#------------------------------------------------------------------------------ #$Date: 2021-11-05 00:58:55 +0200 (Fri, 05 Nov 2021) $ #$Revision: 270307 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/12/92/7129202.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7129202 loop_ _publ_author_name 'Kim, Youyoung' 'Kim, Dongwook' 'Chang, Sukbok' _publ_section_title ; Ir(iii)-Catalysed electrooxidative intramolecular dehydrogenative C--H/N--H coupling for the synthesis of N--H indoles ; _journal_name_full 'Chemical Communications' _journal_paper_doi 10.1039/D1CC05882G _journal_year 2021 _chemical_formula_sum 'C19 H24 Ir N' _chemical_formula_weight 458.59 _space_group_crystal_system orthorhombic _space_group_IT_number 29 _space_group_name_Hall 'P 2c -2ac' _space_group_name_H-M_alt 'P c a 21' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2021-10-03 deposited with the CCDC. 2021-11-01 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.834(3) _cell_length_b 8.0960(16) _cell_length_c 14.131(3) _cell_measurement_reflns_used 45870 _cell_measurement_temperature 223(2) _cell_measurement_theta_max 34.080 _cell_measurement_theta_min 0.372 _cell_volume 1697.1(6) _computing_cell_refinement HKL3000sm _computing_data_collection 'PAL BL2D-SMDC Program' _computing_data_reduction HKL3000sm _computing_structure_refinement SHELXL _computing_structure_solution SHELXS _diffrn_ambient_temperature 223(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Rayonix MX225HS CCD area detector' _diffrn_measurement_method 'omega scan' _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.650 _diffrn_reflns_av_R_equivalents 0.0379 _diffrn_reflns_av_unetI/netI 0.0295 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -17 _diffrn_reflns_number 12196 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 22.955 _diffrn_reflns_theta_max 23.996 _diffrn_reflns_theta_min 2.301 _diffrn_source 'PLSII 2D bending magnet' _exptl_absorpt_coefficient_mu 6.224 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.940 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'HKL3000sm Scalepack' _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.795 _exptl_crystal_description block _exptl_crystal_F_000 888 _exptl_crystal_size_max 0.042 _exptl_crystal_size_mid 0.035 _exptl_crystal_size_min 0.031 _refine_diff_density_max 1.241 _refine_diff_density_min -1.126 _refine_diff_density_rms 0.091 _refine_ls_abs_structure_details ; Flack x determined using 1517 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.002(7) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.048 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 202 _refine_ls_number_reflns 3480 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.048 _refine_ls_R_factor_all 0.0209 _refine_ls_R_factor_gt 0.0193 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0291P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0492 _refine_ls_wR_factor_ref 0.0497 _reflns_Friedel_coverage 0.914 _reflns_Friedel_fraction_full 0.997 _reflns_Friedel_fraction_max 0.997 _reflns_number_gt 3272 _reflns_number_total 3480 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1cc05882g2.cif _cod_data_source_block PO19049_029 _cod_database_code 7129202 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.780 _shelx_estimated_absorpt_t_max 0.830 _shelx_res_file ; TITL PO19049_029 in Pca2(1) PO19049_029.res created by SHELXL-2018/3 at 15:37:05 on 03-May-2019 CELL 0.65000 14.83400 8.09600 14.13100 90.0000 90.0000 90.0000 ZERR 4.00 0.00297 0.00162 0.00283 0.0000 0.0000 0.0000 LATT -1 SYMM -X, -Y, 0.5+Z SYMM 0.5+X, -Y, Z SYMM 0.5-X, Y, 0.5+Z SFAC C H N IR DISP C 0.0024 0.0013 9.52 DISP N 0.0048 0.0027 15.81 DISP Ir -0.8791 6.9422 26194.88 UNIT 76 96 4 4 ACTA OMIT -3 48.00 OMIT 0 0 -2 OMIT 0 0 2 OMIT 6 2 0 OMIT 5 6 10 OMIT 6 1 -4 SIZE 0.042 0.035 0.031 TEMP -50.15 CONF MERG 2 L.S. 12 BOND $H FMAP 2 PLAN 20 LIST 4 DFIX 0.80 N2 H2 WGHT 0.029100 FVAR 0.99197 IR1 4 0.206715 0.548394 0.491077 11.00000 0.02578 0.02549 = 0.02562 0.00009 0.00187 -0.00586 N2 3 0.245621 0.685452 0.386379 11.00000 0.03554 0.02379 = 0.03325 0.00264 0.00064 -0.01065 H2 2 0.214268 0.666547 0.342122 11.00000 -1.50000 C3 1 0.313084 0.798615 0.375190 11.00000 0.02863 0.02047 = 0.03952 -0.00098 0.00740 0.00023 C4 1 0.325615 0.870763 0.285380 11.00000 0.04406 0.02645 = 0.04385 0.00550 0.00935 -0.00328 AFIX 43 H4 2 0.286065 0.842155 0.236059 11.00000 -1.20000 AFIX 0 C5 1 0.393453 0.981111 0.267562 11.00000 0.05192 0.03210 = 0.05978 0.01648 0.01236 0.00026 AFIX 43 H5 2 0.400515 1.026968 0.206901 11.00000 -1.20000 AFIX 0 C6 1 0.451929 1.024485 0.340736 11.00000 0.04092 0.03012 = 0.07949 0.00798 0.01883 -0.00504 AFIX 43 H6 2 0.499267 1.099160 0.329543 11.00000 -1.20000 AFIX 0 C7 1 0.440305 0.958849 0.427680 11.00000 0.03115 0.02854 = 0.06937 -0.00879 0.00070 -0.00220 AFIX 43 H7 2 0.480037 0.991379 0.476034 11.00000 -1.20000 AFIX 0 C8 1 0.371535 0.843530 0.450297 11.00000 0.02388 0.01641 = 0.05141 -0.00489 0.00520 0.00003 C9 1 0.362452 0.774668 0.543722 11.00000 0.02335 0.02734 = 0.03773 -0.01211 -0.00426 0.00003 C10 1 0.301019 0.656976 0.567233 11.00000 0.03030 0.03682 = 0.02377 -0.00229 -0.00268 0.00129 H10 2 0.304122 0.633560 0.624391 11.00000 -1.20000 C11 1 0.427293 0.835479 0.621027 11.00000 0.03300 0.04315 = 0.05509 -0.01708 -0.01377 -0.00166 AFIX 137 H11A 2 0.416270 0.774789 0.679070 11.00000 -1.50000 H11B 2 0.417535 0.952378 0.632046 11.00000 -1.50000 H11C 2 0.489009 0.817660 0.600767 11.00000 -1.50000 AFIX 0 C12 1 0.074365 0.430974 0.449512 11.00000 0.03523 0.04564 = 0.04432 0.00788 -0.00300 -0.03124 C13 1 0.074351 0.498626 0.545456 11.00000 0.01833 0.02864 = 0.04381 0.00822 0.00404 -0.01358 C14 1 0.139489 0.408519 0.601555 11.00000 0.02473 0.01875 = 0.03871 0.00401 0.00246 0.00121 C15 1 0.184089 0.297785 0.539388 11.00000 0.03532 0.01659 = 0.03302 0.00744 0.00870 -0.00989 C16 1 0.142621 0.310769 0.447323 11.00000 0.04834 0.03347 = 0.04071 -0.00710 0.01588 -0.02024 C17 1 0.012880 0.483393 0.372250 11.00000 0.06777 0.08448 = 0.05382 0.03048 -0.02660 -0.03678 AFIX 137 H17A 2 0.046841 0.495181 0.313980 11.00000 -1.50000 H17B 2 -0.014543 0.588368 0.388562 11.00000 -1.50000 H17C 2 -0.033832 0.400881 0.363725 11.00000 -1.50000 AFIX 0 C18 1 0.009960 0.623825 0.584470 11.00000 0.02489 0.03733 = 0.07688 0.00551 0.01348 0.00801 AFIX 137 H18A 2 -0.042155 0.567888 0.610776 11.00000 -1.50000 H18B 2 -0.009249 0.697410 0.534191 11.00000 -1.50000 H18C 2 0.039584 0.687252 0.633707 11.00000 -1.50000 AFIX 0 C19 1 0.156388 0.426741 0.704948 11.00000 0.04930 0.04568 = 0.02877 0.00456 0.00120 -0.00471 AFIX 137 H19A 2 0.116257 0.354161 0.739705 11.00000 -1.50000 H19B 2 0.145470 0.540258 0.723678 11.00000 -1.50000 H19C 2 0.218440 0.397671 0.718784 11.00000 -1.50000 AFIX 0 C20 1 0.257082 0.175652 0.567304 11.00000 0.04505 0.03040 = 0.09086 0.00024 0.01768 0.01101 AFIX 137 H20A 2 0.230816 0.066660 0.574542 11.00000 -1.50000 H20B 2 0.284035 0.209768 0.626712 11.00000 -1.50000 H20C 2 0.303024 0.172509 0.518490 11.00000 -1.50000 AFIX 0 C21 1 0.170310 0.205744 0.364554 11.00000 0.09482 0.06722 = 0.05495 -0.02971 0.03487 -0.04194 AFIX 137 H21A 2 0.153618 0.091780 0.376460 11.00000 -1.50000 H21B 2 0.235056 0.213149 0.355930 11.00000 -1.50000 H21C 2 0.140123 0.244532 0.307863 11.00000 -1.50000 REM ##### REM ##### REM ##### AFIX 0 HKLF 4 REM PO19049_029 in Pca2(1) REM wR2 = 0.0497, GooF = S = 1.048, Restrained GooF = 1.048 for all data REM R1 = 0.0193 for 3272 Fo > 4sig(Fo) and 0.0209 for all 3480 data REM 202 parameters refined using 2 restraints END WGHT 0.0291 0.0000 REM Highest difference peak 1.241, deepest hole -1.126, 1-sigma level 0.091 Q1 1 0.1692 0.6212 0.4931 11.00000 0.05 1.24 Q2 1 0.2064 0.4205 0.4131 11.00000 0.05 0.48 Q3 1 0.2087 0.5494 0.3756 11.00000 0.05 0.46 Q4 1 0.2122 0.5443 0.6130 11.00000 0.05 0.46 Q5 1 0.2162 0.6687 0.4150 11.00000 0.05 0.45 Q6 1 0.1650 0.4742 0.4943 11.00000 0.05 0.43 Q7 1 0.1385 0.5460 0.4005 11.00000 0.05 0.41 Q8 1 0.2039 0.6811 0.5733 11.00000 0.05 0.41 Q9 1 0.2645 0.4554 0.4930 11.00000 0.05 0.38 Q10 1 0.2027 0.4144 0.5714 11.00000 0.05 0.37 Q11 1 0.2012 0.7416 0.4928 11.00000 0.05 0.36 Q12 1 0.2520 0.6232 0.4929 11.00000 0.05 0.34 Q13 1 0.1376 0.5382 0.5823 11.00000 0.05 0.34 Q14 1 0.1654 0.3025 0.4946 11.00000 0.05 0.33 Q15 1 0.2802 0.5384 0.4124 11.00000 0.05 0.32 Q16 1 0.3465 0.5864 0.4408 11.00000 0.05 0.31 Q17 