#------------------------------------------------------------------------------ #$Date: 2019-01-16 01:03:25 +0200 (Wed, 16 Jan 2019) $ #$Revision: 213084 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/12/28/7122841.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7122841 loop_ _publ_author_name 'Gauld, Richard M.' 'Kennedy, Alan R.' 'McLellan, Ross' 'Barker, Jim' 'Reid, Jacqueline' 'Mulvey, Robert E.' _publ_section_title ; Diverse outcomes of CO2 fixation using alkali metal amides including formation of a heterobimetallic lithium--sodium carbamato-anhydride via lithium--sodium bis-hexamethyldisilazide ; _journal_name_full 'Chemical Communications' _journal_paper_doi 10.1039/C8CC08308H _journal_year 2019 _chemical_formula_moiety 'C9 H12 Li N O3' _chemical_formula_sum 'C9 H12 Li N O3' _chemical_formula_weight 189.14 _chemical_properties_physical Air-sensitive,Moisture-sensitive,Oxygen-sensitive _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_Int_Tables_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_primary direct _audit_creation_date 2018-06-04 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2018-10-12 deposited with the CCDC. 2018-12-26 downloaded from the CCDC. ; _cell_angle_alpha 84.577(15) _cell_angle_beta 87.445(14) _cell_angle_gamma 76.369(17) _cell_formula_units_Z 2 _cell_length_a 5.4312(10) _cell_length_b 7.6252(16) _cell_length_c 12.092(2) _cell_measurement_reflns_used 809 _cell_measurement_temperature 153 _cell_measurement_theta_max 29.2934 _cell_measurement_theta_min 3.3532 _cell_volume 484.37(16) _computing_cell_refinement ; CrysAlisPro, Oxford Diffraction Ltd., Version 1.171.34.40 (release 27-08-2010 CrysAlis171 .NET) (compiled Aug 27 2010,11:50:40) ; _computing_data_collection ; CrysAlisPro, Oxford Diffraction Ltd., Version 1.171.34.40 (release 27-08-2010 CrysAlis171 .NET) (compiled Aug 27 2010,11:50:40) ; _computing_data_reduction ; CrysAlisPro, Oxford Diffraction Ltd., Version 1.171.34.40 (release 27-08-2010 CrysAlis171 .NET) (compiled Aug 27 2010,11:50:40) ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _computing_structure_solution 'SIR2004 (Burla et al., 2007)' _diffrn_ambient_temperature 153 _diffrn_detector_area_resol_mean 16.0727 _diffrn_measured_fraction_theta_full 0.9179 _diffrn_measured_fraction_theta_max 0.8932 _diffrn_measurement_details ; #__ type_ start__ end____ width___ exp.time_ 1 omega -46.00 49.00 1.0000 80.0000 omega____ theta____ kappa____ phi______ frames - -20.4381 37.0000 120.0000 95 #__ type_ start__ end____ width___ exp.time_ 2 omega -89.00 -48.00 1.0000 80.0000 omega____ theta____ kappa____ phi______ frames - -20.4381 142.0000 40.0000 41 #__ type_ start__ end____ width___ exp.time_ 3 omega -72.00 -32.00 1.0000 80.0000 omega____ theta____ kappa____ phi______ frames - -20.4381 179.0000 90.0000 40 #__ type_ start__ end____ width___ exp.time_ 4 omega -90.00 5.00 1.0000 80.0000 omega____ theta____ kappa____ phi______ frames - -20.4381 -37.0000 -60.0000 95 ; _diffrn_measurement_device_type 'Xcalibur, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_UB_11 0.0021963000 _diffrn_orient_matrix_UB_12 0.0306183000 _diffrn_orient_matrix_UB_13 -0.0572018000 _diffrn_orient_matrix_UB_21 0.0379054000 _diffrn_orient_matrix_UB_22 0.0781244000 _diffrn_orient_matrix_UB_23 0.0135042000 _diffrn_orient_matrix_UB_31 0.1289443000 _diffrn_orient_matrix_UB_32 -0.0467956000 _diffrn_orient_matrix_UB_33 -0.0044125000 _diffrn_radiation_monochromator graphite _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0239 _diffrn_reflns_av_unetI/netI 0.0749 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -8 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 2777 _diffrn_reflns_theta_full 25.0000 _diffrn_reflns_theta_max 27.00 _diffrn_reflns_theta_min 3.36 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.095 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.47084 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro, Oxford Diffraction Ltd., Version 1.171.34.40 (release 27-08-2010 CrysAlis171 .NET) (compiled Aug 27 2010,11:50:40) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.2968 _exptl_crystal_description block _exptl_crystal_F_000 200.1140 _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.3 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.3836 _refine_diff_density_min -0.4085 _refine_diff_density_rms 0.0958 _refine_ls_d_res_high 0.7829 _refine_ls_d_res_low 6.0634 _refine_ls_goodness_of_fit_ref 1.0978 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 20 _refine_ls_number_parameters 127 _refine_ls_number_reflns 1891 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.0978 _refine_ls_R_factor_all 0.1196 _refine_ls_R_factor_gt 0.0641 _refine_ls_shift/su_max 0.0008 _refine_ls_shift/su_mean 0.0002 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0795P)^2^+0.0363P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1507 _refine_ls_wR_factor_ref 0.1939 _reflns_Friedel_coverage 0.0 _reflns_limit_h_max 6 _reflns_limit_h_min -6 _reflns_limit_k_max 9 _reflns_limit_k_min -9 _reflns_limit_l_max 15 _reflns_limit_l_min 0 _reflns_number_gt 1145 _reflns_number_total 1891 _reflns_threshold_expression I>=2u(I) _iucr_refine_instructions_details ; TITL CELL 0.71073 5.4312 7.6252 12.092 84.577 87.445 76.369 ZERR 2 0.001 0.0016 0.002 0.015 0.014 0.017 LATT 1 SFAC C H Li N O UNIT 18 24 2 2 6 L.S. 4 PLAN 20 SIZE 0.2 0.4 0.3 TEMP -120 FMAP 2 ACTA 50.00 BOND $H CONF MERG 2 OMIT -3 54 WGHT 0.079531 0.036256 FVAR 8.637278 REM REM REM Li1 3 0.33799 0.95824 0.42541 11.00000 0.01958 0.05713 0.02784 = 0.00152 -0.00084 -0.01179 O1 5 -0.02639 0.94145 0.64140 11.00000 0.01766 0.06896 0.03537 = 0.00485 -0.00339 -0.01142 O2 5 0.37934 0.90955 0.58495 11.00000 0.02307 0.05397 0.02655 = 0.00166 0.00208 -0.01403 O3 5 0.50340 0.73650 0.35680 11.00000 0.04248 0.05642 0.04442 = -0.00902 0.00252 0.00276 N1 4 0.28289 0.84450 0.76719 11.00000 0.01786 0.03903 0.02642 = 0.00100 -0.00061 -0.00870 C1 1 0.52704 0.77304 0.79995 11.00000 0.02065 0.04885 0.03673 = 0.00512 -0.00133 -0.00578 AFIX 43 H1 2 0.67410 0.75595 0.75294 11.00000 -1.20000 AFIX 0 C2 1 0.52140 0.73111 0.91131 11.00000 0.03465 0.07017 0.03912 = 0.01424 -0.01101 -0.01678 AFIX 43 H2 2 0.66383 0.67800 0.95598 11.00000 -1.20000 AFIX 0 C3 1 0.26690 0.78009 0.94941 11.00000 0.04388 0.08899 0.02948 = 0.00572 0.00049 -0.03180 AFIX 43 H3 2 0.20708 0.76740 1.02409 11.00000 -1.20000 AFIX 0 C4 1 0.12462 0.84837 0.85970 11.00000 0.02357 0.06175 0.03233 = -0.00261 0.00629 -0.01438 AFIX 43 H4 2 -0.05435 0.89175 0.86026 11.00000 -1.20000 AFIX 0 C5 1 0.20419 0.90332 0.65630 11.00000 