 C12 1 0.167302 0.723941 0.245889 11.00000 0.01810 0.01796 = 0.01442 0.00256 0.00535 0.01077 C11 1 0.214700 0.835641 0.231365 11.00000 0.02732 0.01975 = 0.01820 0.00610 0.00487 0.01557 AFIX 43 H11 2 0.163300 0.859197 0.193251 11.00000 -1.20000 AFIX 0 C10 1 0.334451 0.912389 0.271159 11.00000 0.03122 0.01311 = 0.02188 0.00600 0.00810 0.00801 AFIX 43 H10 2 0.366032 0.986742 0.258313 11.00000 -1.20000 AFIX 0 C14 1 0.008330 0.596029 0.096173 11.00000 0.02110 0.03022 = 0.02375 0.00791 -0.00029 0.00892 AFIX 137 H14A 2 -0.076967 0.541184 0.068645 11.00000 -1.50000 H14B 2 0.057541 0.555441 0.085881 11.00000 -1.50000 H14C 2 0.027515 0.661703 0.067640 11.00000 -1.50000 AFIX 0 C13 1 0.034704 0.642470 0.199718 11.00000 0.01622 0.02130 = 0.02362 0.00819 0.00446 0.01147 AFIX 13 H13 2 0.014445 0.573599 0.226731 11.00000 -1.20000 AFIX 0 C20 1 -0.124469 0.155994 0.038203 11.00000 0.01381 0.01575 = 0.02109 0.00474 -0.00035 0.00207 AFIX 43 H20 2 -0.198485 0.092355 0.000907 11.00000 -1.20000 AFIX 0 C19 1 -0.017110 0.165212 0.026056 11.00000 0.01748 0.01447 = 0.01632 0.00225 0.00062 0.00586 AFIX 43 H19 2 -0.017200 0.105937 -0.019031 11.00000 -1.20000 AFIX 0 C21 1 -0.121991 0.241908 0.106249 11.00000 0.01170 0.02182 = 0.02298 0.01108 0.00435 0.00761 AFIX 43 H21 2 -0.194635 0.236440 0.117053 11.00000 -1.20000 AFIX 0 C22 1 -0.013430 0.335557 0.158319 11.00000 0.01409 0.01648 = 0.01537 0.00489 0.00362 0.00790 AFIX 43 H22 2 -0.011048 0.394385 0.205204 11.00000 -1.20000 AFIX 0 C23 1 0.091921 0.342661 0.141352 11.00000 0.01219 0.01335 = 0.01146 0.00461 0.00169 0.00560 C24 1 0.215141 0.443045 0.188665 11.00000 0.00968 0.01239 = 0.01234 0.00350 0.00293 0.00633 H24 2 0.215837 0.508909 0.166346 11.00000 -1.20000 C25 1 0.422868 0.497815 0.179622 11.00000 0.00934 0.01395 = 0.01281 -0.00106 0.00260 0.00486 C33 1 0.584005 0.335842 0.272064 11.00000 0.02727 0.03178 = 0.03962 0.01433 0.01414 0.02018 AFIX 137 H33A 2 0.567407 0.270892 0.301376 11.00000 -1.50000 H33B 2 0.669425 0.391095 0.297279 11.00000 -1.50000 H33C 2 0.563922 0.305083 0.205437 11.00000 -1.50000 AFIX 0 C26 1 0.442544 0.585370 0.130886 11.00000 0.01341 0.01584 = 0.01574 0.00161 0.00598 0.00798 C32 1 0.537256 0.448636 0.394996 11.00000 0.02762 0.03011 = 0.01821 0.00749 0.00185 0.01292 AFIX 137 H32A 2 0.523332 0.384740 0.425353 11.00000 -1.50000 H32B 2 0.485525 0.486117 0.405620 11.00000 -1.50000 H32C 2 0.621686 0.506665 0.420368 11.00000 -1.50000 AFIX 0 C27 1 0.558755 0.673577 0.150987 11.00000 0.01813 0.01715 = 0.02315 0.00534 0.00963 0.00660 AFIX 43 H27 2 0.571963 0.735231 0.121266 11.00000 -1.20000 AFIX 0 C34 1 0.343803 0.583772 0.053503 11.00000 0.01446 0.01910 = 0.01532 0.00581 0.00470 0.00744 AFIX 13 H34 2 0.267754 0.513179 0.045892 11.00000 -1.20000 AFIX 0 C28 1 0.655567 0.673381 0.213407 11.00000 0.01097 0.01968 = 0.02526 0.00150 0.00665 0.00315 AFIX 43 H28 2 0.734010 0.734949 0.227008 11.00000 -1.20000 AFIX 0 C36 1 0.373542 0.573277 -0.037959 11.00000 0.02634 0.03869 = 0.01907 0.00968 0.01003 0.01748 AFIX 137 H36A 2 0.306019 0.566087 -0.087697 11.00000 -1.50000 H36B 2 0.387696 0.503678 -0.051430 11.00000 -1.50000 H36C 2 0.445873 0.643375 -0.033069 11.00000 -1.50000 AFIX 0 C29 1 0.637002 0.583032 0.255579 11.00000 0.01089 0.02520 = 0.01768 0.00101 0.00238 0.00844 AFIX 43 H29 2 0.704142 0.580975 0.295770 11.00000 -1.20000 AFIX 0 C35 1 0.321912 0.692567 0.075485 11.00000 0.02061 0.02486 = 0.02504 0.00987 0.00808 0.01322 AFIX 137 H35A 2 0.249676 0.682494 0.029168 11.00000 -1.50000 H35B 2 0.391286 0.761853 0.074733 11.00000 -1.50000 H35C 2 0.310772 0.702955 0.136615 11.00000 -1.50000 AFIX 0 C30 1 0.521893 0.494382 0.240697 11.00000 0.01401 0.01837 = 0.01315 0.00073 0.00445 0.00845 C31 1 0.507821 0.399076 0.290977 11.00000 0.01304 0.02219 = 0.01749 0.00464 0.00220 0.00887 AFIX 13 H31 2 0.421601 0.339754 0.267269 11.00000 -1.20000 AFIX 0 C37T 1 0.883317 0.033960 0.310776 11.00000 0.02921 0.02366 = 0.03012 0.00540 0.00422 0.00969 C38T 1 0.853077 0.127406 0.318917 11.00000 0.04606 0.02903 = 0.03093 0.01309 0.00910 0.02030 AFIX 43 H38T 2 0.853743 0.166974 0.271499 11.00000 -1.20000 AFIX 0 C39T 1 0.822134 0.163801 0.394463 11.00000 0.03990 0.02790 = 0.03742 0.01016 0.00962 0.01944 AFIX 43 H39T 2 0.801244 0.227396 0.398271 11.00000 -1.20000 AFIX 0 C40T 1 0.821470 0.107717 0.464849 11.00000 0.02933 0.02811 = 0.03085 0.00678 0.00807 0.00928 AFIX 43 H40T 2 0.800016 0.132263 0.516853 11.00000 -1.20000 AFIX 0 C41T 1 0.852518 0.015599 0.458073 11.00000 0.02944 0.02480 = 0.03311 0.01331 0.00507 0.00661 AFIX 43 H41T 2 0.853262 -0.022907 0.506106 11.00000 -1.20000 AFIX 0 C42T 1 0.882448 -0.020853 0.382033 11.00000 0.02614 0.01792 = 0.03618 0.00781 0.00247 0.00885 AFIX 43 H42T 2 0.902879 -0.084743 0.378335 11.00000 -1.20000 AFIX 0 C43T 1 0.917277 -0.004544 0.228155 11.00000 0.05192 0.03449 = 0.03759 0.00781 0.01447 0.02321 AFIX 137 H43A 2 0.970125 -0.041829 0.245199 11.00000 -1.50000 H43B 2 0.959332 0.063869 0.206805 11.00000 -1.50000 H43C 2 0.844467 -0.060723 0.178707 11.00000 -1.50000 AFIX 0 PART -1 same c43t c40t c39t c38t c37t c42t c41t SAME C1t C2t C7t C6t C5t C4t C3t C1T 1 0.584634 0.005668 0.160793 10.50000 0.03760 0.06429 = 0.05419 0.01038 0.01127 -0.00765 AFIX 137 H1TA 2 0.655304 -0.009556 0.165792 10.50000 -1.50000 H1TB 2 0.524636 -0.054833 0.179200 10.50000 -1.50000 H1TC 2 0.608453 0.082868 0.201258 10.50000 -1.50000 AFIX 0 same c3t c4t c5t c6t c7t c2t C2T 1 0.425565 -0.000738 -0.114839 10.50000 0.05494 0.05270 = 0.05276 0.02743 0.01021 -0.01655 AFIX 43 H2T 2 0.388263 -0.002901 -0.176092 10.50000 -1.20000 AFIX 0 C3T 1 0.402455 0.051474 -0.042878 10.50000 0.02872 0.05618 = 0.08226 0.03759 0.02158 0.00535 AFIX 43 H3T 2 0.349568 0.087065 -0.054052 10.50000 -1.20000 AFIX 0 C4T 1 0.454701 0.053724 0.046578 10.50000 0.02707 0.02599 = 0.06325 0.00880 0.02685 0.01197 AFIX 43 H4T 2 0.437025 0.090036 0.096201 10.50000 -1.20000 AFIX 0 C5T 1 0.532158 0.003426 0.063619 10.50000 0.02055 0.02703 = 0.04814 0.00254 0.01463 0.00132 C6T 1 0.557804 -0.049257 -0.007935 10.50000 0.03375 0.02212 = 0.05176 0.00591 0.02877 0.00547 AFIX 43 H6T 2 0.611332 -0.084046 0.003933 10.50000 -1.20000 AFIX 0 C7T 1 0.505248 -0.051550 -0.097763 10.50000 0.06909 0.02954 = 0.05864 0.00706 0.03530 -0.00719 AFIX 43 H7T 2 0.523191 -0.087389 -0.147447 10.50000 -1.20000 REM ##### REM ##### REM ##### REM ##### REM ##### AFIX 0 HKLF 4 REM p-1 in P-1 REM R1 = 0.0258 for 8098 Fo > 4sig(Fo) and 0.0323 for all 9244 data REM 539 parameters refined using 227 restraints END WGHT 0.0237 1.3016 REM Highest difference peak 0.552, deepest hole -0.382, 1-sigma level 0.058 Q1 1 0.2822 0.3623 0.0904 11.00000 0.05 0.55 Q2 1 0.1750 0.6635 0.4418 11.00000 0.05 0.46 Q3 1 0.2227 0.1922 0.0544 11.00000 0.05 0.41 Q4 1 0.2163 0.4484 0.3187 11.00000 0.05 0.38 Q5 1 0.1621 0.5762 0.3507 11.00000 0.05 0.36 Q6 1 0.4531 -0.0403 -0.1342 11.00000 0.05 0.34 Q7 1 0.1150 0.4841 0.4134 11.00000 0.05 0.34 Q8 1 0.1381 0.6402 0.4629 11.00000 0.05 0.34 Q9 1 0.2269 0.2762 0.3777 11.00000 0.05 0.34 Q10 1 0.5189 0.4572 0.2733 11.00000 0.05 0.33 Q11 1 0.3601 0.5862 0.0116 11.00000 0.05 0.33 Q12 1 0.2201 0.6338 0.3160 11.00000 0.05 0.33 Q13 1 0.2228 0.4591 0.2437 11.00000 0.05 0.32 Q14 1 0.5807 0.5352 0.2431 11.00000 0.05 0.32 Q15 1 0.2475 0.2197 0.0129 11.00000 0.05 0.32 Q16 1 0.4344 0.5541 0.1670 11.00000 0.05 0.32 Q17 1 0.4697 0.7960 0.4644 11.00000 0.05 0.31 Q18 1 0.3976 0.0228 -0.0942 11.00000 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6.79905 7 -9 -2 0 73.1429 5.44251 8 -9 -2 0 63.0410 6.71628 2 9 2 0 82.1103 5.48465 5 9 2 0 92.5408 8.48096 4 9 2 0 77.4315 7.44909 7 9 2 0 70.3191 6.27289 1 9 2 0 81.2318 6.33863 6 -10 -2 0 1.42428 2.19169 1 -10 -2 0 -1.5385 2.05554 2 -10 -2 0 0.41432 1.56273 8 10 2 0 0.71137 1.98190 6 10 2 0 0.53539 2.64208 7 -11 -2 0 11.1812 3.34075 2 -11 -2 0 14.8452 2.74414 8 -11 -2 0 11.2363 3.12983 1 11 2 0 11.1471 3.79446 7 -12 -2 0 -2.4617 2.42163 1 -12 -2 0 0.43821 2.96484 2 -12 -2 0 0.16688 2.07015 8 -13 -2 0 44.6949 5.62808 1 -13 -2 0 37.5861 5.66380 2 -15 3 0 -1.5001 2.24472 8 -15 3 0 0.78489 3.01473 1 -15 3 0 0.37815 2.80060 2 -14 3 0 -2.2014 2.40874 1 -14 3 0 2.54907 2.17583 8 -14 3 0 1.62374 