1 0.3924 0.7760 0.4895 11.00000 0.05 0.31 Q18 1 0.0714 0.4351 0.4937 11.00000 0.05 0.31 Q19 1 0.2822 0.5395 0.5721 11.00000 0.05 0.31 Q20 1 0.1642 0.4544 0.6367 11.00000 0.05 0.30 ; _shelx_res_checksum 68548 _shelx_hkl_file ; 2 0 068917.60 1726.28 1 -2 0 068860.70 1773.24 1 4 0 0 9907.01 315.196 1 -4 0 010307.80 348.429 1 6 0 0 1531.18 100.852 1 -6 0 0 1471.07 73.3532 1 8 0 015419.70 465.138 1 -8 0 014677.20 695.128 1 10 0 018461.00 499.226 1 -10 0 018005.50 529.387 1 12 0 015473.70 798.072 1 -12 0 016104.70 583.25 1 14 0 011426.80 338.228 1 -14 0 010562.40 307.759 1 16 0 0 138.04 59.8508 1 -16 0 0 146.731 52.1228 1 18 0 0 638.187 80.3252 1 -18 0 0 609.056 73.267 1 -18 0 1 4937.61 254.409 1 18 0 -1 4389.08 285.993 1 -16 0 1 8190.68 366.612 1 16 0 -1 9220.55 304.524 1 -14 0 1 3097.39 198.567 1 14 0 -1 2840.91 130.306 1 -12 0 1 373.906 44.2335 1 12 0 -1 311.767 46.3465 1 -10 0 1 3549.90 132.607 1 10 0 -1 3439.39 186.282 1 -8 0 123612.30 715.401 1 8 0 -124521.30 967.399 1 -6 0 149934.40 1378.43 1 6 0 -145734.40 1227.43 1 -4 0 157366.40 1512.66 1 4 0 -159267.30 1519.75 1 -2 0 125444.30 948.289 1 2 0 -122700.10 829.628 1 2 0 125959.80 699.658 1 -2 0 -122493.40 601.086 1 4 0 158303.10 2152.16 1 -4 0 -153752.30 1992.19 1 6 0 146892.10 1291.08 1 -6 0 -147475.00 1884.09 1 8 0 124280.10 949.836 1 -8 0 -126285.20 762.531 1 10 0 1 3690.91 196.867 1 -10 0 -1 3786.77 131.924 1 12 0 1 479.926 64.6051 1 -12 0 -1 305.592 47.1717 1 14 0 1 3033.90 185.997 1 -14 0 -1 2955.90 126.993 1 16 0 1 8621.34 380.691 1 -16 0 -1 9945.22 439.397 1 18 0 1 4818.09 285.957 1 -18 0 -1 4919.16 183.149 1 -18 0 2 523.011 80.2474 1 18 0 -2 420.619 88.5528 1 -16 0 2 344.70 74.5844 1 16 0 -2 241.894 86.6782 1 -14 0 211069.50 471.959 1 14 0 -2 9844.72 451.901 1 -12 0 218627.70 712.043 1 12 0 -218639.50 523.309 1 -10 0 221635.90 624.918 1 10 0 -221895.50 603.548 1 -8 0 212276.50 378.273 1 8 0 -212842.30 399.352 1 -6 0 2 77.659 17.6032 1 6 0 -2 146.004 30.0279 1 -4 0 216055.40 685.083 1 4 0 -217205.30 508.488 1 -2 0 250337.30 1780.08 1 0 0 2109241.0 2940.77 1 0 0 -2107930.0 2836.01 1 2 0 252015.30 1316.86 1 -2 0 -252108.70 1826.61 1 4 0 216125.10 472.712 1 -4 0 -217327.40 546.265 1 6 0 2 45.1526 22.0754 1 -6 0 -2 153.517 31.1003 1 8 0 213232.40 585.505 1 -8 0 -212283.40 542.742 1 10 0 220828.70 582.788 1 -10 0 -220573.70 577.665 1 12 0 219816.10 543.535 1 -12 0 -219773.50 571.982 1 14 0 212228.90 378.819 1 -14 0 -211166.40 333.44 1 16 0 2 277.189 58.6004 1 -16 0 -2 307.887 81.8514 1 18 0 2 549.719 85.4202 1 -18 0 -2 483.75 74.4201 1 -18 0 3 4301.41 252.802 1 18 0 -3 4206.14 198.092 1 -16 0 3 6784.61 294.309 1 16 0 -3 6877.55 236.478 1 -14 0 3 5278.30 181.632 1 14 0 -3 4365.79 189.209 1 -12 0 3 525.914 47.118 1 12 0 -3 513.861 52.5872 1 -10 0 3 1212.14 64.194 1 10 0 -3 1323.12 69.6357 1 -8 0 330265.10 876.817 1 8 0 -332358.80 907.825 1 -2 0 324149.40 617.364 1 2 0 -325339.30 658.323 1 2 0 324371.40 672.506 1 -2 0 -326257.10 708.301 1 4 0 334553.30 917.532 1 -4 0 -337685.20 1007.24 1 6 0 363653.00 1633.75 1 -6 0 -361600.10 1553.71 1 8 0 329014.00 1118.93 1 -8 0 -331444.90 911.605 1 10 0 3 1051.33 77.5705 1 -10 0 -3 1286.09 63.285 1 12 0 3 513.532 79.7051 1 -12 0 -3 440.896 67.5992 1 14 0 3 5746.36 209.617 1 -14 0 -3 4772.38 176.468 1 16 0 3 6898.16 243.263 1 -16 0 -3 6924.68 226.803 1 18 0 3 4568.30 189.585 1 -18 0 -3 5256.27 195.379 1 -18 0 4 61.726 78.1227 1 18 0 -4 79.0856 95.4823 1 -16 0 4 1409.69 91.1525 1 16 0 -4 1548.54 97.5115 1 -14 0 4 7295.85 242.119 1 14 0 -4 7160.36 259.891 1 -12 0 417807.70 481.045 1 12 0 -417783.00 532.746 1 -10 0 423081.30 666.682 1 10 0 -422075.10 602.13 1 -8 0 411507.30 344.276 1 8 0 -411298.10 361.71 1 -6 0 4 415.538 27.5654 1 6 0 -4 273.488 22.264 1 -4 0 4 3013.17 105.599 1 4 0 -4 1964.35 78.9479 1 -2 0 449870.60 1720.56 1 2 0 -446363.60 1147.37 1 0 0 438353.60 1291.61 1 0 0 -432094.80 827.542 1 2 0 450641.00 1884.13 1 -2 0 -447312.80 1242.12 1 4 0 4 3060.35 119.396 1 -4 0 -4 1880.05 77.3175 1 6 0 4 308.962 28.0883 1 -6 0 -4 264.822 27.0869 1 8 0 411820.80 366.565 1 -8 0 -411168.10 357.407 1 10 0 422444.10 609.053 1 -10 0 -422193.10 618.229 1 12 0 419859.70 552.249 1 -12 0 -418780.30 543.208 1 14 0 4 7083.82 361.815 1 -14 0 -4 7736.05 272.079 1 16 0 4 1238.74 148.433 1 -16 0 -4 1536.51 139.435 1 18 0 4 51.8488 100.462 1 -16 0 5 5977.28 220.085 1 16 0 -5 6224.61 228.807 1 -14 0 5 4741.24 186.586 1 14 0 -5 4887.76 176.28 1 -12 0 5 72.9539 37.0605 1 12 0 -5 121.586 39.3727 1 -10 0 5 2553.56 143.009 1 10 0 -5 2442.58 97.2464 1 -8 0 522950.10 946.261 1 8 0 -524526.90 703.004 1 6 0 -545371.30 1659.39 1 -4 0 537887.50 1411.97 1 4 0 -537428.00 1450.52 1 -2 0 516050.00 476.656 1 2 0 -514208.40 564.773 1 2 0 516490.30 492.726 1 -2 0 -514496.10 430.53 1 4 0 537738.80 1004.97 1 -4 0 -537618.90 1387.53 1 6 0 550250.00 1370.31 1 -6 0 -548040.80 1242.80 1 8 0 525299.50 1077.80 1 -8 0 -522641.90 632.126 1 10 0 5 2088.21 92.0388 1 -10 0 -5 2469.66 99.1951 1 12 0 5 173.193 42.0441 1 -12 0 -5 121.135 40.0451 1 14 0 5 5470.49 201.654 1 -14 0 -5 5521.14 213.122 1 16 0 5 6660.38 361.076 1 -16 0 -5 6829.41 220.363 1 -16 0 6 1582.96 98.65 1 16 0 -6 1511.21 103.137 1 -14 0 6 5042.81 168.055 1 14 0 -6 4985.99 281.671 1 -12 0 614196.00 436.322 1 12 0 -615347.90 707.227 1 -10 0 616326.30 640.941 1 10 0 -616863.20 480.113 1 -8 0 611882.90 473.793 1 8 0 -611797.80 355.345 1 -6 0 6 594.042 37.7525 1 6 0 -6 456.355 31.0909 1 -4 0 6 9770.71 305.533 1 4 0 -6 8113.78 255.325 1 2 0 -624586.70 637.817 1 0 0 623276.20 909.078 1 0 0 -623834.50 663.516 1 2 0 631539.80 1313.87 1 -2 0 -625774.20 706.851 1 4 0 610710.00 331.72 1 -4 0 -6 8354.59 272.046 1 6 0 6 605.027 42.114 1 -6 0 -6 475.599 40.0629 1 8 0 612894.10 388.19 1 -8 0 -611795.70 351.96 1 10 0 616566.70 527.28 1 -10 0 -617835.00 903.466 1 12 0 616984.80 467.827 1 -12 0 -615949.10 455.832 1 14 0 6 6132.15 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1 3 2 710221.00 301.597 1 -3 -2 -7 9259.54 302.608 1 4 2 716134.80 491.234 1 -4 -2 -716098.30 453.763 1 5 2 710760.80 329.62 1 -5 -2 -710323.70 311.365 1 6 2 720373.50 850.544 1 -6 -2 -718518.10 723.672 1 7 2 7 9422.07 285.943 1 -7 -2 -7 8688.95 262.621 1 8 2 712509.50 380.881 1 -8 -2 -712343.80 361.689 1 9 2 7 2297.90 160.481 1 -9 -2 -7 2564.71 150.449 1 10 2 7 2168.27 95.1792 1 -10 -2 -7 2186.12 109.055 1 11 2 7 95.5513 80.9316 1 -11 -2 -7 41.9305 39.9745 1 12 2 7 327.036 68.6526 1 -12 -2 -7 365.175 48.6271 1 13 2 7 610.64 63.9352 1 -13 -2 -7 838.584 69.4944 1 14 2 7 2591.62 119.879 1 -14 -2 -7 2148.81 110.931 1 15 2 7 1774.68 150.965 1 -15 -2 -7 1923.93 108.076 1 16 2 7 3309.95 150.264 1 -16 -2 -7 2972.67 144.549 1 -16 2 8 651.401 87.4908 1 16 -2 -8 552.325 88.5431 1 -15 2 8 535.176 77.5583 1 15 -2 -8 439.887 70.9108 1 -14 2 8 3076.02 228.662 1 14 -2 -8 3308.12 152.82 1 -13 2 8 2159.18 136.564 1 13 -2 -8 1846.02 156.578 1 -12 2 8 7127.50 251.909 1 12 -2 -8 7654.00 253.101 1 -11 2 8 3225.73 177.673 1 11 -2 -8 3606.28 216.093 1 -10 2 8 8080.58 250.611 1 10 -2 -8 7746.04 242.208 1 -9 2 8 3240.99 131.066 1 9 -2 -8 3628.25 201.375 1 -8 2 8 2061.93 97.9109 1 8 -2 -8 2512.53 135.651 1 -7 2 8 1298.57 59.397 1 7 -2 -8 1466.28 68.7097 1 -6 2 8 608.352 44.7672 1 6 -2 -8 596.871 47.0591 1 -5 2 8 107.366 31.6446 1 5 -2 -8 177.435 25.9926 1 -4 2 8 4242.49 155.733 1 4 -2 -8 4458.29 160.175 1 -3 2 8 4232.06 156.62 1 3 -2 -8 4480.68 171.959 1 -2 2 816735.90 506.326 1 2 -2 -817911.50 544.11 1 -1 2 810829.90 333.672 1 1 -2 -811274.50 372.046 1 0 2 823150.20 654.172 1 0 -2 -821903.10 645.725 1 1 2 811524.50 348.653 1 -1 -2 -811896.20 496.285 1 2 2 815300.00 440.592 1 -2 -2 -817042.60 498.923 1 3 2 8 4160.41 140.172 1 -3 -2 -8 4613.11 178.583 1 4 2 8 3909.70 137.815 1 -4 -2 -8 4724.18 161.648 1 5 2 8 114.812 36.2019 1 -5 -2 -8 109.648 49.6461 1 6 2 8 622.072 47.4541 1 -6 -2 -8 590.086 47.4541 1 7 2 8 1236.38 90.3624 1 -7 -2 -8 1494.13 72.9051 1 8 2 8 1919.19 95.8018 1 -8 -2 -8 2009.90 145.747 1 9 2 8 3485.90 135.047 1 -9 -2 -8 3573.58 155.198 1 10 2 8 9284.46 309.484 1 -10 -2 -8 8378.83 282.70 1 11 2 8 3976.25 160.255 1 -11 -2 -8 4277.33 174.827 1 12 2 8 9982.56 469.91 1 -12 -2 -8 9964.60 305.398 1 13 2 8 2653.66 126.232 1 -13 -2 -8 2059.99 102.454 1 14 2 8 3747.34 149.473 1 -14 -2 -8 3164.41 176.726 1 15 2 8 385.337 109.975 1 -15 -2 -8 453.335 69.6824 1 16 2 8 685.537 91.5629 1 -16 -2 -8 543.018 91.5629 1 -15 2 9 1222.58 117.983 1 15 -2 -9 1184.37 102.256 