0.02081 0.03316 0.03329 = 0.00084 -0.00147 -0.01024 C6 1 0.71004 0.61089 0.40790 11.00000 0.09952 0.08460 0.05397 = 0.00763 0.00113 0.04643 AFIX 23 H6a 2 0.75888 0.65915 0.47473 11.00000 -1.20000 H6b 2 0.66153 0.49539 0.43115 11.00000 -1.20000 AFIX 0 C7 1 0.91949 0.58052 0.32956 11.00000 0.04071 0.10188 0.09524 = -0.02671 -0.00434 -0.00279 AFIX 23 H7a 2 1.04665 0.64733 0.34700 11.00000 -1.20000 H7b 2 1.00225 0.44989 0.33160 11.00000 -1.20000 AFIX 0 C8 1 0.81177 0.64768 0.21851 11.00000 0.07079 0.06523 0.06530 = -0.00741 0.02631 -0.00786 AFIX 23 H8a 2 0.88844 0.74571 0.18381 11.00000 -1.20000 H8b 2 0.84218 0.54845 0.16875 11.00000 -1.20000 AFIX 0 C9 1 0.53490 0.71702 0.24005 11.00000 0.06098 0.06969 0.04905 = -0.02169 -0.00505 -0.01010 AFIX 23 H9a 2 0.43923 0.63059 0.21827 11.00000 -1.20000 H9b 2 0.47262 0.83520 0.19706 11.00000 -1.20000 AFIX 0 HKLF 4 END Q1 1 0.944444 0.56 0.35 11 0.05 0.38 Q2 1 0.666667 0.6 0.475 11 0.05 0.33 Q3 1 0.333333 0.96 0.525 11 0.05 0.32 Q4 1 0 1.04 0.775 11 0.05 0.29 Q5 1 0.944444 0.76 0.275 11 0.05 0.28 Q6 1 0.888889 0.76 0.725 11 0.05 0.28 Q7 1 0.833333 0.72 1.025 11 0.05 0.27 Q8 1 -0.055556 1.12 0.675 11 0.05 0.27 Q9 1 1.277778 0.48 0.275 11 0.05 0.27 Q10 1 0.666667 0.4 0.375 11 0.05 0.27 Q11 1 0.777778 0.84 0.075 11 0.05 0.26 Q12 1 0.611111 0.52 0.875 11 0.05 0.25 Q13 1 0.833333 0.76 0.45 11 0.05 0.25 Q14 1 0.944444 0.88 0.15 11 0.05 0.25 Q15 1 0.5 0.72 0.425 11 0.05 0.25 Q16 1 0.277778 0.92 0.75 11 0.05 0.25 Q17 1 -0.055556 0.8 0.625 11 0.05 0.24 Q18 1 0.388889 0.76 0.15 11 0.05 0.24 Q19 1 0.5 0.68 0.325 11 0.05 0.24 Q20 1 0.277778 0.76 0.725 11 0.05 0.24 REM The information below was added by Olex2. REM REM R1 = 0.0641 for 1145 Fo > 4sig(Fo) and 0.1196 for all 1891 data REM 127 parameters refined using 0 restraints REM Highest difference peak 0.3836, deepest hole -0.4085 REM Mean Shift 0.0002, Max Shift 0.0008. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.1196 REM R1_gt = 0.0641 REM wR_ref = 0.1939 REM GOOF = 1.0978 REM Shift_max = 0.0008 REM Shift_mean = 0.0002 REM Reflections_all = 1891 REM Reflections_gt = 1145 REM Parameters = 127 REM Hole = -0.4085 REM Peak = 0.3836 REM Flack = n/a ; _cod_data_source_file c8cc08308h2.cif _cod_data_source_block RMG164 _cod_database_code 7122841 _reflns_odcompleteness_completeness 89.34 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 27.01 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2.a Secondary CH2 refined with riding coordinates: C6(H6a,H6b), C7(H7a,H7b), C8(H8a,H8b), C9(H9a,H9b) 2.b Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C3(H3), C4(H4) ; _iucr_refine_fcf_details ; data_RMG164_CCDC1 _computing_structure_refinement 'olex2.refine (Bourhis et al., 2015)' _shelx_refln_list_code 4 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_Int_Tables_number 2 _cell_length_a 5.4312(10) _cell_length_b 7.6252(16) _cell_length_c 12.092(2) _cell_angle_alpha 84.577(15) _cell_angle_beta 87.445(14) _cell_angle_gamma 76.369(17) _cell_volume 484.37(16) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_weight _refln_observed_status -6 -6 1 37.452 40.832 7.118 11.133 o -6 -6 2 0.976 3.529 2.959 77.381 o -6 -5 1 20.511 19.384 4.540 28.629 o -6 -5 2 21.879 17.330 5.069 23.558 o -6 -5 3 16.962 14.695 2.898 64.281 o -6 -5 4 5.986 9.306 2.703 86.853 o -6 -4 1 3.050 5.722 2.897 79.274 o -6 -4 2 29.293 35.619 4.378 25.788 o -6 -4 3 2.776 6.427 2.472 107.680 o -6 -4 4 7.336 2.502 7.324 12.660 o -6 -4 5 0.225 -0.844 2.597 101.374 o -6 -4 6 1.170 7.534 2.835 83.213 o -6 -3 1 17.848 20.387 3.569 43.795 o -6 -3 2 14.259 14.163 2.757 72.844 o -6 -3 3 21.973 25.346 3.587 40.081 o -6 -3 4 11.376 11.281 3.165 60.879 o -6 -3 5 7.472 7.141 1.777 181.731 o -6 -3 6 0.007 -1.466 2.524 107.431 o -6 -2 1 21.218 24.776 3.789 37.306 o -6 -2 2 17.679 20.265 3.144 53.754 o -6 -2 3 4.154 7.504 2.095 143.952 o -6 -2 4 0.077 -3.712 1.654 250.073 o -6 -2 5 2.623 3.933 1.635 240.796 o -6 -2 6 0.857 0.429 1.583 269.857 o -6 -2 7 6.463 7.109 3.419 56.041 o -6 -1 1 10.130 10.927 2.341 104.651 o -6 -1 2 20.920 17.655 2.363 77.869 o -6 -1 3 0.660 -1.306 1.377 357.615 o -6 -1 4 5.713 4.370 1.754 198.808 o -6 -1 5 1.578 4.309 2.605 98.987 o -6 -1 6 0.002 1.085 3.276 63.706 o -6 -1 7 0.745 0.601 2.318 126.700 o -6 0 1 0.302 3.540 2.849 83.648 o -6 0 2 1.636 2.120 2.209 137.858 o -6 0 3 2.244 0.639 2.453 112.246 o -6 0 4 2.198 5.403 3.172 66.795 o -6 0 5 1.042 3.380 1.731 221.903 o -6 0 6 0.010 -0.332 1.676 243.634 o -6 1 1 1.036 3.870 2.317 125.278 o -6 1 2 0.142 -0.546 2.308 128.447 o -6 1 3 0.112 1.444 2.193 141.674 o -6 1 4 0.176 -4.131 2.427 116.147 o -6 2 1 5.012 4.951 3.292 61.229 o -6 2 2 0.177 0.614 2.743 90.793 o -5 -8 1 9.179 8.108 3.729 46.502 o -5 -7 1 4.949 4.352 3.080 69.815 o -5 -7 2 30.669 20.900 4.890 23.075 o -5 -7 3 0.135 2.391 2.486 110.063 o -5 -7 4 20.190 17.015 5.230 22.542 o -5 -6 1 9.677 8.940 3.359 56.164 o -5 -6 2 19.367 14.622 4.404 31.049 o -5 -6 3 0.404 6.809 3.543 53.944 o -5 -6 4 10.443 10.357 3.734 45.614 o -5 -6 5 20.509 31.119 6.408 15.013 o -5 -6 6 12.786 15.782 5.099 24.709 o -5 -5 1 110.050 108.668 9.630 3.964 o -5 -5 2 0.355 0.802 2.584 102.225 o -5 -5 3 53.658 38.243 6.354 12.001 o -5 -5 4 0.668 4.487 2.977 76.392 o -5 -5 5 68.762 66.387 8.961 6.111 o -5 -5 6 6.267 10.745 5.145 25.220 o -5 -5 7 4.128 0.376 2.958 76.836 o -5 -5 8 1.114 4.163 2.092 152.740 o -5 -4 1 122.594 124.552 10.243 3.331 o -5 -4 2 32.370 39.712 6.120 14.757 o -5 -4 3 40.983 36.888 5.957 14.608 o -5 -4 4 5.470 10.699 2.713 86.086 o -5 -4 5 27.187 38.689 4.358 26.117 o -5 -4 6 60.109 57.823 8.803 6.715 o -5 -4 7 12.600 11.886 3.166 59.827 o -5 -4 8 1.172 4.020 2.552 103.404 o -5 -4 9 0.125 2.108 2.375 120.633 o -5 -3 1 142.405 134.955 10.019 2.985 o -5 -3 2 169.224 156.539 8.174 2.794 o -5 -3 3 4.877 5.442 2.204 131.574 o -5 -3 4 91.532 97.407 7.551 5.915 o -5 -3 5 2.256 1.652 1.843 195.645 o -5 -3 6 32.444 26.595 3.126 40.835 o -5 -3 7 9.829 9.308 5.788 19.869 o -5 -3 8 0.558 -0.575 1.853 198.567 o -5 -3 9 0.488 3.897 2.575 102.080 o -5 -2 1 8.454 6.060 1.648 203.341 o -5 -2 2 168.182 184.964 8.625 2.519 o -5 -2 3 66.627 74.880 5.474 10.877 o -5 -2 4 19.307 18.642 2.992 57.280 o -5 -2 5 1.613 2.650 1.350 356.860 o -5 -2 6 15.017 18.011 2.702 72.023 o -5 -2 7 53.116 54.564 4.812 15.816 o -5 -2 8 0.089 4.217 2.522 106.491 o -5 -2 9 3.098 6.087 2.818 83.527 o -5 -2 10 5.402 5.798 2.445 107.369 o -5 -1 1 7.701 5.798 3.754 46.669 o -5 -1 2 129.114 142.509 7.263 4.015 o -5 -1 3 222.725 249.216 8.065 1.659 o -5 -1 4 1.860 3.413 1.627 247.253 o -5 -1 5 91.659 102.813 5.649 7.367 o -5 -1 6 3.196 3.821 1.699 221.914 