2.61139 2 13 -3 0 51.9941 5.25620 6 -13 3 0 44.4763 4.61653 8 -13 3 0 38.0106 4.99504 2 -13 3 0 32.6875 4.55577 1 12 -3 0 33.2447 4.14005 6 12 -3 0 38.4582 4.93748 7 -12 3 0 39.0975 4.54925 2 -12 3 0 27.2001 4.04218 1 -12 3 0 36.0060 4.24583 6 -12 3 0 36.1126 4.08734 8 11 -3 0 197.062 14.7822 3 11 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22.8465 3.09416 7 -8 3 0 21.6414 2.70453 1 -8 3 0 22.4115 2.66167 8 -8 3 0 27.0180 2.95542 6 7 -3 0 221.744 12.5894 1 7 -3 0 233.179 14.2198 6 7 -3 0 253.472 13.6913 2 7 -3 0 214.071 12.4866 8 7 -3 0 211.498 12.5583 1 7 -3 0 206.864 14.2700 7 7 -3 0 230.838 15.7474 3 7 -3 0 226.692 14.0232 4 -7 3 0 226.058 14.3973 7 -7 3 0 217.001 12.6298 1 -7 3 0 231.441 13.6871 2 -7 3 0 230.638 14.1113 6 -7 3 0 220.704 12.4991 8 6 -3 0 18.1293 2.31323 7 6 -3 0 11.3835 2.04700 4 6 -3 0 15.8411 1.74586 2 6 -3 0 15.4644 1.85967 3 6 -3 0 13.7857 1.95024 6 6 -3 0 15.9519 1.35943 5 6 -3 0 14.2401 1.76903 1 6 -3 0 12.2662 1.73504 8 -6 3 0 13.0162 1.21181 5 -6 3 0 13.7332 1.85183 1 -6 3 0 15.8523 1.79718 2 -6 3 0 9.11663 1.51234 1 -6 3 0 16.9957 1.91773 8 -6 3 0 14.6705 1.96711 6 -6 3 0 16.0265 2.29566 7 5 -3 0 119.800 7.11574 1 5 -3 0 117.197 8.07595 6 5 -3 0 115.701 8.13193 7 5 -3 0 133.587 7.59097 2 5 -3 0 119.933 7.95977 4 5 -3 0 136.457 7.59270 5 5 -3 0 120.334 7.12387 1 5 -3 0 126.650 7.15587 8 5 -3 0 144.635 8.80957 3 -5 3 0 124.478 8.22229 7 -5 3 0 107.697 7.05123 1 -5 3 0 135.095 7.63698 2 -5 3 0 121.964 7.51313 5 -5 3 0 115.246 7.12698 1 -5 3 0 114.436 7.08927 8 -5 3 0 130.443 8.09189 6 4 -3 0 4.64464 0.67393 2 4 -3 0 3.66428 0.83743 1 4 -3 0 3.82529 1.01803 6 4 -3 0 1.68097 0.89171 7 4 -3 0 2.58455 0.80563 1 4 -3 0 2.83878 0.80554 8 4 -3 0 4.11321 0.76793 5 -4 3 0 5.71035 1.07620 6 -4 3 0 3.45787 0.84724 8 -4 3 0 2.05129 0.93829 7 -4 3 0 4.03387 0.77960 5 -4 3 0 3.66605 0.90991 1 -4 3 0 3.95204 0.70407 2 3 -3 0 1.12118 0.61432 5 3 -3 0 -0.5304 0.62690 7 3 -3 0 0.83887 0.71107 6 3 -3 0 1.70171 0.62804 1 3 -3 0 0.94413 0.28792 2 3 -3 0 0.98099 0.56337 8 3 -3 0 0.47056 0.54483 1 -3 3 0 -0.4663 0.55710 6 -3 3 0 0.60886 0.57452 1 -3 3 0 0.48719 0.58742 8 -3 3 0 0.67717 0.64405 7 -3 3 0 0.04156 0.58258 5 2 -3 0 238.955 12.8791 1 2 -3 0 233.083 14.4786 5 2 -3 0 231.390 12.7166 8 2 -3 0 243.818 12.8696 1 2 -3 0 236.229 14.4811 7 2 -3 0 275.544 14.7311 6 -2 3 0 261.468 12.8690 1 -2 3 0 251.928 12.7424 8 -2 3 0 232.156 14.4633 5 -2 3 0 245.295 14.6622 6 -2 3 0 239.327 14.4580 7 1 -3 0 799.643 41.4038 1 1 -3 0 792.563 41.3385 1 1 -3 0 784.148 45.4444 4 1 -3 0 814.775 46.5677 5 1 -3 0 750.596 45.7812 2 1 -3 0 872.751 40.7860 8 1 -3 0 760.299 46.8801 6 1 -3 0 809.736 46.6167 7 -1 3 0 786.840 46.5811 7 -1 3 0 863.185 40.7651 8 -1 3 0 754.454 45.7679 2 -1 3 0 808.744 41.3374 1 -1 3 0 850.447 46.9087 6 -1 3 0 788.023 46.5447 5 0 -3 0 81.9199 5.16680 7 0 -3 0 77.2156 4.94522 5 0 -3 0 75.1988 4.76168 6 0 -3 0 65.7223 4.64338 2 0 -3 0 81.7002 5.25865 4 0 -3 0 71.3434 4.32705 1 0 -3 0 76.7161 4.11924 8 0 -3 0 71.5259 4.23778 1 0 3 0 80.7884 5.11078 7 0 3 0 70.6790 4.65469 2 0 3 0 74.6719 4.74501 6 0 3 0 74.2121 4.88519 5 0 3 0 80.8295 4.30546 1 0 3 0 76.2838 4.38204 1 0 3 0 75.3661 5.08590 4 -1 -3 0 604.631 32.5533 1 -1 -3 0 620.214 36.7157 6 -1 -3 0 633.164 36.6466 5 -1 -3 0 651.291 36.1869 4 -1 -3 0 600.173 37.0765 6 -1 -3 0 630.849 36.8411 7 -1 -3 0 651.113 32.6874 1 1 3 0 599.772 36.1640 2 1 3 0 650.358 36.6361 5 1 3 0 644.343 36.9001 7 1 3 0 603.333 32.6443 1 1 3 0 615.637 36.1641 4 1 3 0 660.102 32.6165 1 -2 -3 0 484.699 29.4294 5 -2 -3 0 504.153 29.6542 7 -2 -3 0 501.276 26.3600 1 -2 -3 0 467.158 26.1946 1 -2 -3 0 527.032 29.3227 4 -2 -3 0 503.237 29.7449 6 2 3 0 514.116 26.3041 1 2 3 0 506.302 29.8074 7 2 3 0 496.814 29.3286 4 2 3 0 474.978 26.2958 1 2 3 0 549.520 29.2271 2 2 3 0 498.205 29.8545 6 2 3 0 498.587 29.4015 5 -3 -3 0 400.781 24.6059 2 -3 -3 0 418.691 24.7009 5 -3 -3 0 401.527 22.2166 1 -3 -3 0 424.669 24.7763 4 -3 -3 0 431.859 24.8893 6 -3 -3 0 401.467 22.0554 1 -3 -3 0 418.311 24.9197 7 3 3 0 405.529 25.0033 6 3 3 0 421.649 25.1721 7 3 3 0 440.260 24.9755 4 3 3 0 432.888 22.1974 1 3 3 0 412.596 24.6321 5 3 3 0 426.196 22.2273 1 -4 -3 0 -0.7771 1.20775 2 -4 -3 0 0.09968 1.49268 4 -4 -3 0 -0.5419 1.05957 1 -4 -3 0 -0.5424 0.97574 5 -4 -3 0 0.32431 0.98518 6 -4 -3 0 -0.1422 0.95817 1 -4 -3 0 0.48266 1.08462 7 4 3 0 0.49448 1.50839 7 4 3 0 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4 0 104.756 8.51097 2 -14 4 0 114.059 8.44130 1 -14 4 0 117.856 8.01979 8 13 -4 0 43.2084 4.89337 6 -13 4 0 38.0160 4.25416 8 -13 4 0 35.0986 4.43854 2 -13 4 0 35.4324 4.65166 1 12 -4 0 12.6459 2.78083 6 12 -4 0 8.65890 2.99728 7 12 -4 0 15.9640 3.11579 3 -12 4 0 12.7901 2.53947 8 -12 4 0 6.56568 2.68679 2 -12 4 0 13.9886 2.94362 1 11 -4 0 4.15720 1.96034 6 11 -4 0 -0.6041 1.83806 3 11 -4 0 3.75083 2.28724 7 11 -4 0 2.28975 2.33259 4 11 -4 0 3.80412 2.05878 1 11 -4 0 3.39607 1.93266 1 -11 4 0 5.42352 2.17543 2 -11 4 0 0.61475 2.07178 1 -11 4 0 2.37997 1.84867 8 -11 4 0 1.27307 1.74450 6 10 -4 0 81.3460 6.87141 4 10 -4 0 86.1109 6.99706 3 10 -4 0 57.3320 6.68786 7 10 -4 0 91.2678 6.10600 1 10 -4 0 81.0753 6.49378 6 -10 4 0 81.8655 6.81031 7 -10 4 0 83.9645 6.49085 6 -10 4 0 86.5673 6.13974 2 -10 4 0 95.5678 6.05518 8 -10 4 0 86.5474 6.16207 1 9 -4 0 208.710 14.1204 3 9 -4 0 192.275 12.7755 6 9 -4 0 188.688 11.2912 1 9 -4 0 171.960 12.9118 7 9 -4 0 191.549 11.3327 8 9 -4 0 196.842 12.7926 4 -9 4 0 194.121 12.1845 2 -9 4 0 191.890 11.3071 8 -9 4 0 192.774 11.4647 1 -9 4 0 226.616 13.2987 7 -9 4 0 194.475 12.6653 6 8 -4 0 3.85010 0.88297 5 8 -4 0 3.59535 1.42642 1 8 -4 0 2.84631 1.62708 7 8 -4 0 5.97272 1.62033 8 8 -4 0 2.07910 1.35964 3 8 -4 0 6.25091 1.75958 6 8 -4 0 4.54957 1.81255 4 -8 4 0 3.95613 1.48293 8 -8 4 0 3.14676 1.48455 1 -8 4 0 3.70332 0.73639 5 -8 4 0 4.07757 1.37462 2 -8 4 0 1.18726 1.52633 7 -8 4 0 4.10103 1.59052 6 7 -4 0 127.660 7.97010 5 7 -4 0 124.388 7.70174 8 7 -4 0 130.078 8.69398 4 7 -4 0 108.872 8.72063 7 7 -4 0 148.370 9.48633 3 7 -4 0 135.028 8.09735 2 7 -4 0 122.669 8.70049 6 7 -4 0 128.174 7.66049 1 -7 4 0 125.832 7.88292 5 -7 4 0 142.588 9.02892 7 -7 4 0 131.295 7.74516 8 -7 4 0 134.255 8.71607 6 -7 4 0 137.972 8.16392 2 -7 4 0 124.319 7.78187 1 6 -4 0 1659.12 89.5492 5 6 -4 0 1475.45 80.0158 1 6 -4 0 1555.01 87.8710 4 6 -4 0 1648.49 90.9185 6 6 -4 0 1490.73 79.0816 8 6 -4 0 1757.96 102.823 3 6 -4 0 1692.39 88.5818 2 6 -4 0 1415.08 90.0400 7 -6 4 0 1546.46 90.7756 6 -6 4 0 1403.48 80.0521 1 -6 4 0 1552.43 80.1345 1 -6 4 0 1494.17 90.0693 7 -6 4 0 1591.72 79.1320 8 -6 4 0 1503.07 89.4444 5 -6 4 0 1382.86 80.0289 1 -6 4 0 1610.96 88.6105 2 5 -4 0 28.1255 1.99545 2 5 -4 0 29.4145 2.36089 5 5 -4 0 31.7342 2.92686 6 5 -4 0 29.7966 2.36834 1 5 -4 0 27.0405 2.83471 7 5 -4 0 21.9352 2.29261 8 -5 4 0 23.9239 2.28710 1 -5 4 0 24.6629 2.36239 8 -5 4 0 23.7930 2.25738 1 -5 4 0 19.4497 2.54843 7 -5 4 0 29.9003 2.03796 2 -5 4 0 24.6615 2.67307 6 -5 4 0 25.6598 2.21918 5 4 -4 0 2.19027 0.76289 8 4 -4 0 3.10999 0.88974 5 4 -4 0 3.08513 0.88489 1 4 -4 0 2.32276 1.01196 7 4 -4 0 2.14628 0.80142 1 4 -4 0 1.94362 0.39924 2 4 -4 0 2.89906 1.01131 6 -4 4 0 2.24975 0.77523 1 -4 4 0 2.44187 0.46031 2 -4 4 0 2.13376 0.83561 8 -4 4 0 4.67667 0.98102 5 -4 4 0 2.22350 0.92325 7 -4 4 0 2.01854 0.92601 6 3 -4 0 300.492 17.8819 5 3 -4 0 302.966 15.7819 8 3 -4 0 295.498 17.9434 7 3 -4 0 318.551 18.1849 6 3 -4 0 290.312 15.8804 1 3 -4 0 290.092 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7 -1 7 -10 6.30501 1.40341 1 -1 7 -10 7.80470 2.64324 5 1 -7 10 9.54105 3.08893 7 1 -7 10 6.91683 1.92424 2 -2 7 -10 20.1580 1.90325 1 -2 7 -10 17.5577 4.68085 6 -2 7 -10 16.6681 3.54352 7 -2 7 -10 21.3447 3.49024 5 -2 7 -10 20.5529 1.87228 1 2 -7 10 13.4989 3.77606 7 2 -7 10 18.2205 2.86390 6 2 -7 10 20.6245 2.81119 2 -3 7 -10 292.302 14.2104 1 -3 7 -10 272.657 17.5354 5 -3 7 -10 263.442 14.1502 1 -3 7 -10 268.115 17.7410 7 3 -7 10 263.626 16.9688 7 3 -7 10 257.203 18.0240 7 3 -7 10 249.602 17.0591 6 3 -7 10 271.106 16.7124 2 -4 7 -10 129.843 9.05433 5 4 -7 10 119.562 8.52271 6 4 -7 10 130.378 9.82367 7 4 -7 10 116.751 8.34178 2 4 -7 10 107.141 8.33098 7 -5 7 -10 