#------------------------------------------------------------------------------ #$Date: 2016-03-26 13:46:54 +0200 (Sat, 26 Mar 2016) $ #$Revision: 180235 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/11/21/7112104.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7112104 loop_ _publ_author_name 'Yan Li' 'Kartik Chandra Mondal' 'Peter Stollberg' 'Hongping Zhu' 'Herbert W. Roesky' 'Regine Herbst-Irmer' 'Dietmar Stalke' 'Heike Fliegl' _publ_section_title ; Unusual formation of a N-heterocyclic germylene via homolytic cleavage of a C-C bond ; _journal_name_full Chem.Commun. _journal_page_first 3356 _journal_paper_doi 10.1039/c4cc00251b _journal_volume 50 _journal_year 2014 _chemical_formula_moiety 'C36 H44 Cl6 N4 Si2, C7 H8' _chemical_formula_sum 'C43 H52 Cl6 N4 Si2' _chemical_formula_weight 893.76 _chemical_name_systematic ; ? ; _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2013 _cell_angle_alpha 90 _cell_angle_beta 94.21(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.149(2) _cell_length_b 17.560(2) _cell_length_c 17.357(3) _cell_measurement_reflns_used 9938 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 27.0865 _cell_measurement_theta_min 2.25 _cell_volume 4300.8(11) _computing_cell_refinement 'SAINT V7.68A' _computing_data_collection 'APEX2 v2012.2' _computing_data_reduction 'SAINT V7.68A' _computing_molecular_graphics 'XP Version 5.1' _computing_publication_material 'XSHELL in SHELXTL-97' _computing_structure_refinement 'SHELXL-2012 (Sheldrick, 2012)' _computing_structure_solution 'SHELXS-2012 (Sheldrick, 2012)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker Smart APEX II Quazar' _diffrn_measurement_method 'omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0540 _diffrn_reflns_av_unetI/netI 0.0413 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -22 _diffrn_reflns_number 52526 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.099 _diffrn_reflns_theta_min 1.443 _diffrn_source 'INCOATEC Mo Microsource' _exptl_absorpt_coefficient_mu 0.492 _exptl_absorpt_correction_T_max 0.8620 _exptl_absorpt_correction_T_min 0.7966 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS-2012/1 _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.380 _exptl_crystal_description plate _exptl_crystal_F_000 1872 _exptl_crystal_size_max 0.11 _exptl_crystal_size_mid 0.076 _exptl_crystal_size_min 0.052 _refine_diff_density_max 0.395 _refine_diff_density_min -0.253 _refine_diff_density_rms 0.062 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.033 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 511 _refine_ls_number_reflns 9483 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.033 _refine_ls_R_factor_all 0.0529 _refine_ls_R_factor_gt 0.0340 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0290P)^2^+2.7040P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0716 _refine_ls_wR_factor_ref 0.0787 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7388 _reflns_number_total 9483 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c4cc00251b2.cif _cod_data_source_block p21c_a _cod_database_code 7112104 #BEGIN Tags that were not found in dictionaries: _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelxl_version_number 2013-4 _shelx_res_file ; REM Solution 1 R1 0.095, Alpha = 0.0549 in P2(1)/c REM C43 N4 Si2 Cl6 TITL p21c in P2(1)/c CELL 0.71073 14.149 17.560 17.357 90.000 94.21 90.000 ZERR 4.00 0.002 0.002 0.003 0.000 0.03 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N SI CL UNIT 172 208 16 8 24 TEMP -173.000 L.S. 10 BOND $H OMIT 6 0 0 OMIT 0 6 0 OMIT -6 6 9 LIST 4 ACTA CONF FMAP 2 PLAN 20 sadi c24 h24 c6 h6 WGHT 0.029000 2.704000 FVAR 0.32220 CL1 5 0.678608 0.584514 0.029585 11.00000 0.02188 0.02010 = 0.01348 0.00274 -0.00314 -0.00348 CL2 5 0.893051 0.591722 0.072189 11.00000 0.01879 0.02578 = 0.01576 0.00089 0.00506 -0.00361 CL3 5 0.724591 0.712724 0.145088 11.00000 0.02658 0.01201 = 0.01998 0.00197 -0.00059 0.00229 CL4 5 0.776827 0.365026 0.536840 11.00000 0.02039 0.01785 = 0.01585 0.00480 0.00129 0.00176 CL5 5 0.626827 0.488949 0.548565 11.00000 0.01765 0.02235 = 0.01733 0.00095 0.00680 0.00125 CL6 5 0.870422 0.522255 0.535065 11.00000 0.01589 0.02097 = 0.01572 -0.00044 -0.00251 -0.00153 SI1 4 0.769294 0.598948 0.131979 11.00000 0.01446 0.01205 = 0.01149 0.00122 0.00040 -0.00127 SI2 4 0.745352 0.473357 0.484014 11.00000 0.01289 0.01380 = 0.01118 0.00107 0.00139 0.00030 N1 3 0.853890 0.612655 0.225335 11.00000 0.01307 0.01153 = 0.01315 0.00067 0.00147 -0.00091 N2 3 0.724489 0.523831 0.183372 11.00000 0.01184 0.01061 = 0.00974 -0.00041 -0.00067 -0.00018 N3 3 0.714538 0.572518 0.437506 11.00000 0.01155 0.01354 = 0.01392 -0.00068 0.00157 -0.00093 N4 3 0.739425 0.441987 0.388713 11.00000 0.01424 0.00921 = 0.01088 0.00217 0.00102 0.00139 C1 1 0.918573 0.668800 0.235818 11.00000 0.02118 0.01579 = 0.01722 0.00141 0.00246 -0.00643 AFIX 43 H1 2 0.918986 0.708839 0.199036 11.00000 -1.20000 AFIX 0 C2 1 0.983877 0.669483 0.298402 11.00000 0.01696 0.01671 = 0.02144 -0.00109 0.00122 -0.00661 AFIX 43 H2 2 1.029115 0.709377 0.304879 11.00000 -1.20000 AFIX 0 C3 1 0.982675 0.610926 0.352016 11.00000 0.01366 0.01980 = 0.01629 -0.00262 0.00029 0.00053 AFIX 43 H3 2 1.027274 0.610179 0.395679 11.00000 -1.20000 AFIX 0 C4 1 0.916143 0.553883 0.341279 11.00000 0.01349 0.01405 = 0.01257 0.00013 0.00152 0.00047 AFIX 43 H4 2 0.914354 0.513464 0.377523 11.00000 -1.20000 AFIX 0 C5 1 0.851534 0.556041 0.276780 11.00000 0.01140 0.01212 = 0.01278 -0.00165 0.00400 0.00125 C6 1 0.773095 0.500143 0.257842 11.00000 0.01136 0.01088 = 0.01076 0.00026 0.00175 0.00006 C7 1 0.662084 0.464337 0.149027 11.00000 0.01389 0.01144 = 0.00911 0.00127 -0.00026 -0.00186 C8 1 0.703526 0.399411 0.117666 11.00000 0.01622 0.01261 = 0.00976 0.00050 0.00062 0.00033 C9 1 0.644845 0.339308 0.092602 11.00000 0.02197 0.01279 = 0.01659 -0.00273 0.00139 -0.00020 AFIX 43 H9 2 0.672056 0.294550 0.072880 11.00000 -1.20000 AFIX 0 C10 1 0.547642 0.343664 0.095932 11.00000 0.01880 0.01508 = 0.01695 -0.00173 -0.00076 -0.00622 AFIX 43 H10 2 0.508709 0.301377 0.080810 11.00000 -1.20000 AFIX 0 C11 1 0.507497 0.410035 0.121439 11.00000 0.01448 0.02021 = 0.01366 0.00009 0.00019 -0.00255 AFIX 43 H11 2 0.440475 0.413524 0.121215 11.00000 -1.20000 AFIX 0 C12 1 0.562683 0.471945 0.147465 11.00000 0.01432 0.01454 = 0.00902 0.00114 0.00056 -0.00032 C13 1 0.512306 0.545891 0.165632 11.00000 0.01299 0.01634 = 0.01681 -0.00272 -0.00019 0.00040 AFIX 13 H13 2 0.561411 0.586630 0.173761 11.00000 -1.20000 AFIX 0 C14 1 0.457667 0.541410 0.238491 11.00000 0.01740 0.02332 = 0.01951 -0.00099 0.00271 0.00312 AFIX 137 H14A 2 0.500968 0.526417 0.282538 11.00000 -1.50000 H14B 2 0.406870 0.503619 0.230897 11.00000 -1.50000 H14C 2 0.430208 0.591326 0.248649 11.00000 -1.50000 AFIX 0 C15 1 0.443386 0.569718 0.096506 11.00000 0.02138 0.02155 = 0.01811 -0.00154 -0.00216 0.00556 AFIX 137 H15A 2 0.420366 0.621483 0.104873 11.00000 -1.50000 H15B 2 0.389579 0.534456 0.091954 11.00000 -1.50000 H15C 2 0.476557 0.568306 0.048907 11.00000 -1.50000 AFIX 0 C16 1 0.808544 0.394378 0.103779 11.00000 0.01624 0.01285 = 0.01734 -0.00380 0.00203 -0.00002 AFIX 13 H16 2 0.841651 0.438657 0.130011 11.00000 -1.20000 AFIX 0 C17 1 0.854111 0.321345 0.136624 11.00000 0.01913 0.01910 = 0.02438 -0.00338 -0.00149 0.00402 AFIX 137 H17A 2 0.839971 0.315651 0.190755 11.00000 -1.50000 H17B 2 0.922893 0.323942 0.133379 11.00000 -1.50000 H17C 2 0.828715 0.277568 0.106818 11.00000 -1.50000 AFIX 0 C18 1 0.821885 0.399729 0.016846 11.00000 0.02114 0.02846 = 0.01870 -0.00151 0.00463 0.00133 AFIX 137 H18A 2 0.889687 0.399200 0.008686 11.00000 -1.50000 H18B 2 0.793598 0.447158 -0.003729 11.00000 -1.50000 H18C 2 0.790877 0.356239 -0.009840 11.00000 -1.50000 AFIX 0 C19 1 0.708964 0.638612 0.477291 11.00000 0.01673 0.01895 = 0.01388 -0.00474 0.00302 -0.00145 AFIX 43 H19 2 0.727791 0.639252 0.530963 11.00000 -1.20000 AFIX 0 C20 1 0.676934 0.704408 0.442159 11.00000 0.02060 0.01333 = 0.02161 -0.00449 0.00667 -0.00173 AFIX 43 H20 2 0.673801 0.750364 0.470740 11.00000 -1.20000 AFIX 0 C21 1 0.648984 0.702496 0.363439 11.00000 0.01845 0.01328 = 0.02062 0.00025 0.00464 0.00222 AFIX 43 H21 2 0.625735 0.747258 0.337806 11.00000 -1.20000 AFIX 0 C22 1 0.655267 0.635263 0.322964 11.00000 0.01523 0.01637 = 0.01371 -0.00011 0.00128 0.00065 AFIX 43 H22 2 0.636706 0.633371 0.269277 11.00000 -1.20000 AFIX 0 C23 1 0.689064 0.570350 0.361654 11.00000 0.00794 0.01409 = 0.01288 -0.00007 0.00299 -0.00156 C24 1 0.704582 0.493987 0.325756 11.00000 0.00979 0.01112 = 0.01051 0.00115 0.00079 0.00047 C25 1 0.737924 0.361918 0.365269 11.00000 0.01656 0.01045 = 0.01175 0.00175 0.00285 0.00020 C26 1 0.649702 0.325767 0.349381 11.00000 0.01539 0.01333 = 0.01466 0.00310 0.00248 -0.00130 C27 1 0.648618 0.252696 0.318261 11.00000 0.01914 0.01497 = 0.02654 -0.00117 0.00327 -0.00493 AFIX 43 H27 2 0.589546 0.229107 0.303780 11.00000 -1.20000 AFIX 0 C28 1 0.731569 0.213722 0.307970 11.00000 0.02513 0.01384 = 0.02917 -0.00554 0.00686 -0.00221 AFIX 43 H28 2 0.729543 0.164281 0.285690 11.00000 -1.20000 AFIX 0 C29 1 0.817486 0.247337 0.330391 11.00000 0.01973 0.01435 = 0.02394 0.00100 0.00762 0.00216 AFIX 43 H29 2 0.874183 0.219185 0.326039 11.00000 -1.20000 AFIX 0 C30 1 0.823314 