o -5 -1 7 4.913 2.490 2.795 84.857 o -5 -1 8 0.039 -1.718 2.986 76.774 o -5 -1 9 0.953 0.897 2.301 128.297 o -5 -1 10 10.531 10.814 3.849 42.999 o -5 0 1 11.960 11.380 1.618 174.576 o -5 0 2 15.257 19.063 2.190 96.069 o -5 0 3 46.128 49.266 3.343 25.381 o -5 0 4 21.540 28.453 3.309 44.411 o -5 0 5 15.896 15.914 2.760 69.883 o -5 0 6 1.283 2.301 1.445 316.161 o -5 0 7 0.034 -0.563 2.045 163.549 o -5 0 8 0.938 2.347 2.538 105.236 o -5 0 9 0.675 -0.540 2.409 117.623 o -5 0 10 0.003 -8.109 4.319 36.680 o -5 1 1 12.843 21.706 4.518 30.335 o -5 1 2 61.123 53.067 3.957 17.380 o -5 1 3 8.302 11.741 3.729 46.200 o -5 1 4 105.626 105.556 6.313 5.992 o -5 1 5 4.192 2.586 1.759 206.729 o -5 1 6 5.194 6.627 2.585 96.513 o -5 1 7 0.385 5.278 2.373 119.401 o -5 1 8 0.139 -2.771 2.383 120.456 o -5 1 9 0.515 0.218 2.231 137.109 o -5 2 1 1.345 5.389 3.086 70.815 o -5 2 2 1.565 5.578 2.550 102.713 o -5 2 3 6.008 7.242 2.381 111.084 o -5 2 6 1.061 -0.837 1.934 181.521 o -5 2 7 10.394 13.696 4.422 32.894 o -5 2 8 4.803 8.286 3.615 50.660 o -4 -8 1 3.777 1.583 2.342 121.072 o -4 -8 2 4.353 1.973 3.498 54.978 o -4 -8 3 0.845 5.491 3.680 50.075 o -4 -8 4 2.599 -3.197 3.673 50.433 o -4 -8 5 4.615 6.543 3.527 53.437 o -4 -7 1 24.944 26.291 5.363 20.273 o -4 -7 2 7.023 6.791 3.088 67.803 o -4 -7 3 3.114 4.789 2.989 74.762 o -4 -7 4 1.014 0.313 2.054 160.934 o -4 -7 5 6.281 5.673 3.080 68.854 o -4 -7 6 12.093 11.700 4.331 34.055 o -4 -7 7 0.097 -1.624 2.806 86.916 o -4 -6 1 4.750 5.660 3.030 71.839 o -4 -6 2 9.742 8.875 2.823 77.096 o -4 -6 3 1.617 4.124 2.818 84.809 o -4 -6 4 2.326 6.897 3.824 46.067 o -4 -6 5 18.878 14.163 4.495 30.117 o -4 -6 6 5.169 11.529 4.288 36.050 o -4 -6 7 22.746 24.193 5.720 18.510 o -4 -6 8 0.008 4.923 4.432 34.704 o -4 -5 1 1.873 -5.352 3.341 60.996 o -4 -5 2 146.357 143.651 10.760 2.685 o -4 -5 3 1.792 2.088 2.865 82.468 o -4 -5 4 0.160 -3.715 2.503 109.128 o -4 -5 5 3.338 -4.385 3.003 74.971 o -4 -5 6 51.183 53.291 7.839 8.517 o -4 -5 7 25.843 24.169 5.814 17.654 o -4 -5 8 11.068 9.281 2.811 76.234 o -4 -5 9 19.853 21.141 4.742 26.500 o -4 -5 10 1.169 4.570 2.812 85.295 o -4 -4 1 0.081 0.724 1.912 186.667 o -4 -4 2 5.006 6.467 2.868 79.424 o -4 -4 3 6.289 4.875 2.589 95.990 o -4 -4 4 6.592 5.474 2.709 87.632 o -4 -4 5 24.762 27.861 5.615 18.661 o -4 -4 6 56.030 62.115 4.880 14.486 o -4 -4 7 1.607 -1.709 2.601 100.469 o -4 -4 8 5.336 4.125 2.294 122.312 o -4 -4 9 4.845 6.367 2.634 93.568 o -4 -4 10 0.857 1.777 1.839 199.315 o -4 -4 11 3.148 -0.742 2.119 149.020 o -4 -3 1 80.479 74.176 6.851 7.721 o -4 -3 2 25.002 21.731 4.174 31.242 o -4 -3 3 197.512 188.254 11.711 1.786 o -4 -3 4 0.097 1.817 1.327 382.849 o -4 -3 5 33.820 32.027 3.683 31.464 o -4 -3 6 24.229 21.281 2.980 52.083 o -4 -3 7 51.168 48.480 5.023 15.902 o -4 -3 8 20.270 17.020 4.154 33.752 o -4 -3 9 37.675 44.369 6.747 11.999 o -4 -3 10 2.333 5.004 2.313 123.690 o -4 -3 11 3.951 8.084 3.398 57.434 o -4 -2 1 48.461 45.096 5.209 15.908 o -4 -2 2 9.093 10.205 2.096 129.099 o -4 -2 3 17.519 21.915 2.896 60.279 o -4 -2 4 38.054 45.943 4.255 22.774 o -4 -2 5 3.249 5.458 1.930 172.441 o -4 -2 6 129.977 142.310 6.018 4.421 o -4 -2 7 64.584 69.603 4.894 12.645 o -4 -2 8 25.022 24.613 4.967 23.204 o -4 -2 9 0.426 -1.572 2.032 165.285 o -4 -2 10 2.827 4.607 2.890 80.026 o -4 -2 11 2.358 2.844 2.718 91.041 o -4 -2 12 4.970 2.978 2.842 81.943 o -4 -1 1 144.798 150.695 10.853 2.639 o -4 -1 2 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24.936 30.918 5.405 19.681 o 5 -3 4 7.150 7.671 3.245 61.478 o 5 -3 5 0.331 2.269 1.877 192.033 o 5 -3 6 0.042 0.181 1.873 194.982 o 5 -3 7 2.307 7.331 3.134 68.006 o 5 -2 0 96.788 83.663 8.363 5.376 o 5 -2 1 5.487 4.200 2.405 111.640 o 5 -2 2 5.509 5.677 2.472 105.134 o 5 -2 3 16.598 18.219 4.086 35.696 o 5 -2 4 41.892 45.392 6.208 13.206 o 5 -2 5 0.873 -0.458 1.995 171.002 o 5 -2 6 0.144 1.262 1.571 275.177 o 5 -2 7 1.344 0.709 1.496 299.296 o 5 -2 8 0.103 4.928 2.571 102.292 o 5 -1 0 84.046 89.001 8.372 5.720 o 5 -1 1 87.737 82.026 8.083 5.949 o 5 -1 2 59.536 57.320 6.842 9.665 o 5 -1 3 34.967 31.894 5.164 19.452 o 5 -1 4 52.697 50.518 6.345 11.554 o 5 -1 5 0.041 1.383 1.563 277.844 o 5 -1 6 1.742 0.301 1.831 200.750 o 5 -1 7 0.444 5.839 2.675 94.163 o 5 -1 8 0.040 -2.365 2.192 142.384 o 5 -1 9 3.614 0.246 1.744 215.739 o 5 0 0 26.265 26.444 5.954 16.777 o 5 0 1 62.584 57.069 4.186 15.892 o 5 0 2 5.038 4.869 1.656 222.116 o 5 0 3 0.517 -1.489 2.292 129.909 o 5 0 4 0.682 1.056 1.435 327.119 o 5 0 5 41.449 46.453 6.541 12.197 o 5 0 6 4.841 2.800 2.208 133.208 o 5 0 7 5.176 6.166 3.048 70.692 o 5 0 8 0.312 -0.234 1.864 196.495 o 5 0 9 0.305 5.765 3.166 67.558 o 5 0 10 2.572 4.849 3.112 69.297 o 5 1 0 0.292 1.525 2.513 107.878 o 5 1 1 44.147 42.165 3.847 24.154 o 5 1 2 285.614 283.759 11.795 1.032 o 5 1 3 13.066 14.290 2.381 93.651 o 5 1 4 23.219 16.503 2.631 65.388 o 5 1 5 80.451 77.636 5.687 9.099 o 5 1 6 1.428 2.620 1.335 365.830 o 5 1 7 9.944 14.173 2.857 72.891 o 5 1 8 1.010 -1.029 1.355 367.110 o 5 1 9 12.510 14.085 4.049 38.147 o 5 1 10 3.070 6.911 4.332 35.932 o 5 1 11 3.182 -2.791 3.103 70.328 o 5 2 0 57.291 53.894 4.581 15.927 o 5 2 1 4.129 2.987 2.088 149.242 o 5 2 2 34.656 31.922 4.676 22.591 o 5 2 3 3.177 2.049 1.594 254.360 o 5 2 4 2.852 2.072 2.078 153.686 o 5 2 5 0.399 1.511 2.648 97.183 o 5 2 6 25.612 24.960 4.642 25.780 o 5 2 7 59.069 59.258 7.196 8.999 o 5 2 8 0.775 1.667 2.147 146.995 o 5 2 9 0.235 -3.329 3.314 62.268 o 5 2 10 0.801 -0.761 2.460 112.739 o 5 2 11 10.141 4.853 2.896 74.938 o 5 3 0 0.404 1.629 2.133 149.348 o 5 3 1 0.470 3.343 2.603 100.014 o 5 3 2 5.184 7.805 2.830 80.865 o 5 3 3 130.549 118.274 9.674 3.434 o 5 3 4 1.029 0.977 2.332 124.891 o 5 3 5 0.149 0.205 2.462 112.758 o 5 3 6 25.030 23.368 5.077 22.470 o 5 3 7 23.040 26.302 5.367 20.517 o 5 3 8 35.764 34.033 6.326 13.932 o 5 3 9 16.572 13.618 4.389 32.032 o 5 3 10 0.399 6.069 3.340 60.729 o 5 3 11 1.495 -5.295 3.880 45.332 o 5 4 0 117.561 126.611 10.012 3.482 o 5 4 1 4.412 2.130 2.650 94.561 o 5 4 2 0.057 1.343 2.015 167.698 o 5 4 3 18.344 20.361 4.451 30.034 o 5 4 4 20.473 22.311 4.870 25.076 o 5 4 5 2.757 -3.757 3.190 66.697 o 5 4 6 0.043 -3.767 2.535 106.487 o 5 4 7 22.136 18.353 4.294 31.171 o 5 4 8 34.545 43.064 6.813 12.088 o 5 4 9 3.112 -3.501 2.847 83.401 o 5 4 10 0.067 -8.417 3.206 66.590 o 5 5 0 110.544 113.559 9.997 3.746 o 5 5 1 1.464 2.942 2.450 112.224 o 5 5 2 23.042 18.218 3.883 36.485 o 5 5 3 1.860 -3.130 3.026 74.276 o 5 5 4 16.398 19.290 4.747 27.295 o 5 5 5 3.039 -1.283 2.309 126.058 o 5 5 6 0.105 -0.145 2.949 78.698 o 5 5 7 22.544 22.899 5.804 18.126 o 5 5 8 16.555 