1 -14 2 9 1744.68 106.698 1 14 -2 -9 1970.97 146.563 1 -13 2 9 607.368 73.6607 1 13 -2 -9 786.078 77.2772 1 -12 2 9 143.851 67.6237 1 12 -2 -9 99.5828 67.6237 1 -11 2 9 24.8047 62.0001 1 11 -2 -9 106.635 64.4759 1 -10 2 9 1247.24 71.978 1 10 -2 -9 1279.51 85.6302 1 -9 2 9 1520.07 75.3276 1 9 -2 -9 1662.07 124.72 1 -8 2 9 6428.32 214.077 1 8 -2 -9 6469.91 199.399 1 -7 2 9 7438.29 238.001 1 7 -2 -9 7231.70 242.825 1 -6 2 917794.00 496.524 1 6 -2 -918201.20 752.529 1 -5 2 910217.40 354.021 1 5 -2 -9 9921.96 444.29 1 -4 2 916372.10 469.55 1 4 -2 -917202.80 470.712 1 -3 2 9 5879.17 294.18 1 3 -2 -9 5213.56 186.282 1 -2 2 9 5196.29 173.506 1 2 -2 -9 5491.81 200.369 1 -1 2 9 1241.91 58.5569 1 1 -2 -9 1167.89 60.7735 1 1 2 9 1288.57 58.468 1 -1 -2 -9 1080.66 57.387 1 2 2 9 5068.98 164.488 1 -2 -2 -9 5611.89 206.417 1 3 2 9 5412.75 190.256 1 -3 -2 -9 5072.84 168.884 1 4 2 916993.10 473.212 1 -4 -2 -916426.30 453.011 1 5 2 9 9855.70 306.735 1 -5 -2 -9 9634.64 298.268 1 6 2 915472.30 651.466 1 -6 -2 -916451.60 514.867 1 7 2 9 8178.10 263.503 1 -7 -2 -9 7343.84 236.429 1 8 2 9 6214.02 299.483 1 -8 -2 -9 6012.30 235.674 1 9 2 9 1574.01 85.0837 1 -9 -2 -9 1838.37 89.1285 1 10 2 9 1609.28 118.068 1 -10 -2 -9 1596.38 94.2579 1 11 2 9 80.2399 47.3718 1 -11 -2 -9 82.1701 51.2322 1 12 2 9 175.116 66.4834 1 -12 -2 -9 162.945 64.6136 1 13 2 9 688.81 72.1264 1 -13 -2 -9 730.282 79.3356 1 14 2 9 1829.46 112.133 1 -14 -2 -9 1957.98 108.68 1 15 2 9 1288.97 92.6559 1 -15 -2 -9 1097.92 86.918 1 -14 2 10 3236.08 144.167 1 14 -2 -10 3027.57 139.409 1 -13 2 10 1972.89 122.298 1 13 -2 -10 1945.71 116.119 1 -12 2 10 6086.66 227.685 1 12 -2 -10 6070.21 206.182 1 -11 2 10 2826.62 128.139 1 11 -2 -10 3058.55 138.385 1 -10 2 10 5410.55 310.09 1 10 -2 -10 5715.50 195.581 1 -9 2 10 2154.55 94.9595 1 9 -2 -10 2447.13 110.357 1 -8 2 10 1815.56 90.3909 1 8 -2 -10 1835.94 98.0414 1 -7 2 10 314.641 37.7536 1 7 -2 -10 390.148 37.7536 1 -6 2 10 673.883 50.8805 1 6 -2 -10 702.427 58.3261 1 -5 2 10 595.123 50.101 1 5 -2 -10 713.672 69.6557 1 -4 2 10 1820.80 68.5503 1 4 -2 -10 2021.63 84.1814 1 -3 2 10 3082.49 162.173 1 3 -2 -10 3383.17 120.744 1 -2 2 1013860.80 418.611 1 2 -2 -1012324.00 356.814 1 -1 2 10 9089.53 420.894 1 1 -2 -10 9472.49 294.399 1 0 2 1016979.30 483.861 1 0 -2 -1016637.50 478.18 1 1 2 10 8898.07 279.753 1 -1 -2 -10 8900.32 274.134 1 2 2 1014029.10 401.686 1 -2 -2 -1013090.00 388.335 1 3 2 10 3265.74 126.834 1 -3 -2 -10 3267.94 118.014 1 4 2 10 1713.25 71.0623 1 -4 -2 -10 1923.17 78.7235 1 5 2 10 538.275 48.7384 1 -5 -2 -10 578.353 49.8197 1 6 2 10 740.151 48.2021 1 -6 -2 -10 593.406 44.9839 1 7 2 10 283.187 41.2116 1 -7 -2 -10 295.866 41.2116 1 8 2 10 2008.12 92.4625 1 -8 -2 -10 1956.18 90.3784 1 9 2 10 2868.23 130.184 1 -9 -2 -10 2680.07 111.878 1 10 2 10 6923.06 240.814 1 -10 -2 -10 7485.94 256.662 1 11 2 10 3863.63 169.988 1 -11 -2 -10 3468.91 180.552 1 12 2 10 6606.40 260.957 1 -12 -2 -10 6528.66 232.274 1 13 2 10 1892.40 164.868 1 -13 -2 -10 1991.67 113.451 1 14 2 10 3060.69 138.395 1 -14 -2 -10 3102.03 147.678 1 -14 2 11 1406.53 165.896 1 14 -2 -11 1490.69 105.785 1 -13 2 11 208.676 74.1643 1 13 -2 -11 253.928 61.6023 1 -12 2 11 160.785 55.7607 1 12 -2 -11 88.1718 51.8651 1 -11 2 11-18.4952 62.1071 1 11 -2 -11 7.92829 60.7877 1 -10 2 11 1205.39 113.34 1 10 -2 -11 1338.73 138.67 1 -9 2 11 1323.94 72.0632 1 9 -2 -11 1155.78 70.7308 1 -8 2 11 5692.69 301.364 1 8 -2 -11 5733.84 197.808 1 -7 2 11 3686.13 184.049 1 7 -2 -11 3579.65 128.828 1 -6 2 1110101.00 448.993 1 6 -2 -1110874.40 499.604 1 -5 2 11 5838.58 204.547 1 5 -2 -11 5784.87 296.598 1 -4 2 1110871.00 471.834 1 4 -2 -1111352.90 335.946 1 -3 2 11 2810.34 121.325 1 3 -2 -11 3610.12 128.753 1 -2 2 11 3214.68 181.57 1 2 -2 -11 3620.47 177.92 1 -1 2 11 577.37 58.8224 1 1 -2 -11 664.999 45.6176 1 1 2 11 633.018 71.2471 1 -1 -2 -11 697.258 49.0491 1 2 2 11 3458.81 158.005 1 -2 -2 -11 3825.57 130.327 1 3 2 11 2756.66 113.916 1 -3 -2 -11 3090.42 117.328 1 4 2 1110984.90 318.26 1 -4 -2 -1110773.50 432.969 1 5 2 11 5650.92 180.754 1 -5 -2 -11 5939.23 202.926 1 6 2 11 9336.35 436.48 1 -6 -2 -11 9712.80 293.532 1 7 2 11 3932.79 240.909 1 -7 -2 -11 3316.05 128.487 1 8 2 11 5501.05 260.662 1 -8 -2 -11 5945.96 204.128 1 9 2 11 1290.09 100.88 1 -9 -2 -11 1105.64 77.4431 1 10 2 11 1309.93 80.9414 1 -10 -2 -11 1525.12 88.844 1 11 2 11 8.56425 41.8537 1 -11 -2 -11-26.6334 47.5602 1 12 2 11 145.823 51.0396 1 -12 -2 -11 172.252 52.8594 1 13 2 11 192.766 63.3886 1 -13 -2 -11 262.231 56.4372 1 14 2 11 1084.98 149.71 1 -14 -2 -11 1449.38 106.115 1 -13 2 12 1699.83 105.215 1 13 -2 -12 1649.13 110.277 1 -12 2 12 4506.21 245.438 1 12 -2 -12 4313.56 174.176 1 -11 2 12 1737.79 149.104 1 11 -2 -12 1916.71 103.016 1 -10 2 12 4313.18 177.598 1 10 -2 -12 4643.59 170.713 1 -9 2 12 2282.58 150.97 1 9 -2 -12 1984.80 103.878 1 -8 2 12 2229.57 105.112 1 8 -2 -12 2521.40 100.969 1 -7 2 12 863.824 60.4304 1 7 -2 -12 785.544 52.1911 1 -6 2 12 160.255 46.1745 1 6 -2 -12 198.282 36.671 1 -5 2 12 77.6737 56.2434 1 5 -2 -12 56.2434 34.8258 1 -4 2 12 1764.08 85.6936 1 4 -2 -12 1965.80 121.295 1 -3 2 12 1574.37 75.2151 1 3 -2 -12 1888.22 81.7008 1 -2 2 12 9467.77 429.772 1 2 -2 -12 9475.42 308.615 1 -1 2 12 7957.07 257.125 1 1 -2 -12 7831.65 240.823 1 0 2 1212401.40 361.549 1 0 -2 -1211540.10 346.742 1 -1 -2 -12 8599.84 262.295 1 2 2 12 9163.27 298.751 1 -2 -2 -12 8635.07 254.531 1 3 2 12 1743.24 121.074 1 -3 -2 -12 1809.07 83.4541 1 4 2 12 1663.36 80.8545 1 -4 -2 -12 1461.21 82.0077 1 5 2 12 49.8618 31.7292 1 -5 -2 -12 23.7996 32.8605 1 6 2 12 136.40 39.9173 1 -6 -2 -12 141.935 39.9173 1 7 2 12 750.732 62.7393 1 -7 -2 -12 691.233 60.5794 1 8 2 12 2169.67 114.579 1 -8 -2 -12 2153.91 98.8078 1 9 2 12 2098.09 107.807 1 -9 -2 -12 2046.22 97.6345 1 10 2 12 4479.63 193.875 1 -10 -2 -12 4376.83 241.848 1 11 2 12 2281.76 164.124 1 -11 -2 -12 2156.10 125.675 1 12 2 12 4638.98 176.912 1 -12 -2 -12 4218.15 165.291 1 13 2 12 1614.64 98.2132 1 -13 -2 -12 1491.87 112.607 1 -12 2 13 21.2355 94.2159 1 12 -2 -13 55.7321 58.3944 1 -11 2 13 53.6926 67.4626 1 11 -2 -13 85.3558 93.6152 1 -10 2 13 910.848 117.035 1 10 -2 -13 850.225 81.777 1 -9 2 13 837.043 77.1271 1 9 -2 -13 1065.59 71.4229 1 8 -2 -13 4478.78 153.455 1 -7 2 13 2629.29 155.84 1 7 -2 -13 2603.56 98.6504 1 -6 2 13 8109.54 375.711 1 6 -2 -13 7939.41 233.93 1 -5 2 13 3363.83 135.841 1 5 -2 -13 2968.90 109.237 1 -4 2 13 8076.34 364.217 1 4 -2 -13 8310.86 246.948 1 -3 2 13 2013.45 100.402 1 3 -2 -13 1869.64 89.5527 1 -2 2 13 1856.74 87.9767 1 2 -2 -13 2177.96 90.6381 1 -1 2 13 409.599 57.5828 1 1 -2 -13 397.817 47.1065 1 1 2 13 298.555 42.8304 1 -1 -2 -13 331.301 52.9032 1 2 2 13 1536.10 86.4335 1 -2 -2 -13 1838.63 79.0252 1 3 2 13 1713.31 124.538 1 -3 -2 -13 1638.35 85.8416 1 4 2 13 6165.65 228.14 1 -4 -2 -13 6171.55 217.496 1 5 2 13 2246.22 115.314 1 -5 -2 -13 2043.28 113.001 1 6 2 13 6496.64 211.991 1 -6 -2 -13 5597.07 196.293 1 7 2 13 1980.05 116.348 1 -7 -2 -13 2007.23 97.8626 1 8 2 13 3805.82 218.38 1 -8 -2 -13 3655.69 156.431 1 9 2 13 749.858 63.5812 1 -9 -2 -13 990.058 72.6684 1 10 2 13 762.798 73.3797 1 -10 -2 -13 711.617 70.4878 1 11 2 13 44.1196 66.188 1 -11 -2 -13 41.3664 50.5609 1 12 2 13 74.8866 71.401 1 -12 -2 -13 52.2508 73.1479 1 -10 2 14 2761.01 126.801 1 10 -2 -14 2624.24 115.395 1 -9 2 14 1397.75 106.289 1 9 -2 -14 1311.83 81.5371 1 -8 2 14 1472.33 91.2858 1 8 -2 -14 1674.04 89.8159 1 -7 2 14 360.144 85.6049 1 7 -2 -14 355.71 50.1841 1 -6 2 14 7.34928 38.2135 1 6 -2 -14 0.00 27.9162 1 -5 2 14 52.3888 65.4928 1 5 -2 -14 36.3788 34.9259 1 -4 2 14 1595.04 80.4005 1 4 -2 -14 1569.20 81.8338 1 -3 2 14 1382.54 108.745 1 3 -2 -14 1374.07 73.4323 1 -2 2 14 6455.41 313.28 1 2 -2 -14 6469.27 293.866 1 -1 2 14 4186.83 144.004 1 1 -2 -14 4271.06 149.429 1 0 2 14 8039.94 336.378 1 0 -2 -14 8933.42 279.213 1 1 2 14 3780.60 135.157 1 -1 -2 -14 3904.05 144.252 1 2 2 14 5854.19 192.818 1 -2 -2 -14 6049.54 213.105 1 3 2 14 1004.87 90.2298 1 -3 -2 -14 1062.96 64.2703 1 4 2 14 1231.75 123.775 1 -4 -2 -14 1148.83 80.5168 1 5 2 14 76.9122 54.7648 1 -5 -2 -14 47.7738 41.9461 1 6 2 14 12.3909 46.1793 1 -6 -2 -14 6.75768 41.6706 1 7 2 14 317.852 57.4931 1 -7 -2 -14 391.621 74.8524 1 8 2 14 1585.89 95.7353 1 -8 -2 -14 1502.65 88.4532 1 9 2 14 1430.19 92.4276 1 -9 -2 -14 1271.16 84.4803 1 10 2 14 2426.63 122.845 1 -10 -2 -14 2661.92 135.127 1 9 -2 -15 403.735 67.0443 1 -8 2 15 