Crystallography Open Database

Information card for entry 7121143

Preview

Coordinates	7121143.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	(EMind)ClGe=GeCl(EMind)
Chemical name	dichlorodigermene
Formula	C48 H74 Cl2 Ge2
Calculated formula	C48 H74 Cl2 Ge2
Title of publication	A stable free tetragermacyclobutadiene incorporating fused-ring bulky EMind groups.
Authors of publication	Suzuki, Katsunori; Numata, Yasuyuki; Fujita, Naoko; Hayakawa, Naoki; Tanikawa, Tomoharu; Hashizume, Daisuke; Tamao, Kohei; Fueno, Hiroyuki; Tanaka, Kazuyoshi; Matsuo, Tsukasa
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	18
Pages of publication	2200 - 2203
a	10.9924 ± 0.0004 Å
b	11.3428 ± 0.0004 Å
c	11.8084 ± 0.0005 Å
α	118.544 ± 0.004°
β	92.15 ± 0.003°
γ	113.282 ± 0.003°
Cell volume	1140.33 ± 0.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0552
Residual factor for significantly intense reflections	0.0438
Weighted residual factors for significantly intense reflections	0.1116
Weighted residual factors for all reflections included in the refinement	0.115
Goodness-of-fit parameter for all reflections included in the refinement	1.133
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
228438 (current)	2019-11-17	cif/ Updating files of 7121142, 7121143 Original log message: Adding full bibliography for 7121142--7121143.cif.	7121143.cif
205234	2018-01-16	cif/ Adding structures of 7121142, 7121143 via cif-deposit CGI script.	7121143.cif