14.640 4.896 26.171 o 5 5 9 60.343 49.695 7.685 8.395 o 5 5 10 2.166 -4.521 3.534 54.498 o 5 6 0 13.316 12.949 3.950 39.825 o 5 6 1 47.677 52.311 7.248 9.827 o 5 6 2 0.012 2.277 2.640 97.770 o 5 6 3 1.053 -4.390 2.799 87.009 o 5 6 4 0.073 -1.710 2.195 141.942 o 5 6 5 3.218 6.827 3.216 64.410 o 5 6 6 4.939 1.377 2.751 87.841 o 5 6 7 0.030 -0.481 2.408 117.978 o 5 6 8 3.898 3.588 3.556 53.166 o 5 6 9 14.919 16.646 5.094 24.420 o 5 7 0 19.396 25.969 5.949 17.493 o 5 7 1 35.439 31.318 5.820 16.124 o 5 7 2 11.915 16.017 5.141 24.422 o 5 7 3 13.375 18.290 5.230 23.337 o 5 7 4 0.613 2.575 2.894 81.167 o 5 7 5 0.335 1.026 3.080 71.978 o 5 7 6 3.232 -0.879 2.661 95.191 o 5 7 7 0.212 -1.319 3.039 74.057 o 5 8 0 3.495 7.302 3.738 47.901 o 5 8 1 1.401 -0.195 2.246 134.600 o 5 8 2 8.000 1.696 2.190 130.896 o 5 8 3 0.001 -6.845 3.481 56.495 o 5 8 4 4.845 3.851 3.035 72.035 o 6 -2 0 0.026 -0.642 2.077 158.611 o 6 -2 1 1.408 4.414 2.608 98.813 o 6 -2 2 0.792 4.935 3.193 66.403 o 6 -2 3 3.672 6.001 3.457 55.924 o 6 -2 4 1.895 2.165 1.893 186.032 o 6 -1 0 1.328 5.203 2.866 81.964 o 6 -1 1 3.215 5.810 2.600 97.598 o 6 -1 2 2.326 -1.012 1.818 202.587 o 6 -1 3 7.182 7.656 3.285 60.029 o 6 -1 4 1.889 5.429 3.023 73.531 o 6 -1 5 0.540 1.692 2.662 96.019 o 6 -1 6 0.464 1.016 2.339 124.540 o 6 0 0 12.650 9.410 3.697 45.821 o 6 0 1 8.288 7.318 2.992 70.996 o 6 0 2 3.995 4.910 2.156 139.015 o 6 0 3 5.696 7.235 3.451 55.289 o 6 0 4 13.847 11.045 3.767 43.553 o 6 0 5 1.824 -1.813 3.138 69.133 o 6 0 6 0.080 0.940 2.294 129.728 o 6 0 7 0.152 -1.082 2.199 141.452 o 6 1 0 10.138 12.060 2.448 96.148 o 6 1 1 32.663 27.571 3.591 34.077 o 6 1 2 8.936 2.993 2.524 98.798 o 6 1 3 18.832 18.816 4.572 28.727 o 6 1 4 18.059 17.260 4.641 28.294 o 6 1 5 10.609 13.126 4.667 29.724 o 6 1 6 0.688 -3.482 3.225 65.686 o 6 1 7 0.528 -1.685 2.717 92.571 o 6 1 8 0.007 0.753 2.992 76.379 o 6 2 0 3.664 3.813 1.722 214.758 o 6 2 1 16.929 14.580 3.635 44.297 o 6 2 2 16.108 14.255 2.469 83.725 o 6 2 3 8.359 8.372 2.270 115.991 o 6 2 4 0.719 1.218 1.485 305.134 o 6 2 5 36.218 39.208 4.440 22.947 o 6 2 6 4.507 0.985 1.787 202.263 o 6 2 7 3.850 6.782 4.918 27.929 o 6 2 8 0.465 -5.574 4.373 35.771 o 6 3 0 6.222 7.303 2.371 111.572 o 6 3 1 8.270 7.608 2.616 90.720 o 6 3 2 123.808 116.671 10.023 3.454 o 6 3 3 3.752 7.737 2.789 84.230 o 6 3 4 30.712 29.170 5.426 18.849 o 6 3 5 32.487 23.099 4.992 21.768 o 6 3 6 25.133 26.979 5.234 21.043 o 6 3 7 0.363 -2.621 3.600 52.770 o 6 3 8 0.317 9.238 4.197 38.442 o 6 4 0 53.218 50.644 7.202 9.624 o 6 4 1 0.004 1.041 2.519 107.634 o 6 4 2 11.357 16.977 4.553 30.665 o 6 4 3 14.279 10.165 3.845 41.966 o 6 4 4 20.165 18.892 4.875 25.397 o 6 4 5 1.686 3.910 2.578 101.107 o 6 4 6 33.101 31.511 6.091 15.211 o 6 4 7 0.012 4.158 3.565 53.593 o 6 5 0 8.306 8.792 3.802 44.983 o 6 5 1 4.641 -2.212 2.279 127.518 o 6 5 2 1.663 -3.160 2.187 141.730 o 6 5 3 63.509 63.828 8.336 7.027 o 6 5 4 0.351 -1.945 2.908 80.820 o 6 5 5 10.081 8.122 4.090 38.815 o 6 5 6 12.296 15.507 4.612 29.900 o 6 6 0 9.369 11.338 3.438 53.378 o 6 6 1 12.245 7.174 4.241 35.885 o 6 6 2 0.619 -1.370 2.634 98.429 o 6 6 3 4.913 8.742 3.562 52.040 o 6 6 4 18.644 19.647 4.795 26.368 o 6 6 5 2.992 0.227 2.892 80.849 o ; _olex2_submission_original_sample_id RMG164 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_refinement_flags_posn Li1 Li 0.3380(8) 0.9582(8) 0.4254(4) 0.0347(13) Uani 1.000000 . O1 O -0.0264(3) 0.9414(3) 0.64140(17) 0.0410(7) Uani 1.000000 . O2 O 0.3793(3) 0.9095(3) 0.58495(16) 0.0341(6) Uani 1.000000 . O3 O 0.5034(4) 0.7365(3) 0.35680(19) 0.0500(7) Uani 1.000000 . N1 N 0.2829(4) 0.8445(3) 0.76719(18) 0.0277(6) Uani 1.000000 . C1 C 0.5270(5) 0.7730(4) 0.7999(3) 0.0364(8) Uani 1.000000 . H1 H 0.6741(5) 0.7559(4) 0.7529(3) 0.0436(10) Uiso 1.000000 R C2 C 0.5214(6) 0.7311(5) 0.9113(3) 0.0481(10) Uani 1.000000 . H2 H 0.6638(6) 0.6780(5) 0.9560(3) 0.0578(12) Uiso 1.000000 R C3 C 0.2669(6) 0.7801(5) 0.9494(3) 0.0521(10) Uani 1.000000 . H3 H 0.2071(6) 0.7674(5) 1.0241(3) 0.0626(12) Uiso 1.000000 R C4 C 0.1246(5) 0.8484(5) 0.8597(3) 0.0388(8) Uani 1.000000 . H4 H -0.0543(5) 0.8917(5) 0.8603(3) 0.0465(10) Uiso 1.000000 R C5 C 0.2042(5) 0.9033(4) 0.6563(2) 0.0286(7) Uani 1.000000 . C6 C 0.7100(9) 0.6109(7) 0.4079(4) 0.0917(19) Uani 1.000000 . H6a H 0.7589(9) 0.6591(7) 0.4747(4) 0.110(2) Uiso 1.000000 R H6b H 0.6615(9) 0.4954(7) 0.4311(4) 0.110(2) Uiso 1.000000 R C7 C 0.9195(7) 0.5805(7) 0.3296(4) 0.0803(15) Uani 1.000000 . H7a H 1.0466(7) 0.6473(7) 0.3470(4) 0.0964(18) Uiso 1.000000 R H7b H 1.0023(7) 0.4499(7) 0.3316(4) 0.0964(18) Uiso 1.000000 R C8 C 0.8118(8) 0.6477(6) 0.2185(4) 0.0692(13) Uani 1.000000 . H8a H 0.8884(8) 0.7457(6) 0.1838(4) 0.0830(15) Uiso 1.000000 R H8b H 0.8422(8) 0.5484(6) 0.1688(4) 0.0830(15) Uiso 1.000000 R C9 C 0.5349(7) 0.7170(6) 0.2400(3) 0.0596(11) Uani 1.000000 . H9a H 0.4392(7) 0.6306(6) 0.2183(3) 0.0715(13) Uiso 1.000000 R H9b H 0.4726(7) 0.8352(6) 0.1971(3) 0.0715(13) Uiso 1.000000 R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Li1 0.020(2) 0.057(4) 0.028(3) -0.012(2) -0.0008(19) 0.002(2) O1 0.0177(9) 0.0690(18) 0.0354(13) -0.0114(10) -0.0034(8) 0.0048(11) O2 0.0231(10) 0.0540(15) 0.0265(11) -0.0140(10) 0.0021(8) 0.0017(9) O3 0.0425(13) 0.0564(18) 0.0444(15) 0.0028(12) 0.0025(11) -0.0090(12) N1 0.0179(11) 0.0390(16) 0.0264(13) -0.0087(11) -0.0006(9) 0.0010(11) C1 0.0207(14) 0.049(2) 0.0367(18) -0.0058(14) -0.0013(12) 0.0051(15) C2 0.0346(17) 0.070(3) 0.039(2) -0.0168(17) -0.0110(14) 0.0142(17) C3 0.0439(18) 0.089(3) 0.0295(18) -0.0318(19) 0.0005(14) 0.0057(18) C4 0.0236(14) 0.062(2) 0.0323(18) -0.0144(15) 0.0063(12) -0.0026(15) C5 0.0208(13) 0.0332(18) 0.0333(16) -0.0102(13) -0.0015(11) 0.0008(13) C6 0.100(3) 0.085(4) 0.054(3) 0.046(3) 0.001(3) 0.008(3) C7 0.041(2) 0.102(4) 0.095(4) -0.003(2) -0.004(2) -0.027(3) C8 0.071(3) 0.065(3) 0.065(3) -0.008(2) 0.026(2) -0.007(2) C9 0.061(2) 0.070(3) 0.049(2) -0.010(2) -0.0051(18) -0.022(2) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c _atom_type_scat_source _atom_type_scat_dispersion_source H 0.00000 0.00000 0.49300 0.32291 0.14019 0.04081 10.51090 26.12570 3.14236 57.79970 0.0030380000826 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' C 0.00347 0.00161 2.31000 1.02000 1.58860 0.86500 20.84390 10.20750 0.56870 51.65120 0.215599998832 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' Li -0.00003 0.00005 1.12820 0.75080 0.61750 0.46530 3.95460 1.05240 85.39050 168.26100 0.0377000011504 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' O 0.01158 0.00611 3.04850 2.28680 1.54630 0.86700 13.27710 5.70110 0.32390 32.90890 0.250800013542 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' N 0.00653 0.00323 12.21260 3.13220 2.01250 1.16630 0.00570 9.89330 28.99750 0.58260 -11.5290002823 'International Tables Volume C Table 6.1.1.4 (pp. 500-502)' 'Henke, Gullikson and Davis, At. Data and Nucl. Data Tables, 1993, 54, 2' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O2 Li1 O1 121.7(3) 2_676 2_576 O2 Li1 O1 123.8(3) . 