2701.97 126.40 1 8 -2 -15 2627.61 123.431 1 -7 2 15 2022.58 102.106 1 7 -2 -15 1860.41 93.0975 1 -6 2 15 5225.16 300.641 1 6 -2 -15 4608.84 177.383 1 -5 2 15 2265.62 134.505 1 5 -2 -15 2267.11 100.133 1 -4 2 15 4653.14 178.793 1 4 -2 -15 4406.37 159.588 1 -3 2 15 1735.53 123.656 1 3 -2 -15 1697.71 94.5542 1 -2 2 15 1734.28 91.3498 1 2 -2 -15 1600.11 77.0726 1 -1 2 15 303.079 47.4876 1 1 -2 -15 321.232 47.4876 1 1 2 15 335.966 43.8249 1 -1 -2 -15 286.838 51.7919 1 2 2 15 1611.84 109.694 1 -2 -2 -15 1727.99 78.7244 1 3 2 15 1691.42 122.601 1 -3 -2 -15 1492.51 78.8159 1 4 2 15 3990.15 228.594 1 -4 -2 -15 4008.29 152.396 1 5 2 15 1928.12 100.252 1 -5 -2 -15 2045.87 96.7608 1 6 2 15 4759.88 171.317 1 -6 -2 -15 4318.72 171.317 1 7 2 15 1971.52 166.077 1 -7 -2 -15 1921.17 141.434 1 8 2 15 2978.95 132.763 1 -8 -2 -15 2720.58 129.694 1 9 2 15 335.385 81.4247 1 -9 -2 -15 442.007 63.0017 1 -7 2 16 260.064 62.7673 1 7 -2 -16 171.874 55.2926 1 -6 2 16 3.0086 52.7356 1 6 -2 -16 -1.5043 43.6956 1 5 -2 -16 9.03476 45.1738 1 -4 2 16 1152.04 82.187 1 4 -2 -16 1295.49 74.7142 1 3 -2 -16 963.897 70.7386 1 -2 2 16 3383.73 140.325 1 2 -2 -16 3372.15 133.09 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153.911 1 6 -3 15 2501.11 112.471 1 -5 3 -15 3668.43 155.463 1 5 -3 15 3794.06 135.052 1 -4 3 -15 2378.47 142.74 1 4 -3 15 2336.97 149.383 1 -3 3 -15 2674.65 118.874 1 3 -3 15 2753.31 159.081 1 -9 3 -14 2469.04 112.561 1 9 -3 14 2444.58 117.459 1 -8 3 -14 439.266 70.3812 1 8 -3 14 404.069 69.0799 1 -7 3 -14 494.531 55.2544 1 7 -3 14 439.277 53.8753 1 -6 3 -14 10.1942 42.2449 1 6 -3 14 29.142 55.3616 1 -5 3 -14 331.906 50.4773 1 5 -3 14 286.024 71.8841 1 -4 3 -14 798.324 102.386 1 4 -3 14 1063.89 60.7987 1 -3 3 -14 2852.56 113.436 1 3 -3 14 2767.48 106.759 1 -2 3 -14 3069.54 161.366 1 2 -3 14 3329.81 199.542 1 -11 3 -13 65.9557 70.2733 1 11 -3 13 216.237 112.441 1 -10 3 -13 490.545 75.0194 1 10 -3 13 557.488 79.6395 1 -9 3 -13 1642.40 90.6325 1 9 -3 13 1810.19 107.774 1 -8 3 -13 2312.76 155.045 1 8 -3 13 2042.73 120.156 1 -7 3 -13 4787.90 169.448 1 7 -3 13 4321.59 169.448 1 -6 3 -13 3630.07 130.20 1 6 -3 13 3206.92 196.712 1 -5 3 -13 5548.06 194.202 1 5 -3 13 6102.72 314.852 1 -4 3 -13 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424.184 1 -1 -3 815209.20 599.334 1 -4 -3 8 2531.97 87.2658 1 5 3 -8 412.938 35.2864 1 -5 -3 8 432.545 26.1417 1 -6 -3 8 559.422 34.6362 1 7 3 -8 1087.68 54.3158 1 -7 -3 8 1261.49 95.0494 1 8 3 -8 3400.33 178.46 1 -8 -3 8 3836.10 136.949 1 9 3 -8 6359.46 208.184 1 -9 -3 8 6441.04 198.341 1 10 3 -8 5754.62 280.823 1 -10 -3 8 5785.97 206.687 1 11 3 -8 7739.88 239.981 1 -11 -3 8 6985.43 222.738 1 12 3 -8 3826.82 208.52 1 -12 -3 8 3962.01 143.817 1 13 3 -8 4374.31 161.063 1 -13 -3 8 4019.40 149.653 1 14 3 -8 1925.99 171.67 1 -14 -3 8 2235.82 127.004 1 15 3 -8 1220.48 160.308 1 -15 -3 8 1259.55 111.816 1 -16 3 -7 1055.96 82.6532 1 16 -3 7 1233.08 96.1494 1 -15 3 -7 2291.33 152.398 1 15 -3 7 2581.77 119.225 1 -14 3 -7 718.221 69.9325 1 14 -3 7 727.674 72.7718 1 -13 3 -7 927.012 94.8764 1 13 -3 7 1196.81 86.9646 1 -12 3 -7 59.4848 40.0011 1 12 -3 7 26.6706 44.1065 1 -11 3 -7 94.064 46.5044 1 11 -3 7 108.855 48.6146 1 -10 3 -7 2060.26 90.8964 1 10 -3 7 2203.09 98.4686 1 -9 3 -7 2978.92 133.30 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334.542 1 1 -3 624783.10 1005.09 1 0 3 -617170.00 690.511 1 0 -3 617295.30 494.668 1 1 3 -625363.10 960.82 1 -1 -3 624268.20 874.083 1 2 3 -611423.60 490.851 1 -2 -3 611391.80 355.639 1 -3 -3 611536.30 352.616 1 4 3 -6 3102.35 108.177 1 -4 -3 6 2744.07 104.693 1 5 3 -6 182.87 21.2351 1 -5 -3 6 259.566 29.4913 1 6 3 -6 64.6791 20.3638 1 -6 -3 6 81.4552 17.9721 1 7 3 -6 2031.89 86.3805 1 -7 -3 6 1902.93 86.3805 1 8 3 -6 2021.26 107.484 1 -8 -3 6 2078.09 91.4264 1 9 3 -6 7116.24 343.343 1 -9 -3 6 7297.93 229.312 1 10 3 -6 5462.42 240.911 1 -10 -3 6 5708.41 188.926 1 11 3 -6 7851.21 363.034 1 -11 -3 6 7580.22 331.07 1 12 3 -6 4177.28 170.471 1 -12 -3 6 3902.98 156.371 1 13 3 -6 4451.83 177.354 1 -13 -3 6 3767.91 155.662 1 14 3 -6 2018.52 172.404 1 -14 -3 6 2275.23 118.286 1 15 3 -6 1309.35 107.983 1 -15 -3 6 1460.30 109.22 1 16 3 -6 382.634 85.0335 1 -16 -3 6 458.213 74.4001 1 -16 3 -5 1824.16 108.878 1 16 -3 5 2038.45 115.796 1 -15 3 -5 3321.61 154.834 1 15 -3 5 3485.56 164.853 1 -14 3 -5 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511613.20 344.031 1 7 3 -517283.80 512.016 1 -7 -3 517225.40 493.353 1 8 3 -5 7704.54 373.52 1 -8 -3 5 7614.71 355.796 1 9 3 -5 6072.48 196.275 1 -9 -3 5 5708.65 181.915 1 10 3 -5 1853.80 85.8526 1 -10 -3 5 1792.13 114.884 1 11 3 -5 460.357 45.0561 1 -11 -3 5 479.845 45.0561 1 12 3 -5 85.4482 48.8292 1 -12 -3 5 20.7527 41.5054 1 13 3 -5 976.212 83.8824 1 -13 -3 5 1123.31 115.496 1 14 3 -5 559.514 85.2422 1 -14 -3 5 650.761 74.4428 1 15 3 -5 3116.41 145.553 1 -15 -3 5 3661.04 149.068 1 16 3 -5 1706.49 111.118 1 -16 -3 5 1868.64 108.854 1 -17 3 -4-48.5898 52.7088 1 17 -3 4-4.94121 56.0055 1 -16 3 -4 500.174 63.7231 1 16 -3 4 469.616 73.3255 1 -15 3 -4 1148.83 88.0201 1 15 -3 4 1126.83 132.026 1 -14 3 -4 2964.72 129.857 1 14 -3 4 3265.48 156.592 1 -13 3 -4 6850.15 237.74 1 13 -3 4 6509.81 248.592 1 -12 3 -4 7298.11 263.108 1 12 -3 4 6440.99 234.773 1 -11 3 -411247.30 366.208 1 11 -3 411363.90 369.308 1 -10 3 -4 5452.98 202.93 1 10 -3 4 3867.19 243.727 1 -9 3 -4 7849.68 251.344 1 9 -3 4 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1 3 7 -11 3336.06 232.661 1 -3 -7 11 3224.09 132.947 1 4 7 -11 1436.19 83.7444 1 -4 -7 11 1382.74 69.4961 1 -5 -7 11 3772.82 142.679 1 -6 -7 11 1368.04 81.8661 1 -8 7 -10 605.947 75.4649 1 8 -7 10 621.721 69.8321 1 -7 7 -10 267.026 68.8329 1 7 -7 10 272.962 60.5278 1 -6 7 -10 17.4139 64.6985 1 6 -7 10 12.4452 57.2337 1 -5 7 -10 206.447 110.365 1 5 -7 10 266.173 74.0089 1 -4 7 -10 275.267 78.2591 1 4 -7 10 182.164 55.3202 1 -3 7 -10 2918.72 199.796 1 3 -7 10 2899.15 124.354 1 -2 7 -10 1485.45 126.906 1 2 -7 10 1625.34 89.4166 1 -1 7 -10 6494.97 331.056 1 1 -7 10 6885.41 239.011 1 0 7 -10 2236.47 155.503 1 0 -7 10 2555.09 108.234 1 1 7 -10 6876.21 367.081 1 -1 -7 10 7016.78 246.81 1 2 7 -10 1660.85 87.8384 1 -2 -7 10 1842.91 89.4327 1 3 7 -10 3716.63 200.333 1 -3 -7 10 3224.77 136.812 1 -4 -7 10 273.271 39.7452 1 5 7 -10 437.975 62.0801 1 -5 -7 10 367.487 73.8387 1 6 7 -10 13.5319 81.2232 1 -6 -7 10 37.2326 45.696 1 -7 -7 10 268.047 55.9868 1 8 7 -10 553.626 106.334 1 -8 -7 10 697.08 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85.1906 1 8 -7 8 867.16 80.8189 1 -7 7 -8 240.876 61.3506 1 7 -7 8 110.213 59.0819 1 -6 7 -8-28.2323 64.7082 1 6 -7 8 43.5229 47.0575 1 -5 7 -8 271.713 72.7867 1 5 -7 8 396.654 58.2202 1 -4 7 -8 332.761 73.5268 1 4 -7 8 378.867 87.2368 1 -3 7 -8 3141.87 131.495 1 3 -7 8 3187.82 151.924 1 -2 7 -8 1407.66 114.80 1 2 -7 8 1419.41 92.6211 1 -1 7 -8 8126.96 463.028 1 1 -7 8 7791.67 246.145 1 0 7 -8 2778.80 181.556 1 0 -7 8 2488.86 107.035 1 1 7 -8 8382.33 276.927 1 -1 -7 8 7114.78 225.956 1 2 7 -8 1578.47 99.3479 1 -2 -7 8 1627.44 83.9673 1 -3 -7 8 3838.20 153.301 1 4 7 -8 485.911 57.5045 1 -4 -7 8 531.92 46.009 1 5 7 -8 345.84 62.4894 1 -5 -7 8 488.241 50.8565 1 6 7 -8 1.46234 45.4015 1 -6 -7 8-2.92468 35.1513 1 7 7 -8 167.708 63.2646 1 -7 -7 8 272.151 58.8446 1 8 7 -8 796.937 67.6359 1 -8 -7 8 798.405 61.7503 1 9 7 -8 2022.74 150.426 1 -9 -7 8 1904.44 106.616 1 10 7 -8 1078.07 103.638 1 -10 -7 8 1293.98 99.3139 1 -11 7 -7 324.354 59.8209 1 11 -7 7 321.545 57.0214 1 -10 7 -7 137.771 62.9769 1 10 -7 7 68.8807 60.0297 1 -9 7 -7 2406.19 117.375 1 9 -7 7 2385.60 120.468 1 -8 7 -7 1250.04 114.616 1 8 -7 7 1367.86 92.1184 1 -7 7 -7 6134.24 232.821 1 7 -7 7 5222.92 180.716 1 -6 7 -7 1979.59 106.23 1 6 -7 7 1988.73 118.796 1 -5 7 -7 6184.12 316.529 1 5 -7 7 5419.75 209.845 1 -4 7 -7 1567.40 93.5443 1 4 -7 7 1615.37 87.5467 1 -3 7 -7 3041.49 157.829 1 3 -7 7 3020.69 156.596 1 -2 7 -7 623.974 104.621 1 2 -7 7 515.622 64.7621 1 -1 7 -7 692.341 65.8152 1 1 -7 7 687.275 55.6944 1 1 7 -7 694.152 66.4199 1 -1 -7 7 794.426 66.4199 1 2 7 -7 674.064 87.0657 1 -2 -7 7 689.892 61.9946 1 3 7 -7 3885.55 224.237 1 -3 -7 7 3591.90 125.463 1 4 7 -7 1891.41 90.3916 1 -4 -7 7 2163.94 98.4855 1 5 7 -7 6853.44 221.918 1 -5 -7 7 6295.25 215.109 1 6 7 -7 2416.98 106.938 1 -6 -7 7 2366.26 111.044 1 7 7 -7 5650.42 245.009 1 -7 -7 7 5581.60 188.576 1 8 7 -7 1583.01 139.033 1 -8 -7 7 1198.96 82.5978 