145.113 10.2326 5 5 -7 10 140.409 9.79020 7 5 -7 10 150.300 9.78354 2 5 -7 10 142.772 10.8105 7 5 -7 10 125.225 9.57775 6 -6 7 -10 208.872 14.0676 5 6 -7 10 207.666 13.7510 6 6 -7 10 208.891 13.9205 7 6 -7 10 213.602 14.8255 7 -7 7 -10 3.22641 1.72838 8 7 -7 10 3.35658 2.17562 7 7 -7 10 6.48254 2.22828 6 7 -7 10 5.40378 3.18037 7 -8 7 -10 20.7912 1.90799 1 -8 7 -10 24.3506 2.06877 1 -8 7 -10 26.2257 3.02128 8 8 -7 10 24.0116 3.39314 6 8 -7 10 30.8150 4.06945 7 -9 7 -10 3.44724 1.35075 1 -9 7 -10 2.07112 1.21096 1 -9 7 -10 3.11479 1.78922 8 9 -7 10 -0.5531 2.17478 7 9 -7 10 0.25363 1.97757 6 -10 7 -10 3.67690 1.69094 1 -10 7 -10 3.97778 1.49650 1 -10 7 -10 0.73169 1.92174 8 10 -7 10 3.76872 2.36646 6 10 -7 10 -0.4270 2.42529 7 -11 7 -10 2.98279 1.84799 1 -11 7 -10 -1.2956 1.74556 8 11 6 -10 14.4520 3.75343 5 11 6 -10 11.3270 5.13212 4 11 6 -10 16.1253 5.34811 6 11 6 -10 7.73755 3.71552 1 -11 -6 10 11.0793 3.96732 2 10 6 -10 258.244 19.1798 6 10 6 -10 286.403 16.5258 1 10 6 -10 209.149 17.9394 4 10 6 -10 265.529 17.4597 5 -10 -6 10 262.003 17.2715 2 9 6 -10 176.339 14.1273 4 9 6 -10 177.882 12.2008 1 9 6 -10 197.500 14.9184 6 9 6 -10 187.249 13.1155 5 -9 -6 10 180.401 12.8655 2 8 6 -10 5.65850 3.78939 6 8 6 -10 5.96153 2.88461 5 8 6 -10 5.26950 2.73724 1 8 6 -10 0.83952 2.96926 4 -8 -6 10 1.09638 2.34193 2 7 6 -10 5.92913 3.84826 7 7 6 -10 2.73394 2.97316 4 7 6 -10 -0.6289 2.32957 5 7 6 -10 1.83179 2.50335 1 7 6 -10 0.36012 3.08785 6 -7 -6 10 1.44108 2.11360 2 6 6 -10 -1.2835 2.15311 5 6 6 -10 6.32992 3.53169 6 6 6 -10 1.04063 3.43038 7 6 6 -10 2.38063 2.88082 4 6 6 -10 -0.8579 2.01112 1 -6 -6 10 0.71546 2.11030 2 5 6 -10 71.2747 6.05462 1 5 6 -10 85.1008 5.85929 1 5 6 -10 61.6011 7.67396 6 5 6 -10 60.4351 7.67613 7 5 6 -10 76.0179 7.06115 5 5 6 -10 61.5049 6.80836 4 -5 -6 10 77.1355 6.01005 2 -5 -6 10 70.7787 5.91715 1 4 6 -10 235.119 16.0156 5 4 6 -10 257.741 14.1665 1 4 6 -10 251.997 17.4126 6 4 6 -10 214.679 16.8409 7 4 6 -10 224.492 15.7271 4 -4 -6 10 232.834 16.5573 7 -4 -6 10 245.825 15.2839 2 -4 -6 10 268.429 14.1154 1 3 6 -10 15.8216 3.15140 5 3 6 -10 17.7378 4.05129 6 3 6 -10 23.5736 2.71675 1 3 6 -10 18.3933 3.22016 4 3 6 -10 19.8590 2.74599 1 3 6 -10 14.6019 3.78365 7 -3 -6 10 16.8276 2.72740 2 -3 -6 10 17.5278 3.85284 7 -3 -6 10 15.0478 2.39232 1 2 6 -10 321.117 17.4568 1 2 6 -10 290.634 21.2056 6 2 6 -10 292.103 19.2430 4 2 6 -10 282.917 20.7013 7 2 6 -10 317.338 20.2755 5 2 6 -10 344.538 17.5213 1 -2 -6 10 346.635 17.4858 1 -2 -6 10 325.225 20.9218 7 -2 -6 10 319.186 19.3856 2 1 6 -10 70.4970 7.54863 6 1 6 -10 68.7097 4.56414 1 1 6 -10 58.7786 4.96440 4 1 6 -10 71.0770 4.58749 1 1 6 -10 62.6608 6.76722 7 1 6 -10 73.1646 6.11403 5 -1 -6 10 62.4313 5.04057 2 -1 -6 10 67.6126 6.86060 7 -1 -6 10 64.2505 4.43333 1 0 6 -10 121.706 6.64909 1 0 6 -10 95.8798 6.57523 4 0 6 -10 117.850 6.68580 1 0 6 -10 95.5319 9.75825 6 0 6 -10 106.116 8.67505 7 0 6 -10 126.687 8.61458 5 0 -6 10 117.483 9.12204 7 0 -6 10 118.176 7.72125 2 -1 6 -10 35.4942 2.60413 1 -1 6 -10 29.0858 4.26763 7 -1 6 -10 30.8186 4.99988 6 -1 6 -10 29.4625 2.58312 1 -1 6 -10 27.9963 3.94948 5 1 -6 10 33.6221 3.54115 2 1 -6 10 35.3000 4.75252 7 1 -6 10 34.5391 3.17273 8 -2 6 -10 67.2333 7.64733 6 -2 6 -10 68.1949 4.19224 1 -2 6 -10 65.0576 6.34427 5 -2 6 -10 75.9289 4.18472 1 -2 6 -10 64.0881 6.50956 7 2 -6 10 73.6096 4.91778 8 2 -6 10 70.7759 5.57310 2 2 -6 10 64.1890 6.84336 7 -3 6 -10 12.6854 2.84024 5 -3 6 -10 20.3864 4.46121 6 3 -6 10 14.5172 2.42070 7 3 -6 10 8.89395 3.09042 6 3 -6 10 15.1066 2.52114 6 3 -6 10 16.9245 2.65514 2 3 -6 10 18.8538 2.30083 8 3 -6 10 12.1807 3.27338 7 -4 6 -10 107.957 7.85840 5 4 -6 10 96.5966 7.32620 2 4 -6 10 90.9672 6.27224 8 4 -6 10 106.542 8.80296 6 4 -6 10 105.138 7.34958 7 4 -6 10 114.882 8.50225 7 4 -6 10 92.0335 7.16923 6 5 -6 10 61.4813 6.51968 6 5 -6 10 45.6404 4.77727 7 5 -6 10 52.8125 4.27272 8 5 -6 10 45.8959 4.58710 6 5 -6 10 50.5129 5.80004 7 6 -6 10 315.459 19.5596 7 6 -6 10 277.383 18.5319 6 6 -6 10 308.165 18.8169 7 6 -6 10 291.978 19.9704 6 -7 6 -10 2.52666 0.83221 1 -7 6 -10 0.87143 1.46421 8 -7 6 -10 4.18028 0.99834 1 7 -6 10 0.33754 1.58194 6 7 -6 10 4.28198 2.88622 7 7 -6 10 1.99849 1.90231 7 7 -6 10 0.06834 2.86209 6 -8 6 -10 114.465 7.10196 8 -8 6 -10 114.313 6.36982 1 -8 6 -10 112.794 6.57322 1 8 -6 10 107.322 8.09702 6 8 -6 10 110.572 9.41289 7 8 -6 10 114.871 8.69233 7 -9 6 -10 60.8798 4.99806 8 -9 6 -10 57.8516 4.04532 1 -9 6 -10 65.7845 4.30103 1 9 -6 10 58.5314 6.18576 7 9 -6 10 56.2699 5.86546 5 9 -6 10 63.6364 5.39386 6 -10 6 -10 5.93247 2.09173 8 -10 6 -10 6.80832 1.97570 1 10 -6 10 9.35499 3.08190 7 -11 6 -10 4.47751 2.09544 1 11 5 -10 3.36476 4.13216 6 11 5 -10 0.91029 3.14030 1 11 5 -10 2.01684 2.94137 5 11 5 -10 2.88243 3.95550 4 -11 -5 10 -3.5250 2.91445 2 10 5 -10 173.295 12.1250 5 10 5 -10 157.835 13.1446 4 10 5 -10 162.083 11.2381 1 10 5 -10 169.274 13.5433 6 -10 -5 10 156.584 11.6423 2 9 5 -10 167.582 13.6252 4 9 5 -10 201.692 13.0690 5 9 5 -10 161.065 14.0043 6 9 5 -10 193.982 12.0985 1 -9 -5 10 176.671 12.5451 2 8 5 -10 3.52552 2.51453 1 8 5 -10 -2.3363 2.47356 4 8 5 -10 2.31401 3.24190 7 8 5 -10 13.3009 4.18835 6 8 5 -10 8.71299 2.84787 5 -8 -5 10 1.93673 2.46623 2 7 5 -10 103.338 8.07214 5 7 5 -10 69.8671 8.86104 7 7 5 -10 104.136 7.48158 1 7 5 -10 109.567 8.76689 4 7 5 -10 74.7837 9.14307 6 -7 -5 10 106.568 7.64356 2 -7 -5 10 107.927 7.30741 1 6 5 -10 125.416 10.8548 6 6 5 -10 118.388 8.48556 1 6 5 -10 143.767 9.97878 5 6 5 -10 135.969 10.1747 4 6 5 -10 147.226 8.94833 1 6 5 -10 109.614 11.2005 7 -6 -5 10 139.760 9.30364 2 -6 -5 10 126.148 8.59634 1 5 5 -10 3.25342 2.98843 6 5 5 -10 3.75440 2.12843 1 5 5 -10 3.96861 1.96732 1 5 5 -10 6.50610 2.42334 5 5 5 -10 7.14993 2.73014 4 5 5 -10 9.22581 3.32250 7 -5 -5 10 5.19717 2.03863 2 -5 -5 10 12.2547 3.34753 7 -5 -5 10 3.49362 1.74348 1 4 5 -10 0.36806 1.70472 1 4 5 -10 2.93855 1.97983 5 4 5 -10 3.20201 2.70887 7 4 5 -10 1.06923 2.03185 4 4 5 -10 2.22654 2.47681 6 -4 -5 10 1.03487 1.43214 1 -4 -5 10 1.93334 2.65462 7 -4 -5 10 0.19874 1.62274 2 3 5 -10 10.1704 2.10160 1 3 5 -10 7.39954 3.05303 7 3 5 -10 14.1722 2.68628 4 3 5 -10 12.6525 2.92903 5 3 5 -10 16.7284 3.82125 6 3 5 -10 15.8221 2.24846 1 -3 -5 10 16.6500 3.49735 7 -3 -5 10 11.3521 2.06159 1 -3 -5 10 14.9272 2.43319 2 2 5 -10 96.8008 7.90275 5 2 5 -10 100.538 8.88057 6 2 5 -10 104.848 8.60468 7 2 5 -10 108.078 6.59192 1 2 5 -10 105.903 6.62137 1 2 5 -10 114.097 7.44504 4 -2 -5 10 101.234 8.37767 7 -2 -5 10 108.326 6.51766 1 -2 -5 10 101.442 7.25687 2 1 5 -10 33.1690 4.90970 6 1 5 -10 32.9243 4.47321 7 1 5 -10 31.1152 2.97198 1 1 5 -10 34.6054 3.24109 4 1 5 -10 34.0152 4.13918 5 1 5 -10 37.3601 3.06491 1 -1 -5 10 36.7305 2.91832 1 -1 -5 10 35.2549 4.59833 7 -1 -5 10 33.4762 3.56222 2 0 5 -10 72.9364 4.43390 1 0 5 -10 71.3960 4.46540 1 0 5 -10 61.0192 6.14398 5 0 5 -10 75.7485 7.48052 6 0 5 -10 51.4443 6.00005 7 0 -5 10 57.8005 6.36876 7 0 -5 10 74.4740 5.49522 2 0 -5 10 89.1230 7.59876 6 -1 5 -10 190.157 10.1047 1 -1 5 -10 187.486 13.6104 6 -1 5 -10 193.057 10.1508 1 -1 5 -10 181.540 12.5842 7 -1 5 -10 196.884 12.7033 5 1 -5 10 190.384 10.4972 8 1 -5 10 167.606 12.7133 7 1 -5 10 162.116 12.8553 6 1 -5 10 187.673 11.9839 2 -2 5 -10 14.2741 3.07452 7 -2 5 -10 16.8804 3.97391 6 -2 5 -10 20.0585 1.70318 1 -2 5 -10 20.8661 1.65395 1 -2 5 -10 23.1658 3.42524 5 2 -5 10 23.8229 3.05937 2 2 -5 10 24.5718 4.02742 6 2 -5 10 22.7784 2.38633 8 2 -5 10 18.2670 3.44804 7 -3 5 -10 35.5441 5.19087 6 3 -5 10 34.6263 3.74540 2 3 -5 10 31.9621 4.54119 6 3 -5 10 25.0973 3.11279 7 3 -5 10 30.8940 2.91266 8 3 -5 10 27.2168 3.28426 6 3 -5 10 34.8662 4.40287 7 4 -5 10 76.8467 6.03690 6 4 -5 10 82.4272 6.96847 7 4 -5 10 83.5373 6.13746 7 4 -5 10 81.5190 7.74676 6 4 -5 10 81.5008 5.33316 8 5 -5 10 77.9954 6.18804 7 5 -5 10 98.4963 5.52164 8 5 -5 10 73.1585 7.44325 6 5 -5 10 87.3071 7.15225 7 5 -5 10 66.4032 5.85273 6 -6 5 -10 251.960 13.5365 1 6 -5 10 259.181 14.1937 8 6 -5 10 238.235 16.0793 6 6 -5 10 289.064 17.2792 7 6 -5 10 250.537 16.3833 7 6 -5 10 267.956 17.3340 6 -7 5 -10 3.40433 1.54507 8 -7 5 -10 6.24758 1.10570 1 -7 5 -10 6.09248 1.31834 1 