2_576 O3 Li1 O1 109.3(3) . 2_576 O3 Li1 O2 100.8(2) . 2_676 O3 Li1 O2 107.6(2) . . C5 O1 Li1 160.0(2) . 2_576 C5 O2 Li1 132.2(2) . 2_676 C5 O2 Li1 125.9(2) . . C6 O3 Li1 120.9(3) . . C9 O3 Li1 126.1(3) . . C9 O3 C6 106.1(3) . . C4 N1 C1 108.5(2) . . C5 N1 C1 126.0(2) . . C5 N1 C4 125.5(2) . . H1 C1 N1 126.08(16) . . C2 C1 N1 107.8(3) . . C2 C1 H1 126.08(18) . . H2 C2 C1 125.95(18) . . C3 C2 C1 108.1(3) . . C3 C2 H2 125.95(18) . . H3 C3 C2 126.45(18) . . C4 C3 C2 107.1(3) . . C4 C3 H3 126.45(19) . . C3 C4 N1 108.5(3) . . H4 C4 N1 125.76(15) . . H4 C4 C3 125.76(19) . . O2 C5 O1 127.8(3) . . N1 C5 O1 116.3(2) . . N1 C5 O2 115.9(2) . . H6a C6 O3 110.0(2) . . H6b C6 O3 110.0(3) . . H6b C6 H6a 108.3 . . C7 C6 O3 108.7(4) . . C7 C6 H6a 110.0(3) . . C7 C6 H6b 110.0(3) . . H7a C7 C6 110.5(3) . . H7b C7 C6 110.5(3) . . H7b C7 H7a 108.7 . . C8 C7 C6 106.2(3) . . C8 C7 H7a 110.5(3) . . C8 C7 H7b 110.5(3) . . H8a C8 C7 110.7(3) . . H8b C8 C7 110.7(3) . . H8b C8 H8a 108.8 . . C9 C8 C7 105.0(3) . . C9 C8 H8a 110.7(2) . . C9 C8 H8b 110.7(2) . . C8 C9 O3 106.5(3) . . H9a C9 O3 110.4(2) . . H9a C9 C8 110.4(2) . . H9b C9 O3 110.42(19) . . H9b C9 C8 110.4(2) . . H9b C9 H9a 108.6 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Li1 Li1 2.790(9) 2_676 Li1 O1 1.870(5) 2_576 Li1 O2 1.943(5) . Li1 O2 2.019(5) 2_676 Li1 O3 1.959(6) . O1 C5 1.234(3) . O2 C5 1.262(3) . O3 C6 1.415(4) . O3 C9 1.432(4) . N1 C1 1.370(3) . N1 C4 1.378(4) . N1 C5 1.424(4) . C1 H1 0.9500 . C1 C2 1.355(4) . C2 H2 0.9500 . C2 C3 1.412(4) . C3 H3 0.9500 . C3 C4 1.350(4) . C4 H4 0.9500 . C6 H6a 0.9900 . C6 H6b 0.9900 . C6 C7 1.437(6) . C7 H7a 0.9900 . C7 H7b 0.9900 . C7 C8 1.485(6) . C8 H8a 0.9900 . C8 H8b 0.9900 . C8 C9 1.492(5) . C9 H9a 0.9900 . C9 H9b 0.9900 . loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_scale_group_code 0 0 -2 81212.1 843.423 5 0 0 -3 26765.9 600.728 5 0 0 3 25813.8 637.897 5 0 0 -4 48429.7 942.104 5 0 0 4 48484.2 1006.41 5 0 0 5 60444.3 1274.15 5 0 0 6 7404.42 517.569 5 0 0 7 33551.7 1150.59 5 0 0 8 646.919 200.871 5 0 0 9 6847.12 610.479 5 0 0 10 5100.13 555.236 5 0 0 11 3251.91 502.462 5 0 0 12 1092.19 352.123 5 0 0 13 1535 384.012 5 0 0 14 3161.38 547.813 5 0 0 15 230.263 263.248 5 0 0 16 1285.43 439.206 5 0 -1 16 -27.9787 199.797 5 0 -1 15 248.601 199.568 5 0 -1 14 121.694 195.327 5 0 -1 13 1467.41 338.638 5 0 -1 12 -186.824 193.119 5 0 -1 11 318.17 201.639 5 0 -1 10 1679.86 322.928 5 0 -1 9 -170.077 163.455 5 0 -1 8 1253.69 247.996 5 0 -1 8 762.527 74.7204 3 0 -1 7 21.3514 104.696 5 0 -1 6 162.535 38.3755 3 0 -1 6 149.6 103.248 5 0 -1 5 17072.8 608.553 5 0 -1 4 7556.3 359.251 5 0 -1 3 30822.5 635.886 5 0 -1 3 30495.6 711.551 1 0 -1 2 85312.4 946.059 1 0 1 -1 174.473 61.1976 1 0 -1 -2 57195.5 961.731 5 0 1 2 58026.5 915.43 5 0 1 3 15225.3 572.666 5 0 -1 -3 13890.2 536.363 5 0 1 4 26589.5 829.601 5 0 -1 -4 27909.8 833.576 5 0 1 5 12.3749 125.471 5 0 1 6 99.5521 130.627 5 0 1 7 -155.502 162.676 5 0 1 8 -141.996 166.499 5 0 1 9 2406.36 381.969 5 0 1 10 3495.51 501.614 5 0 1 11 139.844 170.371 5 0 1 12 701.093 229.402 5 0 1 13 247.394 244.413 5 0 1 14 2501.35 518.456 5 0 1 15 220.82 244.494 5 0 -2 16 -223.319 321.052 5 0 -2 15 592.749 266.809 5 0 -2 14 4.14425 215.127 5 0 -2 13 1192.01 344.773 5 0 -2 12 -291.707 208.576 5 0 -2 11 826.281 221.291 5 0 -2 10 5852.64 585.113 5 0 -2 9 1342.96 280.458 5 0 -2 8 1288.84 236.363 5 0 -2 7 3737.96 359.145 5 0 -2 6 24127.3 786.04 5 0 -2 5 1255.99 172.659 5 0 2 -4 40981 616.482 3 0 -2 4 43154.2 881.223 1 0 -2 4 41100.7 884.726 5 0 2 -3 18393.3 653.535 1 0 -2 3 19059.4 533.851 1 0 2 -3 17901.2 430.358 3 0 -2 2 6439.42 292.252 1 0 2 -2 6137.4 306.531 1 0 -2 2 6473.53 379.865 4 0 -2 1 50504.4 760.071 1 0 2 -1 51879.8 971.292 4 0 2 -1 50290.3 735.925 1 0 -2 1 50294.7 933.768 4 0 -2 0 55091.8 779.214 1 0 2 0 55662 869.251 4 0 2 0 56247.3 740.044 1 0 2 1 636484 3267.33 5 0 -2 -1 650044 3324.34 5 0 2 1 641091 2860.77 1 0 2 2 92791.6 1363.17 5 0 -2 -2 92591.6 1457.98 5 0 -2 -3 1980.97 249.753 5 0 2 3 1596.54 229.169 5 0 2 4 913.422 197.19 5 0 2 5 742.664 199.272 5 0 2 6 4012.72 424.543 5 0 2 7 26893.3 1157.2 5 0 2 8 -25.1683 166.617 5 0 2 9 2834.28 420.074 5 0 2 10 2408.82 472.216 5 0 2 11 1545.86 389.815 5 0 2 12 3582.33 543.282 5 0 2 13 100.691 164.97 5 0 2 14 362.437 269.23 5 0 2 15 1014.29 410.359 5 0 -3 15 -15.5919 208.633 5 0 -3 14 158.423 154.621 5 0 -3 13 271.076 206.086 5 0 -3 12 1057.77 296.557 5 0 -3 11 -3.75799 134.543 5 0 -3 10 1283.52 268.452 5 0 -3 9 8777.02 621.325 5 0 -3 8 436.373 150.659 5 0 -3 7 2355 286.283 5 0 -3 6 -26.7297 81.2417 5 0 -3 5 13307.3 749.611 4 0 3 -5 12658.5 420.369 3 0 -3 5 12755.5 564.393 5 0 3 -4 673.643 112.885 3 0 -3 4 563.388 197.978 4 0 3 -3 8205.55 459.684 1 0 -3 3 8380.67 525.155 4 0 -3 3 8658.54 406.807 1 0 -3 2 41478.4 1059.96 4 0 -3 2 42268.3 838.304 1 0 3 -2 41361.4 857.15 1 0 3 -1 89.9972 65.5603 1 0 -3 1 108.426 65.3129 1 0 3 -1 129.742 117.171 4 0 -3 1 165.219 128.434 4 0 3 0 6.89109 71.0768 4 0 -3 0 92.0678 77.0264 5 0 -3 0 121.892 74.2895 1 0 3 0 -73.3693 72.7598 1 0 -3 -1 36349.5 954.823 5 0 3 1 37448.5 805.79 1 0 3 1 35765.4 876.543 4 0 -3 -2 72161.5 1477.17 5 0 3 2 71974.9 1403.56 5 0 3 3 705.413 166.641 5 0 3 4 429.772 154.811 5 0 3 5 20153.2 939.441 5 0 3 6 4775.42 489.207 5 0 3 7 242.737 154.218 5 0 3 8 677.899 263.079 5 0 3 9 9913.91 805.975 5 0 3 10 333.66 223.753 5 0 3 11 7022.27 749.836 5 0 3 12 -183.19 224.433 5 0 3 13 137.921 233.201 5 0 3 14 -441.507 285.161 5 0 3 15 1113.1 382.419 5 0 -4 13 296.624 188.043 5 0 -4 13 716.351 417.002 4 0 -4 12 200.171 135.881 5 0 -4 12 147.089 277.084 4 0 -4 11 1107.78 277.271 5 0 -4 11 1075.49 406.382 4 0 -4 10 436.095 195.302 5 0 -4 10 8.7408 313.053 4 0 -4 9 559.984 172.011 5 0 -4 9 1046.21 335.226 4 0 -4 8 594.624 272.252 4 0 -4 8 727.393 170.612 5 0 -4 7 2780.73 423.694 4 0 -4 7 2455.26 281.185 5 0 -4 6 40.8285 209.796 4 0 -4 6 4.83848 77.1245 5 0 4 -6 -39.7049 76.9957 3 0 -4 5 14028.7 814.239 4 0 4 -5 13023.4 531.648 3 0 4 -4 4106.34 412.755 1 0 -4 4 3614.91 406.378 4 0 -4 3 21872.3 919.574 4 0 4 -3 22694.5 805.96 1 0 -4 2 11373.2 643.08 4 0 -4 2 11125.2 499.698 1 0 4 -2 12088.1 526.758 1 0 4 -1 1723.79 190.941 1 0 -4 1 1892.93 266.286 4 0 -4 1 1598.66 204.368 