1 9 7 -7 2510.18 132.835 1 -9 -7 7 2288.32 120.504 1 10 7 -7 63.6071 56.8385 1 -10 -7 7 109.624 51.4338 1 11 7 -7 285.265 75.6276 1 -11 -7 7 493.566 74.303 1 -11 7 -6 4555.34 196.966 1 11 -7 6 4231.08 170.023 1 -10 7 -6 2076.38 123.627 1 10 -7 6 2088.07 114.871 1 -9 7 -6 2631.71 128.744 1 9 -7 6 2560.74 104.416 1 -8 7 -6 1535.98 88.1928 1 8 -7 6 1392.15 83.9903 1 -7 7 -6 421.954 59.5105 1 7 -7 6 455.50 53.0193 1 -6 7 -6 163.201 47.7433 1 6 -7 6 146.544 42.191 1 -5 7 -6 342.779 49.9443 1 5 -7 6 322.35 46.5342 1 -4 7 -6 659.43 59.0022 1 4 -7 6 889.654 63.6331 1 -3 7 -6 4178.15 204.678 1 3 -7 6 4515.75 182.321 1 -2 7 -6 1661.58 103.846 1 2 -7 6 1706.94 95.4927 1 -1 7 -6 6015.96 316.884 1 1 -7 6 6577.17 235.846 1 0 7 -6 4449.59 179.945 1 0 -7 6 3488.68 146.891 1 1 7 -6 5188.76 302.019 1 -1 -7 6 6535.46 238.892 1 2 7 -6 1664.62 98.8027 1 -2 -7 6 1883.47 95.0452 1 3 7 -6 4259.04 162.891 1 -3 -7 6 4637.85 172.987 1 4 7 -6 635.565 54.7731 1 -4 -7 6 915.764 73.8705 1 5 7 -6 351.582 60.3051 1 -5 -7 6 350.301 48.7637 1 6 7 -6 123.885 45.1639 1 -6 -7 6 91.6162 37.4219 1 7 7 -6 451.817 56.9663 1 -7 -7 6 354.723 55.6739 1 8 7 -6 1621.95 165.684 1 -8 -7 6 1304.81 84.1344 1 9 7 -6 2459.88 123.705 1 -9 -7 6 2595.19 128.862 1 10 7 -6 2104.51 108.415 1 -10 -7 6 2056.04 110.962 1 11 7 -6 4543.23 185.541 1 -11 -7 6 4429.15 178.019 1 -12 7 -5 69.3454 55.2994 1 12 -7 5 207.151 80.7541 1 -11 7 -5 98.643 53.4674 1 11 -7 5 315.282 56.2372 1 -10 7 -5 94.2677 65.4121 1 10 -7 5 143.327 41.3673 1 -9 7 -5 2730.85 190.576 1 9 -7 5 2928.41 130.706 1 -8 7 -5 1080.83 81.3213 1 8 -7 5 1131.28 71.0253 1 -7 7 -5 7872.34 266.355 1 7 -7 5 8425.14 257.903 1 -6 7 -5 3109.78 128.63 1 6 -7 5 2838.48 116.739 1 -5 7 -510458.60 322.766 1 5 -7 5 9064.01 290.82 1 -4 7 -5 1991.63 118.674 1 4 -7 5 2348.76 116.428 1 -3 7 -5 4200.04 178.223 1 3 -7 5 4069.50 178.223 1 -2 7 -5 691.658 60.8898 1 2 -7 5 808.849 59.7428 1 -1 7 -5 614.317 63.874 1 1 -7 5 955.725 63.874 1 1 7 -5 832.807 100.552 1 -1 -7 5 941.637 63.8744 1 -2 -7 5 861.115 59.6363 1 3 7 -5 3931.93 237.938 1 -3 -7 5 3748.07 158.621 1 4 7 -5 1724.02 139.129 1 -4 -7 5 2094.23 101.629 1 5 7 -5 8463.78 287.151 1 -5 -7 5 8551.39 294.45 1 6 7 -5 2572.09 174.73 1 -6 -7 5 2030.80 109.973 1 7 7 -5 7229.32 276.736 1 -7 -7 5 5028.94 326.937 1 8 7 -5 1037.54 72.1832 1 -8 -7 5 1125.63 72.1832 1 9 7 -5 2272.50 127.868 1 -9 -7 5 2396.71 114.471 1 10 7 -5 95.2906 54.2798 1 -10 -7 5 160.42 51.8714 1 11 7 -5 187.596 64.1087 1 -11 -7 5 395.365 72.4284 1 12 7 -5 131.086 113.682 1 -12 -7 5 136.888 67.2803 1 -12 7 -4 1105.52 120.505 1 12 -7 4 1249.60 85.5755 1 -11 7 -4 6407.94 229.377 1 11 -7 4 5841.35 213.841 1 -10 7 -4 2820.30 130.182 1 10 -7 4 2814.60 116.883 1 -9 7 -4 3322.19 172.889 1 9 -7 4 3524.55 166.995 1 -8 7 -4 1524.42 121.226 1 8 -7 4 1797.18 100.008 1 -7 7 -4 641.22 67.2206 1 7 -7 4 564.688 54.8109 1 -6 7 -4 499.933 60.1187 1 6 -7 4 554.777 53.791 1 -5 7 -4 816.972 67.5442 1 5 -7 4 710.824 58.9711 1 -4 7 -4 548.918 71.7435 1 4 -7 4 684.788 94.5626 1 -3 7 -4 4274.27 158.344 1 3 -7 4 4358.94 158.344 1 -2 7 -4 3356.19 195.464 1 2 -7 4 3378.40 167.704 1 -1 7 -4 7983.65 285.653 1 1 -7 4 7792.10 246.448 1 0 7 -4 5936.27 297.995 1 0 -7 4 5849.36 182.858 1 1 7 -4 8201.54 276.192 1 -1 -7 4 7124.06 225.045 1 2 7 -4 3037.69 147.543 1 -2 -7 4 3205.82 125.805 1 3 7 -4 4116.56 173.685 1 -3 -7 4 4180.97 147.22 1 4 7 -4 456.582 57.7981 1 -4 -7 4 506.291 54.3252 1 5 7 -4 562.87 58.0305 1 -5 -7 4 630.181 55.7023 1 6 7 -4 411.939 61.6713 1 -6 -7 4 353.753 50.0429 1 7 7 -4 496.121 96.6663 1 -7 -7 4 500.772 64.0567 1 8 7 -4 1615.89 104.628 1 -8 -7 4 1461.28 94.1608 1 9 7 -4 2766.18 121.42 1 -9 -7 4 2892.23 126.049 1 10 7 -4 2964.01 144.305 1 -10 -7 4 3114.04 176.374 1 11 7 -4 6171.34 310.20 1 -11 -7 4 6198.42 251.545 1 12 7 -4 1318.82 90.4921 1 -12 -7 4 1070.50 88.2885 1 -13 7 -3 353.562 66.9108 1 13 -7 3 300.694 66.0861 1 -12 7 -3 190.065 72.0387 1 12 -7 3 236.069 53.8104 1 -11 7 -3 260.802 92.367 1 11 -7 3 266.235 47.9916 1 -10 7 -3 149.28 63.8433 1 10 -7 3 274.146 50.6944 1 -9 7 -3 4350.53 256.487 1 9 -7 3 3914.99 174.218 1 -8 7 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288.445 81.0644 1 13 7 -3 269.114 92.0949 1 -13 -7 3 297.766 72.6466 1 -13 7 -2 4058.77 171.107 1 13 -7 2 4284.99 171.107 1 -12 7 -2 1813.90 113.799 1 12 -7 2 1744.07 90.5192 1 -11 7 -2 5703.37 192.03 1 11 -7 2 6207.66 228.819 1 -10 7 -2 2494.77 124.371 1 10 -7 2 2359.26 114.161 1 -9 7 -2 4178.29 177.559 1 9 -7 2 4307.16 179.465 1 -8 7 -2 1324.88 84.0256 1 8 -7 2 1378.62 77.1883 1 -7 7 -2 818.575 77.6781 1 7 -7 2 1149.20 78.6723 1 -6 7 -2 79.9007 78.891 1 6 -7 2 176.995 44.5036 1 -5 7 -2 932.999 68.6202 1 5 -7 2 906.367 65.5432 1 -4 7 -2 697.29 82.7643 1 4 -7 2 665.223 58.9698 1 -3 7 -2 5904.58 210.687 1 3 -7 2 5126.48 181.491 1 -2 7 -2 3204.36 176.382 1 2 -7 2 3274.70 148.041 1 -1 7 -211080.20 367.333 1 1 -7 210718.10 313.499 1 0 7 -2 3542.13 260.808 1 0 -7 2 3537.90 151.608 1 1 7 -2 9893.58 407.531 1 -1 -7 210140.40 347.942 1 2 7 -2 2966.92 154.745 1 -2 -7 2 3447.17 141.939 1 3 7 -2 5511.44 204.33 1 -3 -7 2 4904.88 183.998 1 4 7 -2 713.657 55.7196 1 -4 -7 2 722.225 63.2182 1 5 7 -2 985.515 79.3563 1 -5 -7 2 861.122 72.9225 1 6 7 -2 84.6805 38.5847 1 -6 -7 2 164.00 40.7351 1 7 7 -2 751.915 63.102 1 -7 -7 2 1107.02 73.8003 1 8 7 -2 1193.71 84.1254 1 -8 -7 2 1425.85 85.1885 1 9 7 -2 3826.36 156.437 1 -9 -7 2 4124.44 153.261 1 10 7 -2 2091.54 108.703 1 -10 -7 2 2262.96 126.473 1 11 7 -2 4572.08 266.46 1 -11 -7 2 5030.93 198.564 1 12 7 -2 1762.29 107.754 1 -12 -7 2 1639.44 109.765 1 13 7 -2 4230.69 185.091 1 -13 -7 2 4226.78 161.589 1 -13 7 -1 224.272 73.6676 1 13 -7 1 253.736 74.4848 1 -12 7 -1 260.266 59.0733 1 12 -7 1 255.984 77.0549 1 -11 7 -1 651.906 72.0366 1 11 -7 1 782.636 70.2608 1 -10 7 -1 88.1416 63.3499 1 10 -7 1 64.2665 41.3166 1 -9 7 -1 4467.01 180.042 1 9 -7 1 4247.38 175.328 1 -8 7 -1 1791.37 101.122 1 8 -7 1 1809.68 95.3442 1 -7 7 -1 8671.30 273.428 1 7 -7 1 9020.20 294.012 1 -6 7 -1 4459.25 153.047 1 6 -7 1 4107.43 158.017 1 -5 7 -1 9719.45 329.613 1 5 -7 1 8973.81 301.475 1 -4 7 -1 5665.72 200.72 1 4 -7 1 5718.43 209.838 1 -3 7 -1 5801.46 222.502 1 3 -7 1 6152.56 204.132 1 -2 7 -1 2159.85 108.766 1 2 -7 1 2435.87 106.708 1 -1 7 -1 353.362 57.6937 1 1 -7 1 289.487 66.96 1 1 7 -1 327.281 58.0015 1 -1 -7 1 312.785 53.8558 1 2 7 -1 2010.38 91.2824 1 -2 -7 1 2328.85 97.506 1 3 7 -1 5629.67 187.935 1 -3 -7 1 5555.95 205.586 1 4 7 -1 5741.76 278.313 1 -4 -7 1 6419.89 228.47 1 5 7 -1 9223.99 289.515 1 -5 -7 1 8658.46 276.028 1 6 7 -1 4227.29 157.414 1 7 7 -1 8007.55 267.224 1 -7 -7 1 7512.31 246.593 1 8 7 -1 1668.77 91.2882 1 -8 -7 1 1725.17 90.2546 1 9 7 -1 4134.85 160.638 1 -9 -7 1 3943.71 148.439 1 10 7 -1 61.2561 46.1903 1 -10 -7 1 144.595 47.1928 1 11 7 -1 620.11 69.1181 1 -11 -7 1 733.664 68.1323 1 12 7 -1 216.374 64.7222 1 -12 -7 1 217.339 61.82 1 13 7 -1 175.653 85.4775 1 -13 -7 1 174.715 67.6336 1 -13 7 0 4702.74 208.36 1 13 -7 0 4574.96 148.131 1 -12 7 0 1613.46 104.564 1 12 -7 0 1514.86 94.3557 1 -11 7 0 5528.63 221.321 1 11 -7 0 5613.28 198.392 1 -10 7 0 1986.04 98.1661 1 10 -7 0 1660.64 97.2586 1 -9 7 0 4912.67 271.165 1 9 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1 5 7 4 919.547 73.6373 1 -5 -7 -4 917.709 64.4305 1 6 7 4 625.148 63.7885 1 -6 -7 -4 452.004 55.5918 1 7 7 4 638.299 67.52 1 -7 -7 -4 710.321 63.0176 1 8 7 4 1838.16 91.375 1 -8 -7 -4 1771.63 94.9261 1 9 7 4 3509.92 141.195 1 -9 -7 -4 3658.96 146.424 1 10 7 4 3192.62 152.757 1 -10 -7 -4 3438.40 190.31 1 11 7 4 6471.17 234.736 1 -11 -7 -4 5750.31 218.092 1 12 7 4 1522.42 99.449 1 -12 -7 -4 1131.91 84.0824 1 -12 7 5 105.194 50.5582 1 12 -7 -5 97.8523 49.7441 1 -11 7 5 334.733 63.3943 1 11 -7 -5 181.736 54.0957 1 -10 7 5 197.55 51.3423 1 10 -7 -5 88.7671 42.6459 1 -9 7 5 2613.08 156.75 1 9 -7 -5 2840.18 134.488 1 -8 7 5 1303.88 95.2031 1 8 -7 -5 1122.53 82.5127 1 -7 7 5 8476.37 338.213 1 7 -7 -5 8277.85 286.745 1 -6 7 5 3133.09 134.563 1 6 -7 -5 3338.18 141.066 1 -5 7 510538.70 368.072 1 5 -7 -510807.70 346.585 1 -4 7 5 2750.94 128.496 1 4 -7 -5 2350.45 109.742 1 -3 7 5 5275.03 317.589 1 3 -7 -5 4680.25 204.835 1 -2 7 5 995.969 73.2911 1 2 -7 -5 855.971 62.0169 1 -1 7 5 1074.13 66.6011 1 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1989.86 99.2325 1 9 -7 -8 2173.66 115.633 1 -8 7 8 738.292 74.0076 1 8 -7 -8 935.637 68.7219 1 -7 7 8 209.377 61.7386 