0.321358 0.359201 11.00000 0.01603 0.01369 = 0.01439 0.00225 0.00391 -0.00081 C31 1 0.921269 0.351966 0.385631 11.00000 0.01427 0.01443 = 0.01868 -0.00175 0.00211 0.00114 AFIX 13 H31 2 0.912445 0.401184 0.413183 11.00000 -1.20000 AFIX 0 C32 1 0.982218 0.367872 0.318022 11.00000 0.01422 0.01782 = 0.02233 -0.00184 0.00439 0.00066 AFIX 137 H32A 2 1.043778 0.388200 0.337838 11.00000 -1.50000 H32B 2 0.950113 0.405129 0.283149 11.00000 -1.50000 H32C 2 0.991749 0.320459 0.289834 11.00000 -1.50000 AFIX 0 C33 1 0.974495 0.296911 0.442883 11.00000 0.02032 0.02217 = 0.02302 0.00332 0.00110 0.00455 AFIX 137 H33A 2 0.934969 0.285765 0.485553 11.00000 -1.50000 H33B 2 1.033924 0.320501 0.463294 11.00000 -1.50000 H33C 2 0.988407 0.249491 0.416177 11.00000 -1.50000 AFIX 0 C34 1 0.556795 0.358677 0.374079 11.00000 0.01437 0.01284 = 0.02172 0.00249 0.00292 -0.00218 AFIX 13 H34 2 0.566093 0.414374 0.383962 11.00000 -1.20000 AFIX 0 C35 1 0.473269 0.348814 0.313796 11.00000 0.01663 0.02340 = 0.02638 0.00390 0.00051 -0.00164 AFIX 137 H35A 2 0.417915 0.375873 0.330813 11.00000 -1.50000 H35B 2 0.458349 0.294550 0.307708 11.00000 -1.50000 H35C 2 0.490032 0.369698 0.264245 11.00000 -1.50000 AFIX 0 C36 1 0.532910 0.320570 0.449937 11.00000 0.01787 0.02465 = 0.02382 0.00636 0.00535 0.00019 AFIX 137 H36A 2 0.477446 0.345477 0.469415 11.00000 -1.50000 H36B 2 0.587037 0.325383 0.488217 11.00000 -1.50000 H36C 2 0.519015 0.266546 0.440561 11.00000 -1.50000 AFIX 0 C40T 1 0.136147 0.319470 0.106456 11.00000 0.03587 0.03234 = 0.03410 0.00854 0.01369 0.00427 AFIX 137 H37A 2 0.070890 0.316472 0.083467 11.00000 -1.50000 H37B 2 0.151150 0.273255 0.136560 11.00000 -1.50000 H37C 2 0.179779 0.324115 0.065392 11.00000 -1.50000 AFIX 0 C41T 1 0.146241 0.387421 0.158217 11.00000 0.02084 0.03225 = 0.02548 0.00700 0.01107 0.00191 C42T 1 0.094642 0.454115 0.142190 11.00000 0.02581 0.03391 = 0.02155 0.00279 0.00174 0.00380 AFIX 43 H42 2 0.051156 0.456211 0.097858 11.00000 -1.20000 AFIX 0 C43T 1 0.105782 0.516960 0.189654 11.00000 0.03423 0.03204 = 0.02813 0.00247 0.00347 0.00314 AFIX 43 H43 2 0.070238 0.561873 0.177728 11.00000 -1.20000 AFIX 0 C44T 1 0.168779 0.514761 0.254793 11.00000 0.02753 0.04277 = 0.02828 -0.00532 0.00774 -0.01055 AFIX 43 H44 2 0.176204 0.557834 0.287800 11.00000 -1.20000 AFIX 0 C45T 1 0.220138 0.449853 0.271003 11.00000 0.01828 0.06864 = 0.02292 0.00332 0.00247 -0.00098 AFIX 43 H45 2 0.263815 0.448231 0.315236 11.00000 -1.20000 AFIX 0 C46T 1 0.209139 0.387037 0.223935 11.00000 0.02174 0.05064 = 0.02750 0.01412 0.00584 0.01114 AFIX 43 H46 2 0.245116 0.342468 0.236435 11.00000 -1.20000 AFIX 0 H6 2 0.799034 0.448343 0.255060 11.00000 -1.20000 H24 2 0.642289 0.476747 0.301424 11.00000 -1.20000 HKLF 4 REM p21c in P2(1)/c REM R1 = 0.0340 for 7388 Fo > 4sig(Fo) and 0.0529 for all 9483 data REM 511 parameters refined using 1 restraints END WGHT 0.0287 2.9760 REM Highest difference peak 0.395, deepest hole -0.253, 1-sigma level 0.062 Q1 1 0.7401 0.4988 0.2921 11.00000 0.05 0.40 Q2 1 0.7073 0.6047 0.4568 11.00000 0.05 0.33 Q3 1 0.7561 0.3959 0.1066 11.00000 0.05 0.32 Q4 1 0.5211 0.3534 0.3394 11.00000 0.05 0.31 Q5 1 0.8155 0.3949 0.0616 11.00000 0.05 0.31 Q6 1 0.8139 0.5270 0.2663 11.00000 0.05 0.30 Q7 1 0.9545 0.3655 0.3566 11.00000 0.05 0.30 Q8 1 0.7604 0.5426 0.1600 11.00000 0.05 0.30 Q9 1 0.6810 0.6042 0.3401 11.00000 0.05 0.29 Q10 1 0.7076 0.5378 0.4601 11.00000 0.05 0.28 Q11 1 0.6003 0.3296 0.1174 11.00000 0.05 0.28 Q12 1 0.7084 0.5733 0.4002 11.00000 0.05 0.28 Q13 1 0.5391 0.5084 0.1521 11.00000 0.05 0.28 Q14 1 0.6160 0.4752 0.1484 11.00000 0.05 0.28 Q15 1 0.6892 0.4782 0.5137 11.00000 0.05 0.27 Q16 1 0.9323 0.6689 0.2800 11.00000 0.05 0.27 Q17 1 0.8422 0.5961 0.1195 11.00000 0.05 0.27 Q18 1 0.6782 0.7072 0.4010 11.00000 0.05 0.27 Q19 1 0.8782 0.3380 0.3662 11.00000 0.05 0.27 Q20 1 0.8248 0.6071 0.1880 11.00000 0.05 0.27 ; _shelx_res_checksum 27136 _shelx_hkl_file ; -1 0 0 44.6933 3.42527 2 1 0 0 44.4014 2.96729 1 1 0 0 43.8961 3.27737 4 -1 0 0 38.3022 2.81796 1 -2 0 0 9945.74 202.075 4 2 0 0 9822.53 189.395 1 -2 0 0 9682.51 189.194 1 2 0 0 9999.99 202.025 4 -2 0 0 9804.66 196.681 2 -3 0 0 212.265 11.0554 4 -3 0 0 216.143 10.3733 1 -3 0 0 206.662 11.0220 2 3 0 0 224.711 10.5506 1 -4 0 0 277.321 14.0894 4 -4 0 0 279.429 13.7927 2 4 0 0 286.734 13.3869 1 -4 0 0 287.575 13.3319 1 -5 0 0 2633.79 64.2821 4 -5 0 0 2615.39 61.4629 2 5 0 0 2544.72 60.6678 1 -5 0 0 2599.45 60.4379 1 -6 0 0 187.776 14.6060 4 6 0 0 197.462 13.8089 1 7 0 0 150.627 7.81271 5 -7 0 0 134.183 12.9893 1 -7 0 0 157.014 14.9288 4 -7 0 0 187.002 14.8234 2 7 0 0 140.778 13.4509 1 -8 0 0 865.560 33.9164 4 8 0 0 966.355 21.7801 5 8 0 0 943.363 20.9975 6 8 0 0 894.116 33.1151 1 -8 0 0 906.297 32.5901 2 -9 0 0 664.439 28.8879 2 -9 0 0 734.527 31.6118 4 9 0 0 694.544 18.3374 5 9 0 0 707.076 17.7165 6 9 0 0 702.075 29.8859 1 10 0 0 223.637 10.2474 6 -10 0 0 194.273 19.4254 4 10 0 0 186.140 9.38626 5 10 0 0 211.543 19.7451 1 -10 0 0 208.076 18.7779 2 -11 0 0 169.295 20.2514 4 11 0 0 176.694 10.3218 5 11 0 0 170.732 18.8424 1 11 0 0 155.923 9.97370 6 -11 0 0 162.059 18.9950 2 12 0 0 42.1791 6.02438 6 12 0 0 26.3432 6.08344 5 12 0 0 17.9107 10.3679 1 -12 0 0 49.0743 12.1944 2 -12 0 0 26.2306 11.8425 4 13 0 0 15.7547 11.2440 1 -13 0 0 29.2330 12.0905 4 13 0 0 23.2560 5.73010 6 -13 0 0 8.66349 9.05374 2 13 0 0 13.1576 5.50997 5 14 0 0 55.0385 8.14361 5 -14 0 0 63.5629 15.6876 4 14 0 0 61.0501 7.54224 6 -14 0 0 62.0331 14.3909 2 -15 0 0 52.1970 15.7861 4 15 0 0 36.1219 7.74141 5 -15 0 0 55.9407 14.6446 2 16 0 0 31.4237 7.90541 5 -16 0 0 26.6802 13.8786 4 -17 0 0 88.1584 21.6741 4 17 0 0 71.6389 10.1707 5 18 0 0 12.8565 8.42583 5 -18 0 0 4.85652 14.5242 4 1 -1 0 91.0407 5.00211 4 -1 -1 0 103.045 5.29988 3 -1 -1 0 102.695 4.68690 1 -1 -1 0 82.8097 4.55211 2 1 -1 0 90.9089 3.79611 1 1 1 0 97.0046 4.03246 4 -1 1 0 95.2699 4.02187 1 -1 1 0 91.1828 4.96297 4 1 1 0 97.2159 4.74722 1 -2 -1 0 62.9900 5.56865 3 2 -1 0 62.3042 5.09340 1 2 -1 0 59.0655 5.57087 4 -2 -1 0 55.5907 5.01930 2 -2 -1 0 50.4733 5.17160 1 2 1 0 63.4878 5.71145 1 -2 1 0 58.5948 4.96687 1 -2 1 0 61.4388 5.88716 4 2 1 0 55.6626 4.70006 4 -3 -1 0 59.9203 6.73522 1 3 -1 0 57.6776 6.55960 1 -3 -1 0 55.4961 6.21311 2 -3 -1 0 70.5586 6.85019 3 -3 1 0 62.6939 7.18282 4 3 1 0 57.1802 6.63206 1 -3 1 0 62.9779 6.63683 1 3 1 0 54.6136 6.04638 4 -4 -1 0 3120.94 69.5825 2 -4 -1 0 3047.45 69.3974 3 4 -1 0 3154.13 68.0127 1 -4 -1 0 3146.39 68.5952 1 -4 -1 0 3084.22 71.4351 4 -4 1 0 3148.38 67.7565 1 4 1 0 3109.12 68.8265 1 -4 1 0 3103.13 72.9721 4 5 -1 0 282.118 14.2354 1 -5 -1 0 283.702 14.9322 4 -5 -1 0 317.724 15.5544 2 -5 -1 0 300.235 14.9789 3 -5 -1 0 313.018 15.5549 1 5 1 0 285.253 14.8585 1 -5 1 0 269.702 14.6818 2 -5 1 0 287.130 15.9383 4 -5 1 0 309.449 15.0519 1 -6 -1 0 1164.48 35.7865 4 -6 -1 0 1158.89 34.5198 2 6 -1 0 1137.73 24.1351 5 6 -1 0 1092.70 34.0532 1 -6 -1 0 1199.98 33.6484 3 -6 -1 0 1145.59 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26.0729 7.81596 3 -3 -5 0 24.4959 3.70080 4 3 -5 0 29.5184 4.81833 1 3 5 0 29.5518 3.99152 4 3 5 0 31.0037 3.89813 6 3 5 0 32.0887 6.70077 1 -3 5 0 32.9279 7.00907 4 -4 -5 0 163.908 12.0813 1 -4 -5 0 173.920 13.8515 3 4 -5 0 166.462 7.41980 5 4 -5 0 163.584 9.65141 1 -4 -5 0 167.721 9.15067 4 4 -5 0 160.825 12.4867 3 4 5 0 168.337 12.2063 1 -4 5 0 169.928 9.79055 1 4 5 0 161.652 7.74316 6 -4 5 0 177.906 13.2744 4 4 5 0 165.767 9.46826 4 5 -5 0 7.50122 3.32403 5 -5 -5 0 9.08984 6.10108 1 -5 -5 0 6.49760 7.13292 3 -5 -5 0 9.67564 4.49688 4 5 -5 0 5.79800 4.81911 1 5 -5 0 2.32638 5.83851 3 5 5 0 7.49483 3.70236 6 5 5 0 12.5696 6.74882 1 -5 5 0 10.0082 4.99408 1 -5 5 0 1.63314 6.14313 4 -6 -5 0 177.273 15.3300 1 -6 -5 0 187.998 15.2954 2 6 -5 0 197.559 12.9698 1 6 -5 0 208.264 14.4118 3 -6 -5 0 186.518 12.2104 4 6 -5 0 183.765 8.16399 5 -6 -5 0 179.923 15.0815 3 -6 5 0 204.368 12.5153 1 6 5 0 176.615 8.69853 6 6 5 0 172.007 13.7990 1 -6 5 0 188.017 15.5728 4 7 -5 0 40.3924 8.12929 1 7 -5 0 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6 11 -5 0 103.019 15.2346 1 11 -5 0 105.250 8.87965 5 -11 -5 0 140.038 17.0091 4 11 -5 0 133.290 15.6360 3 -11 -5 0 101.248 14.6637 2 -11 -5 0 104.047 16.7868 3 11 5 0 118.224 9.08678 6 11 5 0 114.982 17.3874 1 -11 5 0 117.431 17.3090 2 -11 5 0 96.2337 18.0623 4 11 5 0 113.082 8.17264 5 -12 -5 0 161.267 19.7086 3 -12 -5 0 145.014 18.4430 2 12 -5 0 157.751 18.7457 1 12 -5 0 168.782 12.1175 5 -12 -5 0 174.985 19.6058 4 12 -5 0 130.898 16.7429 3 12 5 0 149.800 20.4137 1 -12 5 0 186.457 23.3073 4 12 5 0 188.246 10.5458 5 -12 5 0 153.015 19.7301 2 12 5 0 171.865 12.0867 6 -13 -5 0 120.670 17.4947 4 -13 -5 0 130.443 18.1476 2 13 -5 0 81.7650 10.2669 5 13 -5 0 51.9936 13.3529 1 -13 5 0 74.1460 17.4321 4 -13 5 0 107.676 17.9243 2 13 5 0 85.1263 9.18420 6 13 5 0 92.7173 8.35028 5 -14 -5 0 9.10432 10.5821 2 -14 -5 0 4.37705 10.4565 4 14 -5 0 13.2218 11.9196 1 14 -5 0 25.0800 7.45381 5 14 5 0 27.3246 7.27626 6 14 5 0 26.4168 6.68370 5 -14 5 0 19.4739 14.3915 4 -14 5 0 17.6580 11.9471 2 15 -5 0 102.503 10.9910 5 -15 -5 0 69.4696 16.7700 4 -15 5 0 82.3536 19.5492 4 15 5 0 95.7842 9.59938 5 15 5 0 115.074 11.0617 6 -15 5 0 133.430 20.4211 2 16 -5 0 -3.4865 7.16495 5 -16 5 0 -4.4995 11.7065 2 16 5 0 -5.6522 