Crystallography Open Database

Information card for entry 7121809

Preview

Coordinates	7121809.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C25 H37 B N6 O2 Si W
Calculated formula	C25 H37 B N6 O2 Si W
Title of publication	Bis(alkylidynyl)arsines.
Authors of publication	Frogley, Benjamin J.; Hill, Anthony F.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2018
Journal volume	54
Journal issue	55
Pages of publication	7649 - 7652
a	12.636 ± 0.0004 Å
b	14.8272 ± 0.0005 Å
c	16.3046 ± 0.0006 Å
α	90°
β	109.839 ± 0.004°
γ	90°
Cell volume	2873.47 ± 0.18 Å³
Cell temperature	150 ± 0.1 K
Ambient diffraction temperature	150 ± 0.1 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0525
Residual factor for significantly intense reflections	0.0327
Weighted residual factors for significantly intense reflections	0.061
Weighted residual factors for all reflections included in the refinement	0.0708
Goodness-of-fit parameter for all reflections included in the refinement	1.103
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
228060 (current)	2019-11-17	cif/ Updating files of 7121808, 7121809, 7121810 Original log message: Adding full bibliography for 7121808--7121810.cif.	7121809.cif
208151	2018-06-06	cif/ Adding structures of 7121808, 7121809, 7121810 via cif-deposit CGI script.	7121809.cif