1 0 -4 0 246.076 107.953 1 0 4 0 472.112 120.615 1 0 4 1 5511.48 345.945 1 0 4 2 29756.9 884.346 1 0 4 3 5728.99 413.75 1 0 4 3 5693.75 469.822 5 0 4 4 3524.87 404.504 5 0 4 5 4501.72 485.531 5 0 4 6 866.236 260.875 5 0 4 7 6277.07 588.076 5 0 4 8 208.114 197.022 5 0 4 9 -154.476 190.438 5 0 4 10 388.056 213.976 5 0 4 11 4537.85 639.156 5 0 4 12 3266.8 564.998 5 0 4 13 626.065 308.47 5 0 4 14 578.498 363.973 5 0 -5 12 1121.53 452.251 4 0 -5 11 65.9366 252.729 4 0 -5 10 239.779 130.774 5 0 -5 10 888.097 361.743 4 0 -5 9 4130.59 581.439 4 0 -5 9 2722.76 335.059 5 0 -5 8 797.194 171.194 5 0 -5 8 1367.6 374.774 4 0 -5 7 272.71 208.312 4 0 -5 7 361.099 124.186 5 0 -5 6 1497.95 314.292 4 0 -5 5 316.821 198.56 4 0 5 -4 4900.64 480.546 1 0 -5 4 3567.24 434.053 4 0 5 -3 165.052 128.158 1 0 -5 3 336.444 180.255 4 0 5 -2 194.407 118.471 1 0 -5 2 285.568 214.383 4 0 5 -1 1651.01 220.412 1 0 5 0 2649.7 275.987 1 0 5 1 3825.64 332.774 1 0 5 2 118.472 112.225 1 0 5 3 4424.17 390.152 1 0 5 4 1484.88 251.361 1 0 5 4 1328.63 286.649 5 0 5 5 263.842 172.436 5 0 5 6 343.343 234.805 5 0 5 7 237.428 180.693 5 0 5 8 466.418 184.684 5 0 5 9 584.224 240.289 5 0 5 10 2318.23 433.936 5 0 5 11 1617.73 396.557 5 0 5 12 2859.75 525.724 5 0 5 13 -8.28305 230.205 5 0 -6 11 -327.203 308.843 4 0 -6 10 471.669 210.414 4 0 -6 9 397.145 233.561 4 0 -6 8 -11.9016 270.32 4 0 -6 7 2040.22 371.464 4 0 -6 7 2021.17 279.418 5 0 -6 6 620.61 302.197 4 0 -6 5 413.611 191.684 4 0 6 -4 10708.6 799.922 1 0 -6 4 7525.44 660.595 4 0 -6 3 8908.95 724.363 4 0 6 -3 10185.8 665.508 1 0 6 -2 958.448 212.018 1 0 6 -1 3817.68 372.368 1 0 6 0 7759.19 500.911 1 0 6 1 3931.48 370.926 1 0 6 2 523.651 162.089 1 0 6 3 2625.98 331.059 1 0 6 4 2216.54 319.756 1 0 6 5 115.828 135.676 1 0 6 6 2541.33 442.295 5 0 6 6 2439.85 342.9 1 0 6 7 -51.7494 151.832 5 0 6 8 829.6 275.98 5 0 6 9 835.75 311.598 5 0 6 10 504.723 270.362 5 0 6 11 218.655 161.446 5 0 6 12 734.452 314.873 5 0 -7 10 372.703 286.705 4 0 -7 9 1374.28 432.088 4 0 -7 8 899.554 289.325 4 0 -7 7 -479.179 272.903 4 0 -7 6 153.528 200.458 4 0 -7 5 1363.22 319.022 4 0 -7 4 -403.749 241.129 4 0 7 -2 362.96 176.534 1 0 7 -1 490.785 169.431 1 0 7 0 -144.678 97.9735 1 0 7 1 280.839 114.205 1 0 7 2 383.614 186.555 1 0 7 3 -130.719 127.315 1 0 7 4 77.2098 123.81 1 0 7 5 -111.594 173.712 1 0 7 6 137.706 146.45 1 0 7 7 -149.938 192.533 1 0 7 8 1116.15 351.177 5 0 7 8 1088.58 265.381 1 0 7 9 645.044 293.883 5 0 7 9 97.9071 142.25 1 0 7 10 359.738 231.833 5 0 7 11 112.969 264.431 5 0 -8 9 501.203 324.463 4 0 -8 8 258.946 286.825 4 0 -8 7 -146.707 308.83 4 0 -8 6 -76.4576 262.32 4 0 8 6 458.204 183.474 1 0 8 7 -87.8394 133.306 1 0 8 8 -94.6931 196.677 1 0 8 9 329.811 177.174 1 0 8 10 -862.083 304.151 1 0 8 11 31.3195 215.248 1 -1 8 10 407.652 259.845 5 -1 7 11 -452.083 312.894 5 -1 7 10 444.355 266.017 5 -1 7 9 248.51 201.591 5 -1 7 8 969.215 254.652 1 -1 7 8 598.749 231.467 5 -1 7 7 714.823 290.357 5 1 -7 6 863.639 325.906 4 1 -7 7 179.059 237.341 4 1 -7 8 778.016 312.429 4 1 -7 9 263.723 224.506 4 -1 6 12 405.384 274.199 5 -1 6 11 61.0047 181.22 5 -1 6 10 36.0358 200.758 5 -1 6 9 167.109 213.792 5 -1 6 8 429.194 240.605 5 -1 6 7 -199.305 166.025 5 -1 6 6 -11.6172 138.846 5 -1 6 5 167.399 168.964 5 -1 6 5 474.525 150.076 1 -1 6 4 250.623 152.557 1 -1 6 3 -92.6576 106.678 1 -1 6 2 2976.92 287.029 1 -1 6 1 -18.131 89.3859 1 -1 6 0 6118.25 366.906 1 1 -6 5 2039.9 455.715 4 1 -6 6 846.037 287.265 4 1 -6 7 768.442 277.968 4 1 -6 8 119.874 215.007 4 1 -6 9 27.1017 187.261 4 1 -6 10 852.129 375.449 4 -1 5 13 1114.86 349.05 5 -1 5 12 582.438 336.277 5 -1 5 11 178.227 230.372 5 -1 5 10 -330.995 231.928 5 -1 5 9 732.962 271.929 5 -1 5 8 3207.49 515.407 5 -1 5 7 91.5337 180.571 5 -1 5 6 3059.98 451.909 5 -1 5 5 184.715 191.124 5 -1 5 4 926.239 254.585 5 -1 5 3 156.375 148.875 5 -1 5 3 -52.4447 105.978 1 -1 5 2 62.1407 90.4579 1 -1 5 1 133.65 91.1687 1 -1 5 0 1949.01 187.175 1 1 -5 1 206.845 124.786 5 -1 5 -1 334.729 97.8149 1 -1 5 -2 10263.5 524.217 1 1 -5 3 -279.889 276.812 4 1 -5 4 387.49 227.989 4 1 -5 5 694.138 274.678 4 1 -5 5 169.79 88.4153 5 1 -5 6 -86.9193 207.158 4 1 -5 6 304.914 97.0125 5 1 -5 7 -85.6127 214.882 4 1 -5 8 1431.06 389.017 4 1 -5 9 3371.91 556.843 4 1 -5 10 190.073 224.852 4 1 -5 11 -484.486 319.659 4 1 -5 12 960.881 422.958 4 -1 4 14 363.46 194.054 5 -1 4 13 1855.24 424.123 5 -1 4 12 1443.12 415.357 5 -1 4 11 42.3971 181.475 5 -1 4 10 2202.37 493.497 5 -1 4 9 4629.18 639.566 5 -1 4 8 2726.92 469.846 5 -1 4 7 490.888 212.222 5 -1 4 6 5766.66 577.766 5 -1 4 5 1794.74 324.177 5 -1 4 4 118.45 174.349 5 -1 4 3 159.45 139.535 5 -1 4 2 884.277 214.153 5 -1 4 2 1376.08 175.372 1 1 -4 -1 7394.7 519.45 5 -1 4 1 9228.68 370.948 1 1 -4 0 11388.5 607.961 5 -1 4 0 13430.7 398.176 1 1 -4 1 196.349 86.0337 5 -1 4 -1 242.979 61.5552 1 1 -4 2 -70.1588 71.2172 5 1 -4 2 -83.9559 61.4507 1 1 -4 3 6926.93 614.225 4 1 -4 3 6375.74 298.328 1 1 -4 4 27137.3 1197.32 4 1 -4 4 28633 692.598 1 1 -4 5 1260.23 167.552 5 1 -4 5 1488.13 325.063 4 1 -4 6 11.1525 65.9287 5 1 -4 6 423.044 281.263 4 1 -4 7 3819.19 364.388 5 1 -4 7 5561.33 601.468 4 1 -4 8 0.11504 195.199 4 1 -4 8 89.962 85.8974 5 1 -4 9 422.691 280.311 4 1 -4 9 520.771 184.195 5 1 -4 10 2748.97 497.894 4 1 -4 11 -281.702 229.996 4 1 -4 12 127.354 273.333 4 1 -4 13 101.097 262.989 4 -1 3 14 -420.256 290.695 5 -1 3 13 71.4138 183.993 5 -1 3 12 4328.48 676.25 5 -1 3 11 1568.44 357.22 5 -1 3 10 5792.85 662.953 5 -1 3 9 -84.0699 197.887 5 -1 3 8 218.329 218.156 5 -1 3 7 5569.95 583.392 5 -1 3 6 89.2345 142.91 5 -1 3 5 1848.83 302.173 5 -1 3 4 4031.96 392.542 5 -1 3 3 564.308 163.154 5 1 -3 -2 4991.13 369.322 5 -1 3 2 5478.98 384.165 5 -1 3 1 8971.56 325.774 1 -1 3 1 8055.95 431.121 5 1 -3 -1 9067.53 448.974 5 -1 3 0 2872.56 152.402 1 1 -3 0 3049.02 243.501 5 -1 3 -1 492.464 67.9479 1 1 -3 1 687.812 110.43 5 1 -3 2 7918.38 253.143 1 1 -3 2 9005.7 615.494 4 1 -3 3 759.99 94.6645 1 1 -3 3 660.945 215.777 4 1 -3 4 1589.86 148.275 5 1 -3 4 1886.52 333.839 4 1 -3 4 1537.36 153.015 1 1 -3 5 141.879 205.877 4 1 -3 5 -78.8669 78.287 1 1 -3 5 -3.82661 68.2465 5 1 -3 6 765.86 146.701 5 1 -3 6 758.496 258.019 4 1 -3 7 627.637 263.737 4 1 -3 7 833.035 181.81 5 1 -3 8 2223.55 397.444 4 1 -3 8 1869.46 264.379 5 1 -3 9 5335.47 490.255 5 1 -3 9 5815.41 670.993 4 1 -3 10 1238.29 422.29 4 1 -3 10 1544.25 317.774 5 1 -3 11 2213.38 498.964 4 1 -3 11 1749.14 353.932 5 1 -3 12 -163.678 307.506 4 1 -3 12 -348.526 247.091 5 1 -3 13 278.7 409.779 4 -1 2 15 540.076 306.804 5 -1 2 14 63.5004 187.943 5 -1 2 13 -70.9939 233.322 5 -1 2 12 2578.91 518.159 5 -1 2 11 14452.1 