6.95110 6 -16 5 0 -11.104 13.0683 4 17 -5 0 54.3177 10.4053 5 17 5 0 41.1005 9.66474 6 -17 5 0 47.0915 19.1490 4 0 -6 0 416.896 14.2493 4 0 -6 0 447.281 20.1708 3 0 -6 0 448.406 13.1166 1 0 6 0 446.701 14.7261 4 -1 -6 0 48.5565 5.73324 1 1 -6 0 37.1637 8.27983 3 -1 -6 0 47.9515 8.95732 3 -1 -6 0 38.8374 4.15214 4 1 -6 0 39.2575 4.25762 1 1 6 0 38.6568 4.22076 4 1 6 0 47.8864 6.02290 1 -1 6 0 39.7208 5.85393 4 2 -6 0 424.082 18.9876 3 -2 -6 0 432.904 15.7050 1 2 -6 0 412.848 12.3861 1 -2 -6 0 442.188 19.7020 3 -2 -6 0 439.116 11.6981 4 -2 -6 0 400.901 11.6433 4 -2 6 0 409.058 16.9166 4 2 6 0 421.529 15.7596 1 2 6 0 438.354 12.1309 6 -3 -6 0 3.76877 6.57182 3 -3 -6 0 6.59163 2.85713 4 -3 -6 0 4.33756 4.73639 1 3 -6 0 -2.5233 3.27253 1 3 6 0 8.25748 3.42210 6 3 6 0 3.83280 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257.688 10.8631 5 -11 6 0 228.173 23.9316 4 11 6 0 242.423 13.2108 6 12 -6 0 182.430 19.8724 1 12 -6 0 179.565 11.3780 5 -12 -6 0 189.338 21.7933 3 -12 -6 0 198.767 20.3811 4 -12 -6 0 148.125 18.8069 2 12 6 0 135.824 19.6400 1 12 6 0 149.005 9.98440 5 12 6 0 156.938 11.1615 6 -12 6 0 155.544 20.4110 2 -12 6 0 150.256 21.3530 4 -13 -6 0 20.7047 11.3905 2 -13 -6 0 11.1701 10.2184 4 -13 -6 0 40.3267 14.8827 3 13 -6 0 16.5816 6.94020 5 13 -6 0 19.6671 11.1774 1 13 6 0 21.6164 5.60702 5 -13 6 0 8.43595 10.8976 2 -13 6 0 30.3954 13.9422 4 13 6 0 26.7688 7.48700 6 14 -6 0 148.600 12.3828 5 -14 -6 0 178.113 21.4945 2 -14 -6 0 141.339 20.1943 4 14 -6 0 163.200 20.9282 1 -14 6 0 178.958 26.4517 4 -14 6 0 163.076 22.2743 2 14 6 0 165.898 12.7089 6 15 -6 0 42.0273 8.88265 5 -15 6 0 48.5428 14.9529 2 -15 6 0 58.9853 18.0590 4 15 6 0 31.4495 8.36232 6 16 -6 0 -2.0559 7.17824 5 -16 6 0 -7.6586 13.9261 4 -16 6 0 12.0787 12.4766 2 16 6 0 4.34862 7.31812 6 17 -6 0 1.10592 7.86293 5 -17 6 0 8.27462 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331.067 24.2955 4 9 7 0 343.164 10.9733 5 9 7 0 366.861 23.0651 1 9 7 0 332.188 14.1616 6 -10 -7 0 58.3329 10.4057 4 10 -7 0 54.4727 11.1083 1 -10 -7 0 74.3520 14.9692 3 -10 -7 0 47.6175 11.9959 2 10 -7 0 57.0633 11.7293 3 10 -7 0 56.9088 6.95771 5 10 7 0 51.3139 7.25709 6 10 7 0 47.6004 12.8632 1 -10 7 0 53.7137 13.0091 4 10 7 0 56.8815 5.50523 5 -11 -7 0 215.775 19.7192 4 11 -7 0 237.206 21.5201 3 -11 -7 0 239.159 23.6059 3 -11 -7 0 227.205 21.9922 2 11 -7 0 229.300 12.8043 5 11 -7 0 227.239 20.5582 1 11 7 0 213.177 9.99730 5 -11 7 0 205.308 23.3428 4 11 7 0 205.745 12.1730 6 11 7 0 201.804 21.8828 1 -12 -7 0 10.0648 12.6816 3 12 -7 0 18.6411 6.50067 5 12 -7 0 7.18207 8.81822 1 -12 -7 0 5.49019 8.42186 4 -12 -7 0 11.5659 9.69586 2 12 7 0 2.74822 5.77317 6 -12 7 0 -8.1098 8.27645 4 12 7 0 4.02322 10.4851 1 -13 -7 0 108.532 19.7144 3 13 -7 0 95.2103 9.87252 5 -13 -7 0 95.4708 16.9447 2 13 -7 0 77.0182 15.3399 1 13 7 0 108.910 10.5556 6 -13 7 0 139.078 21.6474 4 -13 7 0 51.1451 14.9885 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12 -2 -2 8.81055 9.32367 1 12 -2 -2 12.3045 10.1076 3 -12 -2 2 14.3916 9.97211 4 -12 2 2 13.3898 9.66113 2 12 2 -2 0.51435 8.49145 1 12 2 -2 6.66668 4.69468 5 -12 2 2 -4.7737 8.78801 4 12 2 -2 8.64959 5.41864 6 11 -2 -2 44.6302 12.1598 3 -11 -2 2 72.6982 14.3247 2 11 -2 -2 49.6696 11.9574 1 -11 -2 2 56.2257 12.4881 4 11 -2 -2 43.2038 6.35011 5 11 2 -2 42.7529 5.91094 5 -11 2 2 37.6448 11.6269 4 -11 2 2 58.1652 12.7964 2 11 2 -2 61.8314 12.9241 1 11 2 -2 49.7816 6.64692 6 -10 -2 2 341.755 24.6256 2 -10 -2 2 341.888 22.3614 4 10 -2 -2 342.875 13.0710 5 10 -2 -2 339.439 22.1212 1 10 -2 -2 338.003 22.1422 3 -10 2 2 351.235 24.0286 4 10 2 -2 309.937 21.6604 1 -10 2 2 364.541 23.8279 2 10 2 -2 356.467 12.3102 5 10 2 -2 336.882 13.1781 6 -9 -2 2 462.694 25.3321 2 9 -2 -2 349.361 21.5045 3 9 -2 -2 362.748 21.5795 1 -9 -2 2 386.405 21.2673 4 9 -2 -2 409.629 13.1746 5 -9 2 2 421.421 24.7780 4 9 2 -2 399.480 13.1375 6 9 2 -2 415.196 12.6959 5 -9 2 2 459.434 25.1183 2 9 2 -2 368.991 22.3901 1 8 -2 -2 1846.98 37.6845 5 -8 -2 2 1897.38 54.9146 2 8 -2 -2 1911.62 54.1373 3 8 -2 -2 1871.88 52.6041 1 -8 2 2 1750.82 55.8965 4 -8 2 2 1885.58 55.3416 2 8 2 -2 1833.23 53.3668 1 8 2 -2 1796.27 36.3902 5 7 -2 -2 34.2497 4.41395 5 -7 -2 2 38.4207 8.96089 2 7 -2 -2 49.8832 8.96350 1 -7 2 2 39.6457 7.96386 1 -7 2 2 47.1749 9.73671 4 7 2 -2 39.3581 9.19798 1 7 2 -2 41.9909 4.26248 5 -7 2 2 36.8160 8.80461 2 -6 -2 2 953.403 30.8919 4 6 -2 -2 951.813 21.0846 5 6 -2 -2 945.907 30.8092 1 -6 -2 2 945.010 33.0327 2 -6 -2 2 995.684 31.8120 1 -6 -2 2 948.967 31.8144 3 -6 2 2 1005.31 30.7491 1 -6 2 2 950.247 33.7053 4 -6 2 2 962.395 33.3478 2 6 2 -2 975.463 31.8609 1 5 -2 -2 830.677 18.6933 5 -5 -2 2 875.071 27.3983 4 5 -2 -2 908.877 27.5691 1 -5 -2 2 873.328 29.2667 2 -5 -2 2 852.079 27.6786 1 -5 -2 2 881.936 28.8782 3 -5 2 2 854.739 29.8282 4 -5 2 2 860.992 26.8520 1 5 2 -2 858.522 27.7471 1 -4 -2 2 161.628 12.6781 3 -4 -2 2 136.117 10.1984 1 4 -2 -2 147.785 12.3981 3 4 -2 -2 147.300 10.0796 1 -4 -2 2 133.702 9.82718 4 -4 -2 2 114.848 10.6982 2 4 2 -2 143.173 10.4295 1 -4 2 2 151.185 12.6534 4 -4 2 2 134.422 10.6825 1 -3 -2 2 23.0355 5.56267 1 3 -2 -2 24.0122 6.69470 3 -3 -2 2 15.3116 4.48431 4 3 -2 -2 20.7992 5.52143 1 -3 -2 2 21.7581 6.13522 3 -3 -2 2 10.3169 5.18515 2 -3 2 2 27.1875 5.67206 1 -3 2 2 25.4257 6.18769 4 3 2 -2 24.8217 4.85316 4 3 2 -2 25.4131 5.89291 1 -2 -2 2 33.2532 4.63861 1 2 -2 -2 31.1576 6.27159 3 -2 -2 2 35.8628 6.25902 3 -2 -2 2 30.4905 4.16789 4 -2 -2 2 30.4209 5.39446 2 2 -2 -2 41.4495 5.78759 1 -2 2 2 37.8781 6.10400 4 2 2 -2 30.5803 4.11617 4 2 2 -2 37.2345 5.24184 1 1 -2 -2 412.668 14.4461 4 -1 -2 2 403.130 11.7067 1 1 -2 -2 394.815 15.0688 3 -1 -2 2 401.700 14.1830 3 -1 -2 2 411.526 11.6816 4 -1 2 2 426.851 14.5986 4 1 2 -2 392.912 11.6666 4 0 -2 -2 453.038 14.1166 1 0 -2 -2 452.490 15.3727 3 0 -2 2 451.381 13.1320 4 0 -2 -2 453.733 14.7852 4 0 2 2 457.490 14.9013 4 0 2 2 440.733 13.8714 1 0 2 -2 472.757 13.1682 4 1 -2 2 536.553 15.9830 4 -1 -2 -2 513.307 16.3028 3 1 -2 2 533.968 13.9033 3 1 -2 2 515.855 13.2195 1 -1 -2 -2 520.431 16.2725 1 1 2 2 523.321 16.0131 1 -1 2 -2 518.745 13.1661 1 -1 2 -2 515.033 15.9966 4 2 -2 2 1078.47 25.1687 1 -2 -2 -2 1073.82 27.6085 3 -2 -2 -2 1078.52 27.9386 1 -2 2 -2 1061.06 28.8726 4 -2 2 -2 1077.40 25.0882 1 2 2 2 1047.76 28.0642 1 3 -2 2 2035.80 44.9377 1 3 -2 2 2019.78 43.1816 3 -3 -2 -2 2011.57 46.7193 3 -3 -2 -2 1984.44 47.3532 1 3 2 2 1975.37 47.4657 1 -3 2 -2 2005.12 44.6847 1 -4 -2 -2 1665.39 42.6297 4 -4 -2 -2 1600.25 41.5684 1 -4 -2 -2 1617.54 39.5822 3 4 -2 2 1551.47 36.4981 3 4 -2 2 1629.40 39.6623 1 -4 -2 -2 1601.61 37.9313 2 -4 2 -2 1575.16 43.7671 4 -4 2 -2 1673.67 39.5840 1 4 2 2 1593.67 41.9630 1 -5 -2 -2 1841.73 44.7183 2 5 -2 2 1946.59 47.0708 1 5 -2 2 1846.28 43.2976 3 -5 -2 -2 1868.31 45.9449 3 -5 -2 -2 1929.03 48.7556 1 -5 -2 -2 1848.55 49.6391 4 5 2 2 1863.06 49.0925 1 -5 2 -2 1927.63 46.5577 1 -5 2 -2 1847.48 51.2174 4 6 -2 2 254.418 9.74940 5 -6 -2 -2 258.912 16.1509 4 -6 -2 -2 248.453 13.7996 2 -6 -2 -2 261.993 15.7436 1 -6 -2 -2 260.424 13.9044 3 6 -2 2 255.643 12.1464 3 6 -2 2 275.223 15.3719 1 6 2 2 247.366 8.88843 5 -6 2 -2 230.112 16.9883 4 -6 2 -2 258.466 14.9417 1 6 2 2 250.018 8.93985 6 6 2 2 227.172 15.1871 1 -7 -2 -2 332.136 18.8827 4 7 -2 2 321.211 11.4178 5 -7 -2 -2 317.492 16.1687 2 -7 -2 -2 323.894 16.2336 3 7 -2 2 333.659 15.0180 3 7 -2 2 329.466 18.0500 1 7 2 2 343.583 10.7702 5 -7 2 -2 328.124 17.7239 1 7 2 2 333.165 10.6371 6 -7 2 -2 326.525 20.0875 4 7 2 2 304.579 18.3167 1 -8 -2 -2 127.226 12.0077 2 -8 -2 -2 140.721 14.9569 4 8 -2 2 133.246 14.1928 1 8 -2 2 125.955 7.57620 5 -8 -2 -2 147.102 13.0631 3 8 -2 2 133.397 11.0899 3 8 2 2 114.016 7.47871 5 8 2 2 118.482 13.9017 1 8 2 2 112.104 7.98761 6 -8 2 -2 129.952 12.7706 2 -8 2 -2 109.627 14.3525 4 9 -2 2 64.4487 11.4234 1 9 -2 2 65.3221 9.32358 3 9 -2 2 54.7091 6.08093 5 9 -2 2 56.3482 4.70589 6 -9 -2 -2 42.7785 8.72423 2 -9 -2 -2 59.2520 9.93709 3 -9 -2 -2 89.0993 13.4438 4 -9 2 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4 1655.39 41.6797 2 2 1 -4 1617.03 39.4366 1 -2 1 4 1651.85 43.0819 4 -1 -1 4 880.486 25.0756 4 1 -1 -4 801.953 25.4257 3 -1 -1 4 830.766 24.3661 2 -1 1 4 853.152 25.9828 4 -1 1 4 823.892 23.9947 2 0 -1 -4 1157.87 30.1324 1 0 -1 4 1170.75 28.5720 2 0 -1 -4 1155.61 30.5319 3 0 1 -4 1158.15 29.0812 1 0 1 4 1089.53 28.0283 2 0 1 4 1186.41 30.6458 1 1 -1 4 296.980 12.9667 1 -1 -1 -4 299.229 13.5682 1 -1 -1 -4 325.357 15.2022 4 -1 -1 -4 315.915 12.8096 3 1 1 4 335.208 14.2439 1 -1 1 -4 319.432 14.5417 4 1 1 4 322.549 10.1061 2 -1 1 -4 321.796 12.8097 1 -2 -1 -4 2015.16 46.0119 3 -2 -1 -4 2043.99 48.5844 1 2 -1 4 2021.79 47.1862 1 -2 -1 -4 2054.03 51.4909 4 -2 1 -4 2054.78 46.9893 1 2 1 4 2103.50 49.1364 1 -2 1 -4 2019.33 51.1905 4 3 -1 4 452.923 17.1212 1 -3 -1 -4 408.600 17.3283 1 -3 -1 -4 379.988 13.3666 3 -3 -1 -4 412.920 18.2248 4 3 1 4 381.986 17.3127 1 -3 1 -4 409.797 16.3758 1 -3 1 -4 411.861 18.4108 4 4 -1 4 311.432 9.60598 5 -4 -1 -4 308.716 16.7070 4 -4 -1 -4 327.202 9.27722 2 4 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794.059 22.7931 1 3 2 4 728.734 24.9696 1 -3 2 -4 722.406 25.7556 4 -4 -2 -4 53.9310 8.62737 4 4 -2 4 38.8689 4.28960 5 4 -2 4 41.5398 7.18148 1 -4 -2 -4 58.4230 9.02561 1 -4 -2 -4 44.0442 