#------------------------------------------------------------------------------ #$Date: 2019-11-17 07:13:40 +0200 (Sun, 17 Nov 2019) $ #$Revision: 228603 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/12/11/7121123.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7121123 loop_ _publ_author_name 'Li, Tao' 'Tan, Gengwen' 'Cheng, Cheng' 'Zhao, Yue' 'Zhang, Li' 'Wang, Xinping' _publ_section_title ; Syntheses, structures and theoretical calculations of stable triarylarsine radical cations. ; _journal_issue 12 _journal_name_full 'Chemical communications (Cambridge, England)' _journal_page_first 1493 _journal_page_last 1496 _journal_paper_doi 10.1039/c7cc09544a _journal_volume 54 _journal_year 2018 _chemical_formula_sum 'C68 H63 As B F24' _chemical_formula_weight 1421.91 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _audit_update_record ; 2017-11-21 deposited with the CCDC. 2018-01-09 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 105.786(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 19.0845(17) _cell_length_b 19.3689(16) _cell_length_c 19.0896(19) _cell_measurement_reflns_used 9959 _cell_measurement_temperature 153(2) _cell_measurement_theta_max 27.15 _cell_measurement_theta_min 3.04 _cell_volume 6790.3(11) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Ortep 3v2' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 153(2) _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.996 _diffrn_measurement_device_type 'PHOTON100 CMOS detector' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0426 _diffrn_reflns_av_unetI/netI 0.0397 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.996 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -22 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 24252 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.996 _diffrn_reflns_theta_full 25.009 _diffrn_reflns_theta_max 25.009 _diffrn_reflns_theta_min 2.057 _exptl_absorpt_coefficient_mu 0.606 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.5291 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Bruker, 2014)' _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.391 _exptl_crystal_description block _exptl_crystal_F_000 2900 _exptl_crystal_size_max 0.220 _exptl_crystal_size_mid 0.190 _exptl_crystal_size_min 0.170 _refine_diff_density_max 0.593 _refine_diff_density_min -0.334 _refine_diff_density_rms 0.048 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 583 _refine_ls_number_reflns 5971 _refine_ls_number_restraints 175 _refine_ls_restrained_S_all 1.065 _refine_ls_R_factor_all 0.0580 _refine_ls_R_factor_gt 0.0489 _refine_ls_shift/su_max 0.012 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0634P)^2^+9.0020P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1299 _refine_ls_wR_factor_ref 0.1368 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5117 _reflns_number_total 5971 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file c7cc09544a2.cif _cod_data_source_block 1_a_CCDC1 _cod_depositor_comments 'Adding full bibliography for 7121122--7121123.cif.' _cod_database_code 7121123 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.878 _shelx_estimated_absorpt_t_max 0.904 _shelx_res_file ; TITL 1_a.res in C2/c 1_a.res created by SHELXL-2016/6 at 10:04:53 on 14-Nov-2017 CELL 0.71073 19.0845 19.3689 19.0896 90.000 105.786 90.000 ZERR 4.000 0.0017 0.0016 0.0019 0.000 0.003 0.000 LATT 7 SYMM -X, Y, 1/2-Z SFAC C H B F As UNIT 272 252 4 96 4 OMIT -3.00 50.02 L.S. 20 ACTA BOND $H FMAP 2 PLAN 20 sump 1 .0001 1 2 1 3 1 4 isor .01 $f $as size .22 .19 .17 FREE F8B F9 FREE F7B F8 FREE F10A F12A FREE F8A F9A FREE F7 F9 TEMP 23.000 WGHT 0.063400 9.002000 FVAR 0.33832 0.50923 0.13771 0.35307 AS1 5 -0.014209 0.449358 0.236327 10.50000 0.03409 0.02950 = 0.03987 -0.00301 0.01418 -0.00162 B1 3 1.000000 0.939235 0.250000 10.50000 0.02537 0.02999 = 0.02642 0.00000 0.00400 0.00000 C1 1 0.151515 0.564054 0.410797 11.00000 0.10994 0.07329 = 0.10812 -0.00288 -0.05101 -0.00304 AFIX 137 H1A 2 0.173922 0.561109 0.371555 11.00000 -1.50000 H1B 2 0.175068 0.532505 0.448681 11.00000 -1.50000 H1C 2 0.156196 0.610254 0.429717 11.00000 -1.50000 AFIX 0 C2 1 0.071930 0.545659 0.383199 11.00000 0.12150 0.06504 = 0.08167 0.02250 -0.03307 -0.03907 AFIX 13 H2 2 0.069523 0.496144 0.372240 11.00000 -1.20000 AFIX 0 C3 1 0.032827 0.556571 0.441130 11.00000 0.18128 0.30829 = 0.08058 0.05867 0.01551 -0.09465 AFIX 137 H3A 2 0.033177 0.604799 0.452819 11.00000 -1.50000 H3B 2 0.056979 0.530969 0.483952 11.00000 -1.50000 H3C 2 -0.016571 0.540894 0.423502 11.00000 -1.50000 AFIX 0 C4 1 0.033719 0.582026 0.314308 11.00000 0.05036 0.04526 = 0.06134 0.00192 0.00370 -0.01474 C5 1 0.031638 0.653760 0.312526 11.00000 0.05685 0.04469 = 0.06781 -0.00940 0.00651 -0.01572 AFIX 43 H4 2 0.052331 0.678257 0.355023 11.00000 -1.20000 AFIX 0 C6 1 0.000000 0.689328 0.250000 10.50000 0.04775 0.03316 = 0.08484 0.00000 0.01373 0.00000 AFIX 43 H5 2 -0.000003 0.737343 0.250002 10.50000 -1.20000 AFIX 0 C7 1 0.000000 0.547895 0.250000 10.50000 0.03413 0.03120 = 0.06598 0.00000 0.01134 0.00000 C8 1 0.039579 0.399177 0.184737 11.00000 0.04309 0.04774 = 0.04148 0.00782 0.01394 0.01642 C9 1 0.112160 0.412346 0.183700 11.00000 0.04485 0.06238 = 0.05406 0.00662 0.02050 0.01420 C10 1 0.139525 0.371281 0.138052 11.00000 0.05719 0.10085 = 0.08418 -0.01738 0.03730 0.00860 AFIX 43 H9 2 0.186702 0.379017 0.135011 11.00000 -1.20000 AFIX 0 C11 1 0.098916 0.319093 0.096809 11.00000 0.07797 0.12261 = 0.08842 -0.03986 0.04004 0.01435 AFIX 43 H10 2 0.119415 0.291542 0.067699 11.00000 -1.20000 AFIX 0 C12 1 0.028615 0.307810 0.098655 11.00000 0.06691 0.09809 = 0.07387 -0.03633 0.01543 0.00927 AFIX 43 H11 2 0.001739 0.272914 0.070101 11.00000 -1.20000 AFIX 0 C13 1 -0.003568 0.347483 0.142398 11.00000 0.04779 0.06824 = 0.04746 -0.00632 0.00672 0.01379 C14 1 0.159271 0.466722 0.228982 11.00000 0.04380 0.06187 = 0.09360 -0.00190 0.02646 0.00523 AFIX 13 H13 2 0.131838 0.486575 0.260678 11.00000 -1.20000 AFIX 0 C15 1 0.174930 0.524728 0.182547 11.00000 0.13459 0.08737 = 0.18499 0.04007 0.03861 -0.02116 AFIX 137 H14A 2 0.203058 0.507378 0.151637 11.00000 -1.50000 H14B 2 0.201815 0.560368 0.213362 11.00000 -1.50000 H14C 2 0.129870 0.543305 0.153128 11.00000 -1.50000 AFIX 0 C16 1 0.229916 0.436920 0.278521 11.00000 0.04523 0.08633 = 0.11716 -0.01006 0.00679 0.00138 AFIX 137 H15A 2 0.218556 0.399186 0.306152 11.00000 -1.50000 H15B 2 0.255108 0.472164 0.311119 11.00000 -1.50000 H15C 2 0.260310 0.420753 0.249305 11.00000 -1.50000 AFIX 0 C17 1 -0.082798 0.334549 0.139406 11.00000 0.04431 0.08542 = 0.07077 -0.02032 0.00418 0.00398 AFIX 13 H16 2 -0.096665 0.370344 0.169375 11.00000 -1.20000 AFIX 0 C18 1 -0.093085 0.265805 0.173261 11.00000 0.07312 0.11485 = 0.12088 -0.00650 0.01378 -0.02612 AFIX 137 H17A 2 -0.078179 0.229125 0.146684 11.00000 -1.50000 H17B 2 -0.143478 0.259987 0.171552 11.00000 -1.50000 H17C 2 -0.064113 0.264770 0.222987 11.00000 -1.50000 AFIX 0 C19 1 -0.132353 0.342959 0.063579 11.00000 0.06139 0.15831 = 0.08226 -0.02950 -0.01405 0.02827 AFIX 137 H18A 2 -0.122857 0.306859 0.032937 11.00000 -1.50000 H18B 2 -0.123611 0.386971 0.044412 11.00000 -1.50000 H18C 2 -0.182157 0.340406 0.065088 11.00000 -1.50000 AFIX 0 C20 1 0.932386 0.885094 0.244121 11.00000 0.02602 0.02690 = 0.02455 -0.00115 0.00350 0.00317 C21 1 0.891725 0.859625 0.176943 11.00000 0.02922 0.03184 = 0.02353 0.00136 0.00488 0.00205 AFIX 43 H20 2 0.897936 0.879415 0.134649 11.00000 -1.20000 AFIX 0 C22 1 0.842293 0.805771 0.170937 11.00000 0.02663 0.03305 = 0.02899 -0.00643 0.00127 0.00181 C23 1 0.831526 0.774511 0.232024 11.00000 0.03307 0.03166 = 0.03735 -0.00525 0.00962 -0.00554 AFIX 43 H22 2 0.798506 0.738450 0.228107 11.00000 -1.20000 AFIX 0 C24 1 0.871610 0.798595 0.299752 11.00000 0.03858 0.03350 = 0.02913 -0.00121 0.01113 -0.00144 C25 1 0.920372 0.852722 0.305317 11.00000 0.03251 0.03293 = 0.02299 -0.00355 0.00333 -0.00041 AFIX 43 H24 2 0.945977 0.868032 0.351337 11.00000 -1.20000 AFIX 0 C26 1 0.803181 0.781416 0.096183 11.00000 0.03334 0.04388 = 0.03387 -0.00907 0.00171 -0.00146 C27 1 0.862343 0.763826 0.366798 11.00000 0.06337 0.04730 = 0.03869 -0.00030 0.01776 -0.01532 C28 1 1.014578 0.990808 0.320233 11.00000 0.02981 0.02819 = 0.02963 0.00086 0.00300 -0.00035 C29 1 1.084023 1.017263 0.352516 11.00000 0.03199 0.03783 = 0.04672 -0.00803 0.00518 0.00030 AFIX 43 H28 2 1.122673 1.002788 0.335187 11.00000 -1.20000 AFIX 0 C30 1 1.097434 1.064255 0.409384 11.00000 0.03845 0.04576 = 0.06286 -0.02289 -0.00052 -0.00330 C31 1 1.041357 1.088014 0.435834 11.00000 0.05507 0.04841 = 0.05191 -0.02546 0.00336 -0.00022 AFIX 43 H30 2 1.050234 1.119483 0.474039 11.00000 -1.20000 AFIX 0 C32 1 0.971893 1.064030 0.404327 11.00000 0.04763 0.04067 = 0.04566 -0.01018 0.01466 0.00027 C33 1 0.959218 1.016032 0.347882 11.00000 0.03232 0.03467 = 0.03703 -0.00365 0.00696 -0.00184 AFIX 43 H32 2 0.911963 1.000253 0.327928 11.00000 -1.20000 AFIX 0 C34 1 1.173599 1.087802 0.443027 11.00000 0.04523 0.07528 = 0.12315 -0.05315 -0.00462 -0.00745 C35 1 0.910309 1.090818 0.430219 11.00000 0.06624 0.06298 = 0.07814 -0.02600 0.03301 0.00123 PART 1 F1 4 0.849187 0.757243 0.059871 11.00000 0.04687 0.06608 = 0.03478 -0.01832 0.00450 0.00706 F2 4 0.755842 0.730897 0.096334 11.00000 0.06079 0.07481 = 0.04739 -0.02112 0.00371 -0.03459 F3 4 0.765868 0.831835 0.054709 11.00000 0.05389 0.06438 = 0.03531 -0.00772 -0.01181 0.01572 F4 4 0.800422 0.781409 0.381646 10.70000 0.08366 0.12801 = 0.07257 0.03103 0.05559 0.01308 F5 4 0.853592 0.696868 0.359498 10.70000 0.17470 0.04495 = 0.05759 -0.00058 0.03925 -0.04248 F6 4 0.912190 0.781138 0.427817 10.70000 0.10641 0.07950 = 0.02529 0.00252 0.00613 -0.04337 F7 4 1.178623 1.153731 0.463228 10.60000 0.06003 0.06748 = 0.10543 -0.03531 -0.00280 -0.02088 F8 4 1.205740 1.060028 0.504022 10.20000 0.05954 0.08375 = 0.11717 0.02652 -0.03455 -0.00968 F9 4 1.210139 1.099953 0.393579 10.25000 0.05601 0.14077 = 0.10010 -0.03624 0.02815 -0.04625 F10 4 0.927558 1.132278 0.484901 21.00000 0.10561 0.13106 = 0.10563 -0.07115 0.05064 -0.00071 F11 4 0.863661 1.129087 0.377065 21.00000 0.09702 0.12980 = 0.13392 -0.00347 0.04615 0.06460 F12 4 0.868049 1.038080 0.443415 21.00000 0.08035 0.09046 = 0.10223 0.00542 0.05909 0.01086 PART 2 F4A 4 0.847124 0.808661 0.410993 10.20000 0.13364 0.08672 = 0.04845 -0.01249 0.06219 -0.02679 F5A 4 0.803040 0.731251 0.356879 10.20000 0.07067 0.10806 = 0.07360 0.02212 0.03226 -0.03604 F6A 4 0.924247 0.753561 0.412264 10.20000 0.09787 0.05654 = 0.01681 0.00932 -0.00321 -0.01871 F7A 4 1.183160 1.082658 0.530179 10.25000 0.08089 0.06937 = 0.03719 -0.00605 -0.02188 -0.01175 F8A 4 1.225583 1.042902 0.436133 10.25000 0.02666 0.12334 = 0.05962 -0.04586 0.00123 -0.00952 F9A 4 1.197373 1.130215 0.418219 10.30000 0.05855 0.08416 = 0.11311 0.01698 -0.00124 -0.02128 F10A 4 0.914873 1.157320 0.442826 31.00000 0.06530 0.03647 = 0.07098 -0.02008 0.01853 0.00415 F12A 4 0.902627 1.061745 0.489029 31.00000 0.09896 0.11067 = 0.06519 0.01854 0.04728 0.01614 F11A 4 0.843423 1.091086 0.374326 31.00000 0.04837 0.10439 = 0.08386 -0.01089 0.02090 0.02251 PART 3 F10B 4 0.933140 1.096203 0.507861 41.00000 0.09252 0.10119 = 0.04904 -0.02203 0.03583 0.00578 F11B 4 0.890835 1.151432 0.406624 41.00000 0.08862 0.09576 = 0.09361 0.00720 0.03579 0.05138 F12B 4 0.852387 1.055031 0.414224 41.00000 0.05619 0.07665 = 0.10968 -0.03613 0.04379 -0.01103 F6B 4 0.895175 0.703674 0.377117 10.30000 0.21840 0.10467 = 0.12085 0.07134 0.09887 0.08629 F7B 4 1.182502 1.117514 0.506375 10.25000 0.05732 0.08309 = 0.06938 -0.04313 -0.00550 -0.01475 F8B 4 1.219018 1.038540 0.462952 10.60000 0.04727 0.12571 = 0.07117 -0.01608 -0.00758 0.00848 F9B 4 1.199263 1.121461 0.371365 10.30000 0.04954 0.06288 = 0.08875 -0.00383 0.01569 -0.02375 PART 0 HKLF 4 REM 1_a.res in C2/c REM R1 = 0.0489 for 5117 Fo > 4sig(Fo) and 0.0580 for all 5971 data REM 583 parameters refined using 175 restraints END WGHT 0.0615 9.9827 REM Highest difference peak 0.593, deepest hole -0.334, 1-sigma level 0.048 Q1 1 0.0935 0.4678 0.3405 11.00000 0.05 0.59 Q2 1 0.0000 0.3458 0.2500 10.50000 0.05 0.41 Q3 1 -0.0361 0.3106 0.1877 11.00000 0.05 0.31 Q4 1 0.0402 0.4906 0.1819 11.00000 0.05 0.29 Q5 1 1.0023 0.9632 0.2885 11.00000 0.05 0.26 Q6 1 0.0000 0.5085 0.2500 10.50000 0.05 0.23 Q7 1 0.9600 0.9177 0.2449 11.00000 0.05 0.23 Q8 1 0.0376 0.5438 0.4297 11.00000 0.05 0.23 Q9 1 0.8243 0.7958 0.1401 11.00000 0.05 0.22 Q10 1 -0.0413 0.2291 0.1857 11.00000 0.05 0.22 Q11 1 -0.0873 0.2400 0.1266 11.00000 0.05 0.21 Q12 1 0.1156 