7 -5 10 4.94971 1.79731 6 7 -5 10 5.58429 1.69608 8 7 -5 10 6.27787 2.91347 6 7 -5 10 2.72723 1.98932 7 7 -5 10 4.09414 2.78301 7 -8 5 -10 74.3387 4.93147 1 -8 5 -10 78.7257 4.71622 1 -8 5 -10 74.4072 5.24445 8 8 -5 10 76.0201 6.44607 7 8 -5 10 63.0668 7.23804 7 8 -5 10 78.1874 6.58801 5 8 -5 10 82.1907 6.05262 6 -9 5 -10 240.838 13.5836 1 -9 5 -10 252.107 14.0027 8 -9 5 -10 259.990 13.9119 1 9 -5 10 253.372 15.9234 6 9 -5 10 243.189 16.4442 7 -10 5 -10 7.97594 2.15236 1 -10 5 -10 9.48344 2.22898 8 10 -5 10 12.5715 3.12100 7 -11 5 -10 15.6448 2.73008 1 11 -5 10 11.7729 3.33617 7 12 4 -10 123.607 11.8607 4 12 4 -10 122.924 11.7668 6 -12 -4 10 103.207 9.04299 2 11 4 -10 55.7390 7.66906 6 11 4 -10 65.3139 6.69227 1 11 4 -10 54.2099 7.52751 4 -11 -4 10 57.3537 5.88383 8 -11 -4 10 51.8104 6.08065 2 10 4 -10 8.20464 2.93638 5 10 4 -10 6.63265 3.52354 4 10 4 -10 5.98054 2.90314 1 10 4 -10 17.7332 4.61993 6 -10 -4 10 9.26719 3.16862 2 9 4 -10 62.6700 6.26520 1 9 4 -10 63.8868 6.53958 5 9 4 -10 84.2329 8.45031 6 9 4 -10 63.3278 7.42899 4 -9 -4 10 63.2094 6.19873 2 8 4 -10 81.0033 6.67959 1 8 4 -10 77.0214 8.27379 6 8 4 -10 84.7015 6.87314 5 8 4 -10 63.6687 7.97138 7 8 4 -10 62.3842 7.14832 4 -8 -4 10 69.1746 6.41081 2 -8 -4 10 67.9109 6.26553 1 7 4 -10 42.4452 5.28423 4 7 4 -10 45.2284 4.61986 1 7 4 -10 36.7582 4.68769 5 7 4 -10 31.2717 5.39765 7 7 4 -10 36.4178 5.66322 6 -7 -4 10 44.4550 4.44859 1 -7 -4 10 34.4695 4.17395 2 6 4 -10 50.5067 6.32520 7 6 4 -10 55.6463 5.88955 4 6 4 -10 56.5490 5.15211 1 6 4 -10 53.0073 4.89931 1 6 4 -10 63.2751 5.97470 5 6 4 -10 50.0899 6.41495 6 -6 -4 10 59.0048 6.08195 7 -6 -4 10 49.7586 4.92893 2 -6 -4 10 53.8816 4.93302 1 5 4 -10 8.48024 2.67158 4 5 4 -10 6.80997 1.99414 1 5 4 -10 11.1870 3.27873 7 5 4 -10 12.8639 2.49837 1 5 4 -10 12.5353 2.90353 5 5 4 -10 3.84033 2.87226 6 -5 -4 10 11.0268 2.23497 2 -5 -4 10 8.03773 2.97633 7 -5 -4 10 8.61010 2.07584 1 4 4 -10 20.1174 2.81587 1 4 4 -10 22.0787 3.51896 5 4 4 -10 19.4507 4.01487 7 4 4 -10 23.3112 4.18223 6 4 4 -10 25.3230 3.36968 4 -4 -4 10 28.7044 4.09212 7 -4 -4 10 18.3699 2.75970 2 -4 -4 10 17.0321 2.43690 1 3 4 -10 87.2090 5.74596 1 3 4 -10 92.4762 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4.70335 1.96155 2 -5 10 -11 45.0770 3.38701 1 -5 10 -11 50.5591 3.29740 1 -5 10 -11 49.4059 5.81315 5 5 -10 11 48.4302 5.36267 7 5 -10 11 43.7739 5.19682 6 5 -10 11 57.1724 5.02054 2 -6 10 -11 1.14327 1.11234 1 -6 10 -11 2.10784 0.97567 1 -6 10 -11 1.55488 2.62846 5 6 -10 11 2.60120 2.13169 2 6 -10 11 1.74821 2.27979 6 6 -10 11 1.16014 2.19987 7 -7 10 -11 68.5181 6.96437 5 7 -10 11 64.0966 6.55251 6 7 -10 11 70.2387 5.97463 2 -8 10 -11 129.201 10.1952 5 8 -10 11 138.246 9.62137 2 8 -10 11 127.985 9.92073 6 -9 10 -11 3.94097 2.63752 5 -9 10 -11 3.29396 0.93626 1 9 -10 11 4.59702 2.58687 2 9 -10 11 2.43973 2.50016 6 -10 10 -11 17.8999 2.00797 1 -10 10 -11 19.0604 1.82316 1 -10 10 -11 17.4451 3.24207 8 10 -10 11 19.6976 3.66273 6 8 9 -11 5.71786 3.51255 5 8 9 -11 -1.0645 4.80035 6 8 9 -11 17.2507 4.05336 1 8 9 -11 9.28500 4.46130 4 -8 -9 11 16.2688 3.95181 2 7 9 -11 33.4065 5.06711 5 7 9 -11 26.9338 6.69616 6 7 9 -11 24.6248 5.52665 4 7 9 -11 22.5023 4.28414 1 -7 -9 11 32.6837 4.66950 2 6 9 -11 4.06928 3.30665 5 6 9 -11 9.69510 4.16680 4 6 9 -11 6.68150 4.46135 6 6 9 -11 3.04278 2.69014 1 -6 -9 11 3.28891 2.79050 2 5 9 -11 184.684 11.7460 1 5 9 -11 172.214 13.5693 4 5 9 -11 180.941 15.1343 6 5 9 -11 210.562 13.9108 5 -5 -9 11 174.044 12.4557 2 4 9 -11 42.6289 5.54593 5 4 9 -11 37.8989 4.47006 1 4 9 -11 37.2945 7.03924 6 4 9 -11 37.2815 5.47215 4 -4 -9 11 39.0813 4.52972 2 3 9 -11 10.3866 2.71477 1 3 9 -11 5.66288 2.97180 4 3 9 -11 7.19577 3.09891 5 3 9 -11 12.9858 4.71674 6 3 9 -11 9.78107 4.14509 7 -3 -9 11 10.5927 2.67626 2 2 9 -11 5.48117 4.04034 6 2 9 -11 6.69382 2.25099 1 2 9 -11 13.0899 3.33240 5 2 9 -11 11.1842 2.94925 4 2 9 -11 3.39273 3.39802 7 -2 -9 11 8.54312 2.47571 2 1 9 -11 39.0576 3.70918 1 1 9 -11 33.8450 4.98928 5 1 9 -11 25.4344 5.16523 7 1 9 -11 33.3156 3.78284 4 1 9 -11 34.5888 6.41593 6 -1 -9 11 39.1835 4.07645 2 0 9 -11 86.9590 5.66195 1 0 9 -11 80.1303 8.40634 7 0 9 -11 91.8851 8.17325 5 0 9 -11 79.7286 5.79852 4 0 9 -11 64.0197 9.02168 6 0 9 -11 87.2718 5.61754 1 0 -9 11 77.5348 6.24282 2 -1 9 -11 250.281 19.1377 6 -1 9 -11 236.115 17.7342 7 -1 9 -11 255.599 17.2953 5 -1 9 -11 277.080 14.3828 1 -1 9 -11 267.563 14.3011 1 1 -9 11 233.159 16.7855 6 1 -9 11 269.546 16.1888 2 -2 9 -11 24.8115 2.47863 1 -2 9 -11 22.5210 2.42548 1 -2 9 -11 27.5192 4.80042 7 -2 9 -11 24.3875 4.10082 5 2 -9 11 20.7774 3.50077 6 2 -9 11 24.1671 3.16523 2 -3 9 -11 106.417 8.78414 5 -3 9 -11 96.3450 9.53899 7 -3 9 -11 107.043 6.30251 1 -3 9 -11 103.271 6.26560 1 3 -9 11 112.118 7.75901 2 3 -9 11 116.264 8.35332 6 -4 9 -11 33.8427 2.52616 1 -4 9 -11 32.7744 4.67794 5 -4 9 -11 31.2715 2.47681 1 4 -9 11 29.1366 3.69663 2 4 -9 11 34.1606 4.13280 6 4 -9 11 33.3357 4.23382 7 -5 9 -11 82.0557 7.82045 5 5 -9 11 86.9414 6.97698 7 5 -9 11 85.7864 7.05679 6 5 -9 11 89.0093 6.80959 2 -6 9 -11 32.5413 4.66072 5 6 -9 11 34.7490 4.12837 2 6 -9 11 26.7960 4.14675 7 6 -9 11 40.1580 4.53481 6 -7 9 -11 -0.4546 2.60796 5 7 -9 11 3.28361 2.20497 7 7 -9 11 1.66420 2.20511 6 7 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4 8 -11 296.638 20.4509 4 4 8 -11 306.131 22.0872 7 4 8 -11 323.342 22.5391 6 -4 -8 11 319.034 19.9171 2 3 8 -11 70.3228 8.80104 6 3 8 -11 83.6616 5.68920 1 3 8 -11 60.5220 7.75083 7 3 8 -11 72.5467 7.22019 5 3 8 -11 74.3868 6.91175 4 -3 -8 11 67.1409 5.91287 2 2 8 -11 153.201 12.3131 7 2 8 -11 149.532 12.7203 6 2 8 -11 133.805 10.5247 4 2 8 -11 159.839 9.56137 1 2 8 -11 176.048 9.62272 1 2 8 -11 155.649 11.4907 5 -2 -8 11 150.339 10.2606 2 1 8 -11 1.30340 2.94526 7 1 8 -11 3.14886 1.76686 1 1 8 -11 0.43039 1.85670 4 1 8 -11 2.48998 1.58836 1 1 8 -11 1.71666 3.32682 6 1 8 -11 2.97905 2.55090 5 -1 -8 11 4.12066 1.61880 1 -1 -8 11 5.18220 2.09997 2 0 8 -11 7.47499 3.32350 7 0 8 -11 11.7081 4.66466 6 0 8 -11 14.7666 2.20585 1 0 8 -11 11.5658 2.06368 1 0 8 -11 10.8174 3.04867 5 0 8 -11 13.9721 1.87952 4 0 -8 11 21.0167 4.53220 7 0 -8 11 12.0153 2.42621 2 -1 8 -11 279.304 14.4516 1 -1 8 -11 263.953 14.4839 1 -1 8 -11 240.040 17.8039 7 -1 8 -11 281.405 19.3306 6 -1 8 -11 264.051 17.6138 5 1 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14 45.2818 5.52997 2 7 7 -14 34.2983 6.89953 6 7 7 -14 44.3505 6.15415 4 7 7 -14 52.0808 5.43748 1 7 7 -14 37.6139 5.68515 5 -7 -7 14 30.6925 4.68762 2 6 7 -14 17.2132 4.26528 4 6 7 -14 16.7664 3.52577 1 6 7 -14 33.0356 5.08263 5 6 7 -14 14.9614 5.15202 6 -6 -7 14 19.9532 3.66342 2 5 7 -14 19.4842 4.33666 5 5 7 -14 19.5057 3.45433 1 5 7 -14 22.8298 5.62035 6 5 7 -14 19.8220 3.95468 4 -5 -7 14 13.5492 3.10842 2 4 7 -14 104.911 11.7793 6 4 7 -14 131.109 12.1208 7 4 7 -14 140.454 8.70703 1 4 7 -14 140.781 10.5962 5 4 7 -14 112.835 9.16460 4 -4 -7 14 115.569 9.03228 2 3 7 -14 52.3119 5.41993 4 3 7 -14 57.6065 6.79493 5 3 7 -14 61.3758 8.02931 6 3 7 -14 59.5970 5.25085 1 3 7 -14 43.2083 6.81627 7 -3 -7 14 57.8400 5.54704 2 2 7 -14 44.7922 4.28092 4 2 7 -14 43.6174 7.19732 6 2 7 -14 53.6012 4.51436 1 2 7 -14 50.1944 6.06987 5 2 7 -14 35.2421 6.02803 7 -2 -7 14 45.8464 4.92549 2 1 7 -14 27.6390 3.21241 1 1 7 -14 32.3410 5.17520 7 1 7 -14 26.2507 4.73977 5 1 7 -14 24.2962 5.72965 6 1 7 -14 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-18 24.9695 4.55042 1 8 3 -18 27.1773 4.80899 4 -8 -3 18 16.4505 3.78762 2 -8 -3 18 25.7435 5.62158 5 7 3 -18 5.34795 3.12404 4 7 3 -18 5.34675 3.08238 1 -7 -3 18 1.36178 2.75607 2 -7 -3 18 5.63268 3.89949 5 6 3 -18 135.582 12.5584 7 6 3 -18 154.606 9.95755 1 6 3 -18 139.542 10.3451 4 -6 -3 18 133.250 12.7461 5 -6 -3 18 124.699 10.1206 2 5 3 -18 57.4301 5.70796 1 5 3 -18 63.1736 7.74997 7 5 3 -18 63.4253 6.11135 4 5 3 -18 59.8334 8.44241 6 -5 -3 18 64.3295 6.62329 2 -5 -3 18 67.0691 8.08552 5 4 3 -18 34.3544 4.32473 4 4 3 -18 48.6562 6.25201 7 4 3 -18 44.0221 4.70005 1 4 3 -18 49.9708 7.59530 6 -4 -3 18 35.8607 5.03855 2 -4 -3 18 41.7945 6.56448 5 3 3 -18 145.263 12.5375 6 3 3 -18 153.494 9.22276 1 3 3 -18 130.339 9.11356 4 -3 -3 18 