6.52169 3 -4 2 -4 48.3581 8.55319 4 4 2 4 40.6628 4.05197 5 -4 2 -4 34.4472 6.96788 1 4 2 4 29.6586 7.21902 1 5 -2 4 254.271 9.32661 5 -5 -2 -4 251.652 12.7116 3 5 -2 4 272.229 15.1906 1 -5 -2 -4 263.882 16.3246 1 -5 -2 -4 274.906 16.5320 4 5 2 4 258.071 16.0620 1 5 2 4 246.514 9.19424 5 -5 2 -4 301.066 15.4496 1 -5 2 -4 282.058 17.4499 4 6 -2 4 13.3014 3.09020 3 6 -2 4 7.44171 6.29286 1 -6 -2 -4 14.1989 6.99534 4 -6 -2 -4 22.2185 6.00654 3 -6 -2 -4 15.9613 4.26170 2 6 -2 4 11.1543 3.74642 5 -6 2 -4 16.3092 6.89958 1 6 2 4 26.3017 8.38564 1 6 2 4 10.4262 3.75314 5 6 2 4 13.4043 3.56825 6 -6 2 -4 10.5580 6.92948 4 7 -2 4 16.8088 7.02901 1 -7 -2 -4 7.38945 6.21041 4 -7 -2 -4 12.5968 4.61359 2 7 -2 4 1.13400 3.39095 5 -7 -2 -4 6.55508 5.57031 3 7 -2 4 7.55641 3.71330 3 7 2 4 11.4897 3.54255 6 -7 2 -4 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190.704 19.0430 2 8 4 -4 181.584 7.88363 5 8 4 -4 170.527 17.0766 1 7 -4 -4 165.198 17.3834 3 -7 -4 4 131.142 12.4325 4 7 -4 -4 121.415 13.2459 1 7 -4 -4 124.355 8.23257 5 -7 -4 4 111.793 13.6928 2 -7 -4 4 139.108 15.7635 3 -7 4 4 129.640 15.0715 4 7 4 -4 139.990 6.50095 5 7 4 -4 129.685 14.0165 1 -6 -4 4 26.4818 7.54756 1 6 -4 -4 29.4558 9.03677 3 -6 -4 4 19.9571 7.46772 2 -6 -4 4 36.1168 7.17660 4 -6 -4 4 30.7960 9.64884 3 6 -4 -4 34.6510 4.47128 5 6 -4 -4 33.5719 8.00136 1 6 4 -4 27.4386 8.11921 1 -6 4 4 33.2223 8.98414 4 5 -4 -4 1143.73 34.4184 1 -5 -4 4 1115.34 32.1314 4 5 -4 -4 1155.96 38.1917 3 -5 -4 4 1084.98 37.3756 2 -5 -4 4 1062.95 36.4139 3 5 -4 -4 1085.86 24.0199 5 -5 -4 4 1116.70 33.8837 1 -5 4 4 1170.93 38.7619 4 5 4 -4 1141.56 34.4165 1 4 -4 -4 107.473 6.30554 5 -4 -4 4 93.8338 11.6401 3 -4 -4 4 90.4968 10.8152 2 4 -4 -4 98.8330 12.3595 3 -4 -4 4 118.587 8.76891 4 4 -4 -4 104.017 10.5687 1 -4 4 4 109.398 12.2517 4 4 4 -4 98.6377 9.95106 1 3 -4 -4 1970.62 37.2750 5 -3 -4 4 1938.72 50.7703 3 3 -4 -4 1935.80 52.8997 3 -3 -4 4 1955.09 51.5775 2 -3 -4 4 1914.44 45.8096 4 3 4 -4 1893.29 46.2022 1 -3 4 4 1984.09 53.0773 4 -2 -4 4 151.907 12.5100 2 -2 -4 4 172.822 10.0830 1 2 -4 -4 169.973 13.5676 3 -2 -4 4 175.820 13.0317 3 2 4 -4 160.183 9.66949 1 2 4 -4 162.520 9.21926 4 -2 4 4 190.248 13.3787 4 1 -4 -4 260.756 13.9809 1 1 -4 -4 211.688 14.5853 3 -1 -4 4 266.861 13.9498 3 -1 4 4 228.012 14.5095 4 1 4 -4 247.119 11.2656 4 1 4 -4 254.584 10.4670 1 1 4 -4 267.937 11.7048 4 0 -4 -4 1086.58 30.7159 1 0 -4 -4 1079.38 32.9851 3 0 4 -4 1067.43 28.8753 4 0 4 -4 1064.78 25.9119 1 0 4 4 1120.45 31.2909 1 0 4 4 1067.68 32.1288 4 -1 -4 -4 127.871 11.8472 3 1 -4 4 113.264 8.85163 3 -1 -4 -4 97.6080 9.75827 1 -1 4 -4 101.984 9.01590 4 -1 4 -4 97.3167 6.89259 1 1 4 4 97.5246 10.1587 1 2 -4 4 12.1096 4.55008 3 -2 -4 -4 14.5290 6.87701 3 -2 -4 -4 16.4133 6.06911 1 -2 -4 -4 0.05986 2.44914 4 2 -4 4 15.3654 4.23523 1 2 4 4 11.9890 6.39623 1 -2 4 -4 10.8699 4.05560 1 -2 4 -4 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4.32777 5 -9 4 -5 4.51338 7.60058 4 9 4 5 13.4942 9.00264 1 9 4 5 20.7718 5.00055 6 10 -4 5 79.6027 8.12377 5 -10 -4 -5 78.9530 12.0840 3 10 -4 5 86.3484 13.9447 1 -10 -4 -5 99.8423 15.2933 4 -10 4 -5 64.9574 13.6662 4 10 4 5 51.6083 13.2055 1 10 4 5 80.2723 7.67230 5 10 4 5 83.3336 7.55990 6 11 -4 5 253.879 13.5372 5 11 -4 5 271.086 21.2975 1 -11 -4 -5 240.420 24.1634 4 11 4 5 231.397 11.9516 6 11 4 5 247.764 12.1669 5 -11 4 -5 216.856 24.8352 4 11 4 5 208.548 22.5791 1 -12 -4 -5 28.0436 12.1022 4 12 -4 5 21.5596 11.1491 1 12 -4 5 28.3827 6.80885 5 -12 4 -5 35.4916 14.7603 4 12 4 5 24.0565 6.37199 6 12 4 5 19.1191 11.9834 1 12 4 5 22.8420 6.31879 5 13 -4 5 198.310 14.0652 5 13 -4 5 210.653 23.0003 1 -13 -4 -5 207.953 24.3860 4 13 4 5 209.749 12.5438 6 -13 4 -5 231.537 27.1560 4 13 4 5 235.511 13.2487 5 -14 -4 -5 24.9787 13.3749 4 14 -4 5 8.72104 6.53627 5 -14 4 -5 -5.8284 10.9271 4 14 4 5 -0.1835 6.94811 5 -15 -4 -5 10.1113 12.5700 4 15 -4 5 5.38520 7.05689 5 -15 4 -5 5.03081 14.3365 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16.0525 6 -12 -5 5 215.243 24.2150 2 -12 -5 5 198.442 20.8960 4 12 -5 -5 205.284 24.9619 3 12 -5 -5 216.678 12.8538 5 12 -5 -5 183.104 20.8002 1 -12 5 5 204.195 25.1705 4 12 5 -5 219.707 23.9720 1 12 5 -5 211.391 13.9191 6 12 5 -5 193.499 10.5509 5 -12 5 5 237.404 26.7211 2 -11 -5 5 114.383 17.5968 2 11 -5 -5 107.591 16.2581 1 11 -5 -5 105.220 18.3120 3 -11 -5 5 103.199 14.8371 4 11 -5 -5 90.5842 8.49300 5 11 5 -5 93.5762 9.26662 6 11 5 -5 97.1899 7.19257 5 11 5 -5 106.617 17.2282 1 -11 5 5 94.6177 16.9986 2 -11 5 5 88.8885 17.1834 4 -10 -5 5 41.4924 12.7568 2 -10 -5 5 43.7390 10.1401 4 10 -5 -5 53.6013 11.6356 1 10 -5 -5 63.2551 7.22696 5 10 -5 -5 71.2391 14.8311 3 -10 5 5 56.2324 13.5927 2 10 5 -5 51.3782 13.0839 1 10 5 -5 69.8977 7.93079 6 -10 5 5 58.8365 14.6417 4 10 5 -5 56.9625 5.53740 5 9 -5 -5 82.5678 7.55820 5 -9 -5 5 79.8700 14.0313 2 -9 -5 5 96.2661 15.9967 3 9 -5 -5 96.8464 13.7557 1 9 -5 -5 121.937 17.1000 3 -9 -5 5 118.369 13.5452 4 9 5 -5 110.632 8.95685 6 -9 5 5 95.0376 16.0303 4 9 5 -5 70.6015 12.7705 1 9 5 -5 95.5923 6.70429 5 -9 5 5 65.4023 13.6701 2 8 -5 -5 497.821 16.1222 5 8 -5 -5 532.502 28.1771 3 -8 -5 5 528.691 28.9943 2 8 -5 -5 506.606 25.0237 1 -8 -5 5 512.074 28.0807 3 -8 -5 5 557.086 23.7246 4 -8 5 5 539.762 29.1947 4 8 5 -5 548.209 26.6790 1 8 5 -5 533.582 13.6937 5 7 -5 -5 360.320 22.6899 3 7 -5 -5 353.959 19.8535 1 -7 -5 5 368.224 22.8595 2 7 -5 -5 355.715 12.2846 5 -7 -5 5 368.310 18.0534 4 -7 -5 5 343.409 22.7004 3 7 5 -5 351.931 20.1518 1 7 5 -5 348.956 9.88428 5 -7 5 5 353.132 22.6078 4 -6 -5 5 1977.74 57.5560 3 6 -5 -5 1947.78 52.9543 1 -6 -5 5 1764.81 49.6386 4 -6 -5 5 2049.45 58.4767 2 6 -5 -5 1920.01 39.2890 5 6 -5 -5 1903.20 58.2915 3 6 5 -5 1958.69 53.0520 1 -6 5 5 1949.89 59.0851 4 -5 -5 5 3065.20 78.4316 2 -5 -5 5 3027.70 71.0915 4 5 -5 -5 3024.61 72.9154 1 -5 -5 5 2996.33 77.7128 3 5 -5 -5 3039.34 57.4954 5 5 -5 -5 3034.11 79.7929 3 -5 5 5 3102.97 80.9934 4 5 5 -5 2959.38 71.9448 1 4 -5 -5 514.966 25.3153 3 -4 -5 5 529.411 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32.2338 2 2 -5 -10 784.487 35.1650 3 -2 -5 10 784.823 19.2869 5 2 5 -10 877.605 30.8949 1 2 5 -10 798.760 31.2960 4 -2 5 10 778.375 20.7090 5 -2 5 10 818.051 36.1701 4 1 -5 -10 369.892 23.8018 3 -1 -5 10 378.342 12.0900 5 -1 5 10 377.735 13.6181 5 -1 5 10 389.019 24.1013 4 1 5 -10 420.554 21.6938 4 1 5 -10 405.738 20.6794 1 0 -5 -10 12.5469 8.99580 3 0 -5 10 13.9536 4.18512 5 0 5 -10 24.9169 7.86945 4 0 5 10 25.6684 4.95643 5 0 5 -10 17.9937 7.17811 1 1 -5 10 692.590 18.2935 5 -1 -5 -10 750.719 31.5908 3 1 5 10 684.669 31.4923 1 -1 5 -10 668.656 29.5796 4 -1 5 -10 763.865 27.6254 1 1 5 10 740.524 19.6595 5 2 -5 10 79.5962 6.62568 5 -2 -5 -10 65.7288 12.6877 4 -2 -5 -10 96.0691 13.7179 3 2 5 10 57.7273 11.9981 1 2 5 10 56.7989 6.22600 5 -2 5 -10 85.3168 10.8265 1 -2 5 -10 50.5920 10.8306 4 -3 -5 -10 202.381 19.9155 4 -3 -5 -10 215.232 17.2295 3 3 -5 10 184.807 14.7213 1 3 -5 10 183.400 9.88458 5 -3 5 -10 211.805 14.8989 1 3 5 10 209.737 20.3798 1 -3 5 -10 216.315 17.5159 4 3 5 10 188.222 10.2236 5 -4 -5 -10 532.417 29.2226 4 -4 -5 -10 548.516 25.3506 3 4 -5 10 540.598 24.0991 1 4 -5 10 529.870 16.4936 5 -4 5 -10 582.969 24.3773 1 4 5 10 502.602 28.0963 1 4 5 10 514.918 16.4903 5 -4 5 -10 569.856 28.4376 4 -5 -5 -10 191.980 20.1960 4 5 -5 10 157.601 15.7921 1 5 -5 10 179.368 10.5145 5 -5 -5 -10 188.920 15.7838 3 -5 5 -10 163.803 18.3549 4 5 5 10 160.993 10.3139 5 5 5 10 163.150 19.2475 1 -6 -5 -10 332.133 19.8939 3 -6 -5 -10 327.615 24.5377 4 6 -5 10 327.215 20.2182 1 6 -5 10 314.985 13.7091 5 6 5 10 326.372 24.2556 1 6 5 10 306.653 13.3399 5 -6 5 -10 307.590 23.0927 4 7 -5 10 40.2481 10.4892 1 7 -5 10 50.4870 7.50083 5 -7 -5 -10 63.6251 13.8466 4 -7 5 -10 80.8019 14.5629 4 7 5 10 42.8878 6.97711 5 7 5 10 53.9984 13.1720 1 7 5 10 48.8025 6.65690 6 8 -5 10 37.0698 6.96481 5 -8 -5 -10 27.6710 11.6341 4 8 -5 10 38.8123 10.6767 1 8 5 10 50.6278 7.42144 5 8 5 10 36.1253 12.5139 1 8 5 10 49.9563 6.97504 6 -8 5 -10 34.6412 12.0562 4 9 -5 10 163.626 12.1145 5 -9 -5 -10 169.151 21.0276 4 9 -5 10 193.859 20.1557 1 9 5 10 170.038 11.4516 6 9 5 10 148.311 20.8284 1 -9 5 -10 198.726 24.0353 4 9 5 10 196.739 11.8727 5 10 -5 10 22.2198 7.40442 5 10 -5 10 6.28434 9.50335 1 -10 -5 -10 16.2694 11.3985 4 -10 5 -10 15.9862 11.0761 4 10 5 10 30.5119 6.87221 6 10 5 10 22.2350 7.06687 5 11 -5 10 105.200 11.0789 5 -11 -5 -10 98.4158 18.6601 4 11 -5 10 106.128 17.4315 1 11 5 10 88.1645 10.3256 5 -11 5 -10 120.613 20.7308 4 -12 -5 -10 100.612 19.1908 4 12 -5 10 99.2799 10.8257 5 12 5 10 84.6391 10.1692 5 -12 5 -10 73.2812 17.1718 4 -13 -5 -10 58.2016 17.3526 4 13 -5 10 70.4118 10.5757 5 13 5 10 80.6721 10.5055 5 -13 5 -10 45.7969 15.8989 4 -14 -5 -10 34.1614 17.3635 4 14 -5 10 42.4268 9.91155 5 -14 5 -10 30.6866 14.8652 4 14 5 10 48.3288 9.66429 5 -15 -5 -10 102.519 22.2304 4 15 -5 10 74.2439 11.6254 5 15 5 10 93.7200 11.8684 5 16 -6 -10 18.3116 8.73278 5 -16 -6 10 24.9358 18.0183 2 16 -6 -10 4.28671 14.8265 3 16 6 -10 12.7810 9.26173 6 15 -6 -10 23.0000 17.0614 3 15 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46.4089 7.36597 5 9 -6 -10 36.4541 11.3650 1 -9 -6 10 37.5204 12.9551 2 9 -6 -10 44.8515 16.0809 3 -9 6 10 34.0530 13.2425 2 -9 6 10 80.3607 16.3938 4 9 6 -10 