1110.71 5 -1 2 10 -149.561 214.985 5 -1 2 9 872.625 248.345 5 -1 2 8 5204.48 592.046 5 -1 2 7 37189.9 1397.52 5 -1 2 6 23949.7 1058.12 5 -1 2 5 7079.71 528.448 5 -1 2 4 18821.1 791.538 5 -1 2 3 7022.59 447.236 5 1 -2 -3 7086.56 396.583 5 -1 2 2 844.96 145.395 5 1 -2 -2 1051.75 142.414 5 1 -2 -1 846.842 111.336 5 -1 2 1 937.592 130.699 5 -1 2 0 6278.85 382.109 3 -1 2 0 5510.2 406.731 4 -1 2 0 5673.7 245.538 5 1 -2 0 5938.73 242.238 5 -1 2 -1 11189.8 499.31 3 1 -2 1 9763.7 267.31 5 1 -2 2 15938.5 711.287 4 1 -2 2 14317.7 307.94 1 -1 2 -2 15486.7 565.816 3 1 -2 2 16077.3 508.974 3 -1 2 -3 19673.9 671.269 3 1 -2 3 19413 458.856 1 1 -2 3 19451.1 827.447 4 1 -2 3 19907.6 559.829 3 1 -2 3 19202.5 395.88 5 1 -2 4 1204.24 147.631 1 1 -2 4 1194.78 129.365 5 1 -2 4 1277.74 261.597 4 1 -2 4 1287.9 149.873 3 1 -2 5 66471.3 1166.38 5 1 -2 5 65415.5 1227.09 1 1 -2 5 68803 1711.11 4 1 -2 5 68982.8 1016.69 3 1 -2 6 5967.03 555.866 4 1 -2 6 5725.02 379.236 5 1 -2 6 5864.65 298.044 3 1 -2 7 14733.9 465.96 3 1 -2 7 14374.9 892.599 4 1 -2 7 13300.5 662.022 5 1 -2 8 7.85755 217.079 4 1 -2 8 96.2729 147.013 5 1 -2 8 229.762 67.7518 3 1 -2 9 714.951 328.23 4 1 -2 9 490.062 155.91 5 1 -2 9 485.911 93.3021 3 1 -2 10 614.009 211.48 5 1 -2 10 1098.42 340.246 4 1 -2 11 12994.8 1124.24 4 1 -2 11 13804.3 934.92 5 1 -2 12 70.7088 187.909 5 1 -2 12 313.125 265.145 4 1 -2 13 -311.29 316.967 4 1 -2 13 -44.208 137.691 5 1 -2 14 637.816 439.778 4 1 -2 14 -9.17837 206.297 5 -1 1 15 119.442 275.185 5 -1 1 14 355.097 262.597 5 -1 1 13 1346.41 403.373 5 -1 1 12 683.68 302.56 5 -1 1 11 16678.6 1141.74 5 -1 1 10 369.247 231.943 5 -1 1 9 24296.6 1236.61 5 -1 1 8 6830.06 622.506 5 -1 1 7 1115.6 243.805 5 -1 1 6 3800.9 406.603 5 -1 1 5 11423.5 623.117 5 -1 1 4 20100.3 750.962 5 -1 1 4 21068.9 620.073 3 -1 1 3 80.562 67.8055 3 -1 1 3 88.0151 105.526 5 1 -1 -3 114.786 71.5193 5 1 -1 -2 5233.8 247.9 5 -1 1 2 5057.76 277.222 5 -1 1 2 4749.32 278.085 3 -1 1 1 8506.61 292.058 1 -1 1 1 10275.1 331.483 5 -1 1 1 9789.18 382.339 3 1 -1 -1 9344.88 278.635 5 1 -1 -1 9044.73 376.788 3 1 -1 0 5313.74 273.73 3 -1 1 0 5923.16 177.33 5 1 -1 0 5319.14 155.061 5 -1 1 0 5514.22 286.165 3 -1 1 -1 421.953 110.264 3 1 -1 1 740.541 134.408 3 -1 1 -1 778.819 153.329 4 1 -1 1 1118.53 230.516 4 1 -1 2 30906.8 661.429 3 1 -1 2 32504.1 877.411 4 -1 1 -2 32138.9 829.762 4 1 -1 3 421.07 73.4324 5 1 -1 3 330.891 150.115 4 1 -1 3 346.317 83.9535 3 -1 1 -3 484.925 70.6924 5 1 -1 4 47.2223 62.711 3 1 -1 4 -126.011 157.277 4 1 -1 4 12.6519 61.2654 5 -1 1 -4 16.397 49.8704 5 1 -1 5 23749.9 616.064 3 1 -1 5 24431.9 967.002 4 -1 1 -5 23269.6 669.498 5 1 -1 5 23256 716.998 5 1 -1 6 8143.23 369.157 3 1 -1 6 8041.34 480.272 5 1 -1 7 6391.27 491.039 5 1 -1 8 3288.91 384.738 5 1 -1 8 3021.97 235.598 3 1 -1 9 19003.6 998.707 5 1 -1 9 19248.9 594.12 3 1 -1 10 206.127 159.186 5 1 -1 11 728.415 253.609 5 1 -1 12 861.452 315.113 5 1 -1 13 -26.0968 144.701 5 1 -1 14 -52.4682 179.506 5 1 -1 15 66.3232 156.82 5 1 -1 16 -163.319 201.657 5 -1 0 15 -65.5499 201.165 5 -1 0 14 865.653 361.051 5 -1 0 13 42.3796 194.686 5 -1 0 12 407.192 267.43 5 -1 0 11 1397.09 359.308 5 -1 0 10 16943.4 1057.07 5 -1 0 9 648.683 246.484 5 -1 0 8 2238.74 176.625 3 -1 0 8 2407.15 355.05 5 -1 0 7 3440.33 415.581 5 -1 0 7 3237.6 211.924 3 -1 0 6 10902.5 369.334 3 -1 0 6 11594.9 633.389 5 -1 0 5 32129.6 950.397 5 -1 0 5 30749.3 593.362 3 -1 0 4 197.663 44.1793 3 -1 0 4 176.611 83.6938 5 -1 0 3 1518.56 182.745 1 -1 0 3 1682.25 180.033 5 1 0 -3 1385.35 173.32 5 -1 0 3 1741.24 133.527 3 -1 0 2 1745.02 170.948 5 1 0 -2 2028.22 178.81 1 -1 0 2 1679.05 167.176 1 1 0 -2 1813.96 146.106 3 -1 0 2 1805.49 131.121 3 1 0 -1 166531 1291.24 1 -1 0 1 166255 1310.8 1 1 0 -1 166534 1320.49 3 -1 0 1 165762 1393.09 3 1 0 0 42654.4 719.797 3 -1 0 0 42477.7 570.565 1 -1 0 -1 143054 1291.06 4 1 0 1 142408 1384.35 4 1 0 1 142937 1078.11 1 -1 0 -2 8164.65 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827.159 1 3 3 4 145.682 170.91 1 3 3 5 8180.01 630.59 1 3 3 6 329.893 131.214 4 3 3 6 148.707 162.951 1 3 3 7 6479.3 617.821 1 3 3 7 7127.89 504.32 4 3 3 8 3106.33 372.351 4 3 3 8 2825.52 421.737 1 3 3 9 136.224 144.471 5 3 3 9 357.023 218.972 4 3 3 10 1853.15 405.18 5 3 3 10 2503.99 409.893 4 3 3 11 2366.07 435.36 5 3 3 11 2582.24 426.621 4 3 3 12 291.757 145.363 5 3 3 12 749.408 326.353 4 3 3 13 310.417 208.229 5 3 3 13 165.432 187.053 4 3 3 14 186.263 230.245 5 3 3 15 -128.379 167.356 5 -3 -4 12 349.236 227.236 5 -3 -4 11 402.948 191.476 5 -3 -4 10 756.457 247.199 5 -3 -4 9 22.5225 141.437 5 -3 -4 8 371.645 194.196 5 3 4 -7 1437.96 375.866 1 3 4 -6 -107.156 203.332 1 3 4 -5 959.575 242.255 1 3 4 -4 848.652 252.334 1 3 4 -3 4282.25 454.852 1 3 4 -2 63.694 148.604 1 3 4 -1 2832.84 355.794 1 3 4 0 595.052 183.219 1 -3 -4 -1 597.56 76.4549 4 3 4 1 1036.73 253.655 1 3 4 2 1124.17 254.009 1 3 4 3 7511.09 600.875 1 3 4 4 3290.01 413.723 1 3 4 5 2348.31 382.648 1 3 4 6 193.574 102.664 4 3 4 6 113.502 173.77 1 3 4 7 1080.1 179.649 4 3 4 7 895.502 263.225 1 3 4 8 5772.03 635.312 1 3 4 8 6167.66 446.967 4 3 4 9 13.2786 160.196 4 3 4 9 -32.1647 172.862 1 3 4 10 26.4601 165.208 1 3 4 11 2370.93 471.811 1 3 4 11 2337.21 489.239 5 3 4 12 191.094 231.432 5 3 4 13 100.306 198.933 5 3 4 14 181.399 216.115 5 -3 -5 11 73.3346 137.362 5 -3 -5 10 559.542 215.983 5 -3 -5 9 2122.98 375.528 5 3 5 -8 4329.38 726.937 1 -3 -5 8 3775.51 531.816 5 3 5 -7 134.68 220.619 1 3 5 -6 138.598 173.793 1 3 5 -5 999.44 257.815 1 3 5 -4 719.744 219.38 1 3 5 -3 5097.22 549.162 1 3 5 -2 2495.26 385.465 1 3 5 -1 34.2492 141.452 1 -3 -5 0 1079.44 105.809 4 3 5 0 562.844 252.927 1 3 5 1 637.567 221.254 1 3 5 2 591.541 240.336 1 3 5 3 554.982 210.705 1 3 5 4 1368.21 322.49 1 3 5 5 47.9223 176.257 1 3 5 6 1965.59 387.02 1 3 5 7 296.672 213.581 1 3 5 8 388.006 235.176 1 3 5 9 352.191 221.801 1 3 5 10 -70.6686 159.642 1 3 5 11 -312.963 215.214 1 3 5 12 909.224 347.951 1 3 5 13 157.276 185.689 1 3 5 13 499.681 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538.609 1 4 -1 2 13674.7 791.333 3 4 -1 3 171.882 94.8469 1 4 -1 3 259.379 152.324 3 4 -1 4 948.282 175.156 1 4 -1 4 991.336 249.641 3 4 -1 5 1761.33 309.849 3 4 -1 5 1818.64 232.513 1 4 -1 6 13358.8 645.534 1 4 -1 6 13610.1 833.67 3 4 -1 7 1452.93 294.508 3 4 -1 8 -59.876 224.489 4 4 -1 8 65.503 119.74 3 4 -1 9 305.352 219.507 4 4 -1 9 287.081 135.824 3 4 -1 10 2373.76 525.999 4 4 -1 10 2699.43 384.498 3 4 -1 11 4730.4 729.994 4 4 -1 12 730.151 305.682 4 -4 0 12 217.798 265.718 5 -4 0 11 257.021 199.228 5 -4 0 10 609.211 275.051 5 -4 0 9 2153.6 403.551 5 -4 0 8 -469.404 220.45 5 -4 0 7 20302.6 1121.85 