144.611 12.1453 5 -3 -3 18 131.326 10.5686 2 2 3 -18 6.40447 4.42844 6 2 3 -18 6.99291 2.22749 1 -2 -3 18 3.98071 2.99319 2 -2 -3 18 9.41059 4.11331 5 1 3 -18 105.942 6.71673 1 1 3 -18 82.9910 10.2574 6 -1 -3 18 96.4589 8.31481 2 -1 -3 18 91.6483 9.92016 5 0 3 -18 62.5033 4.89125 1 0 3 -18 54.0069 8.11244 6 0 -3 18 73.6933 7.48849 2 0 -3 18 65.5298 8.36234 5 -1 3 -18 1.44386 1.86160 1 -1 3 -18 -5.3190 4.13448 6 1 -3 18 3.30468 3.20452 2 1 -3 18 4.86340 4.06040 5 -2 3 -18 51.0864 4.09561 1 2 -3 18 41.9443 6.97328 5 2 -3 18 41.4918 6.08273 2 8 2 -18 39.6575 5.34761 1 8 2 -18 55.9080 6.51046 4 -8 -2 18 35.4664 5.06199 2 -8 -2 18 46.3984 6.81583 5 7 2 -18 4.40892 2.92275 1 7 2 -18 2.58264 3.02590 4 7 2 -18 2.90538 3.53897 7 -7 -2 18 5.76297 2.93979 2 -7 -2 18 -1.7220 3.38096 5 6 2 -18 12.6640 3.59569 4 6 2 -18 5.99592 2.92254 1 6 2 -18 6.78125 3.70580 7 -6 -2 18 4.73945 3.85453 5 -6 -2 18 10.3857 3.32120 2 5 2 -18 -1.4365 3.91917 6 5 2 -18 -2.3119 2.51738 4 5 2 -18 3.23922 2.73568 1 -5 -2 18 4.06782 2.98953 2 -5 -2 18 -1.3261 3.02085 5 4 2 -18 7.94882 4.41780 6 4 2 -18 4.21224 2.53380 1 4 2 -18 1.79583 2.28137 4 -4 -2 18 3.28380 3.35348 5 -4 -2 18 2.55000 2.89016 2 3 2 -18 89.6578 6.34705 1 3 2 -18 80.6776 9.39403 6 3 2 -18 75.2592 6.06376 4 -3 -2 18 64.5560 8.36505 5 -3 -2 18 77.5839 7.63275 2 2 2 -18 5.31932 4.26648 6 2 2 -18 3.05456 2.22760 1 2 2 -18 4.57498 1.86884 4 -2 -2 18 4.67522 3.12588 2 -2 -2 18 5.73049 3.87045 5 1 2 -18 98.3193 10.3611 6 -1 -2 18 97.4430 10.2789 5 -1 -2 18 95.7556 8.93948 2 0 2 -18 221.593 12.7960 1 0 2 -18 228.694 16.8902 6 0 -2 18 214.856 15.5386 2 0 -2 18 220.917 16.6123 5 -1 2 -18 8.33723 2.29393 1 -1 2 -18 7.32683 4.49029 6 1 -2 18 10.5547 4.43495 5 1 -2 18 11.9024 3.61743 2 -2 2 -18 56.8886 4.66481 1 2 -2 18 50.6193 6.67042 2 2 -2 18 60.9917 7.72601 5 9 1 -18 16.9605 4.35689 4 9 1 -18 22.6146 4.31186 1 -9 -1 18 20.7747 5.15176 5 -9 -1 18 12.4578 3.39495 2 8 1 -18 16.3261 4.78523 7 8 1 -18 9.27989 3.50793 1 8 1 -18 10.2358 3.76425 4 -8 -1 18 11.3352 3.34311 2 -8 -1 18 17.6195 4.91709 5 -8 -1 18 12.5178 3.28379 8 7 1 -18 12.3156 3.49540 1 7 1 -18 12.3593 3.63263 4 -7 -1 18 12.8261 3.47652 2 -7 -1 18 2.51258 3.79927 5 6 1 -18 51.9756 6.07968 4 6 1 -18 76.8215 8.95971 6 6 1 -18 70.2415 6.25138 1 -6 -1 18 51.6786 6.11714 2 -6 -1 18 56.3684 7.58527 5 5 1 -18 80.9451 6.41944 1 5 1 -18 64.0133 6.33461 4 5 1 -18 65.1813 8.35968 6 -5 -1 18 61.4244 8.01149 5 -5 -1 18 56.7840 6.48673 2 4 1 -18 3.56934 2.42320 4 4 1 -18 4.98586 2.55231 1 4 1 -18 7.72216 3.98367 6 -4 -1 18 2.07951 2.83722 2 -4 -1 18 6.75322 4.13705 5 3 1 -18 -2.1238 1.98017 4 3 1 -18 1.66947 2.23068 1 3 1 -18 1.92967 3.67782 6 -3 -1 18 -5.0798 2.42493 2 -3 -1 18 -1.8324 3.40472 5 2 1 -18 6.36069 2.00357 4 2 1 -18 1.03220 3.56752 6 2 1 -18 4.01331 2.42635 1 -2 -1 18 7.98763 3.30879 2 -2 -1 18 4.39931 3.91662 5 1 1 -18 9.99609 4.52962 6 1 1 -18 14.0575 2.73830 1 -1 -1 18 9.18741 3.44684 2 -1 -1 18 11.9377 4.55587 5 0 1 -18 198.453 11.3154 1 0 1 -18 196.423 14.7943 6 0 -1 18 166.562 13.5816 2 0 -1 18 189.423 14.7171 5 -1 1 -18 72.6707 5.55407 1 1 -1 18 69.9499 8.64077 5 1 -1 18 72.4252 7.85388 2 9 0 -18 22.2590 5.04089 7 9 0 -18 13.8763 4.23556 4 9 0 -18 14.4489 3.85522 1 -9 0 18 22.8115 5.21571 5 -9 0 18 16.7361 3.51457 8 -9 0 18 14.5037 3.67014 2 8 0 -18 22.8360 4.66960 4 8 0 -18 31.6110 4.61547 1 -8 0 18 20.4431 3.79713 8 -8 0 18 23.5700 5.18059 5 -8 0 18 19.7343 3.91254 2 7 0 -18 99.7933 8.09134 1 7 0 -18 93.4531 8.67352 4 -7 0 18 80.1036 8.09394 2 -7 0 18 100.798 7.18989 8 6 0 -18 11.8581 3.08586 1 6 0 -18 8.57453 3.23067 4 6 0 -18 7.99180 4.46758 6 -6 0 18 11.0542 2.78640 8 -6 0 18 0.80810 3.59134 5 -6 0 18 7.32507 3.06339 2 5 0 -18 79.1792 7.57887 4 5 0 -18 76.7813 9.20042 6 5 0 -18 99.4101 7.05920 1 -5 0 18 84.4216 6.38050 8 -5 0 18 79.2476 9.03627 5 -5 0 18 76.6409 7.78611 2 4 0 -18 31.6873 4.13294 1 4 0 -18 33.8109 5.91473 6 4 0 -18 28.6323 4.22695 4 -4 0 18 33.0765 4.87938 2 -4 0 18 31.2666 5.76698 5 3 0 -18 3.62023 2.38790 4 3 0 -18 1.93686 3.73187 6 3 0 -18 2.51378 2.39890 1 -3 0 18 0.37220 3.52405 5 -3 0 18 1.63822 2.92094 2 2 0 -18 54.1883 4.82739 4 2 0 -18 43.0726 6.97971 6 2 0 -18 47.0054 4.70161 1 -2 0 18 50.7750 7.25039 5 -2 0 18 40.6350 5.64051 2 1 0 -18 4.69296 2.48526 1 1 0 -18 4.19532 4.18726 6 1 0 -18 5.45866 1.90305 4 -1 0 18 3.28050 3.87470 5 -1 0 18 4.77213 3.09126 2 0 0 -18 45.4334 4.61642 1 0 0 18 52.8967 6.56593 2 0 0 18 58.4118 7.55904 5 9 -1 -18 33.7833 4.89529 1 9 -1 -18 16.1535 4.57772 4 -9 1 18 26.0910 4.08723 8 -9 1 18 25.8809 5.63485 5 -9 1 18 18.0926 3.96874 2 8 -1 -18 -2.3557 2.89933 4 8 -1 -18 2.53987 3.05744 1 -8 1 18 2.30340 2.85558 2 -8 1 18 -0.2645 2.37507 8 -8 1 18 -0.3791 3.47379 5 7 -1 -18 6.10982 4.33887 6 7 -1 -18 6.97291 3.27807 4 7 -1 -18 4.29541 2.93400 1 -7 1 18 2.25241 2.85354 2 -7 1 18 3.13354 2.47496 8 -7 1 18 2.36489 3.68973 5 6 -1 -18 3.29386 2.95129 4 6 -1 -18 4.95056 2.83536 1 6 -1 -18 1.97708 3.91847 6 -6 1 18 4.50051 3.76453 5 -6 1 18 1.88280 2.14522 8 -6 1 18 3.71551 3.12475 2 5 -1 -18 16.5796 4.89375 6 5 -1 -18 16.3927 3.84551 4 5 -1 -18 24.5759 3.78126 1 -5 1 18 20.9484 4.07991 2 -5 1 18 14.1786 4.70808 5 4 -1 -18 94.0038 6.84586 1 4 -1 -18 86.2574 9.41995 6 4 -1 -18 78.8948 7.54870 4 -4 1 18 91.8641 8.39968 2 -4 1 18 72.0417 8.99469 5 3 -1 -18 -0.0071 2.29804 1 3 -1 -18 1.86185 2.52506 4 3 -1 -18 1.84982 3.44170 6 -3 1 18 0.67794 2.92237 2 -3 1 18 2.02945 3.44413 5 2 -1 -18 201.042 12.6494 4 2 -1 -18 196.801 11.7587 1 2 -1 -18 164.301 14.2219 6 -2 1 18 196.972 14.7060 5 -2 1 18 177.895 13.5687 2 1 -1 -18 34.7837 4.13140 1 1 -1 -18 32.7540 3.96026 4 -1 1 18 29.2158 5.78320 5 -1 1 18 22.3868 4.85484 2 0 -1 -18 6.80878 2.32477 4 9 -2 -18 78.6346 8.56121 4 8 -2 -18 -0.7832 2.65232 1 8 -2 -18 0.93866 3.09708 4 -8 2 18 -0.4863 3.17696 5 -8 2 18 2.36633 2.47808 8 -8 2 18 -2.3434 2.60321 2 7 -2 -18 35.3174 5.57988 4 7 -2 -18 38.8939 5.00924 1 7 -2 -18 32.6695 6.09044 6 -7 2 18 37.0907 4.41951 8 -7 2 18 35.4975 6.00879 5 -7 2 18 36.9448 5.26313 2 6 -2 -18 41.8325 5.75552 4 6 -2 -18 31.5208 6.13172 6 6 -2 -18 56.0942 5.59884 1 -6 2 18 49.5565 7.09715 5 -6 2 18 45.9728 5.75556 2 5 -2 -18 30.5056 4.22324 1 5 -2 -18 21.1526 5.10843 6 5 -2 -18 25.1090 4.49576 4 -5 2 18 24.5424 5.16234 5 -5 2 18 15.9458 4.16461 2 4 -2 -18 3.52634 2.74129 1 4 -2 -18 5.71480 4.05793 6 4 -2 -18 3.26101 2.96240 4 -4 2 18 3.52107 3.15181 2 -4 2 18 5.33151 4.13354 5 3 -2 -18 5.94748 3.89457 6 3 -2 -18 0.82716 2.56102 1 3 -2 -18 5.99336 2.92071 4 -3 2 18 2.57266 3.53373 5 -3 2 18 0.87078 2.90441 2 2 -2 -18 25.7959 3.89293 1 2 -2 -18 16.8565 3.72655 4 -2 2 18 19.8456 4.53433 2 -2 2 18 22.0312 4.92012 5 8 -3 -18 60.3207 6.39646 1 8 -3 -18 59.4019 7.33536 4 -8 3 18 56.5621 6.43012 2 -8 3 18 56.4809 7.70809 5 7 -3 -18 2.51756 3.09481 1 7 -3 -18 4.34323 3.40868 4 7 -3 -18 2.75019 4.11150 6 -7 3 18 3.43252 3.20774 2 -7 3 18 4.36098 3.82612 5 6 -3 -18 290.579 21.0380 6 6 -3 -18 304.456 19.9980 4 6 -3 -18 331.540 18.1823 1 -6 3 18 299.014 19.8405 2 -6 3 18 275.168 20.9125 5 5 -3 -18 7.34067 3.17187 1 5 -3 -18 9.79780 4.24384 6 5 -3 -18 9.24718 3.67163 4 -5 3 18 8.82520 4.35916 5 -5 3 18 15.9092 3.97372 2 4 -3 -18 192.390 14.0074 4 4 -3 -18 226.864 12.8601 1 4 -3 -18 193.619 14.9898 6 -4 3 18 177.468 13.9811 2 -4 3 18 210.611 15.5716 5 3 -3 -18 116.920 9.10791 4 3 -3 -18 95.4911 10.1338 6 3 -3 -18 105.951 8.18428 1 -3 3 18 111.844 9.52308 2 -3 3 18 117.917 11.2442 5 4 5 -19 3.44371 2.43432 4 4 5 -19 1.56409 2.55415 1 -4 -5 19 -2.5416 2.72214 2 3 5 -19 2.21260 2.35729 1 -3 -5 19 1.98314 2.88481 2 2 5 -19 -0.0236 2.14453 1 -2 -5 19 0.73234 2.70164 2 1 5 -19 6.46674 4.79887 6 1 5 -19 10.6892 2.58537 1 -1 -5 19 9.29946 4.74348 5 -1 -5 19 11.4229 3.72786 2 5 4 -19 291.727 16.6781 1 5 4 -19 264.611 19.8263 7 5 4 -19 267.995 17.6424 4 -5 -4 19 300.307 20.6311 5 -5 -4 19 273.514 18.4393 2 4 4 -19 65.2473 5.82838 1 4 4 -19 56.2793 5.34940 4 -4 -4 19 57.3552 7.91605 5 -4 -4 19 55.7612 6.46203 2 3 4 -19 61.6370 5.30454 1 -3 -4 19 60.4692 8.08783 5 -3 -4 19 45.7213 5.94282 2 2 4 -19 53.6976 4.81633 1 2 4 -19 40.1676 7.35138 6 -2 -4 19 52.2220 6.25707 2 -2 -4 19 43.2913 7.01348 5 1 4 -19 