41.8477 12.4922 1 -8 -6 10 0.56330 7.92421 2 -8 -6 10 0.87536 6.61292 4 8 -6 -10 -0.6512 4.89425 5 8 -6 -10 13.1195 8.59551 1 8 -6 -10 14.2317 12.0211 3 8 6 -10 1.38318 3.60983 5 -8 6 10 18.0327 10.2966 2 -8 6 10 -2.2393 8.13504 4 8 6 -10 -8.9692 8.08566 1 7 -6 -10 655.290 31.9390 1 -7 -6 10 648.738 29.1211 4 7 -6 -10 684.598 20.5044 5 7 -6 -10 621.655 35.9220 3 -7 -6 10 673.014 35.8892 2 7 6 -10 661.050 30.8774 1 -7 6 10 602.190 34.6565 4 7 6 -10 699.220 17.3653 5 -7 6 10 681.787 35.8387 2 -6 -6 10 5.59169 5.91589 4 -6 -6 10 10.2849 8.55874 2 6 -6 -10 14.7721 5.00681 5 6 -6 -10 7.87121 6.99659 1 6 -6 -10 21.0085 10.2802 3 6 6 -10 6.09369 7.54454 1 -6 6 10 32.6406 10.3451 4 6 6 -10 13.2037 3.59827 5 -6 6 10 6.98302 8.95456 2 -5 -6 10 19.3764 9.57106 2 -5 -6 10 30.2789 4.50088 5 5 -6 -10 27.9573 5.60827 5 5 -6 -10 23.5804 11.9863 3 -5 6 10 28.8766 9.52962 4 5 6 -10 35.1330 9.37981 1 4 -6 -10 183.322 21.8806 3 -4 -6 10 191.016 8.87221 5 -4 -6 10 162.391 17.7993 2 4 6 -10 192.611 14.7393 1 -4 6 10 184.228 19.7976 4 -3 -6 10 287.734 21.9126 2 3 -6 -10 288.825 23.1275 3 -3 -6 10 309.505 10.6164 5 -3 6 10 298.323 12.7155 5 3 6 -10 298.799 17.4401 1 -3 6 10 362.096 23.8287 4 2 -6 -10 453.269 27.3364 3 -2 -6 10 416.328 12.5041 5 2 6 -10 439.681 21.5361 1 -2 6 10 425.639 25.8822 4 2 6 -10 444.803 22.0076 4 2 6 -10 427.352 20.1842 1 -2 6 10 398.920 14.5292 5 1 -6 -10 695.625 32.8869 3 -1 -6 10 660.604 17.0524 5 1 6 -10 724.838 29.0126 4 1 6 -10 698.094 26.7767 1 -1 6 10 637.137 31.9918 4 -1 6 10 687.914 19.1611 5 0 -6 -10 74.0843 13.7055 3 0 -6 10 58.9572 5.82276 5 0 6 10 58.8183 6.54094 5 0 6 -10 60.1417 9.73633 1 0 6 -10 46.3396 9.21145 4 1 -6 10 108.300 7.35051 5 -1 -6 -10 102.911 14.9329 3 -1 6 -10 86.7562 12.0150 4 -1 6 -10 103.364 11.2969 1 1 6 10 116.002 15.7186 1 1 6 10 112.754 8.42291 5 -2 -6 -10 581.073 29.7803 4 2 -6 10 576.041 16.1151 5 -2 -6 -10 538.089 27.6869 3 2 6 10 545.742 28.7502 1 2 6 10 530.607 16.4023 5 -2 6 -10 551.954 22.6776 1 -2 6 -10 571.106 27.7796 4 -3 -6 -10 975.614 40.6761 4 -3 -6 -10 1072.66 38.8821 3 3 -6 10 1033.90 33.8214 1 3 -6 10 1026.48 24.3968 5 -3 6 -10 1080.73 33.5372 1 3 6 10 992.255 24.8115 5 -3 6 -10 983.845 38.8392 4 3 6 10 905.045 38.7747 1 4 -6 10 257.329 16.5646 1 -4 -6 -10 227.646 21.8129 4 4 -6 10 222.381 11.1234 5 -4 -6 -10 227.886 18.5281 3 4 6 10 241.120 11.4426 5 -4 6 -10 235.470 15.2083 1 -4 6 -10 200.534 20.6675 4 4 6 10 229.041 21.6846 1 5 -6 10 520.033 24.0224 1 -5 -6 -10 487.794 25.8743 3 5 -6 10 508.962 16.5744 5 -5 -6 -10 490.123 28.7286 4 5 6 10 494.275 29.3480 1 5 6 10 476.703 16.1942 5 -5 6 -10 545.824 29.2346 4 -6 -6 -10 109.829 14.5075 3 6 -6 10 116.170 9.12793 5 -6 -6 -10 135.464 18.0589 4 6 -6 10 101.781 13.0734 1 -6 6 -10 109.953 16.4302 4 6 6 10 82.6925 15.1740 1 6 6 10 109.459 8.96767 5 6 6 10 130.478 9.55119 6 7 -6 10 57.0574 7.65523 5 7 -6 10 57.7131 11.3573 1 -7 -6 -10 49.1776 12.8134 4 -7 -6 -10 73.5258 12.6649 3 7 6 10 38.0800 13.7064 1 -7 6 -10 50.8450 12.7732 4 7 6 10 57.3835 7.29009 6 7 6 10 65.1861 7.78153 5 8 -6 10 11.0153 5.84572 5 -8 -6 -10 3.80252 9.56683 4 8 -6 10 -7.1409 7.45743 1 8 6 10 14.9534 10.6382 1 8 6 10 12.9683 5.61176 5 8 6 10 4.64860 5.30512 6 -8 6 -10 -4.6323 8.69380 4 9 -6 10 37.6201 10.4643 1 -9 -6 -10 38.5317 13.0711 4 9 -6 10 21.5444 7.12952 5 9 6 10 17.1246 6.41006 6 9 6 10 28.7017 6.90578 5 -9 6 -10 27.2555 12.0404 4 10 -6 10 98.0000 10.2118 5 -10 -6 -10 115.576 20.1776 4 -10 6 -10 125.539 20.3221 4 10 6 10 118.387 10.2529 6 10 6 10 118.211 10.6136 5 11 -6 10 84.9900 10.3534 5 -11 -6 -10 83.1571 17.7959 4 11 6 10 94.2537 9.95572 6 11 6 10 85.0288 9.94927 5 -11 6 -10 105.457 19.6582 4 12 -6 10 178.804 13.8889 5 -12 -6 -10 156.920 22.9030 4 12 6 10 162.484 12.7519 5 -12 6 -10 148.817 22.9235 4 -13 -6 -10 64.7377 17.3881 4 13 -6 10 44.8992 9.30398 5 -13 6 -10 70.4038 18.4581 4 13 6 10 26.2199 8.68198 5 -14 -6 -10 41.9499 17.0293 4 14 -6 10 34.3911 9.41988 5 14 6 10 33.5903 9.58887 5 -14 6 -10 39.2605 16.5889 4 15 -7 -10 26.2568 8.85383 5 -15 -7 10 24.5416 16.2107 2 15 -7 -10 26.2452 16.9995 3 -15 7 10 23.4743 16.0757 2 -15 7 10 4.90545 15.2603 4 15 7 -10 22.1866 8.93821 6 14 -7 -10 -7.3180 6.41198 5 -14 -7 10 -26.392 9.64677 2 14 -7 -10 9.47129 14.4215 3 14 7 -10 -6.2136 7.44395 6 -14 7 10 5.40895 13.1649 2 -14 7 10 5.76701 13.5451 4 13 -7 -10 176.100 13.7290 5 -13 -7 10 131.858 22.9841 2 13 -7 -10 156.638 27.1346 3 13 7 -10 159.288 13.8940 6 -13 7 10 189.873 28.9158 4 -13 7 10 162.396 25.6291 2 -12 -7 10 -7.0200 10.3071 2 12 -7 -10 9.16246 6.38538 5 12 -7 -10 8.34446 13.5543 3 -12 7 10 -17.088 9.08364 2 -12 7 10 -13.823 10.4423 4 12 7 -10 4.97423 7.52878 6 -11 -7 10 280.454 29.4358 2 11 -7 -10 361.024 35.6862 3 11 -7 -10 331.498 16.2374 5 -11 7 10 276.467 30.4369 2 -11 7 10 321.617 33.2632 4 10 -7 -10 75.0187 9.11047 5 -10 -7 10 49.5664 15.4007 2 10 -7 -10 88.5786 19.7526 3 10 -7 -10 74.6731 15.0315 1 -10 7 10 102.387 19.4407 4 10 7 -10 78.0834 15.6736 1 -10 7 10 61.6213 15.9673 2 9 -7 -10 100.841 9.66466 5 9 -7 -10 102.157 16.3975 1 9 -7 -10 73.7419 18.4563 3 -9 -7 10 72.7546 16.1366 2 -9 7 10 86.9664 16.9734 2 -9 7 10 120.469 19.9634 4 9 7 -10 70.1534 14.6760 1 8 -7 -10 95.7877 19.5850 3 8 -7 -10 47.9204 12.2065 1 8 -7 -10 64.1583 8.05007 5 -8 -7 10 43.8854 9.68150 4 -8 -7 10 91.7852 16.7077 2 -8 7 10 71.5967 15.5778 4 8 7 -10 72.9787 13.9420 1 -8 7 10 51.0340 14.2093 2 -7 -7 10 237.059 24.1803 2 7 -7 -10 323.541 27.3251 3 -7 -7 10 287.414 18.7895 4 7 -7 -10 285.505 20.9804 1 7 -7 -10 272.766 12.9248 5 -7 7 10 236.531 24.7244 2 7 7 -10 265.994 20.6950 1 -7 7 10 313.977 25.0217 4 6 -7 -10 -5.2979 7.22411 1 6 -7 -10 2.15193 9.15954 3 -6 -7 10 7.01819 8.87438 2 6 -7 -10 4.22307 4.50252 5 6 7 -10 3.95936 3.14638 5 -6 7 10 -3.5992 5.85852 4 6 7 -10 -2.5487 6.83647 1 -5 -7 10 142.637 18.4139 2 5 -7 -10 137.544 9.84249 5 -5 -7 10 133.435 7.70204 5 5 -7 -10 136.007 19.8586 3 -5 7 10 138.301 18.8144 4 5 7 -10 129.176 14.8113 1 4 -7 -10 100.636 16.8378 3 -4 -7 10 74.2137 13.6731 3 4 -7 -10 57.9189 6.92642 5 -4 -7 10 77.3212 5.73139 5 -4 -7 10 59.1184 12.5471 2 -4 7 10 62.5932 13.3816 4 4 7 -10 78.7750 11.2915 1 -3 -7 10 12.0818 8.76854 3 -3 -7 10 9.62254 3.64177 5 3 -7 -10 -0.1669 8.86561 3 3 7 -10 9.71638 6.42720 4 3 7 -10 -1.4627 5.65908 1 -3 7 10 -2.1091 6.73738 4 -3 7 10 5.36892 4.47484 5 -2 -7 10 76.9425 5.99985 5 2 -7 -10 83.1502 15.6521 3 2 7 -10 64.4366 10.1447 1 -2 7 10 62.7137 6.75580 5 -2 7 10 71.9873 13.1163 4 2 7 -10 77.1021 10.8980 4 2 7 -10 51.5957 8.95461 1 -1 -7 10 395.742 21.4554 3 -1 -7 10 368.173 11.7005 5 1 -7 -10 412.211 26.1509 3 -1 7 10 365.161 13.8043 5 1 7 -10 409.035 20.1050 1 -1 7 10 318.509 23.2000 4 1 7 -10 385.487 20.5537 4 1 7 -10 369.181 18.1842 1 0 -7 10 265.920 17.4264 3 0 -7 10 259.911 10.4915 5 0 -7 -10 261.633 21.4942 3 0 7 -10 262.011 15.8491 1 0 7 -10 250.334 17.3473 4 0 7 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19.6020 5 0 -6 -20 348.774 37.5543 4 0 6 20 402.843 19.8860 5 0 6 -20 400.106 32.4002 4 1 -6 20 70.6787 11.0239 5 -1 -6 -20 79.7461 21.6257 4 1 6 20 33.4907 9.77900 5 -1 6 -20 60.3478 17.7352 4 2 -6 20 39.5198 9.70323 5 -2 -6 -20 49.7025 19.4240 4 2 6 20 43.1965 9.73549 5 -2 6 -20 51.9842 17.0367 4 -3 -6 -20 45.2851 19.6896 4 3 -6 20 60.7116 10.5604 5 -3 6 -20 50.3177 17.4379 4 3 6 20 67.1778 11.0829 5 4 -6 20 78.8216 11.7309 5 4 6 20 81.3023 11.7462 5 -4 6 -20 60.1826 18.6948 4 5 -6 20 9.47362 8.72210 5 -5 6 -20 4.11885 14.5476 4 5 6 20 -11.868 8.30462 5 6 -7 -20 3.86689 15.6974 3 6 -7 -20 -0.7565 7.53844 5 6 7 -20 5.95362 14.0753 3 5 -7 -20 46.4389 19.6831 3 5 7 -20 34.2400 16.0518 3 4 -7 -20 152.417 26.7888 3 -4 7 20 151.391 14.0615 5 -3 -7 20 0.18203 7.00608 5 3 -7 -20 -6.9440 13.4590 3 -3 7 20 -1.8967 7.32755 5 2 -7 -20 -14.271 10.8351 3 -2 -7 20 0.34523 7.30074 5 -2 7 20 1.46170 7.71695 5 -1 -7 20 19.6044 8.45058 5 1 -7 -20 13.6238 15.2114 3 1 -7 -20 43.8757 18.9587 4 1 7 -20 45.0598 15.5160 4 -1 7 20 12.2492 8.47693 5 0 -7 20 43.1686 9.77048 5 0 -7 -20 5.87642 15.3103 4 0 7 20 14.9009 8.73031 5 0 7 -20 43.7196 14.4484 4 -1 -7 -20 145.056 26.6261 4 1 -7 20 89.6712 11.6491 5 1 7 20 105.008 12.7381 5 -1 7 -20 116.571 20.1217 4 -2 -7 -20 258.618 34.1184 4 2 -7 20 315.667 17.5562 5 2 7 20 251.659 17.1506 5 -2 7 -20 261.599 29.7918 4 -3 -7 -20 144.141 26.9726 4 3 -7 20 192.549 15.2055 5 3 7 20 131.982 13.9707 5 -3 7 -20 152.992 23.7631 4 4 -7 20 28.4401 9.64811 5 -4 7 -20 22.7737 15.0690 4 4 7 20 27.2499 9.78788 5 5 -8 -20 29.0712 8.65727 5 5 -8 -20 3.46392 16.0478 3 5 8 -20 14.9510 15.6710 3 4 -8 -20 211.242 31.2588 3 -4 8 20 210.343 16.7063 5 3 -8 -20 16.3244 15.5612 3 -3 8 20 3.66294 7.77024 5 2 -8 -20 11.8635 14.0694 3 -2 8 20 32.7615 9.49150 5 1 -8 -20 42.7020 16.7303 3 -1 -8 20 6.85686 7.47700 5 1 -8 -20 -4.2218 14.9322 4 -1 8 20 1.59369 7.76727 5 0 -8 20 46.3131 9.76450 5 0 -8 -20 15.5105 17.0924 4 0 8 20 29.9588 9.75494 5 -1 -8 -20 -1.0568 14.3178 4 1 -8 20 25.3466 8.99252 5 1 8 20 27.5316 9.06425 5 -1 8 -20 9.06638 12.2984 4 -2 -8 -20 -11.990 13.8780 4 2 -8 20 -9.5899 7.74206 5 -2 8 -20 1.39941 11.2377 4 2 8 20 8.24442 8.79596 5 3 -8 20 -3.2632 7.93342 5 3 8 20 -0.4716 8.23396 5 -3 8 -20 11.8655 12.3724 4 4 -9 -20 207.438 31.4041 3 3 -9 -20 24.2113 16.5256 3 -3 9 20 4.21453 7.94893 5 2 -9 -20 100.100 22.3486 