1 7 -7 -8 264.854 57.2637 1 -6 7 8 9.95153 85.9427 1 6 -7 -8 1.80627 61.5155 1 -5 7 8 364.419 81.0869 1 5 -7 -8 286.979 56.4863 1 -4 7 8 481.02 68.5854 1 4 -7 -8 381.341 57.6125 1 -3 7 8 3762.10 221.512 1 3 -7 -8 4028.47 180.328 1 -2 7 8 1751.19 99.6233 1 2 -7 -8 1712.81 92.3149 1 -1 7 8 9187.62 312.354 1 1 -7 -8 9428.03 305.072 1 0 7 8 2826.28 134.928 1 0 -7 -8 3467.42 158.477 1 1 7 8 9326.33 326.28 1 -1 -7 -8 8447.28 273.243 1 2 7 8 1652.81 96.1766 1 -2 -7 -8 1628.76 92.612 1 3 7 8 4424.17 229.84 1 -3 -7 -8 4234.84 188.454 1 4 7 8 505.78 53.0138 1 -4 -7 -8 441.471 53.8814 1 5 7 8 464.657 55.619 1 -5 -7 -8 324.324 53.9103 1 6 7 8 21.8582 36.9872 1 -6 -7 -8-16.8152 38.6655 1 7 7 8 172.929 54.3519 1 -7 -7 -8 223.162 53.522 1 8 7 8 799.52 77.2187 1 -8 -7 -8 635.439 65.9537 1 9 7 8 1934.49 106.515 1 -9 -7 -8 1913.35 139.407 1 10 7 8 1472.17 91.2029 1 -10 -7 -8 1315.61 85.1255 1 -9 7 9 2113.24 111.268 1 9 -7 -9 1871.17 106.172 1 -8 7 9 985.167 91.2157 1 8 -7 -9 905.243 77.3223 1 -7 7 9 4434.66 251.818 1 7 -7 -9 4158.10 171.413 1 -6 7 9 1715.16 148.443 1 6 -7 -9 2122.93 105.523 1 -5 7 9 5446.03 222.596 1 5 -7 -9 5088.25 190.156 1 -4 7 9 1986.32 97.733 1 4 -7 -9 1916.65 95.0142 1 -3 7 9 3738.28 153.989 1 3 -7 -9 3632.30 156.702 1 -2 7 9 662.785 59.681 1 2 -7 -9 849.049 71.4333 1 -1 7 9 510.529 63.0253 1 1 -7 -9 522.232 65.7305 1 1 7 9 383.166 81.5987 1 -1 -7 -9 452.351 61.199 1 2 7 9 727.483 69.3266 1 -2 -7 -9 742.393 67.5744 1 3 7 9 3831.06 151.616 1 -3 -7 -9 3752.22 150.751 1 4 7 9 2020.89 161.294 1 -4 -7 -9 2184.74 116.917 1 5 7 9 5524.10 197.915 1 -5 -7 -9 5184.46 210.498 1 6 7 9 1897.96 100.279 1 -6 -7 -9 2126.47 110.15 1 7 7 9 4368.17 165.502 1 -7 -7 -9 4795.59 202.459 1 8 7 9 857.296 75.1614 1 -8 -7 -9 901.141 82.2034 1 9 7 9 2019.97 109.515 1 -9 -7 -9 1924.14 107.996 1 -8 7 10 708.052 84.451 1 8 -7 -10 517.818 70.8084 1 -7 7 10 304.22 58.239 1 7 -7 -10 205.13 52.1564 1 -6 7 10 22.9083 53.7403 1 6 -7 -10 55.4993 52.8609 1 -5 7 10 405.251 59.5455 1 5 -7 -10 335.929 55.1009 1 -4 7 10 125.012 50.8964 1 4 -7 -10 191.98 49.1135 1 -3 7 10 2953.75 143.038 1 3 -7 -10 3010.07 123.369 1 -2 7 10 1742.64 107.074 1 2 -7 -10 1776.54 91.0143 1 -1 7 10 5723.88 206.931 1 1 -7 -10 6780.73 244.228 1 0 7 10 2832.87 136.66 1 0 -7 -10 2357.64 113.741 1 1 7 10 6148.17 239.255 1 -1 -7 -10 6057.36 230.521 1 2 7 10 1712.51 151.841 1 -2 -7 -10 1674.56 99.2123 1 3 7 10 2883.53 138.61 1 -3 -7 -10 3138.64 141.157 1 4 7 10 245.81 51.0029 1 -4 -7 -10 173.908 45.9869 1 5 7 10 381.264 54.1176 1 -5 -7 -10 265.654 52.4728 1 6 7 10 34.4838 48.9163 1 -6 -7 -10 60.139 50.5174 1 7 7 10 336.239 61.7758 1 -7 -7 -10 286.196 79.7607 1 8 7 10 677.368 67.6637 1 -8 -7 -10 664.443 66.8976 1 -6 7 11 1192.68 96.7304 1 6 -7 -11 1409.46 98.4548 1 -5 7 11 3495.77 213.742 1 5 -7 -11 3578.65 138.715 1 -4 7 11 1323.03 85.9774 1 4 -7 -11 1169.49 84.2256 1 -3 7 11 2920.26 162.575 1 3 -7 -11 2520.40 127.423 1 -2 7 11 539.465 72.8094 1 2 -7 -11 528.064 71.9254 1 -1 7 11 613.563 62.8433 1 1 -7 -11 549.856 59.3497 1 1 7 11 590.229 64.2471 1 -1 -7 -11 513.985 58.2524 1 2 7 11 528.283 65.9319 1 -2 -7 -11 532.51 60.009 1 3 7 11 2538.61 187.148 1 -3 -7 -11 2786.48 131.424 1 4 7 11 1347.76 100.411 1 -4 -7 -11 1275.91 99.5886 1 5 7 11 3383.48 149.402 1 -5 -7 -11 3465.77 160.584 1 6 7 11 1499.31 99.7947 1 -6 -7 -11 1595.99 92.0035 1 -4 7 12 347.105 63.4219 1 4 -7 -12 418.244 63.4219 1 -3 7 12 1944.19 102.237 1 3 -7 -12 2083.38 110.83 1 -2 7 12 914.399 83.2051 1 2 -7 -12 850.067 73.7689 1 -1 7 12 4161.05 167.258 1 1 -7 -12 3552.59 179.209 1 0 7 12 1147.40 82.0779 1 0 -7 -12 768.316 68.5377 1 1 7 12 4103.39 172.298 1 -1 -7 -12 3959.53 180.663 1 2 7 12 958.626 78.3083 1 -2 -7 -12 857.245 74.186 1 3 7 12 1840.97 105.292 1 -3 -7 -12 2026.44 113.393 1 4 7 12 507.841 63.4802 1 -4 -7 -12 366.599 60.3039 1 -4 8 -10 512.362 99.9441 1 4 -8 10 675.564 70.8474 1 -3 8 -10 1184.24 92.2062 1 3 -8 10 1005.09 81.673 1 -2 8 -10 2385.31 127.049 1 2 -8 10 2433.14 114.761 1 -1 8 -10 2385.50 125.632 1 1 -8 10 2426.43 108.695 1 0 8 -10 2727.55 145.321 1 0 -8 10 2705.76 123.518 1 1 8 -10 2429.66 186.324 1 -1 -8 10 2392.40 110.304 1 2 8 -10 2671.78 134.04 1 -2 -8 10 2505.75 121.859 1 3 8 -10 987.505 117.813 1 -3 -8 10 1063.46 74.4053 1 4 8 -10 738.056 97.3633 1 -4 -8 10 646.979 53.3923 1 -6 8 -9 2831.35 146.101 1 6 -8 9 3087.30 143.829 1 -5 8 -9 1818.48 178.543 1 5 -8 9 2082.15 114.689 1 -4 8 -9 2636.23 190.494 1 4 -8 9 2568.63 120.441 1 -3 8 -9 1360.22 103.064 1 3 -8 9 1353.86 83.9849 1 -2 8 -9 1025.16 87.9486 1 2 -8 9 1046.16 76.1298 1 -1 8 -9 292.868 68.8315 1 1 -8 9 211.897 53.9848 1 1 8 -9 173.902 106.032 1 -1 -8 9 195.101 59.3744 1 2 8 -9 1224.40 96.5147 1 -2 -8 9 982.404 80.6686 1 3 8 -9 1394.09 96.5539 1 -3 -8 9 1435.05 81.922 1 -4 -8 9 2485.07 113.973 1 5 8 -9 2026.30 198.30 1 -5 -8 9 1923.40 107.358 1 6 8 -9 2438.53 171.831 1 -6 -8 9 2714.97 125.517 1 -7 8 -8 87.1495 85.0273 1 7 -8 8 18.0686 41.4526 1 -6 8 -8 58.7487 55.4286 1 6 -8 8-22.1756 45.4475 1 -5 8 -8 278.508 63.3022 1 5 -8 8 234.782 52.9397 1 -4 8 -8 718.716 80.9158 1 4 -8 8 825.812 95.1938 1 -3 8 -8 1336.09 127.478 1 3 -8 8 1481.96 87.0247 1 -2 8 -8 2768.87 196.334 1 2 -8 8 2976.54 135.927 1 -1 8 -8 2703.27 137.872 1 1 -8 8 2346.36 106.951 1 0 8 -8 4879.71 192.088 1 0 -8 8 4499.48 172.349 1 1 8 -8 2212.33 194.293 1 -1 -8 8 2540.63 135.343 1 -2 -8 8 3206.10 147.032 1 3 8 -8 1528.48 147.609 1 -3 -8 8 1358.81 81.3859 1 4 8 -8 593.712 69.6871 1 -4 -8 8 843.175 72.4698 1 5 8 -8 291.847 75.7599 1 -5 -8 8 211.871 63.1398 1 6 8 -8 80.1736 71.7349 1 -6 -8 8 12.6646 53.4535 1 7 8 -8 91.1742 65.9266 1 -7 -8 8 108.019 47.6944 1 -8 8 -7 2240.19 170.016 1 8 -8 7 1983.17 143.011 1 -7 8 -7 2182.78 156.431 1 7 -8 7 2585.34 122.023 1 -6 8 -7 4279.23 252.166 1 6 -8 7 4359.31 179.653 1 -5 8 -7 2801.03 178.907 1 5 -8 7 2821.16 126.356 1 -4 8 -7 2413.23 121.989 1 4 -8 7 2612.31 132.34 1 -3 8 -7 1724.47 112.136 1 3 -8 7 1614.70 102.687 1 -2 8 -7 982.533 85.6946 1 2 -8 7 710.943 63.9697 1 -1 8 -7 180.98 76.332 1 1 -8 7 144.049 54.1733 1 1 8 -7 214.997 64.8801 1 -1 -8 7 117.036 53.4257 1 2 8 -7 1063.50 78.6378 1 -2 -8 7 754.119 69.6048 1 3 8 -7 1697.03 156.407 1 -3 -8 7 1544.53 89.9331 1 4 8 -7 2578.02 212.968 1 -4 -8 7 2530.70 111.746 1 5 8 -7 3015.88 215.519 1 -5 -8 7 2789.79 128.251 1 6 8 -7 4007.06 241.166 1 -6 -8 7 4132.93 169.605 1 7 8 -7 2514.97 134.873 1 -7 -8 7 2555.96 126.94 1 8 8 -7 2075.08 120.749 1 -8 -8 7 2143.33 115.495 1 -9 8 -6 1041.13 92.4172 1 9 -8 6 969.452 115.999 1 -8 8 -6 1378.74 116.128 1 8 -8 6 1330.52 88.572 1 -7 8 -6 105.227 74.5805 1 7 -8 6 129.744 57.2127 1 -6 8 -6 146.722 60.1683 1 6 -8 6 190.009 58.0607 1 -5 8 -6 498.532 70.5934 1 5 -8 6 316.059 59.7399 1 -4 8 -6 613.507 74.6028 1 4 -8 6 614.618 60.1206 1 -3 8 -6 1514.45 97.8519 1 3 -8 6 1381.32 89.8896 1 -2 8 -6 2317.99 114.794 1 2 -8 6 2712.25 122.919 1 -1 8 -6 2738.73 202.779 1 1 -8 6 2801.21 172.132 1 0 8 -6 4155.60 191.391 1 0 -8 6 4632.89 177.038 1 1 8 -6 2651.80 124.775 1 -1 -8 6 3070.95 136.892 1 2 8 -6 2030.43 172.675 1 -2 -8 6 2863.17 124.913 1 3 8 -6 1323.41 111.213 1 -3 -8 6 1210.96 77.8469 1 4 8 -6 542.497 57.2344 1 -4 -8 6 651.985 63.4571 1 5 8 -6 518.679 94.9826 1 -5 -8 6 404.944 63.7416 1 6 8 -6 138.933 101.385 1 -6 -8 6 128.924 62.5875 1 7 8 -6 114.904 72.4382 1 -7 -8 6 99.9172 47.4648 1 8 8 -6 1468.88 99.2483 1 -8 -8 6 1525.95 86.8394 1 9 8 -6 1063.74 89.4644 1 -9 -8 6 1034.33 85.7824 1 -10 8 -5 95.2716 69.4516 1 10 -8 5 224.372 46.2983 1 -9 8 -5 1546.69 165.648 1 9 -8 5 1745.83 133.077 1 -8 8 -5 2126.06 143.156 1 8 -8 5 2109.62 106.397 1 -7 8 -5 2918.81 201.053 1 7 -8 5 3268.91 136.039 1 -6 8 -5 4583.31 181.233 1 6 -8 5 5148.63 196.682 1 -5 8 -5 3674.23 157.315 1 5 -8 5 4695.20 171.037 1 -4 8 -5 4566.61 237.343 1 4 -8 5 4431.76 157.51 1 -3 8 -5 2355.24 128.592 1 3 -8 5 2081.57 157.161 1 -2 8 -5 2276.05 134.016 1 2 -8 5 2090.66 98.2741 1 -1 8 -5 582.051 71.3406 1 1 -8 5 468.817 63.4162 1 1 8 -5 559.276 68.3132 1 -1 -8 5 375.166 60.2103 1 2 8 -5 2201.73 133.155 1 -2 -8 5 1815.11 101.615 1 3 8 -5 2250.24 118.808 1 -3 -8 5 1858.53 97.6366 1 4 8 -5 4299.43 248.319 1 -4 -8 5 3831.18 157.264 1 5 8 -5 4029.33 225.363 1 -5 -8 5 3750.59 164.87 1 6 8 -5 4592.74 182.76 1 -6 -8 5 4192.81 176.825 1 7 8 -5 3401.56 249.732 1 -7 -8 5 2827.54 133.745 1 8 8 -5 2131.56 111.696 1 -8 -8 5 2083.36 95.2301 1 9 8 -5 1588.80 124.363 1 -9 -8 5 1811.96 101.113 1 10 8 -5 