5 4 0 -6 1213.86 278.834 3 -4 0 6 856.787 223.67 5 -4 0 5 1088.99 242.288 5 4 0 -5 863.474 247.187 3 -4 0 4 226.641 160.092 5 4 0 -4 202.07 142.239 3 4 0 -3 8813.66 623.79 1 -4 0 3 7484.75 547.706 5 4 0 -3 6644.76 579.706 3 4 0 -2 17160.4 814.831 1 -4 0 2 16926.6 787.021 5 4 0 -2 15465.7 854.783 3 4 0 -1 1248.5 250.227 3 4 0 -1 1260.82 227.322 1 4 0 0 10356.8 562.033 1 4 0 0 10006.8 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5043.73 463.763 3 4 2 -6 11196 960.504 1 4 2 -6 10109.6 659.753 3 -4 -2 6 10892.6 795.766 5 4 2 -5 483.253 246.377 1 4 2 -5 352.439 177.398 3 4 2 -4 3572.71 480.141 1 4 2 -4 3305.5 423.136 3 4 2 -3 1666.02 324.953 3 4 2 -3 1609.37 289.2 1 4 2 -2 837.459 236.074 1 4 2 -2 688.983 208.653 3 4 2 -1 3364.24 388.585 1 4 2 0 12740.4 711.761 1 4 2 1 4451.66 407.276 1 4 2 2 384.186 172.154 1 4 2 3 84.0096 149.404 1 4 2 4 -112.667 199.563 1 4 2 5 552.567 196.087 1 4 2 6 3521.58 460.937 1 4 2 7 1064.84 298.944 1 4 2 8 7606.11 715.827 1 4 2 8 8299.91 670.608 4 4 2 9 580.513 199.378 4 4 2 9 988.305 303.176 1 4 2 10 266.626 191.338 4 4 2 10 293.355 203.663 1 4 2 11 401.504 236.902 4 4 2 11 194.199 210.988 1 4 2 12 1609.2 361.042 4 4 2 12 859.457 334.988 1 4 2 13 1356.43 370.677 1 4 2 14 241.282 264.843 1 -4 -3 11 603.107 253.465 5 -4 -3 10 373.303 172.564 5 -4 -3 9 3310.06 503.31 5 -4 -3 8 1269.73 309.872 5 4 3 -7 3587.42 593.412 1 -4 -3 7 3635.89 483.262 5 4 3 -6 1709.75 389.127 1 4 3 -6 1521.05 270.858 3 4 3 -5 2670.86 469.748 1 4 3 -5 2212.56 338.778 3 4 3 -4 59.5988 127.589 3 4 3 -4 228.992 156.875 1 4 3 -3 14044.2 873.653 1 4 3 -2 1621.19 311.394 1 4 3 -1 5533.75 511.113 1 4 3 0 6146.88 517.042 1 4 3 1 4083.46 424.267 1 4 3 2 11391.2 718.279 1 4 3 3 717.712 207.334 1 4 3 4 1088.67 283.327 1 4 3 5 348.572 202.652 1 4 3 6 3186.74 450.745 1 4 3 7 6026.48 640.276 1 4 3 8 8380.76 758.6 1 4 3 8 8022.57 620.231 4 4 3 9 9442.25 845.97 1 4 3 9 10133.8 723.627 4 4 3 10 597.596 257.498 1 4 3 11 280.329 269.726 1 4 3 12 248.288 262.921 1 4 3 13 670.931 283.054 1 -4 -4 11 -55.3513 158.056 5 -4 -4 10 132.594 137.214 5 -4 -4 9 474.983 196.519 5 -4 -4 8 307.721 171.142 5 4 4 -7 -127.46 194.05 1 4 4 -6 4634.59 448.98 3 4 4 -6 4632.61 622.188 1 4 4 -5 2078.52 418.914 1 4 4 -4 408.388 202.111 1 4 4 -3 363.679 193.173 1 4 4 -2 482.461 213.979 1 4 4 -1 54.0172 142.627 1 4 4 0 2981.11 383.682 1 4 4 1 1047.14 283.034 1 4 4 2 1844.12 342.548 1 4 4 3 -120.443 185.245 1 4 4 4 2045.1 362.337 1 4 4 5 904.819 227.094 1 4 4 6 69.4988 148.045 1 4 4 7 1821.48 367.76 1 4 4 8 19.1829 152.852 1 4 4 9 1798.32 396.459 1 4 4 10 542.526 276.986 1 4 4 11 4.29424 176.214 1 4 4 12 -220.428 261.145 1 4 4 13 391.65 304.283 1 -4 -5 10 340.932 209.774 5 -4 -5 9 1577.2 353.781 5 -4 -5 8 777.559 276.099 5 4 5 -8 592.936 322.514 1 4 5 -7 1803.04 433.754 1 4 5 -6 3975.61 584.801 1 4 5 -5 -327.108 224.014 1 4 5 -4 -277.168 186.767 1 4 5 -3 155.758 213.729 1 4 5 -2 10716.7 802.719 1 4 5 -1 -399.3 249.277 1 4 5 0 160.121 137.415 1 4 5 1 2189.32 357.159 1 4 5 2 -63.9062 158.902 1 4 5 3 7166.27 679.396 1 4 5 4 119.853 187.631 1 4 5 5 1238.51 309.333 1 4 5 6 96.4722 147.069 1 4 5 7 1134.01 283.306 1 4 5 8 4867.81 630.813 1 4 5 9 289.619 231.913 1 4 5 10 2629.55 493.902 1 4 5 11 1395.02 493.055 1 4 5 12 201.949 190.096 1 -4 -6 9 324.34 211.334 5 4 6 -8 367.27 330.648 1 4 6 -7 1804.87 426.735 1 4 6 -6 860.085 319.868 1 4 6 -5 1056.6 335.317 1 4 6 -4 514.525 285.281 1 4 6 -3 307.656 210.251 1 4 6 -2 662.12 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823.998 281.037 3 6 0 5 -135.24 234.091 3 6 0 6 70.1278 171.121 3 6 0 7 -80.7452 164.033 3 6 0 8 -53.7684 149.049 3 6 0 9 2958.49 540.46 3 -6 -1 8 2209.24 477.569 5 6 1 -7 -60.385 246.38 3 -6 -1 7 148.56 242.783 5 -6 -1 6 -145.06 134.886 5 6 1 -6 343.662 156.766 3 -6 -1 5 157.009 188.083 5 6 1 -5 545.644 256.461 3 6 1 -4 485.741 223.6 1 -6 -1 4 454.587 138.227 5 6 1 -4 59.2204 153.796 3 6 1 -3 -89.8267 198.59 1 -6 -1 3 -132.359 195.626 5 6 1 -3 -76.0273 152.054 3 6 1 -2 1506.22 326.295 1 -6 -1 2 1229.48 280.245 5 6 1 -2 1210 315.254 3 6 1 -1 724.248 221.566 1 6 1 -1 931.219 283.725 3 6 1 0 1018.82 262.1 1 6 1 0 749.717 254.601 3 6 1 1 2266.37 331.445 1 6 1 1 1730.57 361.444 3 6 1 2 223.274 188.274 3 6 1 3 1403.72 341.053 3 6 1 4 1287.64 346.249 3 6 1 5 979.207 348.168 3 6 1 6 -259.781 240.598 3 6 1 7 -125.714 202.66 3 6 1 8 56.1992 223.194 3 6 1 9 250.504 298.604 3 -6 -2 8 5358.68 713.31 5 -6 -2 7 530.351 255.048 5 -6 -2 6 -22.8488 142.454 5 6 2 -6 113.376 211.323 3 6 2 -5 307.52 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1573.04 398.59 3 6 3 0 590.501 223.708 1 6 3 0 485.795 288.897 3 6 3 1 782.822 247.774 3 6 3 1 392.536 191.314 1 6 3 2 8703.97 747.767 1 6 3 3 577.215 208.057 1 6 3 4 2176.16 404.828 1 6 3 5 1723.28 372.448 1 6 3 6 2012.72 390.481 1 6 3 7 -195.564 268.571 1 6 3 8 689.21 313.112 1 6 3 9 304.668 169.232 1 6 3 10 -359.821 290.262 1 -6 -4 6 563.933 314.057 5 6 4 -6 560.292 286.084 1 6 4 -5 -62.9941 193.759 1 6 4 -4 -406.546 290.302 1 6 4 -4 686.251 244.483 3 6 4 -3 688.974 292.769 3 6 4 -3 320.16 222.588 1 6 4 -2 2660.26 442.232 1 6 4 -2 2653.69 484.336 3 6 4 -1 426.844 216.117 1 6 4 0 3778.16 537.317 1 6 4 1 77.658 187.918 1 6 4 2 1266.49 339.68 1 6 4 3 758.357 286.87 1 6 4 4 1409.38 363.699 1 6 4 5 291.718 192.29 1 6 4 6 2350.82 454.407 1 6 4 7 310.212 265.937 1 6 4 8 549.046 325.991 1 6 4 9 -71.8387 207.598 1 6 4 10 326.155 232.661 1 6 5 -5 24.118 203.321 1 6 5 -4 763.745 293.789 1 6 5 -4 628.658 277.217 3 6 5 -3 1010.34 291.025 3 6 5 -3 1186.42 322.944 1 6 5 -2 1292.87 378.123 1 6 5 -1 1446.1 338.687 1 6 5 0 655.932 283.623 1 6 5 1 -165.036 170.026 1 6 5 2 -235.725 163.119 1 6 5 3 4761.76 621.92 1 6 5 4 -145.097 216.979 1 6 5 5 605.919 305.121 1 6 5 6 1156.89 344.097 1 6 5 7 1363.23 400.286 1 6 5 8 508.994 263.501 1 6 6 -3 821.568 319.551 1 6 6 -2 263.273 220.766 1 6 6 -1 3046.19 531.009 1 6 6 0 845.824 256.511 1 6 6 1 535.186 316.374 1 6 6 2 -102.229 196.49 1 6 6 3 652.173 265.698 1 6 6 4 1465.73 357.697 1 6 6 5 16.9654 215.74 1 6 6 6 227.742 212.168 1 7 2 -5 -115.938 151.311 3 7 2 -4 -159.484 257.061 3 7 2 -3 20.5375 205.82 3 7 2 -2 391.585 239.692 3 7 2 -1 286.61 202.566 3 7 2 0 1511.36 389.326 3 7 3 -4 3.63084 211.728 1 -7 -3 4 88.5234 169.657 5 7 3 -4 413.888 231.668 3 7 3 -3 126.499 206.761 1 7 3 -3 245.87 220.95 3 7 3 -2 133.062 221.404 1 7 3 -2 141.326 151.959 3 7 3 -1 -377.302 288.611 3 7 3 -1 -348.26 255.575 1 7 3 0 521.247 176.358 1 7 3 0 858.743 334.282 3 7 3 1 916.062 302.268 1 7 3 1 723.686 261.098 3 7 3 2 16.3866 144.521 1 7 4 -3 -21.5642 212.373 3 7 4 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