3 -2 9 20 68.5727 11.4253 5 1 -9 -20 30.6912 15.1589 3 -1 9 20 3.13964 8.32561 5 0 -9 20 95.0272 11.5897 5 0 9 20 97.5944 12.3147 5 1 -9 20 74.5575 11.0769 5 1 9 20 61.2672 11.3022 5 2 -9 20 371.823 18.8858 5 7 0 -21 15.1503 8.03452 5 7 0 -21 28.4927 18.4552 3 -7 0 21 7.77751 14.1331 2 -6 0 21 -4.1551 7.10006 5 6 0 -21 -10.727 13.1754 3 -5 0 21 -2.8645 7.68818 5 5 0 -21 17.9761 13.8364 3 4 0 -21 12.4341 14.6529 4 -4 0 21 3.72066 7.79838 5 4 0 -21 -6.6567 10.3510 3 -3 0 21 1.81848 7.52633 5 3 0 -21 2.39214 11.9163 3 3 0 -21 19.0780 15.3499 4 2 0 -21 -5.6963 13.3478 4 -2 0 21 1.06296 7.32803 5 -1 0 21 -4.9165 7.62613 5 1 0 -21 2.27838 13.9679 4 0 0 -21 21.5763 15.6162 4 0 0 21 -1.5362 7.21314 5 -1 0 -21 -16.579 11.2474 4 1 0 21 -5.4621 7.68590 5 -2 0 -21 1.32650 11.7079 4 2 0 21 -4.6453 7.92386 5 -3 0 -21 -21.903 10.6645 4 3 0 21 -13.950 7.67135 5 4 0 21 -3.6206 7.33395 5 -7 -1 21 287.741 31.5434 2 7 -1 -21 307.802 17.4560 5 7 -1 -21 323.043 37.4256 3 -7 1 21 314.462 34.1875 2 7 1 -21 349.148 38.5851 3 7 1 -21 317.342 17.5644 5 6 -1 -21 223.287 31.3567 3 -6 -1 21 205.119 15.5598 5 6 1 -21 204.357 30.7464 3 -5 -1 21 120.114 12.9234 5 5 -1 -21 117.578 23.5277 3 -5 1 21 115.805 12.8249 5 5 1 -21 114.354 23.1691 3 4 -1 -21 120.143 21.7991 3 -4 -1 21 171.495 14.4092 5 4 1 -21 142.547 26.0336 4 -4 1 21 181.996 14.9661 5 4 1 -21 133.896 23.1702 3 -3 -1 21 -16.031 6.85493 5 3 -1 -21 6.31013 13.9188 3 3 -1 -21 10.8747 14.8263 4 3 1 -21 -3.1165 13.6016 4 -3 1 21 -7.2248 7.30960 5 -2 -1 21 88.4035 11.4026 5 2 -1 -21 80.6898 20.6797 4 -2 1 21 89.5073 11.7825 5 2 1 -21 60.0232 18.4111 4 1 -1 -21 -5.2155 12.5377 4 -1 -1 21 28.3213 8.80021 5 1 1 -21 2.09963 13.4992 4 -1 1 21 8.29968 8.19681 5 0 -1 -21 18.4351 13.8179 4 0 -1 21 25.3500 9.08712 5 0 1 21 46.4726 10.0760 5 0 1 -21 26.1308 17.3912 4 -1 -1 -21 40.2497 16.6055 4 1 -1 21 37.6542 9.88533 5 1 1 21 32.8903 8.90444 5 -1 1 -21 52.8386 17.9910 4 -2 -1 -21 28.4411 16.0009 4 2 -1 21 51.2553 10.2370 5 -2 1 -21 53.5898 17.4457 4 2 1 21 46.7603 10.4604 5 -3 -1 -21 32.6741 14.8854 4 3 -1 21 23.2163 9.26223 5 -3 1 -21 20.2923 15.1885 4 3 1 21 27.9703 9.22325 5 4 -1 21 10.2271 8.12255 5 4 1 21 7.86309 8.98674 5 -7 -2 21 56.6994 18.4103 2 7 2 -21 74.1137 22.0130 3 6 -2 -21 50.8111 19.0014 3 -6 -2 21 47.6265 9.84593 5 6 2 -21 29.0253 17.1884 3 -5 -2 21 7.41442 7.54014 5 5 -2 -21 -0.4279 12.4496 3 5 2 -21 16.3131 14.3059 4 -5 2 21 16.5344 8.72648 5 5 2 -21 7.71253 12.7150 3 -4 -2 21 -2.9874 7.40029 5 4 -2 -21 2.97208 12.2634 3 4 2 -21 11.5591 13.7072 4 -4 2 21 7.70457 7.82101 5 4 2 -21 13.9636 13.5754 3 3 -2 -21 58.0835 18.6286 3 -3 -2 21 56.3678 10.4047 5 3 -2 -21 15.2967 15.3963 4 3 2 -21 26.8017 16.2654 4 -3 2 21 35.2029 9.23377 5 2 -2 -21 298.545 34.4657 4 -2 -2 21 281.498 17.1724 5 2 2 -21 251.269 31.7164 4 -2 2 21 269.720 17.5563 5 -1 -2 21 15.1274 8.70311 5 1 -2 -21 -1.4508 13.2635 4 -1 2 21 11.0551 8.15088 5 1 2 -21 20.0746 15.8192 4 0 -2 -21 189.572 28.6056 4 0 -2 21 249.457 16.8051 5 0 2 -21 230.291 30.9038 4 0 2 21 242.044 15.7489 5 1 -2 21 24.7652 9.10529 5 -1 -2 -21 13.6930 13.6656 4 -1 2 -21 25.4765 15.3770 4 1 2 21 6.58414 7.64611 5 2 -2 21 244.311 17.0202 5 -2 -2 -21 258.965 31.3011 4 2 2 21 200.298 16.3770 5 -2 2 -21 229.876 29.5950 4 3 -2 21 128.530 13.6289 5 -3 -2 -21 89.7887 20.7278 4 3 2 21 113.065 13.2982 5 -3 2 -21 122.678 24.4158 4 4 -2 21 -12.159 7.86561 5 4 2 21 -9.6383 7.85117 5 -6 -3 21 98.2521 12.0294 5 6 -3 -21 84.5133 23.3229 3 6 3 -21 119.828 23.1639 3 5 -3 -21 4.68202 14.5179 3 -5 -3 21 0.24540 7.41873 5 5 3 -21 -4.9000 11.6371 4 -5 3 21 -8.4978 6.33519 5 5 3 -21 0.88898 11.7394 3 -4 -3 21 34.7747 9.37780 5 4 -3 -21 37.2105 15.2588 3 -4 3 21 35.3703 9.06452 5 4 3 -21 32.2070 16.6054 4 4 3 -21 19.0415 15.1882 3 3 -3 -21 91.7655 20.5755 3 -3 -3 21 99.8748 11.7350 5 3 -3 -21 108.447 22.0403 4 3 3 -21 75.0067 18.8775 4 -3 3 21 70.5066 11.2787 5 2 -3 -21 10.9018 14.8791 4 -2 -3 21 9.06878 8.20157 5 2 3 -21 25.3638 15.3723 4 -2 3 21 17.4149 8.75262 5 -1 -3 21 1.10483 7.80905 5 1 -3 -21 -8.6795 12.4333 4 1 3 -21 8.73611 13.7253 4 -1 3 21 17.4004 8.57764 5 0 -3 -21 8.94547 11.1727 4 0 -3 21 7.06850 8.03899 5 0 3 -21 2.33891 13.1440 4 0 3 21 2.03030 8.05466 5 -1 -3 -21 47.7451 16.5164 4 1 -3 21 91.1946 11.9061 5 1 3 21 83.9976 12.0178 5 -1 3 -21 51.9837 17.7878 4 -2 -3 -21 36.0995 15.8629 4 2 -3 21 41.1866 10.1634 5 2 3 21 35.0658 9.77393 5 -2 3 -21 45.1335 18.1819 4 3 -3 21 12.7095 9.05215 5 3 3 21 24.3540 9.07995 5 -3 3 -21 4.32536 14.3401 4 4 -3 21 -14.160 7.49681 5 4 3 21 0.78233 8.33834 5 6 -4 -21 89.4271 23.8663 3 -6 -4 21 91.1132 11.5982 5 6 4 -21 91.9807 21.4274 4 6 4 -21 59.5915 19.3462 3 5 -4 -21 38.2340 18.7366 3 -5 -4 21 20.9382 8.59630 5 -5 4 21 15.0070 8.53654 5 5 4 -21 -4.8051 10.9814 4 5 4 -21 20.3111 15.0701 3 4 -4 -21 147.366 25.9030 3 -4 -4 21 150.836 13.4537 5 4 4 -21 128.991 22.0554 4 -4 4 21 138.545 13.6260 5 -3 -4 21 7.86290 8.17366 5 3 -4 -21 12.2761 13.7782 3 -3 4 21 -14.051 6.81270 5 3 4 -21 5.07250 11.4670 4 -2 -4 21 111.898 12.6621 5 2 -4 -21 117.154 23.4194 4 2 4 -21 138.725 24.1819 4 -2 4 21 110.359 12.4205 5 1 -4 -21 51.9594 18.0727 4 -1 -4 21 36.2681 9.53789 5 1 4 -21 47.6255 17.4264 4 -1 4 21 44.5737 9.87113 5 0 -4 -21 96.4379 20.5675 4 0 -4 21 52.0153 10.3438 5 0 4 21 58.6850 10.7226 5 0 4 -21 77.0486 19.7638 4 1 -4 21 211.839 16.1636 5 -1 -4 -21 196.824 27.7510 4 1 4 21 167.270 14.8655 5 -1 4 -21 182.127 26.5054 4 2 -4 21 97.4667 12.6778 5 2 4 21 77.9678 11.9809 5 -2 4 -21 74.6695 19.3059 4 3 -4 21 57.4841 11.3023 5 -3 4 -21 38.0369 17.9796 4 3 4 21 48.5528 10.9178 5 5 -5 -21 373.286 39.2962 3 -5 -5 21 428.935 20.0618 5 -5 5 21 376.984 20.4467 5 5 5 -21 357.095 36.2880 3 -4 -5 21 0.47420 7.66101 5 4 -5 -21 13.2376 13.8863 3 -4 5 21 -7.5096 6.45886 5 4 5 -21 7.04091 14.2326 4 3 -5 -21 16.7980 13.4691 3 -3 -5 21 2.25920 7.77708 5 3 5 -21 -3.9856 10.2512 4 -3 5 21 2.90347 7.68145 5 2 -5 -21 12.2081 15.6840 3 -2 -5 21 20.7529 8.32862 5 2 -5 -21 -3.1419 11.7573 4 -2 5 21 34.1027 9.60607 5 2 5 -21 56.1935 15.3195 4 1 -5 -21 -2.7064 11.4417 4 -1 -5 21 -5.6922 7.40789 5 -1 5 21 9.56199 8.41988 5 1 5 -21 7.76579 12.1278 4 0 -5 -21 212.030 31.3600 4 0 -5 21 216.905 15.9886 5 0 5 -21 184.649 27.0817 4 0 5 21 179.071 15.2986 5 1 -5 21 291.454 17.8015 5 -1 5 -21 218.607 29.2808 4 1 5 21 283.828 18.1807 5 2 -5 21 34.8315 9.60827 5 2 5 21 26.4397 9.84929 5 -2 5 -21 58.6853 18.6156 4 3 -5 21 -0.0316 8.06591 5 -3 5 -21 1.23594 14.0989 4 3 5 21 -9.5990 7.81672 5 4 -6 -21 22.2104 16.0107 3 -4 -6 21 5.52221 7.68937 5 -4 6 21 28.5433 9.40305 5 3 -6 -21 15.4431 15.6956 3 -3 -6 21 3.12960 8.03905 5 -3 6 21 4.12032 7.56010 5 2 -6 -21 9.96611 15.6939 3 -2 -6 21 7.65009 8.24955 5 2 6 -21 -4.4336 12.7928 4 -2 6 21 -8.4373 7.20213 5 -1 -6 21 28.8360 9.18754 5 1 6 -21 52.0055 16.2692 4 -1 6 21 28.7006 9.32503 5 0 -6 21 63.2560 10.5046 5 0 6 -21 71.7369 17.6189 4 0 6 21 90.7482 12.3002 5 1 -6 21 39.8017 9.93678 5 1 6 21 38.8595 10.2045 5 -1 6 -21 11.0266 13.0013 4 2 -6 21 143.933 14.0614 5 -2 6 -21 103.389 21.6341 4 2 6 21 131.637 14.2428 5 -3 -7 21 11.5487 8.29804 5 3 -7 -21 -4.4754 13.5700 3 -3 7 21 3.76322 8.18690 5 -2 -7 21 -11.161 7.41470 5 2 -7 -21 5.53534 13.9201 3 -2 7 21 0.32322 7.91711 5 -1 -7 21 18.3754 8.76579 5 -1 7 21 2.19170 8.10052 5 0 -7 21 10.3219 8.51285 5 0 7 -21 5.35468 13.0372 4 0 7 21 -6.9972 7.37211 5 -4 0 22 29.7253 9.64702 5 -3 0 22 12.2958 8.61946 5 3 0 -22 24.1667 16.1693 4 -2 0 22 14.0464 9.12452 5 2 0 -22 9.09443 15.0137 4 1 0 -22 60.8330 21.0502 4 -1 0 22 57.9668 10.9759 5 0 0 22 81.5258 12.2297 5 0 0 -22 87.3440 22.0717 4 1 0 22 533.970 23.8327 5 -3 -1 22 21.8653 9.28314 5 -3 1 22 18.5640 8.96002 5 3 1 -22 13.4196 16.1005 4 2 -1 -22 5.01042 17.4511 4 -2 -1 22 37.6853 9.75411 5 -2 1 22 16.5966 9.07679 5 2 1 -22 32.5788 18.3851 4 -1 -1 22 -11.416 7.83375 5 1 1 -22 7.82142 14.5357 4 -1 1 22 1.71601 8.53334 5 0 -1 22 -1.4539 8.29182 5 0 1 22 7.76746 9.14933 5 0 1 -22 16.5892 16.1984 4 1 -1 22 0.01648 8.31933 5 1 1 22 -10.593 7.63443 5 -3 -2 22 11.7921 8.78125 5 3 2 -22 -5.8131 13.2912 4 -3 2 22 -3.3616 7.43857 5 -2 -2 22 108.689 12.4492 5 -2 2 22 98.1148 12.7102 5 2 2 -22 126.285 24.2389 4 -1 -2 22 76.7737 11.6028 5 -1 2 22 93.6041 12.6141 5 1 2 -22 98.5738 23.0794 4 0 -2 22 20.4106 9.33154 5 0 2 -22 13.2529 15.3534 4 0 2 22 10.1545 9.37329 5 -2 -3 22 32.9094 9.36187 5 -2 3 22 16.1108 9.46660 5 2 3 -22 8.89251 14.8223 4 -1 -3 22 9.30027 8.59063 5 -1 3 22 -4.9846 8.06870 5 1 3 -22 -1.8024 13.5303 4 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 17700 #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Cl1 Cl 0.67861(3) 0.58451(3) 0.02959(3) 0.01871(11) Uani 1 1 d . . Cl2 Cl 0.89305(3) 0.59172(3) 0.07219(3) 0.01992(11) Uani 1 1 d . . Cl3 Cl 0.72459(3) 0.71272(3) 0.14509(3) 0.01964(11) Uani 1 1 d . . Cl4 Cl 0.77683(3) 0.36503(3) 0.53684(3) 0.01803(11) Uani 1 1 d . . Cl5 Cl 0.62683(3) 0.48895(3) 0.54857(3) 0.01884(11) Uani 1 1 d . . Cl6 Cl 0.87042(3) 0.52226(3) 0.53506(3) 0.01771(10) Uani 1 1 d . . Si1 Si 0.76929(4) 0.59895(3) 0.13198(3) 0.01270(11) Uani 1 1 d . . Si2 Si 0.74535(3) 0.47336(3) 0.48401(3) 0.01260(11) Uani 1 1 d . . N1 N 0.85389(10) 0.61265(9) 0.22534(9) 0.0126(3) Uani 1 1 d . . N2 N 0.72449(10) 0.52383(9) 0.18337(8) 0.0108(3) Uani 1 1 d . . N3 N 