0.5408 0.1034 11.00000 0.05 0.20 Q13 1 0.1442 0.3571 0.1881 11.00000 0.05 0.19 Q14 1 1.0730 1.0590 0.4421 11.00000 0.05 0.19 Q15 1 0.8178 0.8346 0.3983 11.00000 0.05 0.19 Q16 1 0.8748 0.8183 0.1752 11.00000 0.05 0.18 Q17 1 0.0127 0.5372 0.3593 11.00000 0.05 0.18 Q18 1 0.8686 0.7876 0.3285 11.00000 0.05 0.18 Q19 1 0.1552 0.5423 0.4726 11.00000 0.05 0.17 Q20 1 0.9417 1.0671 0.4229 11.00000 0.05 0.17 ; _shelx_res_checksum 13124 _shelx_hkl_file ; 4 0 0 2016.90 125.09 4 0 0 2078.09 125.19 -4 0 0 2224.68 125.19 -4 0 0 2222.08 125.19 -6 0 0 1808.82 101.29 6 0 0 1600.34 101.09 6 0 0 1727.23 101.19 -6 0 0 1755.82 101.19 8 0 0 1030.80 61.79 8 0 0 1059.69 61.99 -8 0 0 1062.09 62.19 10 0 0 135.69 8.80 10 0 0 125.39 8.40 12 0 0 947.71 56.19 12 0 0 942.61 55.89 14 0 0 93.29 7.60 14 0 0 84.69 6.60 16 0 0 174.78 12.80 16 0 0 182.88 11.90 18 0 0 88.29 8.90 18 0 0 77.19 7.10 20 0 0 5.70 4.80 20 0 0 4.70 3.70 22 0 0 4.10 5.50 22 0 0 3.00 4.40 -3 -1 0 4274.47 250.17 5 -1 0 1801.92 107.39 -5 -1 0 1981.70 107.69 -5 -1 0 1838.62 107.39 5 -1 0 1742.23 107.39 -5 1 0 1860.51 107.49 -5 1 0 1958.40 107.49 5 1 0 1765.22 107.59 5 1 0 1715.73 107.39 -7 -1 0 5982.60 362.16 -7 -1 0 6353.96 362.46 -7 1 0 6285.97 362.26 -7 1 0 6138.29 362.26 9 -1 0 81.19 6.00 9 -1 0 82.49 5.80 9 1 0 91.59 5.70 -9 1 0 80.19 6.50 9 1 0 80.39 6.20 11 -1 0 3.70 2.00 11 -1 0 4.00 2.10 11 1 0 5.60 2.40 11 1 0 6.40 1.80 13 -1 0 24.00 3.30 13 -1 0 22.20 3.00 13 1 0 21.40 2.80 13 1 0 17.80 3.50 15 -1 0 4.90 3.10 15 -1 0 7.60 2.80 15 1 0 9.10 2.60 15 1 0 3.00 3.50 17 -1 0 15.10 4.20 17 -1 0 22.60 3.60 17 1 0 24.50 4.80 17 1 0 20.00 3.40 19 -1 0 -0.40 4.30 19 -1 0 5.40 3.70 19 1 0 2.60 3.30 19 1 0 -2.20 4.40 21 -1 0 6.80 4.20 21 -1 0 7.90 5.10 21 1 0 0.80 4.00 21 1 0 11.20 5.70 23 -1 0 13.80 5.00 23 -1 0 21.60 6.60 23 1 0 19.40 4.90 23 1 0 16.60 6.80 0 -2 0 326.87 20.00 0 -2 0 354.76 20.10 -4 -2 0 6632.94 388.16 6 -2 0 693.13 41.60 -6 -2 0 741.23 42.00 6 -2 0 700.43 41.50 -6 -2 0 714.93 41.60 -6 2 0 710.03 41.60 -6 2 0 729.63 41.70 6 2 0 674.43 41.80 6 2 0 676.43 41.50 8 -2 0 9.60 1.80 -8 -2 0 8.60 1.90 8 -2 0 8.00 1.60 8 2 0 6.60 2.10 -8 2 0 10.50 1.90 10 -2 0 350.26 21.20 10 -2 0 347.27 21.30 -10 2 0 352.26 21.50 10 2 0 354.56 21.60 10 2 0 352.66 21.00 12 -2 0 41.40 4.70 12 -2 0 45.10 4.50 12 2 0 47.50 4.10 12 2 0 46.90 4.90 14 -2 0 18.40 3.20 14 -2 0 17.20 3.20 14 2 0 13.30 3.90 14 2 0 18.20 2.80 16 -2 0 75.09 7.20 16 -2 0 75.99 6.80 16 2 0 78.39 6.30 16 2 0 67.59 8.10 18 -2 0 81.09 7.30 18 -2 0 65.29 8.00 18 2 0 79.29 6.80 18 2 0 77.39 9.00 20 -2 0 44.60 6.10 20 -2 0 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7 9 4 952.10 54.59 9 -9 4 26.20 4.00 9 9 4 28.30 2.60 9 9 4 19.80 5.00 11 -9 4 18.00 4.00 11 9 4 15.40 2.30 11 9 4 19.60 5.70 13 -9 4 103.39 9.30 13 9 4 94.59 11.40 13 9 4 112.09 7.30 15 -9 4 135.49 10.60 15 9 4 115.19 13.10 15 9 4 129.69 8.80 17 -9 4 29.40 5.60 17 9 4 25.30 7.40 17 9 4 33.50 3.80 19 -9 4 57.09 7.00 19 9 4 55.69 6.30 19 9 4 77.99 10.00 22 -10 -4 7.40 5.30 22 10 -4 6.90 3.70 22 10 -4 9.80 8.20 20 -10 -4 1.70 3.50 20 -10 -4 2.30 4.40 -20 10 4 -6.20 4.40 20 10 -4 -0.80 6.70 20 10 -4 -2.40 3.00 18 -10 -4 17.80 4.40 18 -10 -4 20.30 3.80 -18 10 4 12.20 3.70 18 10 -4 14.30 3.00 18 10 -4 17.20 6.30 16 -10 -4 178.28 11.80 16 -10 -4 163.08 11.70 16 10 -4 172.98 10.70 16 10 -4 147.19 13.80 -16 10 4 156.68 11.50 14 -10 -4 66.69 6.50 14 -10 -4 53.09 6.10 14 10 -4 65.49 7.50 14 10 -4 67.19 5.00 -14 10 4 64.49 5.80 12 -10 -4 445.86 29.80 -12 -10 4 444.46 31.00 12 -10 -4 537.65 30.30 12 10 -4 522.85 29.40 -12 10 4 518.35 29.80 12 10 -4 498.65 31.10 10 -10 -4 1175.78 64.59 10 -10 -4 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4.30 12 -14 4 6.50 4.10 12 14 4 5.90 6.40 14 -14 4 36.00 5.50 14 -14 4 38.10 6.10 14 14 4 44.20 8.60 16 -14 4 30.30 5.90 16 -14 4 29.80 6.30 16 14 4 37.70 8.80 18 -14 4 10.30 5.70 18 -14 4 17.70 6.10 18 14 4 1.30 7.90 19 -15 -4 12.50 5.40 19 -15 -4 22.80 5.80 19 15 -4 12.20 7.70 17 -15 -4 15.00 5.20 17 -15 -4 11.10 4.80 17 15 -4 17.40 7.10 15 -15 -4 121.79 11.00 15 -15 -4 108.29 9.30 -15 -15 4 90.89 13.30 15 15 -4 113.89 12.80 -15 15 4 115.79 8.90 13 -15 -4 5.00 4.30 -13 -15 4 1.30 5.30 13 -15 -4 -2.90 3.20 -13 15 4 3.40 3.00 13 15 -4 -2.50 5.80 -11 -15 4 2.70 5.40 11 -15 -4 0.50 4.00 11 -15 -4 3.20 3.20 11 15 -4 3.00 5.30 -11 15 4 1.00 2.90 -9 -15 4 6.40 4.90 9 -15 -4 12.00 2.90 9 -15 -4 7.50 4.30 9 15 -4 9.50 5.20 -9 15 4 11.60 3.20 7 -15 -4 116.99 10.50 -7 -15 4 102.39 10.60 7 -15 -4 113.39 8.10 7 15 -4 139.19 10.40 -7 15 4 116.89 9.10 -5 -15 4 38.90 2.70 5 -15 -4 36.50 3.80 -5 -15 4 37.30 2.50 5 -15 -4 42.90 6.00 -5 -15 4 30.70 5.00 -5 15 4 33.60 4.50 5 15 -4 43.50 5.10 3 -15 -4 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7.20 1.60 10 12 5 5.90 5.70 12 -12 5 40.00 5.40 12 12 5 41.10 3.60 12 12 5 30.00 7.20 14 -12 5 4.70 4.60 14 12 5 4.20 2.10 14 12 5 -4.10 6.40 16 -12 5 12.80 5.60 16 12 5 37.80 8.60 16 12 5 20.30 2.80 18 -12 5 22.40 6.10 18 12 5 8.50 8.10 21 -13 -5 3.20 5.10 21 13 -5 6.00 7.90 19 -13 -5 15.00 5.20 19 -13 -5 18.20 4.90 19 13 -5 10.40 7.60 17 -13 -5 57.19 7.90 17 -13 -5 42.00 5.60 -17 13 5 58.99 6.40 17 13 -5 37.40 7.40 15 -13 -5 -3.00 3.30 15 -13 -5 -3.70 3.50 -15 -13 5 8.10 4.80 15 13 -5 0.30 5.40 -15 13 5 -3.90 2.90 13 -13 -5 8.50 3.80 -13 -13 5 1.20 4.70 13 -13 -5 8.50 3.40 -13 13 5 6.10 2.90 13 13 -5 10.80 5.40 -11 -13 5 100.99 10.80 11 -13 -5 111.49 7.90 11 -13 -5 90.49 9.40 -11 -13 5 105.19 6.90 -11 13 5 121.09 8.10 11 13 -5 109.59 9.90 -9 -13 5 702.73 42.00 9 -13 -5 715.23 43.70 9 -13 -5 675.63 42.50 -9 -13 5 704.03 43.90 -9 13 5 760.22 42.70 9 13 -5 732.73 43.60 -7 -13 5 212.08 13.10 -7 -13 5 233.38 15.20 -7 -13 5 222.28 13.40 7 -13 -5 216.18 15.40 7 -13 -5 212.78 13.60 7 13 -5 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32.80 3.40 13 13 5 31.50 7.70 15 -13 5 88.99 9.50 15 13 5 71.09 10.90 17 -13 5 72.69 8.00 17 13 5 63.19 10.10 20 -14 -5 4.00 5.10 20 14 -5 11.70 7.50 18 -14 -5 4.40 4.70 18 -14 -5 2.90 4.40 18 14 -5 2.40 7.20 16 -14 -5 94.29 8.90 16 -14 -5 102.49 10.30 -16 14 5 112.99 8.50 16 14 -5 83.49 10.20 -14 -14 5 108.59 12.60 14 -14 -5 121.39 9.30 14 -14 -5 120.69 10.90 14 14 -5 109.99 12.00 -14 14 5 122.09 9.10 12 -14 -5 209.68 14.90 -12 -14 5 186.58 16.30 12 -14 -5 188.08 13.30 12 14 -5 218.78 15.60 -12 14 5 212.18 13.40 -10 -14 5 265.47 19.30 -10 -14 5 256.67 16.40 -10 -14 5 269.47 16.30 10 -14 -5 283.27 18.70 10 -14 -5 278.27 17.10 -10 14 5 290.07 17.40 10 14 -5 275.17 18.50 8 -14 -5 106.79 9.80 -8 -14 5 92.29 9.70 -8 -14 5 115.39 6.80 8 -14 -5 97.39 7.50 -8 -14 5 105.79 6.40 -8 14 5 102.69 8.10 8 14 -5 101.39 9.60 -6 -14 5 399.06 23.20 -6 -14 5 401.66 24.70 -6 -14 5 365.06 22.90 6 -14 -5 371.36 23.30 6 -14 -5 383.46 25.30 6 14 -5 414.86 24.60 -6 14 5 393.46 24.00 -4 -14 5 530.55 31.00 4 -14 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15 11 6 16.20 3.10 15 11 6 18.30 7.60 17 -11 6 -0.50 5.40 17 11 6 -1.80 7.90 17 11 6 -5.80 2.90 19 -11 6 9.50 6.30 19 11 6 27.80 9.50 20 -12 -6 3.50 4.90 20 12 -6 16.40 3.60 20 12 -6 2.80 6.70 -20 12 6 -1.70 4.50 18 -12 -6 -0.80 4.20 18 -12 -6 4.40 4.10 -18 12 6 6.80 3.90 18 12 -6 -3.90 6.10 16 -12 -6 134.49 10.80 16 -12 -6 130.39 10.00 -16 12 6 130.79 10.00 16 12 -6 119.99 12.50 14 -12 -6 108.99 8.60 14 -12 -6 120.99 10.00 -14 -12 6 119.79 11.10 -14 12 6 109.69 8.80 14 12 -6 122.89 11.50 -12 -12 6 78.09 9.10 12 -12 -6 91.89 8.40 12 -12 -6 75.09 6.90 -12 12 6 90.39 7.10 12 12 -6 74.99 8.70 10 -12 -6 226.58 15.60 -10 -12 6 219.98 13.60 10 -12 -6 221.88 14.30 -10 -12 6 217.48 15.70 -10 12 6 237.88 14.50 10 12 -6 230.88 15.70 -8 -12 6 5.00 1.40 -8 -12 6 -1.00 2.90 8 -12 -6 -1.70 3.40 8 -12 -6 3.10 2.30 -8 12 6 2.60 2.70 8 12 -6 -1.80 3.30 -6 -12 6 184.78 12.50 6 -12 -6 202.58 14.90 -6 -12 6 222.38 14.00 6 -12 -6 205.48 12.90 -6 -12 6 212.88 13.00 6 12 -6 219.88 14.10 -6 12 6 213.68 13.60 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29.70 9.40 21 -13 -6 15.60 5.60 21 13 -6 15.40 8.50 19 -13 -6 69.19 7.10 19 -13 -6 68.09 8.60 19 13 -6 58.59 9.40 -19 13 6 61.39 6.50 17 -13 -6 12.20 4.30 17 -13 -6 4.90 4.10 17 13 -6 11.80 6.50 -17 13 6 10.40 3.90 15 -13 -6 64.59 6.00 15 -13 -6 53.19 7.60 -15 13 6 59.99 6.80 15 13 -6 56.79 8.00 13 -13 -6 13.90 4.20 13 -13 -6 12.10 3.30 -13 -13 6 14.50 5.30 13 13 -6 11.80 5.60 -13 13 6 8.30 3.20 -11 -13 6 355.96 22.60 -11 -13 6 383.76 25.10 11 -13 -6 369.26 23.20 11 13 -6 395.16 24.80 -11 13 6 402.66 23.40 -9 -13 6 511.45 29.80 9 -13 -6 493.05 30.30 9 -13 -6 467.75 31.60 -9 -13 6 535.75 31.80 9 13 -6 515.55 31.50 -9 13 6 506.35 30.60 -7 -13 6 199.28 13.10 -7 -13 6 169.58 11.00 -7 -13 6 189.78 11.50 7 -13 -6 177.88 11.60 7 -13 -6 156.28 13.40 7 13 -6 197.98 13.00 -7 13 6 193.58 12.30 -5 -13 6 3.60 2.20 5 -13 -6 -2.60 3.50 -5 -13 6 2.30 2.70 -5 -13 6 4.70 1.40 5 -13 -6 1.10 1.90 -5 13 6 -1.60 2.90 5 13 -6 7.30 3.20 -3 -13 6 106.09 7.90 3 -13 -6 101.49 10.50 -3 -13 6 116.79 9.10 3 -13 -6 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6.90 -16 -14 6 47.80 7.90 16 -14 -6 66.09 6.40 16 -14 -6 53.09 8.60 16 14 -6 54.29 8.30 -16 14 6 69.79 7.40 14 -14 -6 40.40 5.10 14 -14 -6 34.90 5.80 -14 -14 6 43.20 7.20 -14 14 6 49.00 5.00 14 14 -6 36.00 6.80 -12 -14 6 0.70 4.70 12 -14 -6 -4.20 3.70 12 -14 -6 -2.30 3.10 12 14 -6 2.70 5.00 -12 14 6 0.00 3.00 10 -14 -6 4.60 4.20 10 -14 -6 8.30 2.90 -10 -14 6 5.30 4.30 -10 -14 6 1.00 1.40 10 14 -6 5.50 4.40 -10 14 6 11.50 3.30 -8 -14 6 10.40 2.20 8 -14 -6 6.10 4.50 8 -14 -6 8.40 2.50 -8 -14 6 6.30 1.40 -8 -14 6 6.10 3.90 -8 14 6 7.80 3.20 8 14 -6 8.50 4.30 -6 -14 6 2.80 1.30 6 -14 -6 -2.20 2.00 -6 -14 6 3.90 2.10 -6 -14 6 3.00 3.30 6 -14 -6 -0.80 4.00 6 14 -6 5.00 3.60 -6 14 6 0.80 3.20 -4 -14 6 41.50 4.30 4 -14 -6 35.80 5.90 4 -14 -6 36.10 3.80 -4 -14 6 38.30 5.90 -4 14 6 39.50 5.00 4 14 -6 39.20 4.70 2 -14 -6 109.29 7.30 -2 -14 6 118.79 7.90 2 -14 -6 107.49 11.40 -2 -14 6 115.39 9.40 -2 14 6 93.09 9.30 2 14 -6 111.29 8.50 0 -14 -6 146.29 15.00 0 -14 6 188.18 13.20 0 -14 6 186.88 12.20 0 14 6 186.98 13.70 0 14 -6 187.68 12.20 0 14 6 200.08 11.40 2 -14 6 82.19 6.30 2 -14 6 80.79 6.80 2 -14 6 75.29 8.10 -2 -14 -6 68.79 10.30 -2 14 -6 88.29 6.20 2 14 6 82.79 5.30 2 14 6 70.19 8.60 4 -14 6 4.60 1.40 -4 -14 -6 6.70 4.80 4 -14 6 8.40 3.90 4 -14 6 0.90 3.20 4 14 6 2.80 1.50 4 14 6 3.30 1.10 -4 14 -6 5.80 1.60 4 14 6 1.70 5.50 6 -14 6 40.80 5.10 6 14 6 41.20 7.30 6 14 6 42.60 2.90 8 -14 6 167.88 12.50 8 14 6 154.88 14.50 8 14 6 179.28 10.30 10 -14 6 10.70 4.40 10 14 6 8.50 6.70 10 14 6 4.10 1.40 12 -14 6 93.09 9.20 12 14 6 82.09 11.00 14 -14 6 2.70 4.90 14 14 6 10.20 7.50 16 -14 6 9.70 5.80 16 14 6 -7.30 8.50 19 -15 -6 -0.70 4.90 19 -15 -6 4.20 5.10 19 15 -6 -8.40 7.40 17 -15 -6 3.70 4.60 17 -15 -6 -3.10 4.40 -17 15 6 0.20 4.20 17 15 -6 -4.50 7.00 15 -15 -6 7.30 4.00 -15 -15 6 15.00 6.20 15 -15 -6 6.30 4.60 15 15 -6 20.80 6.30 -15 15 6 9.00 4.00 -13 -15 6 -2.20 5.50 13 -15 -6 1.30 3.40 13 -15 -6 -0.80 4.10 13 15 -6 0.10 5.20 -13 15 6 4.40 3.50 -11 -15 6 10.50 5.30 -11 -15 6 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-15 -6 9.50 5.60 5 -15 6 19.90 4.80 5 15 6 20.20 6.10 7 -15 6 13.00 4.60 7 -15 6 27.90 4.50 7 15 6 25.00 7.40 9 -15 6 37.70 5.30 9 -15 6 37.50 6.20 9 15 6 33.40 7.80 11 -15 6 59.29 6.70 11 15 6 54.49 9.50 13 -15 6 15.40 5.50 13 15 6 11.00 8.30 15 -15 6 12.40 6.00 15 15 6 17.20 8.80 18 -16 -6 -9.80 4.90 18 -16 -6 14.10 5.60 18 16 -6 4.70 7.30 16 -16 -6 48.70 6.10 -16 -16 6 37.30 8.10 16 -16 -6 50.09 7.10 -16 16 6 53.69 6.10 16 16 -6 48.00 8.30 -14 -16 6 40.90 7.90 14 -16 -6 43.60 6.90 14 -16 -6 51.69 5.60 14 16 -6 34.10 7.20 -14 16 6 58.89 5.90 12 -16 -6 2.30 3.40 12 -16 -6 0.30 4.60 -12 -16 6 -3.80 5.20 12 16 -6 -0.10 5.50 -12 16 6 3.90 3.70 10 -16 -6 37.10 4.40 -10 -16 6 39.60 6.80 10 -16 -6 45.30 6.90 -10 16 6 44.90 5.20 10 16 -6 46.40 6.80 8 -16 -6 48.80 7.30 -8 -16 6 62.39 4.50 8 -16 -6 66.59 5.70 -8 -16 6 54.49 8.90 -8 16 6 70.29 7.30 8 16 -6 74.09 8.60 -6 -16 6 4.00 2.00 6 -16 -6 5.70 2.40 6 -16 -6 0.80 4.70 -6 -16 6 3.20 3.90 -6 16 6 6.00 4.10 6 16 -6 4.00 4.20 4 -16 -6 279.87 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6 184.88 13.60 5 17 6 128.59 15.00 7 -17 6 18.20 4.30 7 -17 6 14.90 5.00 7 17 6 12.00 7.40 9 -17 6 112.19 9.20 9 -17 6 92.49 10.90 9 17 6 82.19 11.10 11 -17 6 32.40 5.70 11 -17 6 24.10 6.30 11 17 6 22.10 9.10 13 -17 6 49.60 6.70 13 -17 6 21.80 6.40 13 17 6 35.50 9.10 15 -17 6 5.30 6.00 15 -17 6 -0.60 6.00 -16 -18 6 18.80 8.20 16 -18 -6 18.70 6.50 16 -18 -6 19.10 5.20 16 18 -6 22.70 8.00 14 -18 -6 67.69 6.60 -14 -18 6 65.49 9.90 14 -18 -6 56.89 8.20 14 18 -6 50.69 