151.919 70.8223 1 -10 -8 5 179.342 54.8246 1 -10 8 -4 2693.74 130.371 1 10 -8 4 2923.66 134.776 1 -9 8 -4 1719.38 107.351 1 9 -8 4 1506.52 99.0896 1 -8 8 -4 1648.95 102.644 1 8 -8 4 1488.33 76.0318 1 -7 8 -4 231.191 58.7827 1 7 -8 4 165.562 48.006 1 -6 8 -4 166.889 74.3971 1 6 -8 4 221.184 51.2741 1 -5 8 -4 506.724 70.919 1 5 -8 4 507.75 63.7265 1 -4 8 -4 916.42 103.682 1 4 -8 4 1042.10 73.3105 1 -3 8 -4 2524.30 126.642 1 3 -8 4 2238.03 168.148 1 -2 8 -4 2927.79 138.078 1 2 -8 4 2715.28 119.739 1 -1 8 -4 3364.53 152.789 1 1 -8 4 3775.96 166.973 1 0 8 -4 5957.78 243.559 1 0 -8 4 4933.96 176.33 1 1 8 -4 2851.28 128.893 1 -1 -8 4 3537.99 151.122 1 2 8 -4 2710.62 135.361 1 -2 -8 4 2830.32 130.893 1 3 8 -4 2331.28 129.326 1 -3 -8 4 2171.59 106.84 1 4 8 -4 703.144 65.4596 1 -4 -8 4 828.429 69.9774 1 5 8 -4 434.125 87.0572 1 -5 -8 4 453.345 63.3124 1 6 8 -4 246.296 68.9216 1 -6 -8 4 160.434 63.2713 1 7 8 -4 201.521 60.7902 1 -7 -8 4 182.381 54.0358 1 8 8 -4 1389.56 153.153 1 -8 -8 4 1472.28 95.0229 1 9 8 -4 1475.47 101.679 1 -9 -8 4 1485.43 93.9452 1 10 8 -4 2901.23 151.091 1 -10 -8 4 2982.77 163.049 1 -10 8 -3 332.619 62.6956 1 10 -8 3 282.987 49.6317 1 -9 8 -3 1389.84 97.6601 1 9 -8 3 1451.33 93.1377 1 -8 8 -3 2827.31 143.841 1 8 -8 3 2669.47 127.962 1 -7 8 -3 3946.24 170.906 1 7 -8 3 3768.61 155.541 1 -6 8 -3 5319.11 201.482 1 6 -8 3 5061.61 201.482 1 -5 8 -3 4527.65 251.591 1 5 -8 3 4332.19 164.389 1 -4 8 -3 4860.82 212.983 1 4 -8 3 5272.52 193.615 1 -3 8 -3 2264.82 108.484 1 3 -8 3 1988.95 103.326 1 -2 8 -3 1886.59 104.525 1 2 -8 3 1730.86 84.6593 1 -1 8 -3 432.662 67.5352 1 1 -8 3 454.826 60.1505 1 1 8 -3 405.721 50.3105 1 -1 -8 3 384.306 52.458 1 2 8 -3 1672.95 130.176 1 -2 -8 3 1715.98 104.357 1 3 8 -3 1908.91 111.208 1 -3 -8 3 1901.35 103.653 1 4 8 -3 4052.73 170.94 1 -4 -8 3 4784.08 168.77 1 5 8 -3 3507.18 192.616 1 -5 -8 3 3942.19 193.697 1 6 8 -3 4347.16 182.53 1 -6 -8 3 4526.45 165.248 1 7 8 -3 3006.01 197.817 1 -7 -8 3 3346.81 173.09 1 8 8 -3 2338.28 118.403 1 -8 -8 3 2503.62 125.877 1 9 8 -3 1468.57 157.082 1 -9 -8 3 1480.16 96.9894 1 10 8 -3 309.021 57.038 1 -10 -8 3 324.579 59.1085 1 -11 8 -2 2456.90 141.173 1 11 -8 2 2333.06 123.009 1 -10 8 -2 2851.05 163.455 1 10 -8 2 2740.93 194.432 1 -9 8 -2 1671.11 117.645 1 9 -8 2 1608.72 91.799 1 -8 8 -2 2322.76 159.814 1 8 -8 2 2103.25 101.944 1 -7 8 -2 205.359 55.5763 1 7 -8 2 148.842 48.9841 1 -6 8 -2 65.4322 54.8471 1 6 -8 2 100.07 47.1529 1 -5 8 -2 390.768 63.6552 1 5 -8 2 210.567 64.6422 1 -4 8 -2 1224.32 133.17 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8 -1 3724.24 153.595 1 7 -8 1 3373.57 161.002 1 -6 8 -1 4739.10 174.54 1 6 -8 1 4800.43 193.414 1 -5 8 -1 3122.46 142.844 1 5 -8 1 3375.55 142.844 1 -4 8 -1 6685.05 235.036 1 4 -8 1 6752.06 221.443 1 -3 8 -1 2611.64 175.676 1 3 -8 1 2649.92 116.794 1 -2 8 -1 2639.31 125.679 1 2 -8 1 2511.65 112.816 1 -1 8 -1 602.574 66.7337 1 1 -8 1 535.84 56.7715 1 1 8 -1 563.301 63.2583 1 -1 -8 1 563.301 60.2509 1 2 8 -1 2403.46 115.694 1 -2 -8 1 2459.80 107.65 1 3 8 -1 2589.96 114.751 1 -3 -8 1 2692.63 110.722 1 4 8 -1 6220.72 212.184 1 -4 -8 1 6275.02 247.379 1 5 8 -1 3087.99 174.513 1 -5 -8 1 3083.99 132.384 1 6 8 -1 5010.12 185.674 1 -6 -8 1 4864.37 195.649 1 7 8 -1 3524.58 142.725 1 -7 -8 1 3393.75 136.779 1 8 8 -1 2226.57 120.704 1 -8 -8 1 2378.67 125.602 1 9 8 -1 1542.30 95.8453 1 -9 -8 1 1729.14 99.7206 1 10 8 -1 277.781 57.083 1 -10 -8 1 349.129 55.1746 1 11 8 -1 350.732 80.9361 1 -11 -8 1 309.795 78.1498 1 -11 8 0 2418.69 164.105 1 11 -8 0 2454.26 151.977 1 -10 8 0 2555.18 180.476 1 10 -8 0 2398.20 120.874 1 -9 8 0 1472.32 93.5909 1 9 -8 0 1456.72 90.9873 1 -8 8 0 2177.78 118.365 1 8 -8 0 2133.29 132.606 1 -7 8 0 382.134 58.2275 1 7 -8 0 343.007 50.9523 1 -6 8 0 98.2048 45.3984 1 6 -8 0 28.7154 40.7652 1 -5 8 0 206.821 52.646 1 5 -8 0 151.35 50.7601 1 -4 8 0 1323.01 110.327 1 4 -8 0 1322.06 84.6532 1 -3 8 0 4021.85 169.896 1 3 -8 0 3902.83 149.736 1 -2 8 0 7931.02 271.614 1 2 -8 0 7043.67 231.02 1 -1 8 0 6675.72 268.152 1 1 -8 0 6524.15 258.443 1 0 8 0 9379.23 298.344 1 0 -8 0 9707.80 318.812 1 1 8 0 6070.57 219.802 1 -1 -8 0 6031.50 211.99 1 2 8 0 7591.10 332.346 1 -2 -8 0 7757.27 269.78 1 3 8 0 4060.87 157.236 1 -3 -8 0 3734.67 147.477 1 4 8 0 1392.28 90.6073 1 -4 -8 0 1436.13 89.6346 1 5 8 0 257.134 50.4544 1 -5 -8 0 238.692 45.6018 1 6 8 0 31.8261 56.8947 1 -6 -8 0 12.5343 46.2859 1 7 8 0 434.12 58.3311 1 -7 -8 0 377.698 54.5036 1 8 8 0 2206.65 125.74 1 -8 -8 0 2359.80 115.339 1 9 8 0 1333.23 100.622 1 -9 -8 0 1245.66 94.1019 1 10 8 0 2424.51 128.956 1 -10 -8 0 2446.46 120.721 1 11 8 0 2090.52 125.131 1 -11 -8 0 2400.65 117.976 1 -11 8 1 485.967 63.9424 1 11 -8 -1 366.069 56.7457 1 -10 8 1 290.995 69.6411 1 10 -8 -1 358.145 59.6934 1 -9 8 1 1728.60 100.88 1 9 -8 -1 1903.85 103.44 1 -8 8 1 2566.94 156.102 1 8 -8 -1 2247.72 107.873 1 -7 8 1 3690.52 159.404 1 7 -8 -1 3574.10 163.883 1 -6 8 1 4822.05 186.725 1 6 -8 -1 5095.31 224.978 1 -5 8 1 3489.89 159.719 1 5 -8 -1 3275.70 190.188 1 -4 8 1 6890.69 232.336 1 4 -8 -1 7053.98 252.865 1 -3 8 1 2667.56 132.628 1 3 -8 -1 2612.06 124.158 1 -2 8 1 2589.60 123.001 1 2 -8 -1 2581.09 115.426 1 -1 8 1 567.105 60.7929 1 1 -8 -1 545.258 54.1455 1 1 8 1 602.199 101.956 1 -1 -8 -1 499.291 66.6966 1 2 8 1 2308.06 121.874 1 -2 -8 -1 2519.45 120.923 1 3 8 1 2440.77 113.061 1 -3 -8 -1 2408.47 114.01 1 4 8 1 6336.79 239.46 1 -4 -8 -1 6313.13 228.103 1 5 8 1 3421.44 133.658 1 -5 -8 -1 2851.98 131.779 1 6 8 1 5041.47 276.501 1 -6 -8 -1 5173.18 187.757 1 7 8 1 3394.20 147.052 1 -7 -8 -1 3687.38 162.775 1 8 8 1 2388.73 119.619 1 -8 -8 -1 2745.77 122.363 1 9 8 1 1615.74 94.3524 1 -9 -8 -1 1782.88 106.938 1 10 8 1 346.26 66.0788 1 -10 -8 -1 401.767 67.8464 1 11 8 1 371.608 62.7961 1 -11 -8 -1 338.059 55.9097 1 -11 8 2 2426.18 128.736 1 11 -8 -2 2366.95 169.803 1 -10 8 2 2860.99 144.891 1 10 -8 -2 3208.90 229.206 1 -9 8 2 1794.11 147.614 1 9 -8 -2 1779.77 109.656 1 -8 8 2 2022.32 99.4284 1 8 -8 -2 2081.98 110.666 1 -7 8 2 160.556 47.6334 1 7 -8 -2 156.144 45.8719 1 -6 8 2 109.369 46.6166 1 6 -8 -2 62.7521 40.3431 1 -5 8 2 325.936 59.01 1 5 -8 -2 453.046 59.9249 1 -4 8 2 949.722 103.591 1 4 -8 -2 1167.90 77.0066 1 -3 8 2 3162.16 139.416 1 3 -8 -2 3142.77 137.564 1 -2 8 2 5957.32 218.028 1 2 -8 -2 6002.79 219.889 1 -1 8 2 6019.63 227.052 1 1 -8 -2 6104.29 223.327 1 0 8 2 8785.65 279.504 1 0 -8 -2 8998.07 321.43 1 1 8 2 5812.33 203.954 1 -1 -8 -2 5222.81 191.849 1 2 8 2 5838.32 199.849 1 -2 -8 -2 6056.76 216.579 1 3 8 2 2950.19 138.939 1 -3 -8 -2 3140.08 125.975 1 4 8 2 1100.28 83.8574 1 -4 -8 -2 1185.06 80.1688 1 5 8 2 334.914 57.649 1 -5 -8 -2 474.008 63.139 1 6 8 2 23.58 81.6119 1 -6 -8 -2 67.1018 47.1515 1 7 8 2 99.4964 44.8219 1 -7 -8 -2 155.074 45.7169 1 8 8 2 2179.16 115.762 1 -8 -8 -2 1979.45 98.0847 1 9 8 2 1551.79 96.3855 1 -9 -8 -2 1870.47 105.938 1 10 8 2 3237.74 171.746 1 -10 -8 -2 2963.11 140.291 1 11 8 2 2568.65 128.514 1 -11 -8 -2 2439.30 129.342 1 -10 8 3 241.562 93.7152 1 10 -8 -3 316.704 59.7857 1 -9 8 3 1745.89 140.639 1 9 -8 -3 1711.77 99.0291 1 -8 8 3 2956.84 188.428 1 8 -8 -3 2417.14 153.472 1 7 -8 -3 4024.75 226.932 1 -6 8 3 5208.23 195.156 1 6 -8 -3 4326.06 216.347 1 -5 8 3 4566.77 189.461 1 5 -8 -3 4916.21 207.339 1 -4 8 3 5185.78 195.672 1 4 -8 -3 5048.73 175.833 1 -3 8 3 2208.69 119.78 1 3 -8 -3 2448.26 117.062 1 -2 8 3 1773.01 112.979 1 2 -8 -3 2005.34 120.264 1 -1 8 3 414.483 54.7811 1 1 -8 -3 482.041 55.6925 1 1 8 3 375.658 54.7119 1 -1 -8 -3 463.192 54.7119 1 2 8 3 1864.28 107.26 1 -2 -8 -3 1631.59 99.0758 1 3 8 3 2184.68 111.273 1 -3 -8 -3 2208.19 115.788 1 4 8 3 5178.47 194.126 1 -4 -8 -3 4986.15 199.518 1 5 8 3 4822.85 188.03 1 -5 -8 -3 4240.04 182.684 1 6 8 3 5631.42 191.328 1 -6 -8 -3 5094.47 184.278 1 7 8 3 4063.92 171.436 1 -7 -8 -3 3524.38 161.863 1 8 8 3 2757.04 113.055 1 -8 -8 -3 2677.39 120.767 1 9 8 3 1526.86 103.363 1 -9 -8 -3 1787.36 95.7965 1 10 8 3 446.101 92.8368 1 -10 -8 -3 345.055 59.1546 1 -10 8 4 3015.59 129.869 1 10 -8 -4 2960.62 131.46 1 -9 8 4 1499.30 132.12 1 9 -8 -4 1543.61 102.58 1 -8 8 4 1407.29 96.6762 1 8 -8 -4 1429.14 89.1147 1 -7 8 4 215.129 65.136 1 7 -8 -4 184.276 47.9984 1 -6 8 4 243.648 73.0968 1 6 -8 -4 137.49 46.1168 1 -5 8 4 442.77 87.1429 1 5 -8 -4 379.396 53.6985 1 4 -8 -4 976.445 104.748 1 -3 8 4 2658.53 123.194 1 3 -8 -4 2611.21 167.832 1 -2 8 4 3439.36 151.37 1 2 -8 -4 2836.57 201.521 1 -1 8 