0.71454(10) 0.57252(9) 0.43751(9) 0.0130(3) Uani 1 1 d . . N4 N 0.73943(10) 0.44199(9) 0.38871(8) 0.0114(3) Uani 1 1 d . . C1 C 0.91857(13) 0.66880(11) 0.23582(11) 0.0180(4) Uani 1 1 d . . H1 H 0.9190 0.7088 0.1990 0.022 Uiso 1 1 calc R U C2 C 0.98388(13) 0.66948(12) 0.29840(11) 0.0184(4) Uani 1 1 d . . H2 H 1.0291 0.7094 0.3049 0.022 Uiso 1 1 calc R U C3 C 0.98268(13) 0.61093(11) 0.35202(11) 0.0166(4) Uani 1 1 d . . H3 H 1.0273 0.6102 0.3957 0.020 Uiso 1 1 calc R U C4 C 0.91614(12) 0.55388(11) 0.34128(11) 0.0133(4) Uani 1 1 d . . H4 H 0.9144 0.5135 0.3775 0.016 Uiso 1 1 calc R U C5 C 0.85153(12) 0.55604(11) 0.27678(10) 0.0119(4) Uani 1 1 d . . C6 C 0.77309(12) 0.50014(11) 0.25784(10) 0.0110(4) Uani 1 1 d D . C7 C 0.66208(12) 0.46434(10) 0.14903(10) 0.0115(4) Uani 1 1 d . . C8 C 0.70353(13) 0.39941(11) 0.11767(10) 0.0129(4) Uani 1 1 d . . C9 C 0.64484(14) 0.33931(11) 0.09260(11) 0.0171(4) Uani 1 1 d . . H9 H 0.6721 0.2945 0.0729 0.021 Uiso 1 1 calc R U C10 C 0.54764(13) 0.34366(11) 0.09593(11) 0.0170(4) Uani 1 1 d . . H10 H 0.5087 0.3014 0.0808 0.020 Uiso 1 1 calc R U C11 C 0.50750(13) 0.41004(11) 0.12144(11) 0.0162(4) Uani 1 1 d . . H11 H 0.4405 0.4135 0.1212 0.019 Uiso 1 1 calc R U C12 C 0.56268(12) 0.47194(11) 0.14747(10) 0.0126(4) Uani 1 1 d . . C13 C 0.51231(13) 0.54589(11) 0.16563(11) 0.0154(4) Uani 1 1 d . . H13 H 0.5614 0.5866 0.1738 0.019 Uiso 1 1 calc R U C14 C 0.45767(14) 0.54141(12) 0.23849(12) 0.0200(4) Uani 1 1 d . . H14A H 0.5010 0.5264 0.2825 0.030 Uiso 1 1 calc R U H14B H 0.4069 0.5036 0.2309 0.030 Uiso 1 1 calc R U H14C H 0.4302 0.5913 0.2486 0.030 Uiso 1 1 calc R U C15 C 0.44339(14) 0.56972(12) 0.09651(11) 0.0205(4) Uani 1 1 d . . H15A H 0.4204 0.6215 0.1049 0.031 Uiso 1 1 calc R U H15B H 0.3896 0.5345 0.0920 0.031 Uiso 1 1 calc R U H15C H 0.4766 0.5683 0.0489 0.031 Uiso 1 1 calc R U C16 C 0.80854(13) 0.39438(11) 0.10378(11) 0.0154(4) Uani 1 1 d . . H16 H 0.8417 0.4387 0.1300 0.019 Uiso 1 1 calc R U C17 C 0.85411(14) 0.32135(12) 0.13662(12) 0.0210(4) Uani 1 1 d . . H17A H 0.8400 0.3157 0.1908 0.032 Uiso 1 1 calc R U H17B H 0.9229 0.3239 0.1334 0.032 Uiso 1 1 calc R U H17C H 0.8287 0.2776 0.1068 0.032 Uiso 1 1 calc R U C18 C 0.82189(14) 0.39973(13) 0.01685(12) 0.0226(5) Uani 1 1 d . . H18A H 0.8897 0.3992 0.0087 0.034 Uiso 1 1 calc R U H18B H 0.7936 0.4472 -0.0037 0.034 Uiso 1 1 calc R U H18C H 0.7909 0.3562 -0.0098 0.034 Uiso 1 1 calc R U C19 C 0.70896(13) 0.63861(11) 0.47729(11) 0.0164(4) Uani 1 1 d . . H19 H 0.7278 0.6393 0.5310 0.020 Uiso 1 1 calc R U C20 C 0.67693(13) 0.70441(11) 0.44216(12) 0.0183(4) Uani 1 1 d . . H20 H 0.6738 0.7504 0.4707 0.022 Uiso 1 1 calc R U C21 C 0.64898(13) 0.70250(11) 0.36344(11) 0.0173(4) Uani 1 1 d . . H21 H 0.6257 0.7473 0.3378 0.021 Uiso 1 1 calc R U C22 C 0.65527(13) 0.63526(11) 0.32296(11) 0.0151(4) Uani 1 1 d . . H22 H 0.6367 0.6334 0.2693 0.018 Uiso 1 1 calc R U C23 C 0.68906(12) 0.57035(11) 0.36165(10) 0.0115(4) Uani 1 1 d . . C24 C 0.70458(12) 0.49399(10) 0.32576(10) 0.0105(4) Uani 1 1 d D . C25 C 0.73792(13) 0.36192(11) 0.36527(10) 0.0128(4) Uani 1 1 d . . C26 C 0.64970(13) 0.32577(11) 0.34938(11) 0.0144(4) Uani 1 1 d . . C27 C 0.64862(14) 0.25270(11) 0.31826(12) 0.0201(4) Uani 1 1 d . . H27 H 0.5895 0.2291 0.3038 0.024 Uiso 1 1 calc R U C28 C 0.73157(14) 0.21372(12) 0.30797(12) 0.0225(5) Uani 1 1 d . . H28 H 0.7295 0.1643 0.2857 0.027 Uiso 1 1 calc R U C29 C 0.81749(14) 0.24734(11) 0.33039(12) 0.0190(4) Uani 1 1 d . . H29 H 0.8742 0.2192 0.3260 0.023 Uiso 1 1 calc R U C30 C 0.82331(13) 0.32136(11) 0.35920(11) 0.0146(4) Uani 1 1 d . . C31 C 0.92127(13) 0.35197(11) 0.38563(11) 0.0157(4) Uani 1 1 d . . H31 H 0.9124 0.4012 0.4132 0.019 Uiso 1 1 calc R U C32 C 0.98222(13) 0.36787(12) 0.31802(12) 0.0180(4) Uani 1 1 d . . H32A H 1.0438 0.3882 0.3378 0.027 Uiso 1 1 calc R U H32B H 0.9501 0.4051 0.2831 0.027 Uiso 1 1 calc R U H32C H 0.9917 0.3205 0.2898 0.027 Uiso 1 1 calc R U C33 C 0.97449(14) 0.29691(12) 0.44288(12) 0.0219(4) Uani 1 1 d . . H33A H 0.9350 0.2858 0.4856 0.033 Uiso 1 1 calc R U H33B H 1.0339 0.3205 0.4633 0.033 Uiso 1 1 calc R U H33C H 0.9884 0.2495 0.4162 0.033 Uiso 1 1 calc R U C34 C 0.55679(13) 0.35868(11) 0.37408(11) 0.0162(4) Uani 1 1 d . . H34 H 0.5661 0.4144 0.3840 0.019 Uiso 1 1 calc R U C35 C 0.47327(14) 0.34881(12) 0.31380(12) 0.0222(5) Uani 1 1 d . . H35A H 0.4179 0.3759 0.3308 0.033 Uiso 1 1 calc R U H35B H 0.4583 0.2946 0.3077 0.033 Uiso 1 1 calc R U H35C H 0.4900 0.3697 0.2642 0.033 Uiso 1 1 calc R U C36 C 0.53291(14) 0.32057(12) 0.44994(12) 0.0219(5) Uani 1 1 d . . H36A H 0.4774 0.3455 0.4694 0.033 Uiso 1 1 calc R U H36B H 0.5870 0.3254 0.4882 0.033 Uiso 1 1 calc R U H36C H 0.5190 0.2665 0.4406 0.033 Uiso 1 1 calc R U C40T C 0.13615(17) 0.31947(14) 0.10646(14) 0.0336(6) Uani 1 1 d . . H37A H 0.0709 0.3165 0.0835 0.050 Uiso 1 1 calc R U H37B H 0.1512 0.2733 0.1366 0.050 Uiso 1 1 calc R U H37C H 0.1798 0.3241 0.0654 0.050 Uiso 1 1 calc R U C41T C 0.14624(14) 0.38742(13) 0.15822(13) 0.0257(5) Uani 1 1 d . . C42T C 0.09464(15) 0.45411(13) 0.14219(13) 0.0271(5) Uani 1 1 d . . H42 H 0.0512 0.4562 0.0979 0.033 Uiso 1 1 calc R U C43T C 0.10578(16) 0.51696(14) 0.18965(13) 0.0314(5) Uani 1 1 d . . H43 H 0.0702 0.5619 0.1777 0.038 Uiso 1 1 calc R U C44T C 0.16878(16) 0.51476(15) 0.25479(14) 0.0326(6) Uani 1 1 d . . H44 H 0.1762 0.5578 0.2878 0.039 Uiso 1 1 calc R U C45T C 0.22014(16) 0.44985(17) 0.27100(14) 0.0366(6) Uani 1 1 d . . H45 H 0.2638 0.4482 0.3152 0.044 Uiso 1 1 calc R U C46T C 0.20914(15) 0.38704(15) 0.22393(13) 0.0331(6) Uani 1 1 d . . H46 H 0.2451 0.3425 0.2364 0.040 Uiso 1 1 calc R U H6 H 0.7990(17) 0.4483(12) 0.2551(14) 0.040 Uiso 1 1 d D U H24 H 0.6423(15) 0.4767(14) 0.3014(14) 0.040 Uiso 1 1 d D U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0219(2) 0.0201(3) 0.0135(2) 0.00274(19) -0.00314(18) -0.00348(19) Cl2 0.0188(2) 0.0258(3) 0.0158(2) 0.0009(2) 0.00506(18) -0.00361(19) Cl3 0.0266(2) 0.0120(2) 0.0200(2) 0.00197(19) -0.00059(19) 0.00229(19) Cl4 0.0204(2) 0.0178(3) 0.0159(2) 0.00480(19) 0.00129(18) 0.00176(19) Cl5 0.0176(2) 0.0223(3) 0.0173(2) 0.0010(2) 0.00680(18) 0.00125(19) Cl6 0.0159(2) 0.0210(3) 0.0157(2) -0.00044(19) -0.00251(17) -0.00153(18) Si1 0.0145(2) 0.0121(3) 0.0115(2) 0.0012(2) 0.00040(19) -0.0013(2) Si2 0.0129(2) 0.0138(3) 0.0112(2) 0.0011(2) 0.00139(19) 0.0003(2) N1 0.0131(7) 0.0115(8) 0.0131(8) 0.0007(6) 0.0015(6) -0.0009(6) N2 0.0118(7) 0.0106(8) 0.0097(7) -0.0004(6) -0.0007(6) -0.0002(6) N3 0.0115(7) 0.0135(9) 0.0139(8) -0.0007(6) 0.0016(6) -0.0009(6) N4 0.0142(7) 0.0092(8) 0.0109(8) 0.0022(6) 0.0010(6) 0.0014(6) C1 0.0212(10) 0.0158(11) 0.0172(10) 0.0014(8) 0.0025(8) -0.0064(8) C2 0.0170(9) 0.0167(11) 0.0214(10) -0.0011(8) 0.0012(8) -0.0066(8) C3 0.0137(9) 0.0198(11) 0.0163(10) -0.0026(8) 0.0003(7) 0.0005(8) C4 0.0135(9) 0.0140(10) 0.0126(9) 0.0001(8) 0.0015(7) 0.0005(7) C5 0.0114(8) 0.0121(10) 0.0128(9) -0.0017(8) 0.0040(7) 0.0013(7) C6 0.0114(8) 0.0109(10) 0.0108(9) 0.0003(7) 0.0017(7) 0.0001(7) C7 0.0139(9) 0.0114(10) 0.0091(8) 0.0013(7) -0.0003(7) -0.0019(7) C8 0.0162(9) 0.0126(10) 0.0098(9) 0.0005(7) 0.0006(7) 0.0003(7) C9 0.0220(10) 0.0128(10) 0.0166(10) -0.0027(8) 0.0014(8) -0.0002(8) C10 0.0188(10) 0.0151(11) 0.0170(10) -0.0017(8) -0.0008(8) -0.0062(8) C11 0.0145(9) 0.0202(11) 0.0137(9) 0.0001(8) 0.0002(7) -0.0025(8) C12 0.0143(9) 0.0145(10) 0.0090(9) 0.0011(7) 0.0006(7) -0.0003(7) C13 0.0130(9) 0.0163(10) 0.0168(10) -0.0027(8) -0.0002(7) 0.0004(7) C14 0.0174(10) 0.0233(12) 0.0195(10) -0.0010(9) 0.0027(8) 0.0031(8) C15 0.0214(10) 0.0216(12) 0.0181(10) -0.0015(9) -0.0022(8) 0.0056(8) C16 0.0162(9) 0.0128(10) 0.0173(10) -0.0038(8) 0.0020(7) 0.0000(7) C17 0.0191(10) 0.0191(11) 0.0244(11) -0.0034(9) -0.0015(8) 0.0040(8) C18 0.0211(10) 0.0285(13) 0.0187(10) -0.0015(9) 0.0046(8) 0.0013(9) C19 0.0167(9) 0.0189(11) 0.0139(9) -0.0047(8) 0.0030(7) -0.0014(8) C20 0.0206(10) 0.0133(10) 0.0216(10) -0.0045(8) 0.0067(8) -0.0017(8) C21 0.0184(9) 0.0133(10) 0.0206(10) 0.0003(8) 0.0046(8) 0.0022(8) C22 0.0152(9) 0.0164(11) 0.0137(9) -0.0001(8) 0.0013(7) 0.0006(8) C23 0.0079(8) 0.0141(10) 0.0129(9) -0.0001(7) 0.0030(7) -0.0016(7) C24 0.0098(8) 0.0111(10) 0.0105(9) 0.0012(7) 0.0008(7) 0.0005(7) C25 0.0166(9) 0.0105(10) 0.0117(9) 0.0017(7) 0.0028(7) 0.0002(7) C26 0.0154(9) 0.0133(10) 0.0147(9) 0.0031(8) 0.0025(7) -0.0013(7) C27 0.0191(10) 0.0150(11) 0.0265(11) -0.0012(9) 0.0033(8) -0.0049(8) C28 0.0251(11) 0.0138(11) 0.0292(12) -0.0055(9) 0.0069(9) -0.0022(8) C29 0.0197(10) 0.0143(11) 0.0239(11) 0.0010(9) 0.0076(8) 0.0022(8) C30 0.0160(9) 0.0137(10) 0.0144(9) 0.0023(8) 0.0039(7) -0.0008(7) C31 0.0143(9) 0.0144(10) 0.0187(10) -0.0018(8) 0.0021(7) 0.0011(7) C32 0.0142(9) 0.0178(11) 0.0223(10) -0.0018(9) 0.0044(8) 0.0007(8) C33 0.0203(10) 0.0222(12) 0.0230(11) 0.0033(9) 0.0011(8) 0.0046(8) C34 0.0144(9) 0.0128(10) 0.0217(10) 0.0025(8) 0.0029(8) -0.0022(7) C35 0.0166(10) 0.0234(12) 0.0264(11) 0.0039(9) 0.0005(8) -0.0016(8) C36 0.0179(10) 0.0247(12) 0.0238(11) 0.0064(9) 0.0054(8) 0.0002(8) C40T 0.0359(13) 0.0323(14) 0.0341(13) 0.0085(11) 0.0137(10) 0.0043(11) C41T 0.0208(10) 0.0322(13) 0.0255(12) 0.0070(10) 0.0111(9) 0.0019(9) C42T 0.0258(11) 0.0339(14) 0.0216(11) 0.0028(10) 0.0017(9) 0.0038(10) C43T 0.0342(12) 0.0320(14) 0.0281(12) 0.0025(11) 0.0035(10) 