8.60 -14 18 6 66.89 6.90 12 -18 -6 53.09 8.00 -12 -18 6 58.49 8.90 12 -18 -6 59.99 6.80 -12 18 6 66.39 6.80 12 18 -6 103.09 11.20 10 -18 -6 33.30 4.20 10 -18 -6 32.00 6.70 -10 -18 6 31.80 6.90 10 18 -6 29.40 6.80 -10 18 6 23.00 5.20 -8 -18 6 18.60 5.80 8 -18 -6 27.60 6.70 8 -18 -6 23.30 3.60 -8 18 6 25.50 5.20 8 18 -6 33.30 6.40 6 -18 -6 31.60 7.20 6 -18 -6 37.40 3.90 -6 -18 6 38.30 6.20 -6 18 6 39.60 6.20 6 18 -6 54.19 6.50 4 -18 -6 18.40 2.60 -4 -18 6 14.60 5.20 4 -18 -6 6.80 6.00 -4 -18 6 16.40 2.50 4 18 -6 13.80 4.80 -4 18 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12.90 7.10 11 -15 7 11.20 5.00 11 15 7 16.00 8.30 13 -15 7 65.59 7.60 13 15 7 53.19 9.70 15 -15 7 85.09 8.90 15 15 7 79.79 12.30 18 -16 -7 74.69 11.00 18 -16 -7 62.89 7.30 18 16 -7 55.49 10.10 -16 -16 7 36.80 8.00 16 -16 -7 44.30 7.00 16 -16 -7 56.09 6.30 16 16 -7 39.40 8.40 -16 16 7 53.59 6.10 -14 -16 7 72.39 12.00 14 -16 -7 74.79 10.50 14 -16 -7 80.89 7.90 -14 16 7 89.09 8.60 14 16 -7 91.29 10.00 12 -16 -7 25.90 4.10 12 -16 -7 17.20 5.60 -12 -16 7 19.60 6.10 -12 16 7 27.70 4.50 12 16 -7 21.10 6.60 -10 -16 7 482.45 31.50 10 -16 -7 480.75 31.80 -10 -16 7 506.65 29.10 10 -16 -7 458.35 29.60 -10 16 7 481.45 30.20 10 16 -7 526.15 31.30 -8 -16 7 690.53 39.90 -8 -16 7 700.33 41.80 8 -16 -7 644.44 40.20 8 -16 -7 618.24 42.30 8 16 -7 693.63 41.50 -8 16 7 694.53 40.90 6 -16 -7 126.29 13.20 -6 -16 7 165.18 11.90 -6 -16 7 148.59 9.70 6 -16 -7 139.79 9.80 -6 16 7 138.39 11.60 6 16 -7 151.98 11.90 -4 -16 7 14.40 4.00 4 -16 -7 4.40 5.50 -4 -16 7 27.00 3.30 4 -16 -7 20.50 2.70 -4 16 7 20.50 5.20 4 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5.00 12 6 9 70.39 8.70 12 6 9 68.89 7.50 14 -6 9 59.69 7.60 14 6 9 63.89 8.80 14 6 9 68.69 6.80 16 -6 9 49.70 7.50 16 6 9 51.19 6.30 16 6 9 50.49 8.80 18 -6 9 40.60 7.40 18 6 9 42.10 6.10 18 6 9 24.20 8.80 23 -7 -9 29.30 5.50 -23 7 9 19.50 7.40 23 7 -9 24.40 4.80 23 7 -9 20.10 8.90 21 -7 -9 8.90 4.50 21 7 -9 -5.30 5.90 21 7 -9 11.20 3.80 -21 7 9 8.80 6.10 19 -7 -9 21.00 4.30 19 7 -9 26.60 6.80 -19 7 9 33.70 6.30 19 7 -9 28.80 4.20 17 -7 -9 175.98 12.50 17 7 -9 175.18 14.90 17 7 -9 195.58 12.40 -17 7 9 196.48 14.50 15 -7 -9 2.90 3.10 15 7 -9 -0.90 4.20 15 7 -9 1.00 2.70 -15 7 9 1.80 4.20 13 -7 -9 29.40 4.50 13 -7 -9 38.10 4.20 -13 -7 9 46.90 4.90 -13 7 9 51.49 5.40 13 7 -9 38.10 5.40 11 -7 -9 52.99 4.50 11 -7 -9 38.30 5.00 -11 7 9 35.40 4.00 11 7 -9 54.29 6.10 -11 7 9 63.69 6.20 9 -7 -9 337.67 20.10 -9 -7 9 334.77 20.00 9 7 -9 311.77 20.60 -9 7 9 319.67 20.40 7 -7 -9 20.80 3.00 -7 7 9 23.40 3.30 7 7 -9 13.10 3.30 5 -7 -9 1206.98 69.69 -5 7 9 1134.79 69.99 5 7 -9 1203.48 70.09 3 7 -9 23.40 3.00 -3 7 9 19.70 3.00 -1 -7 9 992.60 59.89 -1 7 9 1020.20 59.89 1 -7 9 489.35 28.80 1 -7 9 425.26 28.10 1 -7 9 484.85 28.10 1 7 9 484.15 28.80 3 -7 9 204.08 12.50 3 -7 9 203.38 12.50 3 -7 9 203.08 13.80 3 7 9 208.08 14.00 5 -7 9 37.10 3.20 5 -7 9 38.90 4.90 5 -7 9 38.00 3.30 5 7 9 28.20 5.10 5 7 9 39.50 4.30 7 -7 9 20.80 2.40 7 -7 9 21.80 4.70 7 -7 9 19.60 2.40 7 7 9 16.50 5.00 7 7 9 17.70 3.70 9 -7 9 136.19 11.40 9 7 9 150.08 10.80 9 7 9 161.08 13.30 11 -7 9 4.70 4.70 11 7 9 2.20 6.10 11 7 9 6.80 3.80 13 -7 9 47.30 6.70 13 7 9 40.60 5.50 13 7 9 42.50 8.20 15 -7 9 -6.50 5.60 15 7 9 -0.80 4.30 15 7 9 -3.60 6.80 17 -7 9 20.60 6.30 17 7 9 17.00 5.20 17 7 9 14.90 8.40 22 -8 -9 4.20 4.80 22 8 -9 0.90 3.90 22 8 -9 4.50 7.60 -22 8 9 4.20 6.30 20 -8 -9 16.90 4.70 20 8 -9 16.10 6.60 -20 8 9 11.50 5.90 20 8 -9 17.90 4.00 18 -8 -9 12.40 3.80 18 8 -9 17.50 6.50 -18 8 9 18.90 5.40 18 8 -9 14.40 3.60 16 -8 -9 215.28 14.50 16 8 -9 203.08 16.30 16 8 -9 227.18 14.10 -16 8 9 224.78 15.70 14 -8 -9 35.60 4.30 14 -8 -9 27.60 3.80 -14 -8 9 38.30 5.40 -14 8 9 38.20 5.20 14 8 -9 28.10 5.50 12 -8 -9 5.50 3.00 -12 -8 9 6.60 2.60 12 -8 -9 4.70 2.60 -12 8 9 7.90 3.30 12 8 -9 2.90 3.80 10 -8 -9 267.57 17.20 -10 -8 9 298.27 17.30 10 8 -9 257.57 18.10 -10 8 9 276.07 17.70 -8 -8 9 124.79 8.60 8 -8 -9 126.99 8.70 -8 8 9 126.49 9.00 8 8 -9 126.89 9.40 6 -8 -9 564.44 32.20 6 8 -9 524.65 32.70 -6 8 9 525.65 32.60 4 8 -9 26.10 3.50 -4 8 9 27.30 3.70 -2 -8 9 28.20 3.80 2 8 -9 18.10 2.90 -2 8 9 18.80 3.30 0 -8 9 10.40 2.70 0 -8 9 11.90 2.30 0 -8 9 14.50 3.50 0 8 9 13.80 3.40 2 -8 9 699.23 40.80 2 -8 9 635.34 39.80 2 -8 9 671.73 39.80 2 8 9 691.83 40.80 4 -8 9 94.49 8.20 4 -8 9 87.19 5.80 4 -8 9 88.79 5.80 4 8 9 85.79 8.00 4 8 9 87.19 7.20 6 -8 9 189.08 13.70 6 8 9 211.88 13.20 6 8 9 190.68 14.30 8 -8 9 162.98 12.60 8 8 9 175.28 11.60 8 8 9 156.88 13.80 10 -8 9 20.30 5.50 10 8 9 24.30 4.30 10 8 9 20.10 6.80 12 -8 9 31.50 5.80 12 8 9 16.80 7.70 12 8 9 31.30 4.50 14 -8 9 17.40 5.70 14 8 9 10.00 7.10 14 8 9 15.00 4.60 16 -8 9 54.59 7.60 16 8 9 53.59 6.20 16 8 9 49.40 9.40 18 -8 9 11.00 6.50 18 8 9 1.30 4.70 18 8 9 -11.40 8.40 21 -9 -9 5.40 4.70 -21 9 9 2.00 5.80 21 9 -9 0.10 7.00 21 9 -9 5.90 3.90 19 -9 -9 3.10 4.20 19 9 -9 1.90 3.50 -19 9 9 -3.10 5.00 19 9 -9 0.80 6.20 17 -9 -9 2.70 2.80 17 -9 -9 -5.30 3.50 17 9 -9 0.70 3.10 17 9 -9 0.50 4.90 -17 9 9 -5.00 4.20 15 -9 -9 18.90 3.50 15 -9 -9 20.90 4.00 -15 -9 9 16.70 3.60 -15 9 9 40.00 5.00 15 9 -9 23.00 5.60 13 -9 -9 62.09 6.00 13 -9 -9 47.20 6.10 -13 -9 9 54.99 6.50 13 9 -9 53.19 6.50 -13 9 9 59.59 7.00 11 -9 -9 336.37 21.00 -11 -9 9 370.46 21.40 11 -9 -9 295.97 21.60 -11 9 9 371.76 21.60 11 9 -9 341.27 22.20 -9 -9 9 198.48 11.90 9 -9 -9 163.08 11.60 9 -9 -9 152.68 12.50 9 9 -9 184.78 12.70 -9 9 9 193.68 12.30 7 -9 -9 154.18 10.00 -7 -9 9 156.98 10.20 7 9 -9 139.19 10.80 -7 9 9 146.49 10.50 5 -9 -9 8.70 3.40 5 -9 -9 19.70 2.80 5 9 -9 16.20 3.30 -5 9 9 13.20 3.00 -3 9 9 452.65 25.80 3 9 -9 383.96 25.40 -1 -9 9 977.10 57.59 -1 9 9 939.11 57.69 1 9 -9 984.00 57.29 1 -9 9 1434.06 85.49 1 -9 9 1451.25 84.99 1 -9 9 1399.46 84.79 1 9 9 1484.85 85.59 3 -9 9 0.60 1.60 3 -9 9 1.80 1.50 3 -9 9 4.40 3.60 3 9 9 2.20 3.70 5 -9 9 14.70 4.20 5 9 9 17.70 3.30 5 9 9 7.20 5.00 7 -9 9 324.57 20.80 7 9 9 309.77 22.00 7 9 9 325.77 20.10 9 9 9 131.69 12.40 9 9 9 100.39 8.50 11 -9 9 6.00 5.10 11 9 9 2.10 3.40 11 9 9 1.10 6.50 13 -9 9 2.90 4.90 13 9 9 -3.00 7.10 13 9 9 -1.50 3.80 15 -9 9 8.00 6.00 15 9 9 19.60 8.40 15 9 9 12.40 4.40 17 -9 9 3.80 6.60 17 9 9 -3.70 8.50 17 9 9 -5.40 4.10 22 -10 -9 29.60 5.80 22 10 -9 25.40 4.80 22 10 -9 18.10 8.10 -22 10 9 18.80 6.50 20 -10 -9 5.50 4.60 20 10 -9 3.70 6.90 20 10 -9 1.10 3.60 -20 10 9 4.20 5.30 18 -10 -9 50.59 5.60 18 -10 -9 58.99 6.50 -18 10 9 43.10 6.30 18 10 -9 45.70 7.40 16 -10 -9 60.69 6.80 16 -10 -9 66.79 6.90 -16 -10 9 60.29 7.40 16 10 -9 51.79 7.40 -16 10 9 61.79 6.50 14 -10 -9 20.00 3.70 -14 -10 9 22.70 4.30 14 -10 -9 22.00 4.10 14 10 -9 23.40 5.80 -14 10 9 20.30 4.30 -12 -10 9 37.90 5.70 12 -10 -9 30.70 4.50 12 -10 -9 38.30 4.10 -12 10 9 40.40 4.60 12 10 -9 38.50 5.80 -10 -10 9 630.74 35.40 10 -10 -9 587.94 35.00 10 -10 -9 504.95 35.80 10 10 -9 569.04 35.90 -10 10 9 622.74 35.40 8 -10 -9 29.00 4.80 -8 -10 9 38.00 4.90 8 -10 -9 37.70 4.00 -8 10 9 36.50 4.30 -6 -10 9 17.70 3.10 6 -10 -9 32.20 3.30 6 -10 -9 21.60 4.30 6 10 -9 18.30 3.50 -6 10 9 21.60 3.50 4 -10 -9 9.80 3.90 -4 10 9 13.90 3.50 4 10 -9 15.90 3.20 -2 -10 9 477.85 30.00 2 10 -9 505.05 29.90 -2 10 9 493.45 30.10 0 -10 9 144.59 10.10 0 -10 9 111.89 8.90 0 10 9 145.69 10.40 0 10 -9 148.39 9.20 2 -10 9 184.48 11.30 2 -10 9 169.28 12.60 2 -10 9 180.68 11.30 2 10 9 168.38 13.00 4 -10 9 71.69 7.20 4 -10 9 81.29 5.40 4 -10 9 75.39 5.10 4 10 9 82.09 6.60 4 10 9 95.19 9.20 6 -10 9 37.30 5.50 6 10 9 36.40 6.70 6 10 9 40.60 4.40 8 -10 9 265.57 18.90 8 10 9 289.37 17.80 8 10 9 284.17 20.60 10 -10 9 42.40 6.60 10 10 9 50.19 8.50 10 10 9 47.70 4.80 12 -10 9 25.00 5.50 12 10 9 33.80 8.40 12 10 9 34.00 4.40 14 -10 9 8.80 5.90 14 10 9 6.30 3.90 14 10 9 6.40 7.50 16 -10 9 16.50 6.40 16 10 9 21.60 9.30 16 10 9 11.30 4.30 21 -11 -9 3.40 4.80 21 11 -9 8.00 8.10 -21 11 9 6.30 5.80 19 -11 -9 -0.80 4.10 -19 11 9 2.30 4.80 19 11 -9 -0.60 6.50 17 -11 -9 16.00 4.00 17 -11 -9 13.50 3.90 17 11 -9 11.40 5.70 -17 11 9 12.60 4.60 15 -11 -9 83.69 8.50 -15 -11 9 94.99 9.40 15 -11 -9 93.49 7.90 -15 11 9 93.19 8.90 15 11 -9 97.39 10.60 13 -11 -9 99.09 9.20 -13 -11 9 107.49 9.40 13 -11 -9 103.99 8.30 13 11 -9 100.49 10.40 -13 11 9 111.59 9.00 -11 -11 9 -1.50 3.00 11 -11 -9 -3.70 2.70 11 -11 -9 0.10 3.10 -11 11 9 2.20 3.20 11 11 -9 -1.60 4.10 -9 -11 9 155.68 9.90 9 -11 -9 122.29 10.90 9 -11 -9 138.29 9.30 9 11 -9 132.49 10.70 -9 11 9 108.39 9.90 7 -11 -9 87.89 9.20 7 -11 -9 94.89 7.20 -7 -11 9 101.39 8.10 -7 11 9 104.69 8.20 7 11 -9 102.19 8.60 -5 -11 9 138.79 9.80 5 -11 -9 131.29 8.90 5 -11 -9 108.59 11.20 -5 11 9 135.29 9.80 5 11 -9 142.39 9.80 3 -11 -9 224.68 17.40 -3 -11 9 242.08 15.70 -3 11 9 248.48 16.20 3 11 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-12 -9 25.80 5.10 12 12 -9 42.80 6.40 -12 12 9 39.60 4.80 -10 -12 9 3.40 3.20 10 -12 -9 5.00 3.90 10 -12 -9 1.80 3.00 10 12 -9 5.60 4.10 -10 12 9 8.70 3.70 8 -12 -9 1542.85 102.69 -8 -12 9 1871.71 102.09 8 -12 -9 1736.43 101.49 -8 12 9 1755.92 101.89 8 12 -9 1707.23 102.19 6 -12 -9 1028.50 61.19 -6 -12 9 1033.50 61.79 -6 12 9 994.00 61.69 6 12 -9 1086.29 61.99 -4 -12 9 143.79 10.80 4 -12 -9 128.89 12.40 -4 -12 9 154.18 10.50 4 12 -9 153.28 10.70 -4 12 9 170.88 11.10 2 -12 -9 266.57 21.90 -2 -12 9 314.27 20.30 2 12 -9 366.56 20.20 -2 12 9 333.67 20.50 0 -12 9 1221.38 74.59 0 12 -9 1165.58 74.19 0 12 9 1390.26 75.19 2 -12 9 114.39 9.80 2 -12 9 127.39 8.90 2 -12 9 134.39 8.80 2 12 9 125.39 11.30 4 -12 9 346.37 22.30 4 12 9 357.16 21.30 4 12 9 328.97 23.30 6 -12 9 49.70 6.30 6 12 9 56.49 5.70 8 -12 9 87.89 8.70 8 12 9 55.79 8.60 8 12 9 59.69 6.20 10 -12 9 22.40 5.40 10 12 9 30.60 3.80 10 12 9 26.90 8.10 12 -12 9 38.90 6.20 12 12 9 49.20 9.20 12 12 9 34.60 4.30 14 -12 9 47.10 7.60 14 12 9 29.10 9.10 14 12 9 34.00 4.50 16 -12 9 36.40 7.70 16 12 9 62.79 11.30 19 -13 -9 9.90 5.20 19 13 -9 16.90 7.60 -19 13 9 17.40 5.30 17 -13 -9 42.10 6.10 17 -13 -9 38.20 5.40 -17 -13 9 32.30 6.40 17 13 -9 35.40 7.30 -17 13 9 40.70 5.60 15 -13 -9 58.99 8.50 -15 -13 9 65.29 10.30 15 -13 -9 73.29 7.30 -15 13 9 71.99 8.00 15 13 -9 64.29 8.50 13 -13 -9 11.70 4.40 13 -13 -9 7.10 3.50 -13 -13 9 8.70 4.70 -13 13 9 17.00 4.40 13 13 -9 7.40 5.30 11 -13 -9 40.80 6.00 11 -13 -9 50.69 4.80 -11 -13 9 32.40 5.20 -11 13 9 47.60 5.30 11 13 -9 40.10 6.00 -9 -13 9 45.20 6.40 9 -13 -9 35.80 6.10 9 -13 -9 53.49 4.80 -9 13 9 47.90 5.40 9 13 -9 42.10 5.90 7 -13 -9 25.20 5.60 -7 -13 9 36.50 4.40 -7 -13 9 44.30 6.20 7 -13 -9 32.80 3.90 7 13 -9 39.00 5.20 -7 13 9 37.40 4.90 -5 -13 9 9.00 3.10 5 -13 -9 11.60 2.70 -5 -13 9 10.10 3.30 5 -13 -9 2.40 4.50 -5 13 9 9.40 3.70 5 13 -9 10.90 3.80 -3 -13 9 18.40 3.80 3 -13 -9 8.30 4.80 -3 -13 9 16.10 3.70 -3 13 9 18.20 4.20 3 13 -9 18.20 3.60 1 -13 -9 43.90 7.60 -1 -13 9 71.99 6.70 1 13 -9 71.49 6.20 -1 13 9 61.99 6.80 1 -13 9 283.27 18.70 1 -13 9 319.27 19.30 1 13 9 275.27 19.90 -1 13 -9 313.47 18.50 3 -13 9 12.00 2.30 3 -13 9 8.10 4.10 3 -13 9 4.00 2.00 3 13 9 3.60 5.40 5 -13 9 20.00 4.90 5 13 9 6.70 6.10 5 13 9 13.10 3.10 7 -13 9 -8.00 4.20 7 13 9 -0.80 6.10 7 13 9 2.90 2.90 9 -13 9 48.20 6.70 9 13 9 59.69 5.60 9 13 9 59.99 9.10 11 -13 9 24.70 6.10 11 13 9 17.70 8.80 11 13 9 31.70 3.70 13 -13 9 57.79 7.30 13 13 9 46.70 9.70 13 13 9 38.90 4.40 15 -13 9 -1.30 6.60 15 13 9 -15.70 8.90 20 -14 -9 3.10 5.00 -20 14 9 -5.10 5.30 20 14 -9 7.30 7.80 18 -14 -9 52.79 6.50 18 -14 -9 57.59 9.20 18 14 -9 53.59 8.90 -18 14 9 46.70 6.60 16 -14 -9 80.79 10.30 -16 -14 9 87.79 11.40 16 -14 -9 91.09 8.40 16 14 -9 78.79 9.70 -16 14 9 100.99 9.40 14 -14 -9 134.19 10.30 -14 -14 9 127.39 12.80 14 -14 -9 128.29 12.20 14 14 -9 143.49 13.10 -14 14 9 138.99 10.90 12 -14 -9 31.80 5.90 12 -14 -9 29.00 4.50 -12 -14 9 31.50 5.60 12 14 -9 37.90 6.60 -12 14 9 26.40 4.80 10 -14 -9 566.14 34.90 10 -14 -9 526.65 36.70 -10 -14 9 637.04 36.10 -10 14 9 573.14 35.50 10 14 -9 600.94 36.40 -8 -14 9 2.60 3.40 -8 -14 9 -0.40 3.00 8 -14 -9 -2.80 4.70 8 -14 -9 2.10 2.80 8 14 -9 2.70 4.50 -8 14 9 1.80 3.70 -6 -14 9 55.59 5.80 6 -14 -9 47.30 5.20 -6 -14 9 61.99 7.00 6 -14 -9 39.00 6.80 -6 14 9 51.29 6.00 6 14 -9 48.70 5.70 4 -14 -9 192.88 16.70 -4 -14 9 218.08 14.20 -4 -14 9 210.08 14.80 4 14 -9 232.28 14.70 -4 14 9 216.78 15.00 -2 -14 9 163.08 12.60 2 -14 -9 150.18 14.60 -2 -14 9 169.78 11.70 2 14 -9 187.68 11.80 -2 14 9 155.68 12.70 0 -14 9 7.20 4.00 0 -14 9 13.40 4.00 0 -14 -9 4.60 5.40 0 14 -9 17.70 3.20 0 14 9 9.00 5.10 2 -14 9 402.76 23.80 2 -14 9 401.36 24.70 2 14 9 365.76 25.60 4 -14 9 3.80 4.40 4 14 9 0.60 6.20 4 14 9 10.40 3.00 6 -14 9 6.90 4.70 6 14 9 10.70 3.10 6 14 9 12.30 7.10 8 -14 9 -3.90 4.80 8 14 9 -2.30 6.10 8 14 9 1.00 2.60 10 -14 9 24.30 5.80 10 14 9 39.70 9.10 10 14 9 28.50 3.50 12 -14 9 13.30 5.90 12 14 9 10.20 9.00 14 -14 9 8.50 6.20 14 14 9 14.90 9.70 19 -15 -9 51.49 6.70 19 15 -9 48.00 9.10 -19 15 9 48.10 7.10 -17 -15 9 52.69 8.20 17 -15 -9 53.49 7.40 17 -15 -9 74.19 7.00 -17 15 9 63.29 6.80 17 15 -9 54.99 9.30 15 -15 -9 20.30 4.80 -15 -15 9 26.10 6.50 15 -15 -9 22.40 5.70 15 15 -9 20.20 7.00 -15 15 9 30.30 5.20 13 -15 -9 61.19 5.90 13 -15 -9 60.59 9.80 -13 -15 9 64.39 7.90 -13 15 9 57.29 6.30 13 15 -9 54.19 7.80 11 -15 -9 -2.60 4.70 11 -15 -9 0.20 3.20 -11 -15 9 2.90 4.40 11 15 -9 -0.90 5.30 -11 15 9 7.20 3.90 9 -15 -9 99.39 8.00 -9 -15 9 108.89 8.10 9 -15 -9 85.89 11.40 -9 -15 9 105.59 9.90 -9 15 9 115.69 9.60 9 15 -9 103.59 10.50 7 -15 -9 461.45 29.20 -7 -15 9 489.45 29.50 7 -15 -9 428.36 31.70 -7 -15 9 531.75 30.50 -7 15 9 477.05 30.10 7 15 -9 520.75 30.60 5 -15 -9 1.40 5.40 -5 -15 9 13.60 3.50 5 -15 -9 10.20 2.90 -5 -15 9 12.80 4.00 5 15 -9 8.50 4.00 -5 15 9 -0.10 4.10 -3 -15 9 79.19 8.60 3 -15 -9 75.19 11.20 3 15 -9 97.59 8.00 -1 -15 9 9.90 3.90 1 -15 -9 0.60 5.20 -1 -15 9 5.70 4.10 1 15 -9 12.10 3.40 -1 15 9 5.60 4.70 -1 -15 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15.90 -8 16 9 255.87 16.90 8 16 -9 266.77 17.60 -6 -16 9 92.69 7.70 -6 -16 9 104.39 9.20 6 -16 -9 90.49 7.20 6 -16 -9 74.69 11.90 6 16 -9 108.29 9.80 -6 16 9 77.09 9.40 -4 -16 9 15.40 3.50 4 -16 -9 8.70 5.90 -4 -16 9 7.10 4.30 4 16 -9 4.90 4.10 -4 16 9 3.10 4.80 -2 -16 9 88.59 9.60 2 -16 -9 78.79 12.30 -2 -16 9 96.89 8.10 -2 16 9 97.99 10.30 2 16 -9 93.79 8.30 0 -16 -9 583.14 42.80 0 -16 9 672.33 40.00 0 -16 9 670.73 41.00 0 16 9 717.73 41.50 2 -16 9 30.00 5.00 2 -16 9 19.60 4.90 2 16 9 24.80 7.00 4 -16 9 38.20 5.50 4 -16 9 21.40 5.60 4 16 9 25.40 7.30 4 16 9 34.90 3.70 6 -16 9 8.20 4.60 6 16 9 4.20 7.50 8 -16 9 5.70 4.80 8 16 9 2.00 7.70 10 -16 9 3.70 5.60 10 16 9 -9.30 8.10 12 -16 9 2.20 5.80 12 16 9 10.10 9.50 -17 -17 9 50.29 9.00 17 -17 -9 48.20 6.40 17 -17 -9 40.70 7.70 17 17 -9 49.00 9.50 -17 17 9 62.79 7.30 15 -17 -9 51.99 6.20 -15 -17 9 42.90 8.40 15 -17 -9 46.10 7.80 15 17 -9 47.20 8.50 -15 17 9 59.49 7.10 13 -17 -9 23.40 4.40 13 -17 -9 18.20 6.40 -13 -17 9 17.10 6.40 -13 17 9 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18.70 16 4 -10 264.67 17.00 -16 4 10 270.47 19.50 14 -4 -10 6.60 2.90 14 4 -10 6.00 4.60 -14 4 10 6.70 4.50 14 4 -10 4.70 2.90 -12 -4 10 11.60 1.70 12 -4 -10 4.30 2.70 -12 4 10 9.60 4.40 12 4 -10 8.90 4.00 12 4 -10 10.90 2.80 -10 -4 10 3.50 1.40 10 -4 -10 0.80 2.60 -10 4 10 5.40 1.70 -10 4 10 6.60 3.60 10 4 -10 5.60 3.40 8 -4 -10 5.90 2.30 8 4 -10 3.80 3.00 -8 4 10 7.40 2.80 -8 4 10 8.40 2.10 6 4 -10 74.69 6.50 -6 4 10 82.69 6.80 -4 -4 10 200.28 13.40 -4 4 10 193.38 12.80 -2 -4 10 463.45 28.10 -2 4 10 461.25 28.10 0 -4 10 199.78 13.10 0 4 10 214.88 13.40 2 -4 10 269.87 16.80 2 -4 10 279.07 17.70 2 4 10 276.47 17.40 4 -4 10 419.86 25.50 4 -4 10 439.46 26.40 -4 4 -10 425.76 25.70 4 4 10 411.16 26.10 4 4 10 421.96 26.20 6 -4 10 50.49 5.10 6 -4 10 57.49 6.20 -6 4 -10 54.79 5.20 6 4 10 56.69 5.80 6 4 10 45.80 5.80 8 -4 10 20.10 3.60 8 -4 10 18.00 4.90 8 4 10 21.30 4.60 8 4 10 16.90 4.80 10 -4 10 7.90 3.50 10 -4 10 8.40 5.10 10 4 10 -0.40 5.30 10 4 10 2.50 4.10 12 -4 10 38.90 6.40 12 -4 10 32.40 4.50 12 4 10 35.30 6.90 12 4 10 26.00 5.20 14 -4 10 -1.20 5.20 14 -4 10 0.20 3.20 14 4 10 4.50 4.80 14 4 10 -2.20 6.10 16 -4 10 54.49 7.80 16 4 10 49.60 7.10 16 4 10 48.70 8.60 18 -4 10 -3.30 6.70 18 4 10 1.70 5.70 18 4 10 2.40 7.30 23 -5 -10 -0.50 4.80 -23 5 10 -3.40 7.10 23 5 -10 16.10 8.00 23 5 -10 -0.50 4.20 21 -5 -10 2.40 4.20 -21 5 10 10.90 6.90 21 5 -10 5.60 3.90 21 5 -10 8.50 7.40 19 -5 -10 3.60 3.80 19 5 -10 0.60 3.50 -19 5 10 1.20 5.80 19 5 -10 -9.90 5.80 17 -5 -10 232.68 15.30 -17 5 10 230.88 17.40 17 5 -10 214.88 17.40 17 5 -10 238.48 15.00 15 -5 -10 461.45 28.30 15 5 -10 468.25 28.10 15 5 -10 447.66 29.60 -15 5 10 476.15 29.80 -13 -5 10 191.48 11.70 13 -5 -10 182.28 12.30 13 5 -10 169.18 13.80 -13 5 10 191.48 13.80 13 5 -10 196.88 12.30 11 -5 -10 26.10 3.40 -11 -5 10 27.60 3.20 -11 5 10 24.50 4.60 11 5 -10 28.40 4.50 -11 5 10 35.10 3.60 9 -5 -10 19.70 3.30 -9 5 10 18.50 3.90 -9 5 10 25.30 3.60 9 5 -10 28.70 4.40 7 -5 -10 292.97 17.20 7 5 -10 278.67 17.80 -7 5 10 259.47 17.50 5 5 -10 111.29 8.30 -5 5 10 112.09 8.20 -3 -5 10 288.47 18.40 -3 5 10 289.57 18.10 -1 -5 10 35.90 4.20 -1 5 10 33.70 3.90 1 -5 10 27.10 4.00 1 -5 10 25.40 3.00 1 5 10 36.50 4.00 3 -5 10 35.00 4.10 3 -5 10 35.40 3.90 3 -5 10 51.99 5.50 3 5 10 37.00 4.40 5 -5 10 3.90 2.10 5 -5 10 8.30 3.80 5 5 10 1.00 3.60 5 5 10 7.30 3.40 7 -5 10 14.70 4.40 7 -5 10 13.00 2.90 -7 5 -10 14.80 2.90 7 5 10 14.60 4.10 7 5 10 9.70 4.10 9 -5 10 51.39 5.60 9 -5 10 50.59 6.50 -9 5 -10 37.80 4.10 9 5 10 39.80 5.50 9 5 10 42.40 6.80 11 -5 10 16.20 3.40 11 -5 10 26.10 5.70 11 5 10 23.90 6.70 11 5 10 18.60 4.80 13 -5 10 19.50 5.60 13 -5 10 16.00 3.20 13 5 10 18.70 6.80 13 5 10 16.20 4.90 15 -5 10 8.40 5.90 15 5 10 9.60 7.00 15 5 10 5.50 5.00 17 -5 10 7.60 6.30 17 5 10 8.20 5.50 17 5 10 4.00 7.60 22 -6 -10 3.60 4.90 22 6 -10 -3.50 3.90 22 6 -10 1.60 7.40 -22 6 10 -12.20 6.30 20 -6 -10 49.10 5.90 20 6 -10 44.80 5.30 20 6 -10 43.80 8.00 -20 6 10 45.40 7.90 18 -6 -10 111.69 9.40 -18 6 10 119.19 11.60 18 6 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2.50 8 6 10 1.70 5.10 8 6 10 13.70 4.10 10 -6 10 27.00 3.30 10 -6 10 31.10 5.90 10 6 10 33.90 6.90 -10 6 -10 27.90 3.40 10 6 10 32.20 5.10 12 -6 10 1.20 2.30 12 -6 10 3.90 5.50 12 6 10 6.50 4.30 12 6 10 3.70 6.30 14 -6 10 8.60 5.50 14 6 10 -1.10 4.70 14 6 10 3.50 6.90 16 -6 10 -6.80 5.80 16 6 10 -7.50 7.30 16 6 10 14.20 5.30 18 -6 10 5.20 6.70 18 6 10 -15.30 8.00 18 6 10 8.30 5.60 23 -7 -10 4.10 5.10 -23 7 10 2.60 6.90 23 7 -10 3.00 4.40 23 7 -10 15.60 9.00 21 -7 -10 -0.80 4.40 21 7 -10 8.10 7.40 -21 7 10 2.30 6.20 21 7 -10 1.20 3.90 19 -7 -10 1.90 3.90 19 7 -10 2.60 3.50 19 7 -10 2.70 6.40 -19 7 10 -0.30 5.30 17 -7 -10 0.10 3.60 -17 7 10 -4.70 4.70 17 7 -10 -4.40 5.40 17 7 -10 -0.30 3.20 15 -7 -10 39.80 4.80 -15 -7 10 31.50 4.30 -15 7 10 40.80 5.90 15 7 -10 34.20 6.10 13 -7 -10 142.79 10.60 -13 -7 10 165.28 10.70 13 7 -10 158.68 12.60 -13 7 10 158.08 11.90 11 -7 -10 113.89 8.30 -11 -7 10 111.89 7.80 -11 7 10 110.59 9.10 11 7 -10 101.09 9.90 -9 -7 10 132.79 8.60 9 -7 -10 108.99 8.80 9 7 -10 118.49 9.90 -9 7 10 137.69 9.60 7 -7 -10 154.58 9.90 7 7 -10 153.38 10.80 -7 7 10 139.19 10.50 5 7 -10 226.08 14.70 -5 7 10 225.28 14.50 3 7 -10 58.09 5.40 -3 7 10 49.10 5.20 -1 -7 10 90.79 7.50 -1 -7 10 82.09 7.10 -1 7 10 89.99 7.10 1 -7 10 14.70 3.60 1 -7 10 6.30 2.10 1 -7 10 5.10 2.10 1 7 10 6.10 3.10 3 -7 10 373.86 21.70 3 -7 10 339.67 20.20 3 -7 10 349.07 20.20 3 7 10 278.37 21.20 5 -7 10 100.59 9.10 5 -7 10 97.09 6.70 5 -7 10 102.49 6.80 5 7 10 89.59 8.80 5 7 10 114.29 8.30 7 -7 10 164.78 10.70 7 -7 10 177.98 11.10 7 -7 10 170.68 13.00 7 7 10 189.88 12.40 7 7 10 171.68 13.70 9 -7 10 17.70 2.00 9 -7 10 10.90 2.10 9 -7 10 3.00 4.70 9 7 10 16.90 4.30 9 7 10 8.50 6.00 11 -7 10 1.60 1.50 11 -7 10 -1.30 4.90 11 7 10 4.30 4.30 11 7 10 -3.50 6.00 13 -7 10 13.00 5.50 13 7 10 11.30 7.30 13 7 10 19.00 4.80 15 -7 10 -7.80 5.10 15 7 10 6.70 4.90 15 7 10 -0.50 7.50 17 -7 10 38.90 7.60 17 7 10 34.70 6.00 17 7 10 21.90 9.10 22 -8 -10 60.79 6.90 22 8 -10 47.10 5.70 -22 8 10 49.40 8.20 22 8 -10 48.60 9.80 20 -8 -10 39.40 5.50 20 8 -10 22.80 7.70 20 8 -10 29.40 4.70 -20 8 10 33.50 6.60 18 -8 -10 184.98 14.10 18 8 -10 223.98 13.70 -18 8 10 221.18 16.00 18 8 -10 188.48 16.50 16 -8 -10 526.85 32.80 -16 8 10 548.65 33.60 16 8 -10 541.05 34.30 -14 -8 10 162.98 11.40 14 -8 -10 159.48 11.10 -14 8 10 170.08 12.60 14 8 -10 160.08 13.10 -12 -8 10 612.44 35.10 12 -8 -10 589.04 35.00 12 8 -10 533.65 35.70 -12 8 10 578.94 35.50 10 -8 -10 1010.70 59.39 -10 -8 10 1026.80 59.49 10 8 -10 967.00 60.19 8 -8 -10 520.95 30.00 -8 -8 10 465.85 30.00 8 8 -10 489.15 30.70 -8 8 10 515.45 30.40 6 -8 -10 0.90 2.40 6 8 -10 1.70 2.80 -6 8 10 5.30 2.90 -4 8 10 1315.17 78.29 4 8 -10 1325.67 78.19 -2 -8 10 46.60 5.10 2 8 -10 51.99 5.10 -2 8 10 54.89 6.00 0 -8 10 4.70 2.40 0 -8 10 4.50 3.10 0 8 10 1.00 3.20 2 -8 10 29.30 2.90 2 -8 10 32.90 3.10 2 -8 10 22.30 4.40 2 8 10 24.00 4.40 4 -8 10 487.45 28.30 4 -8 10 465.35 29.60 4 -8 10 469.45 28.30 4 8 10 497.35 29.20 4 8 10 462.35 29.80 6 -8 10 31.20 3.40 6 -8 10 37.50 5.40 6 -8 10 30.20 2.90 6 8 10 36.50 6.10 6 8 10 32.70 4.40 8 -8 10 25.60 5.60 8 8 10 28.80 6.70 8 8 10 23.90 4.40 10 -8 10 13.40 5.50 10 8 10 10.80 4.30 10 8 10 14.90 6.70 12 -8 10 16.60 5.60 12 8 10 11.90 7.30 12 8 10 13.70 4.40 14 -8 10 26.30 6.10 14 8 10 22.30 8.30 14 8 10 17.00 4.90 16 -8 10 1.10 6.40 16 8 10 -0.70 4.70 16 8 10 -5.30 8.10 21 -9 -10 0.70 4.60 21 9 -10 4.50 7.60 -21 9 10 5.60 5.90 21 9 -10 0.90 4.10 19 -9 -10 77.19 8.30 -19 9 10 86.79 10.10 19 9 -10 69.69 9.40 17 -9 -10 4.70 3.60 17 9 -10 8.30 6.10 -17 9 10 5.40 4.80 -15 -9 10 57.19 6.60 15 -9 -10 56.29 5.60 15 9 -10 57.19 7.60 -15 9 10 43.10 6.00 13 -9 -10 723.93 44.20 -13 -9 10 764.82 44.60 13 9 -10 746.43 45.40 -13 9 10 722.63 44.80 11 -9 -10 48.30 6.50 -11 -9 10 72.79 6.20 11 -9 -10 70.79 6.40 11 9 -10 67.09 7.50 -11 9 10 69.59 6.80 9 -9 -10 29.20 3.50 -9 -9 10 28.70 4.20 9 -9 -10 16.30 3.70 9 9 -10 30.60 4.60 -9 9 10 21.50 3.70 -7 -9 10 26.50 4.20 7 -9 -10 21.20 3.20 -7 9 10 27.60 4.00 7 9 -10 23.40 4.20 -5 9 10 175.38 11.90 5 9 -10 179.08 12.30 3 9 -10 1223.08 73.29 -3 9 10 1250.57 73.49 -1 -9 10 810.22 47.60 -1 9 10 772.92 47.60 1 -9 10 346.27 21.50 1 -9 10 376.36 21.70 1 -9 10 356.56 22.70 1 9 10 342.27 22.40 3 -9 10 220.58 15.50 3 -9 10 243.88 14.10 3 -9 10 226.18 14.10 3 9 10 221.58 16.10 5 -9 10 268.97 16.00 5 -9 10 270.37 16.00 5 -9 10 266.47 18.00 5 9 10 266.67 17.10 5 9 10 262.87 18.60 7 -9 10 281.87 18.60 7 9 10 276.77 19.50 7 9 10 276.67 17.90 9 -9 10 42.80 6.30 9 9 10 40.30 5.10 9 9 10 27.30 7.30 11 -9 10 42.70 6.80 11 9 10 49.30 5.30 11 9 10 21.50 7.80 13 -9 10 24.00 6.10 13 9 10 3.00 7.80 13 9 10 3.80 4.40 15 -9 10 20.10 6.30 15 9 10 33.40 5.40 15 9 10 26.60 9.20 17 -9 10 38.30 7.70 17 9 10 25.20 5.50 17 9 10 24.10 9.70 22 -10 -10 52.89 6.90 22 10 -10 60.49 10.20 -22 10 10 29.30 7.30 20 -10 -10 65.79 7.20 20 10 -10 76.99 10.10 -20 10 10 63.79 7.80 18 -10 -10 176.88 13.10 -18 10 10 202.08 14.30 18 10 -10 170.78 15.70 -16 -10 10 300.67 19.90 16 -10 -10 330.27 19.70 16 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10 10 32.30 4.30 6 10 10 32.10 6.20 8 -10 10 4.10 5.00 8 10 10 10.80 3.70 8 10 10 10.20 6.60 10 -10 10 112.89 11.30 10 10 10 133.59 13.80 10 10 10 115.39 9.60 12 -10 10 64.79 8.00 12 10 10 65.59 6.30 12 10 10 54.49 9.70 14 -10 10 4.90 6.00 14 10 10 3.00 8.10 14 10 10 14.30 4.50 16 -10 10 14.90 6.80 16 10 10 5.90 4.70 16 10 10 4.40 9.30 21 -11 -10 23.50 5.90 -21 11 10 21.70 6.30 21 11 -10 22.90 8.10 19 -11 -10 10.70 4.60 19 11 -10 12.20 7.20 -19 11 10 14.10 5.30 17 -11 -10 68.99 6.70 -17 -11 10 62.99 8.10 17 -11 -10 67.09 7.60 -17 11 10 66.49 7.10 17 11 -10 76.19 9.00 15 -11 -10 46.10 4.80 -15 -11 10 35.80 5.30 15 -11 -10 31.90 4.90 -15 11 10 38.60 5.30 15 11 -10 33.40 6.60 13 -11 -10 19.10 4.00 -13 -11 10 20.70 4.10 13 -11 -10 14.90 3.70 -13 11 10 26.40 4.50 13 11 -10 21.40 5.30 -11 -11 10 612.14 33.90 11 -11 -10 463.25 34.10 11 -11 -10 555.24 33.30 -11 11 10 565.44 33.80 11 11 -10 564.94 34.40 9 -11 -10 57.39 8.20 -9 -11 10 76.19 6.90 9 -11 -10 74.89 6.40 -9 11 10 77.79 7.50 9 11 -10 70.39 8.00 7 -11 -10 22.30 3.50 -7 -11 10 19.20 3.50 7 -11 -10 13.50 4.50 7 11 -10 21.20 4.50 -7 11 10 20.80 4.10 -5 -11 10 363.66 20.70 5 -11 -10 267.57 21.60 5 11 -10 347.17 20.70 -5 11 10 318.57 20.60 -3 -11 10 448.36 27.90 3 11 -10 476.95 27.90 -3 11 10 435.66 28.20 -1 -11 10 188.18 12.90 -1 11 10 193.38 13.30 1 11 -10 170.98 12.10 1 -11 10 582.94 35.40 1 -11 10 645.04 35.60 1 -11 10 493.25 36.00 1 11 10 643.94 36.70 3 -11 10 112.39 9.70 3 -11 10 109.79 7.30 3 -11 10 111.39 7.60 3 11 10 107.19 10.60 5 -11 10 45.90 6.20 5 11 10 42.60 4.80 5 11 10 43.30 6.70 7 -11 10 69.09 7.30 7 11 10 42.30 7.80 7 11 10 52.79 5.40 9 -11 10 -1.60 5.00 9 11 10 -4.90 3.20 9 11 10 -10.70 6.40 11 -11 10 10.10 5.90 11 11 10 5.10 7.30 11 11 10 4.60 3.60 13 -11 10 15.80 6.60 13 11 10 22.00 4.60 13 11 10 15.80 8.50 15 -11 10 45.90 7.90 15 11 10 38.20 5.40 15 11 10 38.30 10.50 20 -12 -10 9.20 4.80 20 12 -10 5.40 7.10 -20 12 10 8.50 5.50 18 -12 -10 132.69 10.50 18 -12 -10 96.39 10.60 -18 12 10 161.18 11.50 18 12 -10 149.99 13.70 -16 -12 10 86.29 9.50 16 -12 -10 87.39 7.90 16 -12 -10 77.89 8.40 16 12 -10 75.79 8.80 -16 12 10 68.79 8.60 14 -12 -10 59.69 8.20 14 -12 -10 68.29 7.00 -14 -12 10 72.89 8.50 -14 12 10 64.39 7.60 14 12 -10 69.59 8.00 12 -12 -10 95.19 7.80 -12 -12 10 96.69 8.90 12 -12 -10 78.39 9.30 -12 12 10 90.99 8.50 12 12 -10 98.49 10.10 10 -12 -10 328.27 20.70 10 -12 -10 275.97 22.00 -10 -12 10 377.06 21.40 10 12 -10 346.17 22.00 -10 12 10 338.87 21.30 8 -12 -10 622.64 37.00 -8 -12 10 636.34 37.60 -8 12 10 606.54 37.60 8 12 -10 602.34 37.90 6 -12 -10 228.88 18.80 -6 -12 10 264.77 17.50 6 -12 -10 276.47 17.00 -6 12 10 286.87 17.80 6 12 -10 302.67 18.00 4 -12 -10 77.69 10.20 -4 -12 10 123.99 8.50 -4 -12 10 104.89 8.60 4 12 -10 112.89 8.70 -4 12 10 95.89 9.10 -2 -12 10 311.27 19.90 -2 12 10 296.67 20.20 2 12 -10 321.07 19.60 0 -12 10 -1.40 3.60 0 12 10 2.10 4.20 0 12 -10 2.00 2.60 2 -12 10 269.07 18.50 2 -12 10 294.57 17.40 2 -12 10 271.67 17.50 2 12 10 288.97 19.50 4 -12 10 43.10 6.20 4 12 10 45.00 4.80 4 12 10 40.50 6.80 6 -12 10 53.79 6.80 6 12 10 54.59 5.20 6 12 10 45.20 7.60 8 -12 10 27.60 6.00 8 12 10 16.30 7.70 8 12 10 30.20 4.20 10 -12 10 17.60 5.50 10 12 10 25.10 3.70 10 12 10 12.90 7.40 12 -12 10 6.10 5.70 12 12 10 -8.00 7.60 12 12 10 4.10 3.90 14 -12 10 13.30 6.50 14 12 10 0.20 3.80 14 12 10 5.20 8.30 19 -13 -10 3.30 4.80 -19 13 10 5.90 5.30 19 13 -10 -3.00 7.20 17 -13 -10 11.10 4.70 -17 -13 10 8.80 4.80 17 -13 -10 11.40 4.70 17 13 -10 7.70 6.90 -17 13 10 6.80 4.70 15 -13 -10 7.30 4.20 15 -13 -10 0.40 3.70 -15 -13 10 4.20 5.10 -15 13 10 0.00 4.20 15 13 -10 -2.20 5.30 -13 -13 10 174.78 14.30 13 -13 -10 198.98 12.90 13 -13 -10 174.18 14.20 -13 13 10 196.38 13.70 13 13 -10 201.98 15.10 11 -13 -10 56.99 6.20 11 -13 -10 49.90 6.90 -11 -13 10 61.09 7.20 -11 13 10 60.99 6.10 11 13 -10 50.49 6.70 9 -13 -10 3.30 3.00 9 -13 -10 -2.30 4.20 -9 -13 10 4.10 3.20 9 13 -10 5.90 4.30 -9 13 10 3.60 3.90 -7 -13 10 540.75 31.70 7 -13 -10 525.25 30.90 7 -13 -10 441.06 32.90 -7 13 10 510.85 31.60 7 13 -10 543.25 31.90 -5 -13 10 226.88 15.00 5 -13 -10 201.58 17.10 -5 -13 10 216.48 15.30 -5 13 10 238.08 15.60 5 13 -10 256.27 15.70 -3 -13 10 4.80 3.30 -3 -13 10 5.20 3.60 3 -13 -10 0.70 4.50 3 13 -10 2.00 3.20 -3 13 10 0.60 4.00 -1 -13 10 72.59 7.50 1 13 -10 73.49 6.80 -1 13 10 68.79 7.60 1 -13 10 77.29 7.20 1 -13 10 75.79 7.80 1 13 10 79.49 9.50 3 -13 10 52.59 6.30 3 -13 10 60.49 5.00 3 -13 10 47.10 4.50 3 13 10 57.79 5.30 3 13 10 42.80 7.20 5 -13 10 19.60 5.10 5 13 10 20.50 3.80 5 13 10 25.30 6.90 7 -13 10 29.20 5.70 7 13 10 10.80 7.50 7 13 10 24.20 3.80 9 -13 10 3.70 4.90 9 13 10 3.90 3.20 9 13 10 9.10 7.60 11 -13 10 5.40 5.30 11 13 10 0.60 3.10 11 13 10 -5.50 8.40 13 -13 10 88.49 9.50 13 13 10 63.29 10.80 15 -13 10 52.89 8.60 15 13 10 40.90 11.60 20 -14 -10 -13.00 5.30 -20 14 10 -3.80 5.50 20 14 -10 -1.90 8.00 18 -14 -10 11.10 4.70 18 -14 -10 7.90 5.00 18 14 -10 2.20 7.20 -18 14 10 10.10 5.40 16 -14 -10 6.40 5.00 16 -14 -10 2.30 4.40 -16 -14 10 9.50 5.30 -16 14 10 15.00 5.00 16 14 -10 -1.40 6.50 14 -14 -10 6.30 4.90 -14 -14 10 4.00 4.90 14 -14 -10 5.10 3.80 -14 14 10 3.90 4.30 14 14 -10 7.80 6.20 12 -14 -10 58.49 5.40 12 -14 -10 41.90 6.80 -12 -14 10 53.39 6.50 -12 14 10 48.10 5.90 12 14 -10 60.99 7.50 10 -14 -10 39.20 6.70 -10 -14 10 48.20 7.40 10 -14 -10 55.59 5.80 -10 14 10 57.19 6.10 10 14 -10 56.69 7.00 -8 -14 10 13.20 3.80 8 -14 -10 9.80 3.20 8 -14 -10 6.60 5.20 -8 -14 10 12.20 3.70 8 14 -10 7.40 4.50 -8 14 10 13.40 4.40 6 -14 -10 24.10 6.20 -6 -14 10 30.30 4.80 6 -14 -10 34.30 4.00 -6 -14 10 39.40 4.50 -6 14 10 32.60 5.20 6 14 -10 45.20 5.70 -4 -14 10 110.59 8.70 -4 -14 10 89.29 8.90 4 -14 -10 76.39 10.90 4 14 -10 117.89 9.20 -4 14 10 109.39 9.50 2 -14 -10 0.10 5.10 -2 -14 10 3.30 3.80 -2 -14 10 1.70 4.00 -2 14 10 5.50 4.60 2 14 -10 3.00 3.40 0 -14 10 294.37 20.00 0 14 -10 325.87 19.60 0 14 10 309.77 20.90 2 -14 10 12.60 4.70 2 -14 10 10.90 2.90 2 14 10 4.30 5.90 4 -14 10 114.59 10.00 4 14 10 102.79 12.40 4 14 10 103.19 8.20 6 -14 10 83.29 8.00 6 14 10 47.10 8.80 6 14 10 76.89 6.80 8 -14 10 11.10 5.50 8 14 10 12.90 7.90 8 14 10 15.80 3.40 10 -14 10 46.90 6.80 10 14 10 59.99 10.00 10 14 10 50.39 5.50 12 -14 10 29.00 7.20 12 14 10 12.20 9.80 14 -14 10 14.00 7.20 14 14 10 32.40 10.80 19 -15 -10 -6.90 5.10 19 15 -10 12.60 8.10 -19 15 10 -0.20 5.70 17 -15 -10 -1.40 4.50 17 -15 -10 1.80 5.20 -17 -15 10 4.60 5.50 17 15 -10 -11.30 6.60 -17 15 10 4.70 5.20 15 -15 -10 3.60 3.90 -15 -15 10 6.80 5.70 15 -15 -10 6.60 5.30 -15 15 10 4.60 4.60 15 15 -10 16.10 6.50 13 -15 -10 44.60 5.40 13 -15 -10 40.40 6.90 -13 -15 10 53.89 7.00 13 15 -10 45.50 7.50 -13 15 10 47.40 6.00 -11 -15 10 76.09 8.80 11 -15 -10 54.19 7.80 11 -15 -10 77.99 6.90 11 15 -10 76.89 8.40 -11 15 10 65.49 7.90 -9 -15 10 0.80 3.20 9 -15 -10 0.00 5.00 9 -15 -10 4.60 3.20 -9 -15 10 2.00 3.70 -9 15 10 4.10 4.30 9 15 -10 -5.00 4.50 -7 -15 10 13.90 4.20 7 -15 -10 5.60 5.50 -7 -15 10 18.20 3.90 7 -15 -10 12.00 3.30 -7 15 10 13.90 4.60 7 15 -10 11.10 5.00 5 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10.10 5.10 -12 16 10 10.30 4.80 12 16 -10 6.80 6.00 10 -16 -10 41.70 4.70 10 -16 -10 26.20 6.80 -10 -16 10 35.20 5.70 -10 -16 10 48.60 4.70 -10 16 10 41.50 6.10 10 16 -10 40.20 7.00 -8 -16 10 51.89 5.20 8 -16 -10 46.70 4.90 -8 -16 10 52.39 8.10 8 16 -10 55.19 7.00 -8 16 10 41.40 6.20 6 -16 -10 152.38 15.60 6 -16 -10 162.58 11.80 -6 -16 10 178.28 12.50 -6 -16 10 195.08 13.60 -6 16 10 173.28 13.60 6 16 -10 202.68 14.00 -4 -16 10 7.70 4.40 4 -16 -10 3.30 6.00 -4 -16 10 6.80 3.90 -4 16 10 13.80 5.40 4 16 -10 15.30 4.50 -2 -16 10 42.20 6.00 -2 -16 10 49.00 5.70 2 -16 -10 29.60 8.00 -2 16 10 50.09 6.90 2 16 -10 54.19 5.60 0 -16 10 8.10 4.50 0 -16 10 11.40 4.50 0 16 10 5.30 6.10 0 16 -10 12.60 3.70 2 -16 10 122.49 10.60 2 -16 10 128.19 11.70 2 -16 10 128.89 9.60 2 16 10 121.29 12.50 4 -16 10 6.00 4.80 4 16 10 11.70 3.40 4 16 10 2.20 7.20 6 -16 10 44.10 6.30 6 16 10 29.70 5.30 6 16 10 37.10 9.10 8 -16 10 -9.40 4.60 8 16 10 0.10 7.60 10 -16 10 20.00 6.40 10 16 10 3.40 9.20 12 -16 10 15.00 6.70 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4.20 1 -17 10 8.70 4.70 1 -17 10 0.10 4.40 1 17 10 1.60 6.90 -1 17 -10 10.90 3.80 3 -17 10 48.70 6.50 3 -17 10 58.69 9.30 3 17 10 62.59 9.60 3 17 10 65.59 6.20 5 -17 10 17.60 5.70 5 -17 10 28.80 5.50 5 17 10 17.00 7.90 7 -17 10 2.10 4.90 7 17 10 -4.10 7.90 9 -17 10 2.10 5.50 9 17 10 22.00 9.30 11 -17 10 5.00 6.20 11 17 10 13.30 10.00 16 -18 -10 33.30 5.90 16 -18 -10 38.30 7.90 -16 -18 10 48.00 8.70 16 18 -10 45.10 8.90 -16 18 10 40.20 7.30 -14 -18 10 104.89 13.30 14 -18 -10 98.49 13.00 14 -18 -10 102.29 9.10 14 18 -10 86.59 10.50 -14 18 10 88.99 10.90 12 -18 -10 47.40 8.40 12 -18 -10 54.59 6.10 -12 -18 10 85.89 11.10 12 18 -10 67.59 8.80 -12 18 10 59.99 7.30 10 -18 -10 71.49 6.90 -10 -18 10 70.99 10.10 10 -18 -10 57.29 9.20 10 18 -10 74.49 8.90 -10 18 10 69.99 7.70 -8 -18 10 228.58 14.40 8 -18 -10 197.58 18.80 -8 -18 10 232.48 16.80 8 -18 -10 200.08 14.30 -8 18 10 228.98 16.50 8 18 -10 224.38 16.70 6 -18 -10 4.60 6.50 -6 -18 10 14.70 5.30 -6 -18 10 15.10 4.00 -6 18 10 11.20 5.90 6 18 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13 -7 -11 416.26 25.40 -13 -7 11 425.56 25.10 13 7 -11 382.76 26.60 -13 7 11 416.16 26.20 11 -7 -11 30.90 4.20 -11 -7 11 33.10 4.10 11 7 -11 25.40 5.00 -11 7 11 25.00 4.40 9 -7 -11 4.00 2.70 -9 -7 11 3.20 1.90 -9 7 11 5.00 3.20 9 7 -11 2.50 3.70 7 -7 -11 514.95 29.10 -7 7 11 430.26 29.30 7 7 -11 492.65 29.60 -5 7 11 135.29 10.00 5 7 -11 136.89 9.90 -3 -7 11 200.58 14.20 -3 7 11 216.88 13.90 -1 -7 11 348.37 21.50 -1 -7 11 328.27 21.00 -1 7 11 339.77 21.30 1 -7 11 347.47 22.30 1 -7 11 356.16 21.40 1 7 11 348.27 22.10 3 -7 11 112.89 7.80 3 -7 11 112.39 7.70 3 -7 11 120.69 9.30 3 7 11 107.79 9.40 5 -7 11 -2.50 4.00 5 -7 11 -0.40 1.90 5 -7 11 -1.90 2.00 5 7 11 -0.70 3.20 5 7 11 -4.00 4.30 7 -7 11 105.19 7.40 7 -7 11 96.09 6.70 7 -7 11 99.89 9.90 7 7 11 93.19 9.10 7 7 11 85.09 10.30 9 -7 11 13.00 2.60 9 -7 11 12.00 5.80 9 7 11 6.40 4.30 9 7 11 11.00 6.70 11 -7 11 18.90 5.60 11 7 11 24.60 5.30 11 7 11 23.70 7.60 13 -7 11 -8.40 5.80 13 7 11 2.30 7.30 13 7 11 2.00 4.70 15 -7 11 54.69 8.40 15 7 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22.10 2.80 -13 3 13 29.10 3.10 -13 3 13 24.70 5.60 13 3 -13 17.40 5.10 11 -3 -13 1139.79 65.49 11 3 -13 1084.89 66.19 -11 3 13 1083.99 66.29 -11 3 13 1094.89 65.19 -9 -3 13 893.31 55.29 -9 3 13 917.11 54.59 -7 -3 13 38.80 5.60 -7 3 13 50.49 5.40 -5 -3 13 133.19 9.90 -5 3 13 118.09 9.50 -3 -3 13 478.05 30.30 -3 3 13 513.35 30.30 -1 -3 13 39.80 4.30 -1 3 13 36.50 4.60 1 -3 13 200.28 14.60 1 -3 13 208.08 13.80 1 3 13 221.78 14.20 3 -3 13 221.38 14.30 3 -3 13 213.78 15.30 3 3 13 221.78 15.30 3 3 13 222.28 14.80 5 -3 13 12.40 5.40 5 -3 13 14.30 3.40 5 3 13 19.60 5.10 5 3 13 12.70 4.20 7 -3 13 199.28 15.50 7 -3 13 212.08 14.40 7 3 13 225.98 15.60 7 3 13 198.88 15.60 9 -3 13 47.50 5.90 9 -3 13 33.60 7.00 9 3 13 48.10 6.80 9 3 13 37.00 7.00 11 -3 13 29.90 5.60 11 -3 13 29.40 6.70 11 3 13 24.70 7.00 11 3 13 23.20 6.40 13 -3 13 127.29 13.20 13 -3 13 133.29 12.20 13 3 13 135.59 14.60 13 3 13 130.29 12.50 15 -3 13 15.80 7.10 15 3 13 20.00 7.00 15 3 13 23.60 8.20 22 -4 -13 149.29 12.60 22 4 -13 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27.80 8.90 10 8 14 29.00 6.50 12 -8 14 2.40 6.60 12 8 14 3.20 6.00 12 8 14 -10.50 8.40 14 -8 14 -12.50 7.10 14 8 14 5.40 9.90 14 8 14 7.30 6.30 21 -9 -14 23.60 5.60 -21 9 14 17.40 7.20 21 9 -14 31.80 9.00 19 -9 -14 155.88 12.70 -19 9 14 183.88 14.90 19 9 -14 187.98 17.10 17 -9 -14 176.98 13.90 -17 9 14 212.08 15.40 17 9 -14 186.88 16.90 15 -9 -14 268.97 18.40 -15 -9 14 281.97 17.80 -15 9 14 275.27 19.30 15 9 -14 275.77 20.50 -13 -9 14 47.50 5.80 13 -9 -14 61.79 6.30 13 9 -14 43.70 7.70 -13 9 14 52.09 6.60 11 -9 -14 172.18 12.00 -11 -9 14 155.18 11.20 11 9 -14 158.18 13.60 -11 9 14 162.68 12.60 9 9 -14 118.59 10.80 -9 9 14 115.39 9.80 7 9 -14 411.16 26.10 -7 9 14 405.26 25.90 -5 -9 14 202.88 15.60 -5 9 14 218.18 15.00 -3 -9 14 0.90 4.00 -3 -9 14 15.30 4.80 -3 9 14 9.60 4.40 -1 -9 14 -2.50 3.00 -1 -9 14 -6.90 4.20 -1 9 14 -7.60 4.40 1 -9 14 155.28 12.60 1 -9 14 152.38 10.60 1 9 14 148.79 12.50 3 -9 14 139.49 12.20 3 -9 14 123.69 9.10 3 9 14 130.09 10.90 3 9 14 128.59 12.00 5 -9 14 43.00 5.20 5 -9 14 37.60 6.70 5 9 14 41.10 7.40 5 9 14 54.59 6.60 7 -9 14 31.30 7.10 7 9 14 22.70 7.10 7 9 14 21.40 5.80 9 -9 14 15.20 7.30 9 9 14 15.70 7.70 9 9 14 27.50 6.10 11 -9 14 13.70 6.40 11 9 14 12.80 6.30 11 9 14 10.50 9.30 13 -9 14 -7.00 7.00 13 9 14 4.40 6.10 13 9 14 -1.90 8.90 20 -10 -14 14.80 5.70 -20 10 14 5.30 6.50 20 10 -14 21.40 8.70 18 -10 -14 108.89 10.20 -18 10 14 105.79 11.70 18 10 -14 98.39 11.30 16 -10 -14 114.39 9.90 -16 10 14 124.79 11.60 16 10 -14 119.69 13.50 -14 -10 14 52.89 6.40 14 -10 -14 39.50 5.60 14 10 -14 40.30 7.20 -14 10 14 41.30 6.40 -12 -10 14 391.96 23.40 12 -10 -14 378.46 23.70 -12 10 14 356.66 24.10 12 10 -14 357.56 25.00 -10 -10 14 133.89 10.40 -10 10 14 148.79 11.00 10 10 -14 132.09 12.10 8 10 -14 22.40 5.50 -8 10 14 23.20 4.80 6 10 -14 1.70 4.20 -6 10 14 2.20 3.80 -4 -10 14 34.20 5.60 -4 -10 14 31.30 5.70 -4 10 14 19.50 5.00 -2 -10 14 2.20 3.50 -2 -10 14 5.40 4.50 -2 10 14 2.40 4.40 0 -10 14 -0.20 4.90 0 -10 14 5.00 3.10 0 10 14 0.30 4.70 2 -10 14 100.89 7.60 2 -10 14 90.69 9.40 2 10 14 91.09 10.70 4 -10 14 25.50 3.30 4 -10 14 17.10 5.80 4 10 14 24.40 5.80 4 10 14 21.20 6.20 6 -10 14 76.29 9.50 6 10 14 84.79 10.20 6 10 14 97.09 9.90 8 -10 14 13.60 6.60 8 10 14 5.40 5.20 8 10 14 11.80 7.70 10 -10 14 0.00 6.80 10 10 14 8.00 8.50 10 10 14 8.30 5.70 12 -10 14 70.19 9.70 12 10 14 71.99 8.30 12 10 14 61.19 11.40 19 -11 -14 17.00 5.50 -19 11 14 9.00 6.00 19 11 -14 18.80 8.40 17 -11 -14 43.00 6.00 -17 11 14 32.00 6.50 17 11 -14 48.30 8.60 15 -11 -14 257.47 17.30 -15 -11 14 254.77 17.10 15 11 -14 260.97 19.10 -15 11 14 240.48 18.00 -13 -11 14 475.75 28.30 13 -11 -14 467.65 28.30 -13 11 14 437.06 28.80 13 11 -14 421.66 29.70 -11 -11 14 69.39 7.70 11 -11 -14 82.59 8.20 -11 11 14 91.79 9.30 11 11 -14 69.59 8.50 -9 -11 14 166.18 12.40 9 11 -14 174.58 13.90 -9 11 14 177.28 13.20 7 11 -14 120.69 10.60 -7 11 14 104.49 9.60 -5 11 14 129.19 10.60 -3 -11 14 13.50 5.00 -3 -11 14 9.80 4.80 -3 11 14 16.70 5.30 -1 -11 14 23.50 5.30 -1 -11 14 28.00 4.30 -1 11 14 16.10 5.20 1 -11 14 10.30 3.20 1 -11 14 2.90 5.70 1 11 14 12.70 5.60 3 -11 14 -9.70 5.20 3 -11 14 1.90 2.60 3 11 14 -2.20 4.40 3 11 14 -7.50 5.80 5 -11 14 1.70 6.00 5 11 14 -2.00 4.90 5 11 14 1.30 6.70 7 -11 14 2.30 6.60 7 11 14 6.10 5.30 7 11 14 12.20 7.50 9 -11 14 125.29 13.20 9 11 14 99.79 12.50 9 11 14 122.09 11.30 11 -11 14 4.10 