3.37461 4.62691 6 1 4 -19 0.08919 1.98702 1 -1 -4 19 10.1196 4.46812 5 -1 -4 19 2.36401 2.86021 2 0 4 -19 15.0501 2.62965 1 0 4 -19 11.1179 5.22319 6 0 -4 19 12.6088 4.82063 5 0 -4 19 17.7774 4.15670 2 6 3 -19 19.8393 3.88517 1 6 3 -19 13.6981 3.69215 4 -6 -3 19 20.6284 5.29404 5 -6 -3 19 21.6914 4.27179 2 5 3 -19 10.3414 3.24518 4 5 3 -19 6.14288 3.10633 1 -5 -3 19 7.70769 4.22579 5 -5 -3 19 7.03067 3.39425 2 4 3 -19 7.55681 2.89526 1 4 3 -19 4.91002 2.59470 4 -4 -3 19 6.60427 3.29887 2 -4 -3 19 8.16052 4.31983 5 3 3 -19 10.5123 2.14362 4 3 3 -19 7.62763 2.68694 1 3 3 -19 2.69546 4.69427 6 -3 -3 19 11.8373 4.68420 5 -3 -3 19 9.80379 3.53166 2 2 3 -19 128.068 12.8653 6 2 3 -19 140.196 8.45461 1 -2 -3 19 115.589 11.9569 5 -2 -3 19 114.919 9.83862 2 1 3 -19 14.7314 5.21496 6 1 3 -19 9.57658 2.57867 1 -1 -3 19 9.64811 4.47865 5 -1 -3 19 9.55280 3.60589 2 6 2 -19 57.9175 5.70937 1 6 2 -19 41.1354 5.31667 4 -6 -2 19 37.7559 5.48339 2 -6 -2 19 46.5279 7.07084 5 5 2 -19 58.4637 5.90772 4 5 2 -19 68.9636 6.13157 1 -5 -2 19 62.4969 8.05088 5 -5 -2 19 43.4173 6.08959 2 4 2 -19 61.0908 5.65187 1 4 2 -19 50.8465 8.01713 6 4 2 -19 57.1160 5.45086 4 -4 -2 19 55.1769 7.77413 5 -4 -2 19 51.7991 6.37568 2 3 2 -19 22.1445 5.36798 6 3 2 -19 14.8781 2.57626 4 3 2 -19 17.0513 3.24491 1 -3 -2 19 11.6470 4.78626 5 -3 -2 19 17.3036 4.08986 2 2 2 -19 8.25273 2.67480 1 2 2 -19 11.4794 4.89748 6 -2 -2 19 9.97424 3.66339 2 -2 -2 19 10.6981 4.55851 5 1 2 -19 2.45759 2.15266 1 1 2 -19 5.42591 4.55964 6 -1 -2 19 6.61785 3.14766 2 -1 -2 19 0.26412 3.36743 5 7 1 -19 28.7523 4.78530 4 6 1 -19 83.5275 7.42079 1 6 1 -19 86.4764 7.94253 4 -6 -1 19 79.7094 7.92472 2 -6 -1 19 96.3252 10.0853 5 5 1 -19 1.02782 4.28555 6 5 1 -19 -4.3222 2.42960 1 5 1 -19 0.16695 2.60460 4 -5 -1 19 -0.9094 2.71510 2 -5 -1 19 -1.6043 3.42179 5 4 1 -19 105.858 7.93813 4 4 1 -19 111.789 7.78023 1 4 1 -19 90.6061 10.3932 6 -4 -1 19 104.649 10.8788 5 -4 -1 19 93.0846 9.06817 2 3 1 -19 4.48966 2.35647 4 3 1 -19 3.95930 2.60872 1 3 1 -19 -0.6385 3.96047 6 -3 -1 19 -0.0138 3.79112 5 -3 -1 19 0.60624 2.97065 2 2 1 -19 5.75175 4.72472 6 2 1 -19 7.55181 1.91624 4 2 1 -19 8.29272 2.65373 1 -2 -1 19 3.34786 4.03897 5 -2 -1 19 5.84056 3.54233 2 6 0 -19 9.09073 3.45653 4 6 0 -19 19.1190 3.72974 1 -6 0 19 13.8406 4.59093 5 -6 0 19 21.7507 3.58295 8 -6 0 19 20.2977 4.15498 2 5 0 -19 -4.2356 3.27785 6 5 0 -19 -0.8878 2.57900 4 5 0 -19 -1.2289 2.41203 1 -5 0 19 -0.9587 3.40263 5 -5 0 19 -1.0946 3.02674 2 4 0 -19 62.3655 6.03403 4 4 0 -19 74.4840 6.12682 1 4 0 -19 43.7004 7.29537 6 -4 0 19 54.2057 7.66984 5 -4 0 19 53.2180 6.60636 2 3 0 -19 5.88262 2.54616 4 3 0 -19 3.86786 2.72480 1 3 0 -19 8.24965 4.46444 6 -3 0 19 1.04356 3.15462 2 -3 0 19 2.01421 3.70108 5 2 0 -19 1.85281 2.12362 4 6 -1 -19 11.2980 3.59019 4 5 -1 -19 1.65590 3.88572 6 5 -1 -19 3.71646 2.80822 1 5 -1 -19 2.33420 3.02117 4 -5 1 19 3.47469 3.70269 5 -5 1 19 4.29526 3.27087 2 4 -1 -19 -0.0730 2.69647 4 4 -1 -19 1.60020 4.03586 6 4 -1 -19 4.11781 2.80387 1 -4 1 19 0.74343 3.56152 5 -4 1 19 -0.4473 3.02984 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 31634 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ge1 Ge 0.13918(2) 0.57600(2) 0.42417(2) 0.01486(5) Uani 1 1 d . . . . . C1 C 0.12996(15) 0.35381(15) 0.46969(12) 0.0184(4) Uani 1 1 d . . . . . H1 H 0.0981 0.3737 0.5165 0.022 Uiso 1 1 calc R U . . . N1 N 0.16016(12) 0.42546(12) 0.41469(9) 0.0136(3) Uani 1 1 d . . . . . Cl1 Cl -0.07047(4) 0.46540(4) 0.35608(3) 0.02215(10) Uani 1 1 d . . . . . Ge2 Ge 0.25102(2) 0.27418(2) 0.06553(2) 0.01528(5) Uani 1 1 d . . . . . N2 N 0.19410(12) 0.57478(11) 0.31903(9) 0.0125(3) Uani 1 1 d . . . . . C2 C 0.14437(16) 0.25237(16) 0.45949(12) 0.0214(4) Uani 1 1 d . . . . . H2 H 0.1247 0.2031 0.4995 0.026 Uiso 1 1 calc R U . . . Cl2 Cl 0.23187(4) 0.12042(4) 0.13956(3) 0.02293(10) Uani 1 1 d . . . . . C5 C 0.20608(13) 0.40071(14) 0.34770(11) 0.0122(3) Uani 1 1 d . . . . . C4 C 0.21895(14) 0.29747(14) 0.33268(11) 0.0153(3) Uani 1 1 d . . . . . H4 H 0.2484 0.2778 0.2841 0.018 Uiso 1 1 calc R U . . . N4 N 0.30350(11) 0.40718(11) 0.16407(9) 0.0123(3) Uani 1 1 d . . . . . C3 C 0.18849(15) 0.22379(15) 0.38916(12) 0.0199(4) Uani 1 1 d . . . . . H3 H 0.1977 0.1534 0.3799 0.024 Uiso 1 1 calc R U . . . N3 N 0.08798(12) 0.25673(12) 0.07694(9) 0.0135(3) Uani 1 1 d . . . . . C6 C 0.24370(14) 0.49299(14) 0.29554(11) 0.0112(3) Uani 1 1 d D . . . . H6 H 0.3301(14) 0.5299(15) 0.3163(12) 0.013 Uiso 1 1 d D U . . . C16 C 0.44641(15) 0.74982(15) 0.42577(11) 0.0168(3) Uani 1 1 d . . . . . H16 H 0.4003 0.6698 0.4329 0.020 Uiso 1 1 calc R U . . . C7 C 0.24420(14) 0.68942(14) 0.30285(11) 0.0132(3) Uani 1 1 d . . . . . C17 C 0.55728(16) 0.75271(17) 0.40081(13) 0.0260(4) Uani 1 1 d . . . . . H17A H 0.6041 0.7309 0.4479 0.039 Uiso 1 1 calc R U . . . H17B H 0.6069 0.8320 0.3977 0.039 Uiso 1 1 calc R U . . . H17C H 0.5321 0.6971 0.3408 0.039 Uiso 1 1 calc R U . . . C9 C 0.40864(16) 0.88036(15) 0.33014(12) 0.0203(4) Uani 1 1 d . . . . . H9 H 0.4911 0.9337 0.3577 0.024 Uiso 1 1 calc R U . . . C18 C 0.48344(18) 0.83896(16) 0.51792(12) 0.0251(4) Uani 1 1 d . . . . . H18A H 0.5320 0.8205 0.5664 0.038 Uiso 1 1 calc R U . . . H18B H 0.4113 0.8354 0.5333 0.038 Uiso 1 1 calc R U . . . H18C H 0.5306 0.9180 0.5131 0.038 Uiso 1 1 calc R U . . . C8 C 0.36472(15) 0.77156(14) 0.34981(11) 0.0153(3) Uani 1 1 d . . . . . C15 C -0.04620(19) 0.7003(2) 0.21754(17) 0.0392(5) Uani 1 1 d . . . . . H15A H -0.1306 0.6425 0.1912 0.059 Uiso 1 1 calc R U . . . H15B H -0.0317 0.7656 0.1887 0.059 Uiso 1 1 calc R U . . . H15C H -0.0281 0.7298 0.2841 0.059 Uiso 1 1 calc R U . . . C12 C 0.16730(15) 0.72394(15) 0.24589(11) 0.0160(3) Uani 1 1 d . . . . . C11 C 0.21470(16) 0.83564(15) 0.23136(12) 0.0202(4) Uani 1 1 d . . . . . H11 H 0.1633 0.8592 0.1933 0.024 Uiso 1 1 calc R U . . . C10 C 0.33445(17) 0.91239(15) 0.27116(12) 0.0225(4) Uani 1 1 d . . . . . H10 H 0.3660 0.9867 0.2583 0.027 Uiso 1 1 calc R U . . . C14 C 0.00833(17) 0.59603(18) 0.09617(13) 0.0270(4) Uani 1 1 d . . . . . H14A H -0.0770 0.5412 0.0686 0.040 Uiso 1 1 calc R U . . . H14B H 0.0575 0.5554 0.0859 0.040 Uiso 1 1 calc R U . . . H14C H 0.0275 0.6617 0.0676 0.040 Uiso 1 1 calc R U . . . C13 C 0.03470(15) 0.64247(15) 0.19972(12) 0.0193(4) Uani 1 1 d . . . . . H13 H 0.0144 0.5736 0.2267 0.023 Uiso 1 1 calc R U . . . C20 C -0.12447(15) 0.15599(15) 0.03820(12) 0.0194(4) Uani 1 1 d . . . . . H20 H -0.1985 0.0924 0.0009 0.023 Uiso 1 1 calc R U . . . C19 C -0.01711(15) 0.16521(15) 0.02606(12) 0.0175(3) Uani 1 1 d . . . . . H19 H -0.0172 0.1059 -0.0190 0.021 Uiso 1 1 calc R U . . . C21 C -0.12199(15) 0.24191(15) 0.10625(12) 0.0183(4) Uani 1 1 d . . . . . H21 H -0.1946 0.2364 0.1171 0.022 Uiso 1 1 calc R U . . . C22 C -0.01343(14) 0.33556(14) 0.15832(11) 0.0150(3) Uani 1 1 d . . . . . H22 H -0.0110 0.3944 0.2052 0.018 Uiso 1 1 calc R U . . . C23 C 0.09192(14) 0.34266(14) 0.14135(11) 0.0125(3) Uani 1 1 d . . . . . C24 C 0.21514(14) 0.44305(14) 0.18867(11) 0.0110(3) Uani 1 1 d D . . . . H24 H 0.2158(16) 0.5089(14) 0.1663(12) 0.013 Uiso 1 1 d D U . . . C25 C 0.42287(14) 0.49781(14) 0.17962(11) 0.0128(3) Uani 1 1 d . . . . . C33 C 0.58400(18) 0.33584(18) 0.27206(15) 0.0292(4) Uani 1 1 d . . . . . H33A H 0.5674 0.2709 0.3014 0.044 Uiso 1 1 calc R U . . . H33B H 0.6694 0.3911 0.2973 0.044 Uiso 1 1 calc R U . . . H33C H 0.5639 0.3051 0.2054 0.044 Uiso 1 1 calc R U . . . C26 C 0.44254(14) 0.58537(14) 0.13089(11) 0.0145(3) Uani 1 1 d . . . . . C32 C 0.53726(17) 0.44864(17) 0.39500(12) 0.0260(4) Uani 1 1 d . . . . . H32A H 0.5233 0.3847 0.4254 0.039 Uiso 1 1 calc R U . . . H32B H 0.4855 0.4861 0.4056 0.039 Uiso 1 1 calc R U . . . H32C H 0.6217 0.5067 0.4204 0.039 Uiso 1 1 calc R U . . . C27 C 0.55875(15) 0.67358(15) 0.15099(12) 0.0193(4) Uani 1 1 d . . . . . H27 H 0.5720 0.7352 0.1213 0.023 Uiso 1 1 calc R U . . . C34 C 0.34380(15) 0.58377(15) 0.05350(11) 0.0161(3) Uani 1 1 d . . . . . H34 H 0.2678 0.5132 0.0459 0.019 Uiso 1 1 calc R U . . . C28 C 0.65557(15) 0.67338(15) 0.21341(12) 0.0202(4) Uani 1 1 d . . . . . H28 H 0.7340 0.7349 0.2270 0.024 Uiso 1 1 calc R U . . . C36 C 0.37354(17) 0.57328(18) -0.03796(12) 