0.0031(10) C44T 0.0275(12) 0.0428(16) 0.0283(12) -0.0053(11) 0.0077(10) -0.0106(11) C45T 0.0183(11) 0.0686(19) 0.0229(12) 0.0033(12) 0.0025(9) -0.0010(11) C46T 0.0217(11) 0.0506(17) 0.0275(12) 0.0141(12) 0.0058(9) 0.0111(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N2 Si1 N1 83.82(7) N2 Si1 Cl2 123.75(6) N1 Si1 Cl2 86.29(5) N2 Si1 Cl3 122.62(6) N1 Si1 Cl3 87.95(5) Cl2 Si1 Cl3 112.13(3) N2 Si1 Cl1 96.77(5) N1 Si1 Cl1 179.30(6) Cl2 Si1 Cl1 93.07(3) Cl3 Si1 Cl1 92.04(3) N4 Si2 N3 84.01(7) N4 Si2 Cl5 124.29(6) N3 Si2 Cl5 86.65(5) N4 Si2 Cl6 120.68(6) N3 Si2 Cl6 88.03(5) Cl5 Si2 Cl6 113.69(3) N4 Si2 Cl4 96.87(6) N3 Si2 Cl4 178.72(5) Cl5 Si2 Cl4 92.09(3) Cl6 Si2 Cl4 92.30(3) C5 N1 C1 120.20(16) C5 N1 Si1 114.66(12) C1 N1 Si1 124.70(13) C7 N2 C6 112.49(14) C7 N2 Si1 124.31(12) C6 N2 Si1 119.90(11) C23 N3 C19 120.22(16) C23 N3 Si2 114.59(13) C19 N3 Si2 124.87(13) C25 N4 C24 112.96(14) C25 N4 Si2 124.56(12) C24 N4 Si2 119.78(12) N1 C1 C2 121.58(18) N1 C1 H1 119.2 C2 C1 H1 119.2 C1 C2 C3 118.90(18) C1 C2 H2 120.6 C3 C2 H2 120.6 C4 C3 C2 119.33(18) C4 C3 H3 120.3 C2 C3 H3 120.3 C3 C4 C5 119.37(18) C3 C4 H4 120.3 C5 C4 H4 120.3 N1 C5 C4 120.63(17) N1 C5 C6 113.21(16) C4 C5 C6 126.14(17) N2 C6 C5 107.26(15) N2 C6 C24 113.52(14) C5 C6 C24 111.41(15) N2 C6 H6 111.6(15) C5 C6 H6 110.1(14) C24 C6 H6 103.0(15) C8 C7 C12 120.76(17) C8 C7 N2 118.57(15) C12 C7 N2 120.67(16) C9 C8 C7 118.57(17) C9 C8 C16 118.17(17) C7 C8 C16 123.07(16) C10 C9 C8 121.13(18) C10 C9 H9 119.4 C8 C9 H9 119.4 C9 C10 C11 119.53(18) C9 C10 H10 120.2 C11 C10 H10 120.2 C10 C11 C12 121.82(17) C10 C11 H11 119.1 C12 C11 H11 119.1 C11 C12 C7 117.78(17) C11 C12 C13 118.14(16) C7 C12 C13 123.84(16) C12 C13 C14 113.50(16) C12 C13 C15 110.33(15) C14 C13 C15 109.06(15) C12 C13 H13 107.9 C14 C13 H13 107.9 C15 C13 H13 107.9 C13 C14 H14A 109.5 C13 C14 H14B 109.5 H14A C14 H14B 109.5 C13 C14 H14C 109.5 H14A C14 H14C 109.5 H14B C14 H14C 109.5 C13 C15 H15A 109.5 C13 C15 H15B 109.5 H15A C15 H15B 109.5 C13 C15 H15C 109.5 H15A C15 H15C 109.5 H15B C15 H15C 109.5 C8 C16 C17 112.28(16) C8 C16 C18 110.05(16) C17 C16 C18 109.81(16) C8 C16 H16 108.2 C17 C16 H16 108.2 C18 C16 H16 108.2 C16 C17 H17A 109.5 C16 C17 H17B 109.5 H17A C17 H17B 109.5 C16 C17 H17C 109.5 H17A C17 H17C 109.5 H17B C17 H17C 109.5 C16 C18 H18A 109.5 C16 C18 H18B 109.5 H18A C18 H18B 109.5 C16 C18 H18C 109.5 H18A C18 H18C 109.5 H18B C18 H18C 109.5 N3 C19 C20 121.72(18) N3 C19 H19 119.1 C20 C19 H19 119.1 C19 C20 C21 118.50(18) C19 C20 H20 120.7 C21 C20 H20 120.7 C22 C21 C20 119.68(18) C22 C21 H21 120.2 C20 C21 H21 120.2 C21 C22 C23 119.23(18) C21 C22 H22 120.4 C23 C22 H22 120.4 N3 C23 C22 120.64(17) N3 C23 C24 113.34(16) C22 C23 C24 125.98(16) N4 C24 C23 107.18(14) N4 C24 C6 113.74(14) C23 C24 C6 111.35(14) N4 C24 H24 111.2(14) C23 C24 H24 107.2(14) C6 C24 H24 106.0(15) C26 C25 C30 120.54(17) C26 C25 N4 118.80(16) C30 C25 N4 120.66(16) C27 C26 C25 118.39(17) C27 C26 C34 118.23(17) C25 C26 C34 122.91(17) C28 C27 C26 121.44(19) C28 C27 H27 119.3 C26 C27 H27 119.3 C29 C28 C27 119.36(19) C29 C28 H28 120.3 C27 C28 H28 120.3 C28 C29 C30 121.84(18) C28 C29 H29 119.1 C30 C29 H29 119.1 C29 C30 C25 117.95(17) C29 C30 C31 117.73(17) C25 C30 C31 124.26(17) C30 C31 C32 112.58(16) C30 C31 C33 111.27(16) C32 C31 C33 109.39(15) C30 C31 H31 107.8 C32 C31 H31 107.8 C33 C31 H31 107.8 C31 C32 H32A 109.5 C31 C32 H32B 109.5 H32A C32 H32B 109.5 C31 C32 H32C 109.5 H32A C32 H32C 109.5 H32B C32 H32C 109.5 C31 C33 H33A 109.5 C31 C33 H33B 109.5 H33A C33 H33B 109.5 C31 C33 H33C 109.5 H33A C33 H33C 109.5 H33B C33 H33C 109.5 C26 C34 C35 113.78(17) C26 C34 C36 108.90(16) C35 C34 C36 109.23(16) C26 C34 H34 108.3 C35 C34 H34 108.3 C36 C34 H34 108.3 C34 C35 H35A 109.5 C34 C35 H35B 109.5 H35A C35 H35B 109.5 C34 C35 H35C 109.5 H35A C35 H35C 109.5 H35B C35 H35C 109.5 C34 C36 H36A 109.5 C34 C36 H36B 109.5 H36A C36 H36B 109.5 C34 C36 H36C 109.5 H36A C36 H36C 109.5 H36B C36 H36C 109.5 C41T C40T H37A 109.5 C41T C40T H37B 109.5 H37A C40T H37B 109.5 C41T C40T H37C 109.5 H37A C40T H37C 109.5 H37B C40T H37C 109.5 C46T C41T C42T 117.4(2) C46T C41T C40T 121.0(2) C42T C41T C40T 121.6(2) C43T C42T C41T 121.1(2) C43T C42T H42 119.4 C41T C42T H42 119.4 C42T C43T C44T 120.2(2) C42T C43T H43 119.9 C44T C43T H43 119.9 C45T C44T C43T 119.3(2) C45T C44T H44 120.3 C43T C44T H44 120.3 C44T C45T C46T 120.7(2) C44T C45T H45 119.7 C46T C45T H45 119.7 C45T C46T C41T 121.3(2) C45T C46T H46 119.3 C41T C46T H46 119.3 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Cl1 Si1 2.1294(9) Cl2 Si1 2.1038(8) Cl3 Si1 2.1130(8) Cl4 Si2 2.1443(7) Cl5 Si2 2.1020(9) Cl6 Si2 2.1033(8) Si1 N2 1.7380(16) Si1 N1 1.9574(17) Si2 N4 1.7396(16) Si2 N3 1.9550(17) N1 C5 1.338(2) N1 C1 1.348(2) N2 C7 1.466(2) N2 C6 1.479(2) N3 C23 1.340(2) N3 C19 1.356(2) N4 C25 1.463(2) N4 C24 1.480(2) C1 C2 1.374(3) C1 H1 0.9500 C2 C3 1.388(3) C2 H2 0.9500 C3 C4 1.378(3) C3 H3 0.9500 C4 C5 1.393(3) C4 H4 0.9500 C5 C6 1.500(3) C6 C24 1.584(2) C6 H6 0.98(2) C7 C8 1.410(3) C7 C12 1.411(2) C8 C9 1.393(3) C8 C16 1.525(2) C9 C10 1.383(3) C9 H9 0.9500 C10 C11 1.383(3) C10 H10 0.9500 C11 C12 1.394(3) C11 H11 0.9500 C12 C13 1.525(3) C13 C14 1.532(3) C13 C15 1.547(3) C13 H13 1.0000 C14 H14A 0.9800 C14 H14B 0.9800 C14 H14C 0.9800 C15 H15A 0.9800 C15 H15B 0.9800 C15 H15C 0.9800 C16 C17 1.527(3) C16 C18 1.537(3) C16 H16 1.0000 C17 H17A 0.9800 C17 H17B 0.9800 C17 H17C 0.9800 C18 H18A 0.9800 C18 H18B 0.9800 C18 H18C 0.9800 C19 C20 1.368(3) C19 H19 0.9500 C20 C21 1.395(3) C20 H20 0.9500 C21 C22 1.380(3) C21 H21 0.9500 C22 C23 1.390(3) C22 H22 0.9500 C23 C24 1.502(3) C24 H24 1.00(2) C25 C26 1.409(3) C25 C30 1.413(3) C26 C27 1.392(3) C26 C34 1.526(3) C27 C28 1.382(3) C27 H27 0.9500 C28 C29 1.381(3) C28 H28 0.9500 C29 C30 1.393(3) C29 H29 0.9500 C30 C31 1.525(3) C31 C32 1.532(3) C31 C33 1.543(3) C31 H31 1.0000 C32 H32A 0.9800 C32 H32B 0.9800 C32 H32C 0.9800 C33 H33A 0.9800 C33 H33B 0.9800 C33 H33C 0.9800 C34 C35 1.530(3) C34 C36 1.537(3) C34 H34 1.0000 C35 H35A 0.9800 C35 H35B 0.9800 C35 H35C 0.9800 C36 H36A 0.9800 C36 H36B 0.9800 C36 H36C 0.9800 C40T C41T 1.494(3) C40T H37A 0.9800 C40T H37B 0.9800 C40T H37C 0.9800 C41T C46T 1.394(3) C41T C42T 1.397(3) C42T C43T 1.379(3) C42T H42 0.9500 C43T C44T 1.388(3) C43T H43 0.9500 C44T C45T 1.370(4) C44T H44 0.9500 C45T C46T 1.375(4) C45T H45 0.9500 C46T H46 0.9500 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion N1 Si1 N2 C7 -166.45(14) Cl2 Si1 N2 C7 -85.12(14) Cl3 Si1 N2 C7 109.98(13) Cl1 Si1 N2 C7 13.17(14) N1 Si1 N2 C6 -8.54(13) Cl2 Si1 N2 C6 72.79(14) Cl3 Si1 N2 C6 -92.11(13) Cl1 Si1 N2 C6 171.08(12) N3 Si2 N4 C25 -168.25(15) Cl5 Si2 N4 C25 -86.45(15) Cl6 Si2 N4 C25 107.63(14) Cl4 Si2 N4 C25 10.83(14) N3 Si2 N4 C24 -8.19(13) Cl5 Si2 N4 C24 73.62(14) Cl6 Si2 N4 C24 -92.31(13) Cl4 Si2 N4 C24 170.89(12) C5 N1 C1 C2 0.6(3) Si1 N1 C1 C2 -171.47(15) N1 C1 C2 C3 -0.2(3) C1 C2 C3 C4 -0.1(3) C2 C3 C4 C5 0.1(3) C1 N1 C5 C4 -0.6(3) Si1 N1 C5 C4 172.20(13) C1 N1 C5 C6 177.84(16) Si1 N1 C5 C6 -9.37(19) C3 C4 C5 N1 0.3(3) C3 C4 C5 C6 -177.96(17) C7 N2 C6 C5 165.93(14) Si1 N2 C6 C5 5.58(19) C7 N2 C6 C24 -70.56(19) Si1 N2 C6 C24 129.08(13) N1 C5 C6 N2 3.1(2) C4 C5 C6 N2 -178.61(17) N1 C5 C6 C24 -121.73(16) C4 C5 C6 C24 56.6(2) C6 N2 C7 C8 -71.8(2) Si1 N2 C7 C8 87.50(19) C6 N2 C7 C12 108.13(18) Si1 N2 C7 C12 -92.53(19) C12 C7 C8 C9 -6.8(3) N2 C7 C8 C9 173.19(16) C12 C7 C8 C16 168.08(17) N2 C7 C8 C16 -12.0(3) C7 C8 C9 C10 2.0(3) C16 C8 C9 C10 -173.10(17) C8 C9 C10 C11 2.8(3) C9 C10 C11 C12 -3.0(3) C10 C11 C12 C7 -1.6(3) C10 C11 C12 C13 173.03(17) C8 C7 C12 C11 6.6(3) N2 C7 C12 C11 -173.41(16) C8 C7 C12 C13 -167.77(17) N2 C7 C12 C13 12.3(3) C11 C12 C13 C14 70.9(2) C7 C12 C13 C14 -114.8(2) C11 C12 C13 C15 -51.9(2) C7 C12 C13 C15 122.43(19) C9 C8 C16 C17 -54.5(2) C7 C8 C16 C17 130.59(19) C9 C8 C16 C18 68.1(2) C7 C8 C16 C18 -106.8(2) C23 N3 C19 C20 0.5(3) Si2 N3 C19 C20 -172.68(14) N3 C19 C20 C21 0.4(3) C19 C20 C21 C22 -0.8(3) C20 C21 C22 C23 0.3(3) C19 N3 C23 C22 -1.0(3) Si2 N3 C23 C22 172.84(13) C19 N3 C23 C24 176.85(15) Si2 N3 C23 C24 -9.30(18) C21 C22 C23 N3 0.6(3) C21 C22 C23 C24 -176.96(17) C25 N4 C24 C23 167.42(14) Si2 N4 C24 C23 5.17(18) C25 N4 C24 C6 -69.06(18) Si2 N4 C24 C6 128.69(14) N3 C23 C24 N4 3.23(19) C22 C23 C24 N4 -179.05(16) N3 C23 C24 C6 -121.75(16) C22 C23 C24 C6 56.0(2) N2 C6 C24 N4 155.94(15) C5 C6 C24 N4 -82.85(19) N2 C6 C24 C23 -82.84(18) C5 C6 C24 C23 38.4(2) C24 N4 C25 C26 -68.4(2) Si2 N4 C25 C26 92.82(19) C24 N4 C25 C30 112.03(18) Si2 N4 C25 C30 -86.7(2) C30 C25 C26 C27 -8.1(3) N4 C25 C26 C27 172.37(17) C30 C25 C26 C34 163.88(17) N4 C25 C26 C34 -15.7(3) C25 C26 C27 C28 4.5(3) C34 C26 C27 C28 -167.81(19) C26 C27 C28 C29 1.3(3) C27 C28 C29 C30 -3.7(3) C28 C29 C30 C25 0.2(3) C28 C29 C30 C31 177.38(18) C26 C25 C30 C29 5.8(3) N4 C25 C30 C29 -174.68(16) C26 C25 C30 C31 -171.24(17) N4 C25 C30 C31 8.3(3) C29 C30 C31 C32 71.3(2) C25 C30 C31 C32 -111.6(2) C29 C30 C31 C33 -51.9(2) C25 C30 C31 C33 125.1(2) C27 C26 C34 C35 -47.3(2) C25 C26 C34 C35 140.69(19) C27 C26 C34 C36 74.8(2) C25 C26 C34 C36 -97.2(2) C46T C41T C42T C43T 0.0(3) C40T C41T C42T C43T -178.8(2) C41T C42T C43T C44T -0.2(3) C42T C43T C44T C45T 0.5(3) C43T C44T C45T C46T -0.6(3) C44T C45T C46T C41T 0.5(3) C42T C41T C46T C45T -0.2(3) C40T C41T C46T C45T 178.7(2)