7.30 11 11 14 -1.00 9.00 11 11 14 -2.30 5.60 18 -12 -14 58.69 7.10 18 12 -14 43.60 9.60 -18 12 14 46.80 7.30 -16 -12 14 47.30 8.10 16 -12 -14 33.80 5.80 16 12 -14 34.00 8.50 -16 12 14 35.30 6.40 -14 -12 14 166.48 12.20 14 -12 -14 142.99 11.90 14 12 -14 138.09 14.30 -14 12 14 149.88 12.80 12 -12 -14 120.39 10.30 -12 -12 14 125.39 10.10 12 12 -14 127.79 12.90 -12 12 14 121.19 11.30 -10 -12 14 186.38 13.40 -10 12 14 182.08 14.00 10 12 -14 185.88 15.00 -8 -12 14 75.69 8.10 8 12 -14 69.29 7.90 -8 12 14 73.39 8.80 -6 12 14 29.10 5.90 6 12 -14 40.60 6.00 -4 -12 14 0.70 4.60 -4 12 14 3.40 5.00 -2 -12 14 164.18 13.00 -2 -12 14 171.28 13.40 -2 12 14 176.48 13.80 0 -12 14 32.00 4.50 0 -12 14 41.90 6.80 0 12 14 30.20 6.30 2 -12 14 62.49 7.80 2 -12 14 51.39 5.80 2 12 14 64.99 8.70 4 -12 14 15.10 6.30 4 12 14 11.90 5.20 4 12 14 6.50 6.60 6 -12 14 59.79 8.20 6 12 14 92.19 9.70 6 12 14 67.49 9.90 8 -12 14 31.50 7.50 8 12 14 39.00 6.40 8 12 14 41.70 9.80 10 -12 14 56.79 8.30 10 12 14 50.89 7.20 10 12 14 42.70 10.30 12 -12 14 13.00 7.90 12 12 14 6.20 5.80 12 12 14 -12.10 9.70 19 -13 -14 -0.30 5.60 -19 13 14 3.70 6.30 19 13 -14 17.90 8.60 17 -13 -14 45.50 6.80 -17 13 14 41.50 7.00 17 13 -14 42.90 8.70 15 -13 -14 50.79 6.60 -15 -13 14 60.49 8.60 15 13 -14 67.39 9.70 -15 13 14 52.49 7.30 13 -13 -14 35.00 5.50 -13 -13 14 25.50 4.80 -13 13 14 29.10 6.00 13 13 -14 27.40 7.20 -11 -13 14 273.97 18.10 11 -13 -14 272.67 17.90 11 13 -14 266.47 19.70 -11 13 14 254.37 18.50 -9 -13 14 23.60 4.60 -9 13 14 32.90 5.80 9 13 -14 39.10 6.60 -7 -13 14 63.99 7.50 -7 -13 14 71.39 8.10 -7 13 14 77.59 9.00 7 13 -14 83.49 9.60 -5 -13 14 103.79 10.00 5 13 -14 108.39 10.60 -5 13 14 105.39 10.50 -3 -13 14 75.29 8.00 -3 -13 14 88.09 9.80 -3 13 14 58.89 7.40 -1 -13 14 4.60 5.30 -1 -13 14 10.00 4.00 -1 13 14 10.30 5.80 1 -13 14 14.50 5.90 1 -13 14 23.30 3.80 1 13 14 8.10 6.00 3 -13 14 -0.80 5.80 3 -13 14 3.20 3.30 3 13 14 2.40 6.40 3 13 14 2.90 4.60 5 -13 14 28.50 6.90 5 13 14 33.10 8.70 5 13 14 48.20 6.10 7 -13 14 7.30 6.40 7 13 14 -2.80 8.40 7 13 14 -2.40 5.30 9 -13 14 91.39 11.00 9 13 14 97.99 13.10 9 13 14 103.69 10.60 11 -13 14 -4.00 7.20 11 13 14 -22.10 9.60 11 13 14 11.80 5.90 18 -14 -14 5.10 5.90 18 14 -14 13.30 8.60 -18 14 14 9.50 6.40 16 -14 -14 4.50 5.00 -16 14 14 12.30 5.90 16 14 -14 7.70 7.40 14 -14 -14 6.20 4.80 -14 -14 14 5.40 4.40 -14 14 14 13.90 5.40 14 14 -14 0.40 6.70 -12 -14 14 9.00 4.20 12 -14 -14 10.00 4.60 12 14 -14 13.10 6.40 -12 14 14 22.20 5.60 -10 -14 14 24.80 4.90 -10 14 14 18.80 5.50 10 14 -14 26.60 6.70 -8 -14 14 31.20 5.20 -8 -14 14 38.70 6.20 -8 14 14 44.90 6.60 8 14 -14 39.50 6.80 -6 -14 14 3.40 4.80 -6 -14 14 3.50 4.20 6 14 -14 1.70 4.90 -6 14 14 -1.50 4.70 -4 -14 14 60.09 7.00 -4 14 14 56.39 7.50 4 14 -14 58.29 6.80 -2 -14 14 54.09 7.10 -2 -14 14 45.90 6.70 -2 14 14 28.70 6.30 0 -14 14 62.69 7.90 0 -14 14 59.99 6.20 0 14 14 64.59 8.20 2 -14 14 57.09 5.90 2 -14 14 55.89 7.80 2 14 14 70.79 9.40 4 -14 14 12.10 6.50 4 14 14 14.80 5.00 4 14 14 4.60 7.70 6 -14 14 27.20 7.00 6 14 14 24.70 9.00 6 14 14 23.70 5.60 8 -14 14 107.29 10.90 8 14 14 85.19 12.50 8 14 14 89.79 8.90 10 -14 14 29.20 8.20 10 14 14 16.50 10.70 17 -15 -14 9.10 5.40 17 15 -14 19.20 9.00 -17 15 14 9.70 6.40 15 -15 -14 42.00 6.30 -15 -15 14 36.10 6.40 -15 15 14 43.90 7.30 15 15 -14 34.80 8.60 -13 -15 14 4.30 4.50 13 -15 -14 4.80 4.70 13 15 -14 1.90 6.90 -13 15 14 0.40 5.30 -11 -15 14 -0.20 4.00 11 -15 -14 3.60 4.30 -11 15 14 6.40 5.30 11 15 -14 1.30 6.40 -9 -15 14 5.90 4.50 -9 -15 14 -3.40 4.80 -9 15 14 2.10 5.30 9 15 -14 5.40 6.10 -7 -15 14 -0.30 4.90 -7 -15 14 -0.30 4.10 7 15 -14 1.10 5.60 -7 15 14 1.70 5.50 -5 -15 14 3.70 4.40 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6.50 -2 -16 14 100.19 11.60 -2 -16 14 81.69 10.60 -2 -16 14 104.99 10.60 -2 16 14 109.59 12.50 0 -16 14 7.40 5.60 0 -16 14 5.50 3.90 0 16 14 -5.80 7.00 2 -16 14 95.49 9.50 2 16 14 65.39 10.40 2 16 14 85.49 8.00 4 -16 14 8.00 6.30 4 16 14 7.20 8.50 4 16 14 4.30 5.10 6 -16 14 36.50 7.50 6 16 14 25.40 10.20 8 -16 14 5.00 7.10 8 16 14 -2.80 9.90 15 -17 -14 79.99 8.30 -15 -17 14 81.99 11.80 -15 17 14 62.49 8.70 15 17 -14 99.39 11.70 -13 -17 14 62.49 10.20 13 -17 -14 64.99 7.20 -13 17 14 50.09 8.00 13 17 -14 59.29 10.00 -11 -17 14 17.40 5.80 -11 -17 14 17.30 5.60 -11 17 14 9.40 6.10 11 17 -14 26.70 8.00 -9 -17 14 53.99 7.50 -9 -17 14 74.29 10.00 -9 17 14 75.49 8.70 9 17 -14 65.29 9.40 -7 -17 14 24.00 6.10 -7 -17 14 16.30 6.10 7 17 -14 23.90 7.10 -7 17 14 21.00 6.40 -5 -17 14 20.80 5.90 -5 -17 14 20.10 5.40 5 17 -14 29.20 6.80 -3 -17 14 2.60 5.20 -3 -17 14 4.80 5.50 -3 17 14 0.80 6.50 -1 -17 14 5.70 5.00 -1 -17 14 9.70 5.60 -1 -17 14 14.20 5.80 -1 17 14 11.40 7.60 1 -17 14 50.19 7.60 1 17 14 37.80 9.30 3 -17 14 23.50 6.80 3 17 14 13.00 5.30 3 17 14 21.20 9.40 5 -17 14 10.90 6.50 5 17 14 8.80 9.30 7 -17 14 11.70 7.20 7 17 14 2.50 10.20 12 -18 -14 30.40 5.70 -12 -18 14 28.60 6.40 -12 18 14 28.10 7.40 12 18 -14 28.20 8.50 -10 -18 14 2.70 5.30 -10 -18 14 3.70 5.10 10 18 -14 2.50 7.40 -10 18 14 -8.60 6.10 -8 -18 14 107.69 11.90 -8 -18 14 97.29 9.50 -8 18 14 81.09 10.00 8 18 -14 114.89 11.20 -6 -18 14 157.18 13.40 -6 -18 14 169.88 14.70 6 18 -14 167.88 15.40 -6 18 14 150.48 14.80 -4 -18 14 51.29 6.90 -4 -18 14 39.00 6.80 -4 18 14 37.80 8.10 4 18 -14 51.29 7.40 -2 -18 14 14.40 5.80 -2 -18 14 16.00 6.10 -2 -18 14 11.30 5.70 -2 18 14 21.90 7.50 0 -18 14 18.10 5.90 0 -18 14 24.40 6.50 0 18 14 11.40 8.50 2 -18 14 2.30 5.60 2 -18 14 5.10 6.30 2 18 14 -6.60 7.50 4 -18 14 18.90 6.90 4 18 14 17.70 10.00 6 -18 14 -11.90 6.20 6 18 14 5.70 10.70 -11 -19 14 27.90 6.90 -11 19 14 29.60 7.60 11 19 -14 35.60 8.80 -9 -19 14 71.59 11.20 9 19 -14 72.89 10.20 -9 19 14 60.69 9.10 -7 -19 14 46.60 6.80 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5.40 5 -1 15 12.70 4.00 5 -1 15 8.70 5.50 5 1 15 9.60 5.60 5 1 15 3.40 4.30 7 -1 15 15.00 5.00 7 -1 15 1.70 5.90 7 1 15 7.70 5.20 7 1 15 6.70 6.20 9 -1 15 26.50 6.40 9 -1 15 37.80 7.40 9 1 15 25.70 7.10 9 1 15 29.50 6.80 11 -1 15 -0.60 6.70 11 -1 15 10.30 6.60 11 1 15 -0.20 6.20 11 1 15 3.50 6.70 13 -1 15 58.89 9.20 13 -1 15 60.19 8.80 13 1 15 47.80 9.30 13 1 15 47.20 8.60 22 -2 -15 2.30 5.30 22 2 -15 4.90 5.50 -22 2 15 -1.40 8.60 20 -2 -15 36.70 5.90 -20 2 15 33.60 8.90 20 2 -15 32.90 5.90 18 -2 -15 63.69 7.10 -18 2 15 76.39 10.10 -16 -2 15 56.39 9.90 16 -2 -15 59.19 6.50 -16 2 15 58.39 9.00 -14 -2 15 -3.20 6.70 -14 -2 15 1.20 1.50 -14 2 15 9.00 6.30 -12 -2 15 79.89 9.80 -12 2 15 84.69 7.10 -12 2 15 93.69 9.60 -10 -2 15 142.69 12.80 -10 2 15 144.29 11.60 -8 -2 15 209.88 15.60 -8 2 15 220.18 15.30 -6 -2 15 9.70 4.30 -6 2 15 9.60 3.80 -4 -2 15 16.30 4.00 -4 2 15 17.10 4.00 -2 -2 15 38.50 4.80 -2 2 15 47.50 5.30 0 -2 15 158.68 11.20 0 2 15 142.99 11.30 2 -2 15 47.10 5.30 2 -2 15 50.29 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2 -6 21 43.70 9.10 2 -6 21 31.10 6.30 2 6 21 23.90 7.80 2 6 21 54.59 10.20 4 -6 21 33.50 9.40 4 -6 21 27.70 6.70 4 6 21 46.20 9.30 4 6 21 31.20 9.80 -15 -7 21 18.40 9.50 -15 7 21 28.80 8.10 -13 -7 21 9.40 8.80 -13 7 21 19.80 7.30 -11 -7 21 2.80 7.10 -11 7 21 7.00 6.80 -9 -7 21 -12.70 6.10 -9 7 21 -1.70 6.20 -7 -7 21 17.60 6.30 -7 7 21 15.50 6.30 -5 -7 21 4.60 5.50 -5 7 21 -3.10 5.60 -3 -7 21 19.20 6.90 -3 -7 21 12.70 5.50 -3 7 21 17.40 6.70 -1 -7 21 18.80 7.80 -1 -7 21 26.90 6.00 -1 7 21 30.00 7.70 1 -7 21 15.10 5.60 1 -7 21 27.90 8.40 1 7 21 24.60 7.30 1 7 21 22.00 9.40 3 -7 21 36.90 6.40 3 -7 21 21.80 10.10 3 7 21 20.40 8.20 3 7 21 33.30 10.10 5 -7 21 7.40 9.40 5 7 21 25.00 9.20 5 7 21 27.90 10.00 -14 -8 21 7.20 9.70 -14 8 21 21.30 7.60 -12 -8 21 21.50 8.60 -12 8 21 22.30 7.80 -10 -8 21 57.79 9.20 -10 8 21 60.79 9.00 -8 -8 21 -3.00 6.20 -8 8 21 6.80 5.80 -6 -8 21 6.90 6.10 -6 8 21 1.70 6.10 -4 -8 21 4.60 5.50 -4 -8 21 14.40 6.90 -4 8 21 4.30 6.60 -2 -8 21 73.39 10.30 -2 -8 21 91.89 10.50 -2 8 21 107.49 10.80 0 -8 21 6.20 7.50 0 -8 21 -1.90 5.30 0 8 21 -10.30 7.00 2 -8 21 1.20 5.10 2 -8 21 4.30 8.30 2 8 21 3.70 8.90 2 8 21 1.60 7.20 4 -8 21 -7.20 8.10 4 8 21 23.10 9.40 4 8 21 7.80 9.70 -15 -9 21 11.80 10.50 -15 9 21 20.20 8.20 -13 -9 21 12.50 4.40 -13 -9 21 -0.90 8.80 -13 9 21 7.10 7.00 -11 -9 21 15.90 8.10 -11 9 21 17.40 7.30 -9 -9 21 6.70 7.30 -9 9 21 18.30 6.90 -7 -9 21 -0.40 6.10 -7 9 21 13.70 6.60 -5 -9 21 13.80 6.20 -5 -9 21 9.80 6.30 -5 9 21 12.30 7.10 -3 -9 21 43.10 6.80 -3 -9 21 53.79 9.10 -3 9 21 48.50 8.40 -1 -9 21 6.10 5.30 -1 -9 21 -1.70 6.90 -1 9 21 -8.80 6.90 1 -9 21 -16.50 8.10 1 -9 21 2.10 5.40 1 9 21 -9.80 7.20 1 9 21 1.00 8.80 3 -9 21 18.20 8.90 3 9 21 27.00 9.70 3 9 21 20.40 9.40 -14 -10 21 -3.70 10.10 -14 10 21 3.00 7.60 -12 -10 21 -6.10 8.30 -12 10 21 5.20 7.40 -10 -10 21 17.10 8.20 -10 10 21 24.30 7.40 -8 -10 21 8.60 7.00 -8 10 21 6.10 6.10 -6 -10 21 1.50 6.80 -6 -10 21 1.80 6.10 -6 10 21 -2.80 6.80 -4 -10 21 1.50 5.80 -4 -10 21 3.20 6.80 -4 10 21 -3.50 7.10 -2 -10 21 33.30 8.20 -2 -10 21 19.90 5.90 -2 10 21 13.50 7.70 0 -10 21 30.70 9.20 0 -10 21 30.40 6.30 0 10 21 32.40 8.70 2 -10 21 35.00 9.10 2 10 21 25.80 8.90 2 10 21 25.30 9.80 -13 -11 21 12.80 4.90 -13 -11 21 0.20 10.20 -13 11 21 2.10 7.00 -11 -11 21 -14.90 8.40 -11 11 21 2.40 7.00 -9 -11 21 16.60 7.90 -9 11 21 16.20 7.40 -7 -11 21 8.80 6.70 -7 -11 21 11.10 7.00 -7 11 21 -5.20 7.10 -5 -11 21 3.40 7.00 -5 -11 21 -3.20 6.10 -5 11 21 8.00 7.00 -3 -11 21 9.90 6.00 -3 -11 21 28.50 7.90 -3 11 21 16.40 7.70 -1 -11 21 2.10 5.40 -1 -11 21 2.00 8.20 -1 11 21 -15.40 6.50 1 -11 21 4.90 8.70 1 11 21 7.80 7.90 1 11 21 -0.40 9.10 -10 -12 21 -9.10 8.20 -10 12 21 9.10 7.70 -8 -12 21 27.80 7.70 -8 -12 21 21.90 8.10 -8 12 21 28.70 7.80 -6 -12 21 38.80 8.70 -6 -12 21 33.70 7.50 -6 12 21 25.30 8.00 -4 -12 21 -5.20 5.90 -4 -12 21 -5.60 7.00 -4 12 21 -4.50 7.10 -2 -12 21 14.50 6.10 -2 -12 21 19.20 8.20 -2 12 21 18.00 8.10 0 -12 21 5.00 8.80 0 12 21 2.70 9.00 -9 -13 21 25.70 8.10 -9 13 21 7.70 6.70 -7 -13 21 7.50 7.40 -7 -13 21 13.80 7.30 -7 13 21 8.20 8.00 -5 -13 21 11.80 7.70 -5 -13 21 3.70 6.50 -5 13 21 0.80 7.90 -3 -13 21 16.90 9.00 -3 -13 21 4.60 5.90 -3 13 21 7.10 8.00 -16 0 22 150.38 16.20 -14 0 22 146.89 15.60 -12 0 22 4.70 6.40 -10 0 22 16.70 6.80 -8 0 22 15.70 6.60 -6 0 22 5.20 5.80 -4 0 22 12.00 5.90 -2 0 22 8.70 6.20 0 0 22 102.59 12.60 0 0 22 130.79 12.90 2 0 22 3.20 6.50 2 0 22 3.80 8.60 4 0 22 21.30 9.50 4 0 22 6.00 7.30 -17 -1 22 22.20 9.50 -17 1 22 34.30 9.60 -15 -1 22 6.50 7.90 -15 1 22 18.40 8.40 -13 -1 22 43.30 8.80 -13 1 22 52.69 8.90 -11 -1 22 115.59 12.60 -11 1 22 130.99 13.60 -9 -1 22 66.99 8.60 -9 1 22 65.09 8.30 -7 -1 22 24.20 6.40 -7 1 22 30.20 6.90 -5 -1 22 6.30 5.90 -5 1 22 9.10 5.90 -3 -1 22 2.50 5.70 -3 1 22 -4.20 5.80 -1 -1 22 22.50 6.10 -1 -1 22 16.30 8.30 -1 1 22 24.40 6.60 -1 1 22 32.90 8.10 1 -1 22 24.40 7.00 1 -1 22 11.80 8.70 1 1 22 31.30 7.10 1 1 22 33.70 9.40 3 -1 22 26.50 7.70 3 -1 22 37.10 9.70 3 1 22 47.90 10.70 3 1 22 35.70 8.20 5 -1 22 10.30 7.40 5 -1 22 -16.60 9.40 5 1 22 10.90 9.30 5 1 22 8.80 8.00 -16 -2 22 37.40 10.10 -16 2 22 32.00 8.60 -14 -2 22 21.60 7.80 -14 2 22 25.90 8.40 -12 -2 22 54.09 9.00 -12 2 22 40.60 7.70 -10 -2 22 6.80 6.60 -10 2 22 -0.30 6.20 -8 -2 22 0.20 5.90 -8 2 22 -3.50 5.90 -6 -2 22 1.10 5.70 -6 2 22 8.30 6.30 -4 -2 22 13.50 6.00 -4 2 22 16.40 6.10 -2 -2 22 30.90 8.10 -2 -2 22 44.20 7.10 -2 2 22 44.60 7.60 0 -2 22 -5.00 7.50 0 -2 22 -9.20 5.80 0 2 22 1.10 8.60 0 2 22 -3.70 6.30 2 -2 22 7.90 9.00 2 -2 22 13.00 6.60 2 2 22 7.20 9.70 2 2 22 0.50 6.80 4 -2 22 19.00 8.60 4 -2 22 11.50 7.00 4 2 22 2.20 8.90 4 2 22 7.10 7.70 -15 -3 22 11.80 9.10 -15 3 22 11.10 7.80 -13 -3 22 9.40 7.90 -13 3 22 -2.80 6.80 -11 -3 22 31.30 8.00 -11 3 22 28.30 6.90 -9 -3 22 42.30 7.60 -9 3 22 49.30 7.60 -7 -3 22 28.00 6.70 -7 3 22 21.20 6.50 -5 -3 22 9.20 5.50 -5 3 22 13.40 6.10 -3 -3 22 5.50 5.60 -3 3 22 11.80 6.20 -1 -3 22 27.70 6.30 -1 -3 22 10.70 8.10 -1 3 22 20.70 6.90 1 -3 22 7.70 7.60 1 -3 22 23.50 6.50 1 3 22 26.50 7.30 1 3 22 40.40 9.30 3 -3 22 63.99 8.70 3 -3 22 66.19 11.10 3 3 22 64.29 9.40 3 3 22 62.59 11.90 -16 -4 22 -0.50 9.00 -16 4 22 2.00 8.10 -14 -4 22 -5.20 7.60 -14 4 22 -10.50 6.50 -12 -4 22 2.30 7.40 -12 4 22 -4.40 6.70 -10 -4 22 -0.50 6.50 -10 4 22 4.50 6.10 -8 -4 22 5.70 6.40 -8 4 22 -3.70 6.30 -6 -4 22 17.30 6.10 -6 4 22 14.60 6.20 -4 -4 22 13.60 5.80 -4 4 22 14.70 6.50 -2 -4 22 62.99 8.10 -2 -4 22 57.79 9.20 -2 4 22 62.99 8.80 0 -4 22 9.70 7.40 0 -4 22 -4.60 5.60 0 4 22 3.80 8.50 0 4 22 1.00 6.90 2 -4 22 17.70 8.60 2 -4 22 22.70 6.40 2 4 22 11.00 8.90 2 4 22 12.00 7.20 4 -4 22 -14.60 9.60 4 -4 22 19.60 7.00 4 4 22 -15.90 7.50 4 4 22 -10.10 8.70 -15 -5 22 -6.20 8.50 -15 