0.0262(4) Uani 1 1 d . . . . . H36A H 0.3060 0.5661 -0.0877 0.039 Uiso 1 1 calc R U . . . H36B H 0.3877 0.5037 -0.0514 0.039 Uiso 1 1 calc R U . . . H36C H 0.4459 0.6434 -0.0331 0.039 Uiso 1 1 calc R U . . . C29 C 0.63700(15) 0.58303(15) 0.25558(12) 0.0187(4) Uani 1 1 d . . . . . H29 H 0.7041 0.5810 0.2958 0.022 Uiso 1 1 calc R U . . . C35 C 0.32191(16) 0.69257(16) 0.07548(13) 0.0218(4) Uani 1 1 d . . . . . H35A H 0.2497 0.6825 0.0292 0.033 Uiso 1 1 calc R U . . . H35B H 0.3913 0.7619 0.0747 0.033 Uiso 1 1 calc R U . . . H35C H 0.3108 0.7030 0.1366 0.033 Uiso 1 1 calc R U . . . C30 C 0.52189(14) 0.49438(15) 0.24070(11) 0.0151(3) Uani 1 1 d . . . . . C31 C 0.50782(15) 0.39908(15) 0.29098(12) 0.0177(3) Uani 1 1 d . . . . . H31 H 0.4216 0.3398 0.2673 0.021 Uiso 1 1 calc R U . . . C37T C 0.88332(18) 0.03396(17) 0.31078(14) 0.0294(4) Uani 1 1 d D . . . . C38T C 0.8531(2) 0.12741(18) 0.31892(14) 0.0339(5) Uani 1 1 d D . . . . H38T H 0.8537 0.1670 0.2715 0.041 Uiso 1 1 calc R U . . . C39T C 0.8221(2) 0.16380(18) 0.39446(15) 0.0337(5) Uani 1 1 d D . . . . H39T H 0.8012 0.2274 0.3983 0.040 Uiso 1 1 calc R U . . . C40T C 0.82147(18) 0.10772(17) 0.46485(14) 0.0309(4) Uani 1 1 d D . . . . H40T H 0.8000 0.1323 0.5169 0.037 Uiso 1 1 calc R U . . . C41T C 0.85252(18) 0.01560(17) 0.45807(14) 0.0310(5) Uani 1 1 d D . . . . H41T H 0.8533 -0.0229 0.5061 0.037 Uiso 1 1 calc R U . . . C42T C 0.88245(17) -0.02085(16) 0.38203(14) 0.0282(4) Uani 1 1 d D . . . . H42T H 0.9029 -0.0847 0.3783 0.034 Uiso 1 1 calc R U . . . C43T C 0.9173(2) -0.0045(2) 0.22815(15) 0.0400(5) Uani 1 1 d D . . . . H43A H 0.9701 -0.0418 0.2452 0.060 Uiso 1 1 calc R U . . . H43B H 0.9593 0.0639 0.2068 0.060 Uiso 1 1 calc R U . . . H43C H 0.8445 -0.0607 0.1787 0.060 Uiso 1 1 calc R U . . . C1T C 0.5846(6) 0.0057(7) 0.1608(4) 0.0632(19) Uani 0.5 1 d D U P A -1 H1TA H 0.6553 -0.0096 0.1658 0.095 Uiso 0.5 1 calc R U P A -1 H1TB H 0.5246 -0.0548 0.1792 0.095 Uiso 0.5 1 calc R U P A -1 H1TC H 0.6085 0.0829 0.2013 0.095 Uiso 0.5 1 calc R U P A -1 C2T C 0.4256(7) -0.0007(6) -0.1148(5) 0.0664(19) Uani 0.5 1 d D U P A -1 H2T H 0.3883 -0.0029 -0.1761 0.080 Uiso 0.5 1 calc R U P A -1 C3T C 0.4025(5) 0.0515(6) -0.0429(5) 0.0570(16) Uani 0.5 1 d D U P A -1 H3T H 0.3496 0.0871 -0.0541 0.068 Uiso 0.5 1 calc R U P A -1 C4T C 0.4547(7) 0.0537(7) 0.0466(6) 0.0367(18) Uani 0.5 1 d D U P A -1 H4T H 0.4370 0.0900 0.0962 0.044 Uiso 0.5 1 calc R U P A -1 C5T C 0.5322(4) 0.0034(4) 0.0636(4) 0.0351(10) Uani 0.5 1 d D U P A -1 C6T C 0.5578(8) -0.0493(8) -0.0079(5) 0.0358(17) Uani 0.5 1 d D U P A -1 H6T H 0.6113 -0.0840 0.0039 0.043 Uiso 0.5 1 calc R U P A -1 C7T C 0.5052(7) -0.0515(5) -0.0978(5) 0.0599(17) Uani 0.5 1 d D U P A -1 H7T H 0.5232 -0.0874 -0.1474 0.072 Uiso 0.5 1 calc R U P A -1 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ge1 0.01716(9) 0.01620(9) 0.01453(9) 0.00359(7) 0.00752(7) 0.00938(7) C1 0.0162(8) 0.0239(9) 0.0169(8) 0.0084(7) 0.0064(7) 0.0090(7) N1 0.0109(7) 0.0159(7) 0.0134(7) 0.0038(6) 0.0028(5) 0.0059(6) Cl1 0.0163(2) 0.0310(2) 0.0249(2) 0.01011(19) 0.01091(17) 0.01279(18) Ge2 0.01371(9) 0.01589(9) 0.01491(9) -0.00101(7) 0.00379(7) 0.00727(7) N2 0.0137(7) 0.0129(7) 0.0140(7) 0.0035(5) 0.0062(5) 0.0080(6) C2 0.0207(9) 0.0223(9) 0.0246(9) 0.0136(8) 0.0080(8) 0.0096(8) Cl2 0.0243(2) 0.0165(2) 0.0264(2) 0.00048(18) 0.00191(18) 0.01235(18) C5 0.0071(7) 0.0152(8) 0.0106(7) 0.0018(6) -0.0006(6) 0.0037(6) C4 0.0133(8) 0.0165(8) 0.0163(8) 0.0038(7) 0.0039(7) 0.0073(7) N4 0.0091(6) 0.0136(7) 0.0140(7) 0.0008(5) 0.0034(5) 0.0058(5) C3 0.0189(9) 0.0175(9) 0.0255(9) 0.0082(7) 0.0058(7) 0.0097(7) N3 0.0125(7) 0.0134(7) 0.0128(7) 0.0027(5) 0.0006(5) 0.0059(6) C6 0.0080(7) 0.0127(8) 0.0129(8) 0.0023(6) 0.0026(6) 0.0052(6) C16 0.0160(8) 0.0146(8) 0.0162(8) 0.0005(7) 0.0012(7) 0.0065(7) C7 0.0161(8) 0.0138(8) 0.0120(8) 0.0024(6) 0.0063(6) 0.0082(7) C17 0.0193(9) 0.0276(10) 0.0288(10) 0.0020(8) 0.0048(8) 0.0112(8) C9 0.0193(9) 0.0152(8) 0.0199(9) 0.0012(7) 0.0039(7) 0.0035(7) C18 0.0303(10) 0.0235(10) 0.0183(9) 0.0009(8) 0.0014(8) 0.0136(8) C8 0.0170(8) 0.0155(8) 0.0132(8) 0.0014(7) 0.0046(7) 0.0078(7) C15 0.0234(11) 0.0367(12) 0.0611(15) 0.0065(11) 0.0119(10) 0.0196(10) C12 0.0181(8) 0.0180(8) 0.0144(8) 0.0026(7) 0.0054(7) 0.0108(7) C11 0.0273(10) 0.0198(9) 0.0182(9) 0.0061(7) 0.0049(7) 0.0156(8) C10 0.0312(10) 0.0131(8) 0.0219(9) 0.0060(7) 0.0081(8) 0.0080(8) C14 0.0211(9) 0.0302(10) 0.0238(10) 0.0079(8) -0.0003(8) 0.0089(8) C13 0.0162(8) 0.0213(9) 0.0236(9) 0.0082(7) 0.0045(7) 0.0115(7) C20 0.0138(8) 0.0158(8) 0.0211(9) 0.0047(7) -0.0004(7) 0.0021(7) C19 0.0175(8) 0.0145(8) 0.0163(8) 0.0022(7) 0.0006(7) 0.0059(7) C21 0.0117(8) 0.0218(9) 0.0230(9) 0.0111(7) 0.0043(7) 0.0076(7) C22 0.0141(8) 0.0165(8) 0.0154(8) 0.0049(7) 0.0036(7) 0.0079(7) C23 0.0122(8) 0.0134(8) 0.0115(8) 0.0046(6) 0.0017(6) 0.0056(6) C24 0.0097(7) 0.0124(8) 0.0123(8) 0.0035(6) 0.0029(6) 0.0063(6) C25 0.0093(7) 0.0140(8) 0.0128(8) -0.0011(6) 0.0026(6) 0.0049(6) C33 0.0273(10) 0.0318(11) 0.0396(12) 0.0143(9) 0.0141(9) 0.0202(9) C26 0.0134(8) 0.0158(8) 0.0157(8) 0.0016(7) 0.0060(7) 0.0080(7) C32 0.0276(10) 0.0301(10) 0.0182(9) 0.0075(8) 0.0018(8) 0.0129(9) C27 0.0181(9) 0.0171(9) 0.0232(9) 0.0053(7) 0.0096(7) 0.0066(7) C34 0.0145(8) 0.0191(9) 0.0153(8) 0.0058(7) 0.0047(7) 0.0074(7) C28 0.0110(8) 0.0197(9) 0.0253(9) 0.0015(7) 0.0067(7) 0.0031(7) C36 0.0263(10) 0.0387(11) 0.0191(9) 0.0097(8) 0.0100(8) 0.0175(9) C29 0.0109(8) 0.0252(9) 0.0177(8) 0.0010(7) 0.0024(7) 0.0084(7) C35 0.0206(9) 0.0249(9) 0.0250(9) 0.0099(8) 0.0081(8) 0.0132(8) C30 0.0140(8) 0.0184(8) 0.0132(8) 0.0007(7) 0.0044(6) 0.0085(7) C31 0.0130(8) 0.0222(9) 0.0175(8) 0.0046(7) 0.0022(7) 0.0089(7) C37T 0.0292(11) 0.0237(10) 0.0301(11) 0.0054(8) 0.0042(9) 0.0097(9) C38T 0.0461(13) 0.0290(11) 0.0309(11) 0.0131(9) 0.0091(10) 0.0203(10) C39T 0.0399(12) 0.0279(11) 0.0374(12) 0.0102(9) 0.0096(10) 0.0194(10) C40T 0.0293(11) 0.0281(10) 0.0309(11) 0.0068(9) 0.0081(9) 0.0093(9) C41T 0.0294(11) 0.0248(10) 0.0331(11) 0.0133(9) 0.0051(9) 0.0066(9) C42T 0.0261(10) 0.0179(9) 0.0362(11) 0.0078(8) 0.0025(9) 0.0088(8) C43T 0.0519(14) 0.0345(12) 0.0376(12) 0.0078(10) 0.0145(11) 0.0232(11) C1T 0.038(3) 0.064(4) 0.054(4) 0.010(4) 0.011(3) -0.008(3) C2T 0.055(4) 0.053(4) 0.053(4) 0.027(4) 0.010(4) -0.017(3) C3T 0.029(3) 0.056(3) 0.082(4) 0.038(3) 0.022(3) 0.005(3) C4T 0.027(3) 0.026(3) 0.063(5) 0.009(4) 0.027(4) 0.012(2) C5T 0.021(2) 0.027(2) 0.048(3) 0.003(2) 0.015(2) 0.0013(18) C6T 0.034(4) 0.022(3) 0.052(4) 0.006(4) 0.029(4) 0.005(2) C7T 0.069(4) 0.030(3) 0.059(4) 0.007(3) 0.035(3) -0.007(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0015 0.0009 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0030 0.0019 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.0998 0.0984 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ge Ge 0.3016 1.1903 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N2 Ge1 N1 80.65(6) N2 Ge1 Cl1 101.44(5) N1 Ge1 Cl1 90.43(5) N1 C1 C2 121.31(16) N1 C1 H1 119.3 C2 C1 H1 119.3 C1 N1 C5 121.21(14) C1 N1 Ge1 123.65(11) C5 N1 Ge1 115.13(11) N4 Ge2 N3 80.80(6) N4 Ge2 Cl2 103.53(5) N3 Ge2 Cl2 88.37(5) C7 N2 C6 119.33(13) C7 N2 Ge1 112.44(10) C6 N2 Ge1 119.23(10) C1 C2 C3 118.27(16) C1 C2 H2 120.9 C3 C2 H2 120.9 N1 C5 C4 119.74(15) N1 C5 C6 115.42(14) C4 C5 C6 124.81(14) C3 C4 C5 119.26(15) C3 C4 H4 120.4 C5 C4 H4 120.4 C25 N4 C24 117.69(12) C25 N4 Ge2 115.69(10) C24 N4 Ge2 119.45(10) C4 C3 C2 120.16(16) C4 C3 H3 119.9 C2 C3 H3 119.9 C23 N3 C19 121.23(14) C23 N3 Ge2 115.27(11) C19 N3 Ge2 123.48(11) N2 C6 C5 107.45(12) N2 C6 C24 114.43(12) C5 C6 C24 114.80(13) N2 C6 H6 112.2(11) C5 C6 H6 105.5(11) C24 C6 H6 102.1(11) C8 C16 C17 111.25(14) C8 C16 C18 110.94(14) C17 C16 C18 110.50(15) C8 C16 H16 108.0 C17 C16 H16 108.0 C18 C16 H16 108.0 C8 C7 C12 119.50(15) C8 C7 N2 121.40(14) C12 C7 N2 118.78(15) C16 C17 H17A 109.5 C16 C17 H17B 109.5 H17A C17 H17B 109.5 C16 C17 H17C 109.5 H17A C17 H17C 109.5 H17B C17 H17C 109.5 C10 C9 C8 121.41(16) C10 C9 H9 119.3 C8 C9 H9 119.3 C16 C18 H18A 109.5 C16 C18 H18B 109.5 H18A C18 H18B 109.5 C16 C18 H18C 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 C9 C8 C7 