Crystallography Open Database

Information card for entry 7115051

Preview

Coordinates	7115051.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H14 Co N4 O8.5 V3
Calculated formula	C24 H14 Co N4 O8.5 V3
Title of publication	Dehydrogenative coupling of phenanthroline under hydrothermal conditions: crystal structure of a novel layered vanadate complex constructed of 4,8,10-net sheets: [(2,2′-biphen)Co]V3O8.5
Authors of publication	Liu, Cai-Ming; Gao, Song; Kou, Hui-Zhong
Journal of publication	Chemical Communications
Year of publication	2001
Journal issue	17
Pages of publication	1670
a	19.66 ± 0.004 Å
b	18.43 ± 0.004 Å
c	13.64 ± 0.003 Å
α	90°
β	103.2 ± 0.03°
γ	90°
Cell volume	4811.7 ± 1.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0523
Residual factor for significantly intense reflections	0.042
Weighted residual factors for significantly intense reflections	0.1046
Weighted residual factors for all reflections included in the refinement	0.1125
Goodness-of-fit parameter for all reflections included in the refinement	1.014
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7115051.cif
118505	2014-06-30	cif/ Adding structures of 7115051 via cif-deposit CGI script.	7115051.cif