5 22 -3.10 7.70 -13 -5 22 14.70 8.20 -13 5 22 1.20 7.10 -11 -5 22 0.80 7.00 -11 5 22 2.50 6.90 -9 -5 22 2.50 6.60 -9 5 22 -2.20 6.40 -7 -5 22 1.30 5.80 -7 5 22 3.60 6.30 -5 -5 22 33.20 6.70 -5 5 22 34.20 7.00 -3 -5 22 25.00 6.30 -3 -5 22 14.20 7.50 -3 5 22 24.60 7.20 -1 -5 22 -4.70 7.50 -1 -5 22 3.80 5.90 -1 5 22 18.80 7.30 1 -5 22 24.20 8.50 1 -5 22 11.10 5.80 1 5 22 -0.20 7.30 1 5 22 5.90 9.60 3 -5 22 1.10 5.90 3 -5 22 -2.30 8.80 3 5 22 0.30 7.30 3 5 22 3.70 9.90 -14 -6 22 21.60 9.60 -14 6 22 18.70 7.70 -12 -6 22 17.20 8.00 -12 6 22 27.60 7.50 -10 -6 22 -2.10 6.90 -10 6 22 8.30 7.00 -8 -6 22 43.40 7.70 -8 6 22 37.10 7.70 -6 -6 22 5.80 5.90 -6 6 22 1.70 5.50 -4 -6 22 13.10 5.90 -4 -6 22 8.40 7.00 -4 6 22 7.90 6.50 -2 -6 22 101.39 10.20 -2 -6 22 124.19 12.70 -2 6 22 103.39 11.30 0 -6 22 -11.20 7.00 0 -6 22 0.20 5.40 0 6 22 -3.90 7.00 0 6 22 -7.90 8.80 2 -6 22 25.00 6.50 2 -6 22 28.10 9.70 2 6 22 20.80 8.40 2 6 22 23.20 10.30 -13 -7 22 27.80 9.40 -13 7 22 29.70 8.20 -11 -7 22 -5.10 7.60 -11 7 22 -6.40 6.60 -9 -7 22 5.70 6.50 -9 7 22 1.60 6.10 -7 -7 22 -3.80 5.90 -7 7 22 0.10 6.20 -5 -7 22 9.30 6.10 -5 7 22 18.40 7.00 -3 -7 22 23.40 7.50 -3 -7 22 33.00 6.60 -3 7 22 19.20 7.50 -1 -7 22 36.20 6.60 -1 -7 22 18.40 8.10 -1 7 22 34.20 8.20 1 -7 22 6.70 5.70 1 -7 22 -3.50 8.10 1 7 22 0.20 9.30 1 7 22 2.20 7.70 -14 -8 22 8.20 9.30 -14 8 22 15.10 7.80 -12 -8 22 39.40 9.50 -12 8 22 55.69 9.30 -10 -8 22 71.49 10.00 -10 8 22 70.99 9.90 -8 -8 22 13.90 6.90 -8 8 22 10.80 6.90 -6 -8 22 27.50 7.10 -6 8 22 35.70 7.50 -4 -8 22 26.10 8.00 -4 -8 22 21.70 6.50 -4 8 22 23.10 7.80 -2 -8 22 17.00 6.00 -2 -8 22 7.50 8.00 -2 8 22 27.40 8.00 0 -8 22 12.20 8.20 0 -8 22 4.10 5.60 0 8 22 2.20 7.20 2 -8 22 13.20 9.60 2 8 22 9.50 8.60 2 8 22 16.60 10.50 -13 -9 22 -8.30 8.10 -13 9 22 1.40 8.20 -11 -9 22 -10.00 7.40 -11 9 22 2.60 7.40 -9 -9 22 2.70 7.40 -9 9 22 -0.70 6.60 -7 -9 22 9.70 6.80 -7 9 22 10.30 7.10 -5 -9 22 12.10 6.60 -5 -9 22 4.90 7.30 -5 9 22 6.70 7.20 -3 -9 22 51.99 7.60 -3 -9 22 46.50 9.00 -3 9 22 54.99 9.10 -1 -9 22 13.70 6.00 -1 -9 22 1.40 8.00 -1 9 22 12.00 7.90 1 -9 22 -9.60 8.40 1 9 22 -2.10 8.00 1 9 22 12.70 9.70 -10 -10 22 58.09 10.20 -10 10 22 54.39 9.20 -8 -10 22 79.19 10.30 -8 10 22 111.59 12.30 -6 -10 22 27.90 7.60 -6 -10 22 32.70 8.50 -6 10 22 31.30 7.90 -4 -10 22 7.40 7.60 -4 -10 22 -3.90 5.90 -4 10 22 1.40 7.30 -2 -10 22 -4.00 5.60 -2 -10 22 -9.00 7.60 -2 10 22 0.70 7.70 -9 -11 22 10.80 7.90 -9 11 22 -2.60 7.50 -7 -11 22 -3.80 6.90 -7 -11 22 6.90 7.50 -7 11 22 3.60 7.40 -5 -11 22 19.60 7.00 -5 -11 22 24.90 8.40 -5 11 22 18.10 7.90 -3 -11 22 2.90 6.10 -3 -11 22 -5.40 7.60 -3 11 22 7.20 8.20 -14 0 23 7.00 8.20 -12 0 23 3.70 6.90 -10 0 23 6.00 6.50 -8 0 23 12.10 6.50 -6 0 23 1.00 6.40 -4 0 23 3.60 6.10 -2 0 23 5.00 6.30 0 0 23 44.70 9.80 0 0 23 6.60 6.80 2 0 23 -1.00 9.40 2 0 23 5.00 7.20 -15 -1 23 18.20 8.30 -15 1 23 5.00 8.50 -13 -1 23 26.80 8.10 -13 1 23 28.30 8.60 -11 -1 23 14.60 7.00 -11 1 23 1.60 7.00 -9 -1 23 31.10 7.50 -9 1 23 19.60 7.00 -7 -1 23 4.10 6.10 -7 1 23 13.70 6.10 -5 -1 23 31.10 7.00 -5 1 23 18.50 7.00 -3 -1 23 12.40 6.70 -3 1 23 8.70 6.60 -1 -1 23 -7.80 7.20 -1 -1 23 7.30 6.40 -1 1 23 0.30 7.90 -1 1 23 -3.60 6.30 1 -1 23 35.10 7.80 1 -1 23 40.50 10.50 1 1 23 51.29 11.00 1 1 23 32.60 7.90 -14 -2 23 12.00 8.60 -14 2 23 18.80 8.40 -12 -2 23 10.40 7.20 -12 2 23 4.80 7.00 -10 -2 23 1.80 6.90 -10 2 23 7.20 6.90 -8 -2 23 5.30 6.50 -8 2 23 0.00 6.00 -6 -2 23 1.30 5.90 -6 2 23 13.20 6.70 -4 -2 23 -1.40 6.20 -4 2 23 -1.10 6.20 -2 -2 23 8.60 7.40 -2 -2 23 -3.50 5.80 -2 2 23 8.90 6.60 0 -2 23 13.10 8.40 0 -2 23 15.90 6.60 0 2 23 -20.10 8.30 0 2 23 2.10 6.80 2 -2 23 24.50 9.90 2 -2 23 14.30 7.20 2 2 23 3.50 9.30 2 2 23 19.40 7.90 -13 -3 23 4.10 7.40 -13 3 23 12.30 7.80 -11 -3 23 19.30 7.60 -11 3 23 7.50 7.30 -9 -3 23 53.99 8.80 -9 3 23 60.89 9.00 -7 -3 23 6.70 6.40 -7 3 23 1.50 6.60 -5 -3 23 37.20 7.60 -5 3 23 56.19 8.10 -3 -3 23 17.50 6.60 -3 -3 23 -5.20 6.80 -3 3 23 11.40 6.70 -1 -3 23 29.10 8.20 -1 -3 23 18.20 6.70 -1 3 23 14.70 9.40 -1 3 23 -4.10 6.70 1 -3 23 56.29 8.10 1 -3 23 21.80 9.00 1 3 23 43.90 8.90 1 3 23 69.29 11.60 -14 -4 23 14.00 8.80 -14 4 23 15.70 7.90 -12 -4 23 50.49 9.20 -12 4 23 42.20 8.20 -10 -4 23 8.20 6.90 -10 4 23 20.10 7.40 -8 -4 23 -0.30 5.90 -8 4 23 4.80 6.90 -6 -4 23 -2.70 6.00 -6 4 23 -4.10 6.20 -4 -4 23 28.20 7.00 -4 4 23 15.40 6.40 -2 -4 23 13.70 8.20 -2 -4 23 20.60 6.90 -2 4 23 25.50 7.10 0 -4 23 -2.00 7.00 0 -4 23 6.60 6.20 0 4 23 -0.20 7.00 0 4 23 6.10 9.30 2 -4 23 30.10 9.30 2 4 23 34.50 11.50 -13 -5 23 36.00 9.50 -13 5 23 18.30 7.90 -11 -5 23 1.20 7.60 -11 5 23 10.20 7.50 -9 -5 23 -3.80 6.50 -9 5 23 0.80 7.20 -7 -5 23 30.80 7.00 -7 5 23 29.20 7.40 -5 -5 23 27.40 6.90 -5 5 23 27.90 7.80 -3 -5 23 80.39 10.90 -3 -5 23 111.09 11.50 -3 5 23 76.99 9.90 -1 -5 23 37.50 9.50 -1 -5 23 46.80 7.60 -1 5 23 43.60 8.50 1 -5 23 1.00 8.30 1 -5 23 9.00 6.50 1 5 23 18.70 9.80 1 5 23 6.00 7.80 -12 -6 23 5.60 7.70 -12 6 23 7.90 7.60 -10 -6 23 4.10 7.20 -10 6 23 12.60 7.80 -8 -6 23 17.20 7.00 -8 6 23 13.00 7.30 -6 -6 23 -1.50 6.40 -6 6 23 5.70 6.70 -4 -6 23 -5.90 5.70 -4 -6 23 13.40 7.40 -4 6 23 -3.70 6.60 -2 -6 23 -11.90 6.00 -2 -6 23 -3.80 7.70 -2 6 23 -3.60 7.30 0 -6 23 6.80 6.30 0 -6 23 5.80 8.70 0 6 23 -0.50 7.50 0 6 23 7.60 10.00 -11 -7 23 7.80 7.70 -11 7 23 12.20 7.10 -9 -7 23 2.40 7.30 -9 7 23 -7.70 6.80 -7 -7 23 10.20 6.90 -7 7 23 7.70 6.80 -5 -7 23 13.80 6.50 -5 -7 23 19.40 7.80 -5 7 23 1.20 6.90 -3 -7 23 23.20 6.90 -3 -7 23 24.50 8.40 -3 7 23 24.60 7.80 -1 -7 23 18.10 8.60 -1 -7 23 -1.90 6.00 -1 7 23 -16.50 7.30 -10 -8 23 9.00 7.70 -10 8 23 4.80 6.90 -8 -8 23 3.50 7.10 -8 8 23 6.70 7.10 -6 -8 23 21.20 7.20 -6 8 23 26.60 8.20 -4 -8 23 13.20 8.10 -4 -8 23 24.00 6.80 -4 8 23 3.90 7.70 -2 -8 23 21.50 6.50 -2 -8 23 13.60 8.30 -2 8 23 12.30 8.40 -9 -9 23 17.10 7.80 -9 9 23 5.10 7.30 -7 -9 23 11.80 7.20 -7 9 23 9.00 7.30 -5 -9 23 8.30 8.20 -5 -9 23 5.80 6.70 -5 9 23 4.30 7.60 -3 -9 23 4.20 8.00 -12 0 24 -6.30 7.40 -10 0 24 27.70 7.70 -8 0 24 67.59 9.40 -6 0 24 0.60 6.80 -4 0 24 7.70 6.60 -2 0 24 70.79 9.30 -2 0 24 96.69 11.70 -11 -1 24 55.29 9.30 -11 1 24 52.39 9.50 -9 -1 24 9.70 7.10 -9 1 24 10.60 7.20 -7 -1 24 6.60 6.20 -7 1 24 14.90 7.10 -5 -1 24 4.70 6.70 -5 1 24 8.50 6.60 -3 -1 24 6.40 6.30 -3 1 24 8.60 6.60 -1 -1 24 -6.20 6.50 -1 -1 24 15.70 9.50 -1 1 24 7.00 7.00 -1 1 24 20.30 9.90 -12 -2 24 47.90 9.40 -12 2 24 35.30 9.10 -10 -2 24 4.80 6.90 -10 2 24 10.60 7.10 -8 -2 24 17.20 6.80 -8 2 24 6.40 7.20 -6 -2 24 7.40 6.40 -6 2 24 -2.30 6.40 -4 -2 24 -10.40 6.40 -4 2 24 -3.10 6.70 -2 -2 24 -11.00 8.30 -2 -2 24 -2.80 6.70 -2 2 24 13.40 7.60 -11 -3 24 10.00 7.90 -11 3 24 12.10 7.20 -9 -3 24 5.90 6.90 -9 3 24 -1.60 6.80 -7 -3 24 53.79 8.40 -7 3 24 43.90 8.70 -5 -3 24 4.10 6.50 -5 3 24 0.30 6.80 -3 -3 24 17.30 7.10 -3 -3 24 19.20 8.50 -3 3 24 14.70 7.20 -1 -3 24 2.90 9.50 -1 3 24 -9.70 9.90 -1 3 24 7.50 7.80 -10 -4 24 -3.00 7.20 -10 4 24 3.90 7.60 -8 -4 24 6.80 6.90 -8 4 24 1.90 6.70 -6 -4 24 24.80 7.10 -6 4 24 25.50 7.60 -4 -4 24 8.70 6.70 -4 -4 24 -21.60 7.70 -4 4 24 5.30 6.60 -2 -4 24 5.90 6.60 -2 -4 24 0.30 8.70 -2 4 24 -1.50 7.30 -9 -5 24 12.70 7.10 -9 5 24 10.40 7.80 -7 -5 24 0.90 6.60 -7 5 24 11.10 7.10 -5 -5 24 -6.70 6.20 -5 5 24 12.00 7.60 -3 -5 24 16.60 7.20 -3 -5 24 17.30 9.00 -3 5 24 23.50 8.40 -8 -6 24 7.90 6.90 -8 6 24 7.30 7.50 -6 -6 24 7.20 6.90 -6 6 24 6.10 7.20 -4 -6 24 14.70 8.60 -4 6 24 20.10 7.90 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 6413 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group As1 As -0.01421(3) 0.44936(2) 0.23633(4) 0.03368(19) Uani 0.5 1 d . U P . . B1 B 1.000000 0.93923(17) 0.250000 0.0279(7) Uani 1 2 d S T P . . C1 C 0.1515(3) 0.5641(2) 0.4108(3) 0.1129(19) Uani 1 1 d . . . . . H1A H 0.173922 0.561109 0.371555 0.169 Uiso 1 1 calc R U . . . H1B H 0.175068 0.532505 0.448681 0.169 Uiso 1 1 calc R U . . . H1C H 0.156196 0.610254 0.429717 0.169 Uiso 1 1 calc R U . . . C2 C 0.0719(3) 0.5457(2) 0.3832(2) 0.1013(17) Uani 1 1 d . . . . . H2 H 0.069523 0.496144 0.372240 0.122 Uiso 1 1 calc R U . . . C3 C 0.0328(4) 0.5566(4) 0.4411(3) 0.194(4) Uani 1 1 d . . . . . H3A H 0.033177 0.604799 0.452819 0.291 Uiso 1 1 calc R U . . . H3B H 0.056979 0.530969 0.483952 0.291 Uiso 1 1 calc R U . . . H3C H -0.016571 0.540894 0.423502 0.291 Uiso 1 1 calc R U . . . C4 C 0.03372(15) 0.58203(14) 0.31431(16) 0.0546(7) Uani 1 1 d . . . . . C5 C 0.03164(16) 0.65376(14) 0.31253(18) 0.0585(8) Uani 1 1 d . . . . . H4 H 0.052331 0.678257 0.355023 0.070 Uiso 1 1 calc R U . . . C6 C 0.000000 0.68933(19) 0.250000 0.0561(10) Uani 1 2 d S T P . . H5 H -0.000003 0.737343 0.250002 0.067 Uiso 1 2 calc R U P . . C7 C 0.000000 0.54790(16) 0.250000 0.0442(8) Uani 1 2 d S T P . . C8 C 0.03958(13) 0.39918(13) 0.18474(14) 0.0436(6) Uani 1 1 d . . . . . C9 C 0.11216(14) 0.41235(15) 0.18370(16) 0.0524(7) Uani 1 1 d . . . . . C10 C 0.13952(18) 0.3713(2) 0.1381(2) 0.0772(10) Uani 1 1 d . . . . . H9 H 0.186702 0.379017 0.135011 0.093 Uiso 1 1 calc R U . . . C11 C 0.0989(2) 0.3191(2) 0.0968(2) 0.0929(13) Uani 1 1 d . . . . . H10 H 0.119415 0.291542 0.067699 0.112 Uiso 1 1 calc R U . . . C12 C 0.02862(19) 0.3078(2) 0.0987(2) 0.0804(11) Uani 1 1 d . . . . . H11 H 0.001739 0.272914 0.070101 0.096 Uiso 1 1 calc R U . . . C13 C -0.00357(15) 0.34748(16) 0.14240(16) 0.0557(7) Uani 1 1 d . . . . . C14 C 0.15927(16) 0.46672(17) 0.2290(2) 0.0649(8) Uani 1 1 d . . . . . H13 H 0.131838 0.486575 0.260678 0.078 Uiso 1 1 calc R U . . . C15 C 0.1749(3) 0.5247(3) 0.1825(4) 0.137(2) Uani 1 1 d . . . . . H14A H 0.203058 0.507378 0.151637 0.205 Uiso 1 1 calc R U . . . H14B H 0.201815 0.560368 0.213362 0.205 Uiso 1 1 calc R U . . . H14C H 0.129870 0.543305 0.153128 0.205 Uiso 1 1 calc R U . . . C16 C 0.22992(18) 0.4369(2) 0.2785(3) 0.0859(12) Uani 1 1 d . . . . . H15A H 0.218556 0.399186 0.306152 0.129 Uiso 1 1 calc R U . . . H15B H 0.255108 0.472164 0.311119 0.129 Uiso 1 1 calc R U . . . H15C H 0.260310 0.420753 0.249305 0.129 Uiso 1 1 calc R U . . . C17 C -0.08280(16) 0.33455(19) 0.13941(19) 0.0691(9) Uani 1 1 d . . . . . H16 H -0.096665 0.370344 0.169375 0.083 Uiso 1 1 calc R U . . . C18 C -0.0931(2) 0.2658(3) 0.1733(3) 0.1054(15) Uani 1 1 d . . . . . H17A H -0.078179 0.229125 0.146684 0.158 Uiso 1 1 calc R U . . . H17B H -0.143478 0.259987 0.171552 0.158 Uiso 1 1 calc R U . . . H17C H -0.064113 0.264770 0.222987 0.158 Uiso 1 1 calc R U . . . C19 C -0.1324(2) 0.3430(3) 0.0636(2) 0.1072(16) Uani 1 1 d . . . . . H18A H -0.122857 0.306859 0.032937 0.161 Uiso 1 1 calc R U . . . H18B H -0.123611 0.386971 0.044412 0.161 Uiso 1 1 calc R U . . . H18C H -0.182157 0.340406 0.065088 0.161 Uiso 1 1 calc R U . . . C20 C 0.93239(10) 0.88509(10) 0.24412(11) 0.0265(4) Uani 1 1 d . . . . . C21 C 0.89172(11) 0.85963(11) 0.17694(11) 0.0286(4) Uani 1 1 d . . . . . H20 H 0.897936 0.879415 0.134649 0.034 Uiso 1 1 calc R U . . . C22 C 0.84229(11) 0.80577(11) 0.17094(12) 0.0308(5) Uani 1 1 d . . . . . C23 C 0.83153(12) 0.77451(11) 0.23202(12) 0.0340(5) Uani 1 1 d . . . . . H22 H 0.798506 0.738450 0.228107 0.041 Uiso 1 1 calc R U . . . C24 C 0.87161(12) 0.79859(11) 0.29975(12) 0.0334(5) Uani 1 1 d . . . . . C25 C 0.92037(11) 0.85272(11) 0.30532(11) 0.0303(5) Uani 1 1 d . . . . . H24 H 0.945977 0.868032 0.351337 0.036 Uiso 1 1 calc R U . . . C26 C 0.80318(12) 0.78142(13) 0.09618(13) 0.0385(5) Uani 1 1 d . . . . . C27 C 0.86234(16) 0.76383(14) 0.36680(15) 0.0490(7) Uani 1 1 d . . . . . C28 C 1.01458(11) 0.99081(10) 0.32023(12) 0.0302(5) Uani 1 1 d . . . . . C29 C 1.08402(12) 1.01726(12) 0.35252(14) 0.0399(5) Uani 1 1 d . . . . . H28 H 1.122673 1.002788 0.335187 0.048 Uiso 1 1 calc R U . . . C30 C 1.09743(14) 1.06426(14) 0.40938(16) 0.0518(7) Uani 1 1 d . . . . . C31 C 1.04136(15) 1.08801(14) 0.43583(16) 0.0540(7) Uani 1 1 d . . . . . H30 H 1.050234 1.119483 0.474039 0.065 Uiso 1 1 calc R U . . . C32 C 0.97189(14) 1.06403(13) 0.40433(14) 0.0443(6) Uani 1 1 d . . . . . C33 C 0.95922(12) 1.01603(11) 0.34788(13) 0.0352(5) Uani 1 1 d . . . . . H32 H 0.911963 1.000253 0.327928 0.042 Uiso 1 1 calc R U . . . C34 C 1.17360(19) 1.0878(3) 0.4430(3) 0.0866(14) Uani 1 1 d . . . . . C35 C 0.91031(19) 1.09082(18) 0.4302(2) 0.0665(9) Uani 1 1 d . . . . . F1 F 0.84919(8) 0.75724(8) 0.05987(8) 0.0505(4) Uani 1 1 d . U . A 1 F2 F 0.75584(9) 0.73090(9) 0.09633(9) 0.0632(5) Uani 1 1 d . U . B 1 F3 F 0.76587(8) 0.83184(8) 0.05471(8) 0.0559(4) Uani 1 1 d . U . C 1 F4 F 0.8004(2) 0.7814(4) 0.3816(3) 0.0880(11) Uani 0.7 1 d . U P D 1 F5 F 0.8536(5) 0.6969(2) 0.3595(3) 0.091(2) Uani 0.7 1 d . U P D 1 F6 F 