118.75(15) C9 C8 C16 118.25(15) C7 C8 C16 122.86(15) C13 C15 H15A 109.5 C13 C15 H15B 109.5 H15A C15 H15B 109.5 C13 C15 H15C 109.5 H15A C15 H15C 109.5 H15B C15 H15C 109.5 C11 C12 C7 119.10(16) C11 C12 C13 119.13(15) C7 C12 C13 121.77(15) C10 C11 C12 121.33(16) C10 C11 H11 119.3 C12 C11 H11 119.3 C11 C10 C9 119.51(16) C11 C10 H10 120.2 C9 C10 H10 120.2 C13 C14 H14A 109.5 C13 C14 H14B 109.5 H14A C14 H14B 109.5 C13 C14 H14C 109.5 H14A C14 H14C 109.5 H14B C14 H14C 109.5 C12 C13 C14 111.20(15) C12 C13 C15 112.47(15) C14 C13 C15 110.40(16) C12 C13 H13 107.5 C14 C13 H13 107.5 C15 C13 H13 107.5 C19 C20 C21 118.45(16) C19 C20 H20 120.8 C21 C20 H20 120.8 N3 C19 C20 121.20(16) N3 C19 H19 119.4 C20 C19 H19 119.4 C22 C21 C20 119.88(16) C22 C21 H21 120.1 C20 C21 H21 120.1 C21 C22 C23 119.38(16) C21 C22 H22 120.3 C23 C22 H22 120.3 N3 C23 C22 119.80(15) N3 C23 C24 115.15(14) C22 C23 C24 125.04(14) N4 C24 C23 107.72(13) N4 C24 C6 114.28(12) C23 C24 C6 115.06(13) N4 C24 H24 111.3(11) C23 C24 H24 106.9(11) C6 C24 H24 101.2(11) C26 C25 C30 119.92(15) C26 C25 N4 120.95(14) C30 C25 N4 119.03(14) C31 C33 H33A 109.5 C31 C33 H33B 109.5 H33A C33 H33B 109.5 C31 C33 H33C 109.5 H33A C33 H33C 109.5 H33B C33 H33C 109.5 C27 C26 C25 118.74(15) C27 C26 C34 118.20(15) C25 C26 C34 122.96(15) C31 C32 H32A 109.5 C31 C32 H32B 109.5 H32A C32 H32B 109.5 C31 C32 H32C 109.5 H32A C32 H32C 109.5 H32B C32 H32C 109.5 C28 C27 C26 121.46(16) C28 C27 H27 119.3 C26 C27 H27 119.3 C26 C34 C35 111.93(14) C26 C34 C36 110.84(14) C35 C34 C36 109.96(14) C26 C34 H34 108.0 C35 C34 H34 108.0 C36 C34 H34 108.0 C29 C28 C27 119.42(16) C29 C28 H28 120.3 C27 C28 H28 120.3 C34 C36 H36A 109.5 C34 C36 H36B 109.5 H36A C36 H36B 109.5 C34 C36 H36C 109.5 H36A C36 H36C 109.5 H36B C36 H36C 109.5 C28 C29 C30 121.68(16) C28 C29 H29 119.2 C30 C29 H29 119.2 C34 C35 H35A 109.5 C34 C35 H35B 109.5 H35A C35 H35B 109.5 C34 C35 H35C 109.5 H35A C35 H35C 109.5 H35B C35 H35C 109.5 C29 C30 C25 118.48(15) C29 C30 C31 118.86(15) C25 C30 C31 122.65(15) C30 C31 C33 111.92(14) C30 C31 C32 111.10(14) C33 C31 C32 110.83(15) C30 C31 H31 107.6 C33 C31 H31 107.6 C32 C31 H31 107.6 C42T C37T C38T 117.53(19) C42T C37T C43T 121.61(18) C38T C37T C43T 120.85(19) C39T C38T C37T 121.42(19) C39T C38T H38T 119.3 C37T C38T H38T 119.3 C38T C39T C40T 120.20(19) C38T C39T H39T 119.9 C40T C39T H39T 119.9 C41T C40T C39T 118.97(19) C41T C40T H40T 120.5 C39T C40T H40T 120.5 C42T C41T C40T 120.50(19) C42T C41T H41T 119.8 C40T C41T H41T 119.8 C41T C42T C37T 121.38(18) C41T C42T H42T 119.3 C37T C42T H42T 119.3 C37T C43T H43A 109.5 C37T C43T H43B 109.5 H43A C43T H43B 109.5 C37T C43T H43C 109.5 H43A C43T H43C 109.5 H43B C43T H43C 109.5 C5T C1T H1TA 109.5 C5T C1T H1TB 109.5 H1TA C1T H1TB 109.5 C5T C1T H1TC 109.5 H1TA C1T H1TC 109.5 H1TB C1T H1TC 109.5 C3T C2T C7T 119.2(7) C3T C2T H2T 120.4 C7T C2T H2T 120.4 C2T C3T C4T 121.0(7) C2T C3T H3T 119.5 C4T C3T H3T 119.5 C5T C4T C3T 120.0(6) C5T C4T H4T 120.0 C3T C4T H4T 120.0 C6T C5T C4T 120.2(5) C6T C5T C1T 121.5(6) C4T C5T C1T 118.3(6) C5T C6T C7T 119.8(7) C5T C6T H6T 120.1 C7T C6T H6T 120.1 C6T C7T C2T 119.8(7) C6T C7T H7T 120.1 C2T C7T H7T 120.1 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Ge1 N2 1.8987(14) Ge1 N1 2.0405(14) Ge1 Cl1 2.3604(11) C1 N1 1.346(2) C1 C2 1.376(2) C1 H1 0.9500 N1 C5 1.348(2) Ge2 N4 1.8856(14) Ge2 N3 2.0421(14) Ge2 Cl2 2.3827(7) N2 C7 1.442(2) N2 C6 1.4607(19) C2 C3 1.389(3) C2 H2 0.9500 C5 C4 1.390(2) C5 C6 1.512(2) C4 C3 1.382(2) C4 H4 0.9500 N4 C25 1.443(2) N4 C24 1.4667(19) C3 H3 0.9500 N3 C23 1.346(2) N3 C19 1.347(2) C6 C24 1.580(2) C6 H6 0.961(15) C16 C8 1.522(2) C16 C17 1.526(2) C16 C18 1.532(2) C16 H16 1.0000 C7 C8 1.414(2) C7 C12 1.415(2) C17 H17A 0.9800 C17 H17B 0.9800 C17 H17C 0.9800 C9 C10 1.387(3) C9 C8 1.394(2) C9 H9 0.9500 C18 H18A 0.9800 C18 H18B 0.9800 C18 H18C 0.9800 C15 C13 1.530(2) C15 H15A 0.9800 C15 H15B 0.9800 C15 H15C 0.9800 C12 C11 1.395(2) C12 C13 1.519(2) C11 C10 1.377(3) C11 H11 0.9500 C10 H10 0.9500 C14 C13 1.529(3) C14 H14A 0.9800 C14 H14B 0.9800 C14 H14C 0.9800 C13 H13 1.0000 C20 C19 1.377(2) C20 C21 1.389(3) C20 H20 0.9500 C19 H19 0.9500 C21 C22 1.385(2) C21 H21 0.9500 C22 C23 1.389(2) C22 H22 0.9500 C23 C24 1.510(2) C24 H24 0.957(15) C25 C26 1.416(2) C25 C30 1.417(2) C33 C31 1.532(2) C33 H33A 0.9800 C33 H33B 0.9800 C33 H33C 0.9800 C26 C27 1.393(2) C26 C34 1.521(2) C32 C31 1.536(2) C32 H32A 0.9800 C32 H32B 0.9800 C32 H32C 0.9800 C27 C28 1.386(2) C27 H27 0.9500 C34 C35 1.532(2) C34 C36 1.537(2) C34 H34 1.0000 C28 C29 1.379(3) C28 H28 0.9500 C36 H36A 0.9800 C36 H36B 0.9800 C36 H36C 0.9800 C29 C30 1.398(2) C29 H29 0.9500 C35 H35A 0.9800 C35 H35B 0.9800 C35 H35C 0.9800 C30 C31 1.517(2) C31 H31 1.0000 C37T C42T 1.390(3) C37T C38T 1.393(3) C37T C43T 1.506(3) C38T C39T 1.381(3) C38T H38T 0.9500 C39T C40T 1.389(3) C39T H39T 0.9500 C40T C41T 1.382(3) C40T H40T 0.9500 C41T C42T 1.380(3) C41T H41T 0.9500 C42T H42T 0.9500 C43T H43A 0.9800 C43T H43B 0.9800 C43T H43C 0.9800 C1T C5T 1.491(7) C1T H1TA 0.9800 C1T H1TB 0.9800 C1T H1TC 0.9800 C2T C3T 1.356(8) C2T C7T 1.404(9) C2T H2T 0.9500 C3T C4T 1.384(8) C3T H3T 0.9500 C4T C5T 1.374(8) C4T H4T 0.9500 C5T C6T 1.373(7) C6T C7T 1.390(8) C6T H6T 0.9500 C7T H7T 0.9500 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion C2 C1 N1 C5 -0.2(2) C2 C1 N1 Ge1 179.04(13) N1 Ge1 N2 C7 -158.65(11) Cl1 Ge1 N2 C7 112.81(10) N1 Ge1 N2 C6 -11.67(11) Cl1 Ge1 N2 C6 -100.21(11) N1 C1 C2 C3 -1.5(3) C1 N1 C5 C4 2.2(2) Ge1 N1 C5 C4 -177.12(11) C1 N1 C5 C6 -176.02(14) Ge1 N1 C5 C6 4.64(17) N1 C5 C4 C3 -2.4(2) C6 C5 C4 C3 175.66(15) N3 Ge2 N4 C25 -159.36(12) Cl2 Ge2 N4 C25 114.57(11) N3 Ge2 N4 C24 -9.62(11) Cl2 Ge2 N4 C24 -95.69(11) C5 C4 C3 C2 0.7(2) C1 C2 C3 C4 1.3(3) C7 N2 C6 C5 161.12(13) Ge1 N2 C6 C5 16.41(16) C7 N2 C6 C24 -70.14(18) Ge1 N2 C6 C24 145.15(11) N1 C5 C6 N2 -12.71(18) C4 C5 C6 N2 169.15(14) N1 C5 C6 C24 -141.24(14) C4 C5 C6 C24 40.6(2) C6 N2 C7 C8 -63.6(2) Ge1 N2 C7 C8 83.30(16) C6 N2 C7 C12 122.84(16) Ge1 N2 C7 C12 -90.21(15) C10 C9 C8 C7 4.9(3) C10 C9 C8 C16 -170.99(16) C12 C7 C8 C9 -7.6(2) N2 C7 C8 C9 178.97(14) C12 C7 C8 C16 168.13(15) N2 C7 C8 C16 -5.3(2) C17 C16 C8 C9 -64.2(2) C18 C16 C8 C9 59.3(2) C17 C16 C8 C7 120.13(17) C18 C16 C8 C7 -116.42(18) C8 C7 C12 C11 5.1(2) N2 C7 C12 C11 178.77(14) C8 C7 C12 C13 -175.20(15) N2 C7 C12 C13 -1.6(2) C7 C12 C11 C10 0.1(3) C13 C12 C11 C10 -179.55(16) C12 C11 C10 C9 -2.9(3) C8 C9 C10 C11 0.3(3) C11 C12 C13 C14 72.6(2) C7 C12 C13 C14 -107.11(18) C11 C12 C13 C15 -51.8(2) C7 C12 C13 C15 128.48(18) C23 N3 C19 C20 -0.2(2) Ge2 N3 C19 C20 178.20(12) C21 C20 C19 N3 -1.8(3) C19 C20 C21 C22 1.6(2) C20 C21 C22 C23 0.4(2) C19 N3 C23 C22 2.2(2) Ge2 N3 C23 C22 -176.26(11) C19 N3 C23 C24 -176.38(14) Ge2 N3 C23 C24 5.14(17) C21 C22 C23 N3 -2.3(2) C21 C22 C23 C24 176.15(15) C25 N4 C24 C23 163.36(13) Ge2 N4 C24 C23 14.22(16) C25 N4 C24 C6 -67.44(18) Ge2 N4 C24 C6 143.41(11) N3 C23 C24 N4 -11.69(18) C22 C23 C24 N4 169.79(14) N3 C23 C24 C6 -140.44(14) C22 C23 C24 C6 41.0(2) N2 C6 C24 N4 153.66(13) C5 C6 C24 N4 -81.40(16) N2 C6 C24 C23 -80.92(17) C5 C6 C24 C23 44.02(18) C24 N4 C25 C26 -64.39(19) Ge2 N4 C25 C26 85.90(16) C24 N4 C25 C30 119.28(16) Ge2 N4 C25 C30 -90.42(15) C30 C25 C26 C27 -6.2(2) N4 C25 C26 C27 177.51(14) C30 C25 C26 C34 170.16(14) N4 C25 C26 C34 -6.1(2) C25 C26 C27 C28 3.7(2) C34 C26 C27 C28 -172.81(15) C27 C26 C34 C35 -64.28(19) C25 C26 C34 C35 119.35(17) C27 C26 C34 C36 58.9(2) C25 C26 C34 C36 -117.49(17) C26 C27 C28 C29 1.0(3) C27 C28 C29 C30 -3.4(3) C28 C29 C30 C25 0.8(2) C28 C29 C30 C31 -178.70(15) C26 C25 C30 C29 4.0(2) N4 C25 C30 C29 -179.65(14) C26 C25 C30 C31 -176.50(14) N4 C25 C30 C31 -0.1(2) C29 C30 C31 C33 -56.4(2) C25 C30 C31 C33 124.09(17) C29 C30 C31 C32 68.1(2) C25 C30 C31 C32 -111.43(18) C42T C37T C38T C39T -0.6(3) C43T C37T C38T C39T -179.8(2) C37T C38T C39T C40T 0.5(3) C38T C39T C40T C41T 0.2(3) C39T C40T C41T C42T -0.7(3) C40T C41T C42T C37T 0.5(3) C38T C37T C42T C41T 0.1(3) C43T C37T C42T C41T 179.3(2) C7T C2T C3T C4T -1.0(11) C2T C3T C4T C5T 0.6(12) C3T C4T C5T C6T -0.1(14) C3T C4T C5T C1T -178.8(7) C4T C5T C6T C7T 0.0(14) C1T C5T C6T C7T 178.7(7) C5T C6T C7T C2T -0.5(12) C3T C2T C7T C6T 0.9(11)