0.9122(3) 0.7811(3) 0.4278(2) 0.0727(15) Uani 0.7 1 d . U P D 1 F7 F 1.1786(2) 1.1537(3) 0.4632(5) 0.0826(13) Uani 0.6 1 d . U P E 1 F8 F 1.2057(10) 1.0600(10) 0.5040(18) 0.098(7) Uani 0.2 1 d . U P E 1 F9 F 1.2101(13) 1.1000(14) 0.3936(17) 0.098(7) Uani 0.25 1 d . U P E 1 F10 F 0.9276(5) 1.1323(9) 0.4849(8) 0.110(4) Uani 0.509(3) 1 d . U P F 1 F11 F 0.8637(8) 1.1291(8) 0.3771(9) 0.117(4) Uani 0.509(3) 1 d . U P F 1 F12 F 0.8680(7) 1.0381(6) 0.4434(9) 0.084(3) Uani 0.509(3) 1 d . U P F 1 F4A F 0.8471(13) 0.8087(6) 0.4110(7) 0.082(4) Uani 0.2 1 d . U P D 2 F5A F 0.8030(8) 0.7313(13) 0.3569(7) 0.082(4) Uani 0.2 1 d . U P D 2 F6A F 0.9242(11) 0.7536(9) 0.4123(7) 0.061(4) Uani 0.2 1 d . U P D 2 F7A F 1.1832(9) 1.0827(9) 0.5302(7) 0.070(4) Uani 0.25 1 d . U P E 2 F8A F 1.2256(10) 1.0429(14) 0.4361(10) 0.072(6) Uani 0.25 1 d . U P E 2 F9A F 1.1974(6) 1.1302(8) 0.4182(11) 0.090(4) Uani 0.3 1 d . U P E 2 F10A F 0.9149(14) 1.1573(11) 0.443(2) 0.058(6) Uani 0.138(3) 1 d . U P F 2 F12A F 0.903(2) 1.062(2) 0.489(2) 0.087(6) Uani 0.138(3) 1 d . U P F 2 F11A F 0.8434(13) 1.091(2) 0.3743(19) 0.078(7) Uani 0.138(3) 1 d . U P F 2 F10B F 0.9331(8) 1.0962(9) 0.5079(6) 0.078(3) Uani 0.353(3) 1 d . U P F 3 F11B F 0.8908(10) 1.1514(10) 0.4066(10) 0.091(5) Uani 0.353(3) 1 d . U P F 3 F12B F 0.8524(8) 1.0550(8) 0.4142(11) 0.077(4) Uani 0.353(3) 1 d . U P F 3 F6B F 0.8952(13) 0.7037(9) 0.3771(11) 0.138(7) Uani 0.3 1 d . U P D 3 F7B F 1.1825(5) 1.1175(10) 0.5064(10) 0.074(3) Uani 0.25 1 d . U P E 3 F8B F 1.2190(5) 1.0385(6) 0.4630(5) 0.086(3) Uani 0.6 1 d . U P E 3 F9B F 1.1993(10) 1.1215(8) 0.3714(9) 0.068(3) Uani 0.3 1 d . U P E 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 As1 0.0341(5) 0.0295(2) 0.0399(5) -0.00301(19) 0.0142(3) -0.00162(18) B1 0.0254(15) 0.0300(16) 0.0264(17) 0.000 0.0040(13) 0.000 C1 0.110(3) 0.073(2) 0.108(3) -0.003(2) -0.051(3) -0.003(2) C2 0.121(3) 0.065(2) 0.082(3) 0.0225(19) -0.033(3) -0.039(2) C3 0.181(7) 0.308(11) 0.081(4) 0.059(5) 0.016(4) -0.095(7) C4 0.0504(15) 0.0453(15) 0.0613(18) 0.0019(13) 0.0037(13) -0.0147(12) C5 0.0569(16) 0.0447(15) 0.068(2) -0.0094(14) 0.0065(14) -0.0157(13) C6 0.048(2) 0.0332(18) 0.085(3) 0.000 0.014(2) 0.000 C7 0.0341(17) 0.0312(17) 0.066(2) 0.000 0.0113(16) 0.000 C8 0.0431(13) 0.0477(14) 0.0415(14) 0.0078(11) 0.0139(11) 0.0164(11) C9 0.0448(14) 0.0624(17) 0.0541(16) 0.0066(13) 0.0205(12) 0.0142(12) C10 0.0572(18) 0.101(3) 0.084(2) -0.017(2) 0.0373(18) 0.0086(18) C11 0.078(2) 0.123(3) 0.088(3) -0.040(3) 0.040(2) 0.014(2) C12 0.067(2) 0.098(3) 0.074(2) -0.036(2) 0.0154(18) 0.0093(18) C13 0.0478(15) 0.0682(18) 0.0475(16) -0.0063(14) 0.0067(12) 0.0138(13) C14 0.0438(15) 0.0619(18) 0.094(2) -0.0019(17) 0.0265(16) 0.0052(13) C15 0.135(4) 0.087(3) 0.185(6) 0.040(4) 0.039(4) -0.021(3) C16 0.0452(17) 0.086(3) 0.117(3) -0.010(2) 0.0068(19) 0.0014(17) C17 0.0443(15) 0.085(2) 0.071(2) -0.0203(18) 0.0042(14) 0.0040(15) C18 0.073(3) 0.115(4) 0.121(4) -0.006(3) 0.014(2) -0.026(2) C19 0.061(2) 0.158(4) 0.082(3) -0.030(3) -0.014(2) 0.028(2) C20 0.0260(10) 0.0269(10) 0.0246(10) -0.0012(8) 0.0035(8) 0.0032(8) C21 0.0292(10) 0.0318(10) 0.0235(11) 0.0014(8) 0.0049(8) 0.0020(8) C22 0.0266(10) 0.0331(11) 0.0290(11) -0.0064(9) 0.0013(9) 0.0018(8) C23 0.0331(11) 0.0317(11) 0.0373(13) -0.0052(9) 0.0096(9) -0.0055(9) C24 0.0386(12) 0.0335(11) 0.0291(12) -0.0012(9) 0.0111(9) -0.0014(9) C25 0.0325(11) 0.0329(11) 0.0230(11) -0.0036(8) 0.0033(8) -0.0004(9) C26 0.0333(11) 0.0439(13) 0.0339(12) -0.0091(10) 0.0017(10) -0.0015(10) C27 0.0634(17) 0.0473(15) 0.0387(15) -0.0003(12) 0.0178(14) -0.0153(13) C28 0.0298(10) 0.0282(10) 0.0296(11) 0.0009(9) 0.0030(9) -0.0003(8) C29 0.0320(11) 0.0378(12) 0.0467(14) -0.0080(11) 0.0052(10) 0.0003(9) C30 0.0384(13) 0.0458(14) 0.0629(18) -0.0229(13) -0.0005(12) -0.0033(11) C31 0.0551(16) 0.0484(15) 0.0519(16) -0.0255(13) 0.0034(13) -0.0002(12) C32 0.0476(14) 0.0407(13) 0.0457(15) -0.0102(11) 0.0147(11) 0.0003(11) C33 0.0323(11) 0.0347(11) 0.0370(12) -0.0036(9) 0.0070(9) -0.0018(9) C34 0.0452(19) 0.075(3) 0.123(4) -0.053(3) -0.005(2) -0.007(2) C35 0.066(2) 0.063(2) 0.078(2) -0.0260(19) 0.0330(18) 0.0012(17) F1 0.0469(8) 0.0661(10) 0.0348(8) -0.0183(7) 0.0045(6) 0.0071(7) F2 0.0608(10) 0.0748(11) 0.0474(9) -0.0211(8) 0.0037(7) -0.0346(8) F3 0.0539(9) 0.0644(10) 0.0353(8) -0.0077(7) -0.0118(7) 0.0157(7) F4 0.084(3) 0.128(4) 0.073(2) 0.031(2) 0.056(2) 0.013(3) F5 0.175(6) 0.045(2) 0.058(2) -0.0006(18) 0.039(3) -0.042(4) F6 0.106(4) 0.080(3) 0.0253(19) 0.0025(19) 0.0061(18) -0.043(3) F7 0.060(2) 0.067(3) 0.105(4) -0.035(3) -0.003(3) -0.0209(19) F8 0.060(9) 0.084(12) 0.117(16) 0.027(11) -0.035(10) -0.010(8) F9 0.056(9) 0.141(17) 0.100(13) -0.036(14) 0.028(9) -0.046(11) F10 0.106(5) 0.131(9) 0.106(9) -0.071(6) 0.051(7) -0.001(7) F11 0.097(9) 0.130(10) 0.134(9) -0.003(8) 0.046(7) 0.065(7) F12 0.080(6) 0.090(5) 0.102(7) 0.005(5) 0.059(6) 0.011(4) F4A 0.134(11) 0.087(7) 0.048(6) -0.012(5) 0.062(7) -0.027(8) F5A 0.071(7) 0.108(10) 0.074(8) 0.022(8) 0.032(6) -0.036(7) F6A 0.098(8) 0.057(9) 0.017(6) 0.009(5) -0.003(6) -0.019(8) F7A 0.081(8) 0.069(8) 0.037(5) -0.006(5) -0.022(5) -0.012(6) F8A 0.027(4) 0.123(12) 0.060(10) -0.046(10) 0.001(6) -0.010(5) F9A 0.059(5) 0.084(9) 0.113(12) 0.017(7) -0.001(6) -0.021(6) F10A 0.065(11) 0.036(7) 0.071(15) -0.020(10) 0.019(12) 0.004(7) F12A 0.099(14) 0.111(15) 0.065(13) 0.019(11) 0.047(11) 0.016(11) F11A 0.048(9) 0.104(17) 0.084(13) -0.011(14) 0.021(9) 0.023(11) F10B 0.093(6) 0.101(8) 0.049(4) -0.022(6) 0.036(4) 0.006(7) F11B 0.089(11) 0.096(9) 0.094(10) 0.007(8) 0.036(8) 0.051(7) F12B 0.056(6) 0.077(8) 0.110(12) -0.036(7) 0.044(7) -0.011(6) F6B 0.218(15) 0.105(12) 0.121(13) 0.071(10) 0.099(11) 0.086(11) F7B 0.057(5) 0.083(9) 0.069(8) -0.043(6) -0.005(6) -0.015(7) F8B 0.047(3) 0.126(5) 0.071(6) -0.016(5) -0.008(4) 0.008(3) F9B 0.050(5) 0.063(5) 0.089(9) -0.004(6) 0.016(5) -0.024(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' As As 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 As1 As1 C8 87.99(15) 2 . As1 As1 C7 80.45(2) 2 . C8 As1 C7 120.34(9) . . As1 As1 C8 72.90(15) 2 2 C8 As1 C8 115.55(15) . 2 C7 As1 C8 116.10(8) . 2 C28 B1 C28 104.6(2) . 2_755 C28 B1 C20 113.68(10) . . C28 B1 C20 112.27(10) 2_755 . C28 B1 C20 112.27(10) . 2_755 C28 B1 C20 113.68(10) 2_755 2_755 C20 B1 C20 100.7(2) . 2_755 C2 C1 H1A 109.5 . . C2 C1 H1B 109.5 . . H1A C1 H1B 109.5 . . C2 C1 H1C 109.5 . . H1A C1 H1C 109.5 . . H1B C1 H1C 109.5 . . C4 C2 C1 113.6(4) . . C4 C2 C3 111.0(5) . . C1 C2 C3 111.3(4) . . C4 C2 H2 106.9 . . C1 C2 H2 106.9 . . C3 C2 H2 106.9 . . C2 C3 H3A 109.5 . . C2 C3 H3B 109.5 . . H3A C3 H3B 109.5 . . C2 C3 H3C 109.5 . . H3A C3 H3C 109.5 . . H3B C3 H3C 109.5 . . C7 C4 C5 116.8(3) . . C7 C4 C2 123.4(3) . . C5 C4 C2 119.8(3) . . C6 C5 C4 121.8(3) . . C6 C5 H4 119.1 . . C4 C5 H4 119.1 . . C5 C6 C5 119.5(4) 2 . C5 C6 H5 120.2 2 . C5 C6 H5 120.2 . . C4 C7 C4 123.1(3) 2 . C4 C7 As1 109.63(15) 2 . C4 C7 As1 127.08(17) . . C4 C7 As1 127.08(17) 2 2 C4 C7 As1 109.63(15) . 2 As1 C7 As1 19.10(4) . 2 C13 C8 C9 123.0(2) . . C13 C8 As1 110.65(19) . . C9 C8 As1 126.3(2) . . C13 C8 As1 124.5(2) . 2 C9 C8 As1 111.6(2) . 2 As1 C8 As1 19.11(3) . 2 C10 C9 C8 116.4(3) . . C10 C9 C14 119.9(3) . . C8 C9 C14 123.7(2) . . C11 C10 C9 122.0(3) . . C11 C10 H9 119.0 . . C9 C10 H9 119.0 . . C12 C11 C10 120.2(3) . . C12 C11 H10 119.9 . . C10 C11 H10 119.9 . . C11 C12 C13 121.5(3) . . C11 C12 H11 119.3 . . C13 C12 H11 119.3 . . C12 C13 C8 116.9(3) . . C12 C13 C17 118.9(3) . . C8 C13 C17 124.1(3) . . C9 C14 C15 111.6(4) . . C9 C14 C16 112.4(3) . . C15 C14 C16 111.1(3) . . C9 C14 H13 107.1 . . C15 C14 H13 107.1 . . C16 C14 H13 107.1 . . C14 C15 H14A 109.5 . . C14 C15 H14B 109.5 . . H14A C15 H14B 109.5 . . C14 C15 H14C 109.5 . . H14A C15 H14C 109.5 . . H14B C15 H14C 109.5 . . C14 C16 H15A 109.5 . . C14 C16 H15B 109.5 . . H15A C16 H15B 109.5 . . C14 C16 H15C 109.5 . . H15A C16 H15C 109.5 . . H15B C16 H15C 109.5 . . C19 C17 C18 112.6(4) . . C19 C17 C13 112.1(3) . . C18 C17 C13 111.8(3) . . C19 C17 H16 106.6 . . C18 C17 H16 106.6 . . C13 C17 H16 106.6 . . C17 C18 H17A 109.5 . . C17 C18 H17B 109.5 . . H17A C18 H17B 109.5 . . C17 C18 H17C 109.5 . . H17A C18 H17C 109.5 . . H17B C18 H17C 109.5 . . C17 C19 H18A 109.5 . . C17 C19 H18B 109.5 . . H18A C19 H18B 109.5 . . C17 C19 H18C 109.5 . . H18A C19 H18C 109.5 . . H18B C19 H18C 109.5 . . C21 C20 C25 115.62(18) . . C21 C20 B1 121.22(16) . . C25 C20 B1 122.23(15) . . C22 C21 C20 122.4(2) . . C22 C21 H20 118.8 . . C20 C21 H20 118.8 . . C23 C22 C21 120.93(19) . . C23 C22 C26 121.2(2) . . C21 C22 C26 117.8(2) . . C22 C23 C24 117.9(2) . . C22 C23 H22 121.0 . . C24 C23 H22 121.0 . . C25 C24 C23 120.8(2) . . C25 C24 C27 120.5(2) . . C23 C24 C27 118.7(2) . . C24 C25 C20 122.28(19) . . C24 C25 H24 118.9 . . C20 C25 H24 118.9 . . F2 C26 F3 106.62(18) . . F2 C26 F1 106.51(19) . . F3 C26 F1 105.5(2) . . F2 C26 C22 113.1(2) . . F3 C26 C22 112.49(19) . . F1 C26 C22 112.09(18) . . F5A C27 F6A 130.5(10) . . F5A C27 F4A 94.7(11) . . F6A C27 F4A 89.5(10) . . F5 C27 F6 112.5(4) . . F5 C27 F4 100.4(4) . . F6 C27 F4 102.3(4) . . F5A C27 C24 113.9(6) . . F6A C27 C24 110.4(8) . . F4A C27 C24 110.7(5) . . F6B C27 C24 111.4(7) . . F5 C27 C24 113.3(3) . . F6 C27 C24 114.3(3) . . F4 C27 C24 112.6(3) . . C33 C28 C29 115.5(2) . . C33 C28 B1 123.26(16) . . C29 C28 B1 121.01(18) . . C30 C29 C28 122.5(2) . . C30 C29 H28 118.8 . . C28 C29 H28 118.8 . . C31 C30 C29 120.6(2) . . C31 C30 C34 120.1(3) . . C29 C30 C34 119.2(3) . . C32 C31 C30 118.5(2) . . C32 C31 H30 120.8 . . C30 C31 H30 120.8 . . C31 C32 C33 120.4(2) . . C31 C32 C35 119.4(2) . . C33 C32 C35 120.2(2) . . C28 C33 C32 122.5(2) . . C28 C33 H32 118.7 . . C32 C33 H32 118.7 . . F8B C34 F7B 98.4(9) . . F8 C34 F7 99.3(11) . . F8 C34 F9 120.2(16) . . F7 C34 F9 91.5(12) . . F9A C34 F8A 92.2(13) . . F9A C34 C30 120.5(8) . . F8B C34 C30 113.8(6) . . F8 C34 C30 115.7(9) . . F7B C34 C30 113.5(6) . . F7 C34 C30 113.8(3) . . F9 C34 C30 112.6(11) . . F8A C34 C30 114.6(9) . . F9A C34 F7A 122.6(11) . . F8A C34 F7A 100.3(10) . . C30 C34 F7A 104.3(6) . . F8B C34 F9B 101.8(8) . . F7B C34 F9B 125.5(12) . . C30 C34 F9B 103.3(6) . . F12B C35 F11B 105.5(10) . . F12A C35 F10A 106.6(18) . . F10 C35 F12 110.5(8) . . F10 C35 F11 103.5(7) . . F12 C35 F11 104.1(7) . . F12A C35 F11A 111.1(18) . . F10A C35 F11A 97.8(16) . . F12B C35 F10B 106.8(9) . . F11B C35 F10B 106.0(8) . . F12B C35 C32 116.4(6) . . F11B C35 C32 112.6(7) . . F10 C35 C32 115.9(5) . . F12A C35 C32 114.9(10) . . F10A C35 C32 112.7(12) . . F12 C35 C32 111.1(6) . . F11 C35 C32 110.8(6) . . F11A C35 C32 112.4(11) . . F10B C35 C32 108.9(6) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 As1 As1 0.6424(8) 2 As1 C8 1.876(3) . As1 C7 1.935(3) . As1 C8 1.961(3) 2 B1 C28 1.634(3) . B1 C28 1.634(3) 2_755 B1 C20 1.643(3) . B1 C20 1.643(3) 2_755 C1 C2 1.509(6) . C1 H1A 0.9600 . C1 H1B 0.9600 . C1 H1C 0.9600 . C2 C4 1.495(5) . C2 C3 1.508(9) . C2 H2 0.9800 . C3 H3A 0.9600 . C3 H3B 0.9600 . C3 H3C 0.9600 . C4 C7 1.389(3) . C4 C5 1.390(4) . C5 C6 1.368(4) . C5 H4 0.9300 . C6 H5 0.9300 . C8 C13 1.404(4) . C8 C9 1.414(4) . C9 C10 1.383(4) . C9 C14 1.497(5) . C10 C11 1.382(5) . C10 H9 0.9300 . C11 C12 1.369(5) . C11 H10 0.9300 . C12 C13 1.394(4) . C12 H11 0.9300 . C13 C17 1.518(4) . C14 C15 1.510(6) . C14 C16 1.533(5) . C14 H13 0.9800 . C15 H14A 0.9600 . C15 H14B 0.9600 . C15 H14C 0.9600 . C16 H15A 0.9600 . C16 H15B 0.9600 . C16 H15C 0.9600 . C17 C19 1.507(5) . C17 C18 1.516(6) . C17 H16 0.9800 . C18 H17A 0.9600 . C18 H17B 0.9600 . C18 H17C 0.9600 . C19 H18A 0.9600 . C19 H18B 0.9600 . C19 H18C 0.9600 . C20 C21 1.396(3) . C20 C25 1.399(3) . C21 C22 1.390(3) . C21 H20 0.9300 . C22 C23 1.378(3) . C22 C26 1.496(3) . C23 C24 1.392(3) . C23 H22 0.9300 . C24 C25 1.387(3) . C24 C27 1.499(3) . C25 H24 0.9300 . C26 F2 1.332(3) . C26 F3 1.334(3) . C26 F1 1.342(3) . C27 F5A 1.264(10) . C27 F6A 1.277(18) . C27 F4A 1.298(11) . C27 F6B 1.312(14) . C27 F5 1.310(5) . C27 F6 1.331(6) . C27 F4 1.332(4) . C28 C33 1.392(3) . C28 C29 1.398(3) . C29 C30 1.386(4) . C29 H28 0.9300 . C30 C31 1.381(4) . C30 C34 1.492(4) . C31 C32 1.379(4) . C31 H30 0.9300 . C32 C33 1.394(3) . C32 C35 1.487(4) . C33 H32 0.9300 . C34 F9A 1.105(13) . C34 F8B 1.276(11) . C34 F8 1.28(2) . C34 F7B 1.308(12) . C34 F7 1.330(6) . C34 F9 1.34(3) . C34 F8A 1.35(2) . C34 F7A 1.627(15) . C34 F9B 1.703(18) . C35 F12B 1.270(13) . C35 F11B 1.276(15) . C35 F10 1.287(8) . C35 F12A 1.30(2) . C35 F10A 1.31(2) . C35 F12 1.367(12) . C35 F11 1.371(14) . C35 F11A 1.42(3) . C35 F10B 1.430(12) .