4 4263.92 177.553 1 1 -8 -4 3393.20 128.231 1 0 8 4 5431.94 187.28 1 0 -8 -4 6569.05 263.446 1 1 8 4 4246.43 194.846 1 -1 -8 -4 3515.30 155.525 1 2 8 4 3632.88 215.37 1 -2 -8 -4 3223.49 131.717 1 3 8 4 2521.09 114.999 1 -3 -8 -4 2598.06 141.534 1 4 8 4 920.597 78.1091 1 -4 -8 -4 943.418 76.3486 1 5 8 4 422.272 77.3332 1 -5 -8 -4 418.802 57.3494 1 6 8 4 225.733 48.0665 1 -6 -8 -4 270.364 48.0665 1 7 8 4 202.129 53.2802 1 -7 -8 -4 167.455 52.4359 1 8 8 4 1410.17 93.0724 1 -8 -8 -4 1588.84 90.5758 1 9 8 4 1468.34 99.2968 1 -9 -8 -4 1618.91 97.6716 1 10 8 4 3021.42 164.456 1 -10 -8 -4 2966.60 132.677 1 -10 8 5 282.487 76.1147 1 10 -8 -5 234.619 63.5582 1 -9 8 5 1839.40 110.768 1 9 -8 -5 1735.10 98.6371 1 -8 8 5 2009.80 105.21 1 8 -8 -5 1846.59 101.067 1 -7 8 5 3242.64 141.898 1 7 -8 -5 3002.75 130.92 1 -6 8 5 4993.03 191.214 1 6 -8 -5 4506.85 210.936 1 -5 8 5 4770.46 238.477 1 5 -8 -5 4277.02 164.765 1 -4 8 5 4468.76 207.182 1 4 -8 -5 4568.41 184.45 1 -3 8 5 2276.69 101.925 1 3 -8 -5 2594.77 109.837 1 -2 8 5 2368.19 149.775 1 2 -8 -5 2614.87 125.106 1 -1 8 5 468.892 78.4462 1 1 -8 -5 789.717 72.2701 1 1 8 5 393.69 71.0199 1 -1 -8 -5 718.986 91.1862 1 2 8 5 2286.50 115.979 1 -2 -8 -5 2202.78 143.888 1 3 8 5 2557.12 119.457 1 -3 -8 -5 2598.67 119.457 1 4 8 5 4806.70 276.142 1 -4 -8 -5 4582.01 164.656 1 5 8 5 4160.72 153.443 1 -5 -8 -5 4459.13 179.72 1 6 8 5 4871.69 199.817 1 -6 -8 -5 5242.06 203.164 1 7 8 5 3234.45 140.628 1 -7 -8 -5 3170.31 143.92 1 8 8 5 2035.95 112.12 1 -8 -8 -5 2319.09 124.222 1 9 8 5 2034.11 157.743 1 -9 -8 -5 1859.80 91.4888 1 10 8 5 180.616 52.2643 1 -10 -8 -5 231.346 53.799 1 -9 8 6 1013.37 78.7438 1 9 -8 -6 1279.83 85.1116 1 -8 8 6 1354.47 95.4117 1 8 -8 -6 1318.59 94.5899 1 -7 8 6 125.592 51.5667 1 7 -8 -6 133.072 48.2376 1 -6 8 6 176.494 50.6711 1 6 -8 -6 180.717 46.4479 1 -5 8 6 468.001 66.616 1 5 -8 -6 437.259 62.3449 1 -4 8 6 772.924 72.302 1 4 -8 -6 619.711 55.9431 1 -3 8 6 1357.81 76.1026 1 3 -8 -6 1803.20 102.054 1 -2 8 6 3305.49 143.867 1 2 -8 -6 2758.63 118.734 1 -1 8 6 3473.51 156.825 1 1 -8 -6 2926.79 155.087 1 0 8 6 5394.79 192.731 1 0 -8 -6 5233.17 197.917 1 1 8 6 3525.61 163.459 1 -1 -8 -6 2985.33 140.236 1 2 8 6 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236.121 1 4 -9 -5 4251.00 171.726 1 -3 9 5 398.579 90.6243 1 3 -9 -5 244.605 55.3353 1 2 -9 -5 1974.18 166.126 1 -1 9 5 20.2123 52.5565 1 1 -9 -5 40.4322 89.7519 1 1 9 5 13.7117 64.5247 1 -1 -9 -5 71.787 62.9143 1 2 9 5 1410.86 98.7151 1 -2 -9 -5 1952.57 113.16 1 3 9 5 332.17 61.3399 1 -3 -9 -5 258.886 53.3723 1 4 9 5 4846.52 205.85 1 -4 -9 -5 4109.88 174.302 1 5 9 5 666.721 73.2113 1 -5 -9 -5 580.269 70.1009 1 6 9 5 4729.33 197.151 1 -6 -9 -5 4368.02 178.741 1 -5 9 6 147.474 52.9969 1 5 -9 -6 191.255 53.7637 1 -4 9 6 1118.60 85.5053 1 4 -9 -6 1239.86 86.2814 1 -3 9 6 903.795 90.1432 1 3 -9 -6 972.779 72.1146 1 -2 9 6 3118.30 152.842 1 2 -9 -6 2827.58 143.389 1 -1 9 6 709.725 78.1537 1 1 -9 -6 692.356 72.6292 1 0 -9 -6 5522.74 208.254 1 1 9 6 555.797 92.7661 1 -1 -9 -6 883.614 77.0398 1 2 9 6 3228.76 217.232 1 -2 -9 -6 2963.09 218.012 1 3 9 6 1131.08 103.815 1 -3 -9 -6 987.76 121.633 1 4 9 6 1064.87 92.696 1 -4 -9 -6 1179.02 136.363 1 5 9 6 98.2262 57.4213 1 -5 -9 -6 172.271 58.9371 1 -4 9 7 3167.54 146.463 1 4 -9 -7 3503.71 160.879 1 -3 9 7 462.125 65.7985 1 3 -9 -7 510.326 70.3888 1 -2 9 7 1551.28 119.918 1 2 -9 -7 1850.31 114.539 1 -1 9 7 157.059 73.9108 1 1 -9 -7 141.658 56.2035 1 1 9 7 156.16 50.525 1 -1 -9 -7 92.6219 48.2251 1 2 9 7 1547.63 139.862 1 -2 -9 -7 1830.40 111.741 1 3 9 7 604.495 115.179 1 -3 -9 -7 509.643 63.2366 1 4 9 7 2962.95 210.42 1 -4 -9 -7 3648.48 192.57 1 -1 9 8 342.501 82.4383 1 1 -9 -8 509.629 61.4528 1 0 9 8 3876.54 180.25 1 0 -9 -8 3970.03 170.529 1 1 9 8 426.416 65.4844 1 -1 -9 -8 534.319 58.7909 1 -2 10 -2 2900.06 158.836 1 2 -10 2 3073.74 143.129 1 -1 10 -2-0.88293 59.256 1 1 -10 2 53.9501 53.0672 1 0 10 -2 4096.98 245.673 1 0 -10 2 4492.74 184.924 1 1 10 -2 35.9871 56.6794 1 -1 -10 2 57.5776 53.0782 1 2 10 -2 3274.52 153.565 1 -2 -10 2 3239.29 149.95 1 -2 10 -1 706.753 95.0286 1 2 -10 1 498.037 86.5422 1 -1 10 -1 35.1909 74.6746 1 1 -10 1 57.5116 65.2321 1 1 10 -1 35.6897 64.4186 1 -1 -10 1 21.7598 55.7114 1 2 10 -1 668.58 83.7924 1 -2 -10 1 576.937 75.9335 1 -2 10 0 2967.68 149.376 1 2 -10 0 3039.47 154.327 1 -1 10 0-7.50652 54.1867 1 1 -10 0 12.5083 49.185 1 0 10 0 3891.73 174.649 1 0 -10 0 4058.81 191.437 1 1 10 0 7.59183 50.5937 1 -1 -10 0-6.74212 48.0604 1 2 10 0 2904.39 141.838 1 -2 -10 0 2795.47 120.734 1 -2 10 1 602.323 82.718 1 2 -10 -1 637.653 78.7016 1 -1 10 1 81.8371 61.5762 1 1 -10 -1 29.1665 57.5241 1 1 10 1 10.6241 58.8557 1 -1 -10 -1 0.00 52.3119 1 2 10 1 554.268 72.7608 1 -2 -10 -1 756.189 77.6654 1 -2 10 2 3281.66 154.782 1 2 -10 -2 3078.41 142.273 1 -1 10 2 89.8093 57.5109 1 1 -10 -2 77.2031 48.0581 1 0 10 2 4794.25 200.252 1 0 -10 -2 4552.84 187.594 1 1 10 2 70.5759 52.3382 1 -1 -10 -2 73.7424 46.7817 1 2 10 2 3325.45 155.259 1 -2 -10 -2 2968.98 138.629 1 0 0 0 0.00 0.00 1 ; _shelx_hkl_checksum 49205 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y, z' '-x+1/2, y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ir1 Ir 0.20671(2) 0.54839(2) 0.49108(6) 0.02563(8) Uani 1 1 d . . . . . N2 N 0.2456(4) 0.6855(6) 0.3864(4) 0.0309(10) Uani 1 1 d D . . . . H2 H 0.214(4) 0.667(11) 0.342(4) 0.046 Uiso 1 1 d D U . . . C3 C 0.3131(4) 0.7986(7) 0.3752(5) 0.0295(13) Uani 1 1 d . . . . . C4 C 0.3256(5) 0.8708(7) 0.2854(5) 0.0381(13) Uani 1 1 d . . . . . H4 H 0.286065 0.842155 0.236059 0.046 Uiso 1 1 calc R U . . . C5 C 0.3935(5) 0.9811(9) 0.2676(6) 0.0479(19) Uani 1 1 d . . . . . H5 H 0.400515 1.026968 0.206901 0.058 Uiso 1 1 calc R U . . . C6 C 0.4519(5) 1.0245(7) 0.3407(7) 0.050(2) Uani 1 1 d . . . . . H6 H 0.499267 1.099160 0.329543 0.060 Uiso 1 1 calc R U . . . C7 C 0.4403(5) 0.9588(7) 0.4277(7) 0.0430(17) Uani 1 1 d . . . . . H7 H 0.480037 0.991379 0.476034 0.052 Uiso 1 1 calc R U . . . C8 C 0.3715(4) 0.8435(7) 0.4503(5) 0.0306(14) Uani 1 1 d . . . . . C9 C 0.3625(4) 0.7747(7) 0.5437(5) 0.0295(14) Uani 1 1 d . . . . . C10 C 0.3010(4) 0.6570(9) 0.5672(5) 0.0303(13) Uani 1 1 d . . . . . H10 H 0.304(4) 0.634(10) 0.624(6) 0.036 Uiso 1 1 d . U . . . C11 C 0.4273(4) 0.8355(8) 0.6210(5) 0.0437(16) Uani 1 1 d . . . . . H11A H 0.416270 0.774789 0.679070 0.066 Uiso 1 1 calc R U . . . H11B H 0.417535 0.952378 0.632046 0.066 Uiso 1 1 calc R U . . . H11C H 0.489009 0.817660 0.600767 0.066 Uiso 1 1 calc R U . . . C12 C 0.0744(6) 0.4310(9) 0.4495(7) 0.042(2) Uani 1 1 d . . . . . C13 C 0.0744(5) 0.4986(8) 0.5455(6) 0.0303(15) Uani 1 1 d . . . . . C14 C 0.1395(4) 0.4085(7) 0.6016(4) 0.0274(12) Uani 1 1 d . . . . . C15 C 0.1841(5) 0.2978(7) 0.5394(5) 0.0283(14) Uani 1 1 d . . . . . C16 C 0.1426(5) 0.3108(9) 0.4473(6) 0.0408(18) Uani 1 1 d . . . . . C17 C 0.0129(7) 0.4834(12) 0.3722(7) 0.069(3) Uani 1 1 d . . . . . H17A H 0.046841 0.495181 0.313980 0.103 Uiso 1 1 calc R U . . . H17B H -0.014543 0.588368 0.388562 0.103 Uiso 1 1 calc R U . . . H17C H -0.033832 0.400881 0.363725 0.103 Uiso 1 1 calc R U . . . C18 C 0.0100(4) 0.6238(8) 0.5845(6) 0.0464(17) Uani 1 1 d . . . . . H18A H -0.042155 0.567888 0.610776 0.070 Uiso 1 1 calc R U . . . H18B H -0.009249 0.697410 0.534191 0.070 Uiso 1 1 calc R U . . . H18C H 0.039584 0.687252 0.633707 0.070 Uiso 1 1 calc R U . . . C19 C 0.1564(6) 0.4267(8) 0.7049(5) 0.0412(15) Uani 1 1 d . . . . . H19A H 0.116257 0.354161 0.739705 0.062 Uiso 1 1 calc R U . . . H19B H 0.145470 0.540258 0.723678 0.062 Uiso 1 1 calc R U . . . H19C H 0.218440 0.397671 0.718784 0.062 Uiso 1 1 calc R U . . . C20 C 0.2571(5) 0.1757(8) 0.5673(6) 0.055(2) Uani 1 1 d . . . . . H20A H 0.230816 0.066660 0.574542 0.083 Uiso 1 1 calc R U . . . H20B H 0.284035 0.209768 0.626712 0.083 Uiso 1 1 calc R U . . . H20C H 0.303024 0.172509 0.518490 0.083 Uiso 1 1 calc R U . . . C21 C 0.1703(7) 0.2057(11) 0.3646(6) 0.072(3) Uani 1 1 d . . . . . H21A H 0.153618 0.091780 0.376460 0.108 Uiso 1 1 calc R U . . . H21B H 0.235056 0.213149 0.355930 0.108 Uiso 1 1 calc R U . . . H21C H 0.140123 0.244532 0.307863 0.108 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ir1 0.02578(11) 0.02549(11) 0.02562(12) 0.0001(2) 0.0019(2) -0.00586(6) N2 0.036(3) 0.024(2) 0.033(3) 0.003(2) 0.001(2) -0.011(2) C3 0.029(3) 0.020(3) 0.040(4) -0.001(2) 0.007(3) 0.000(2) C4 0.044(3) 0.026(3) 0.044(4) 0.006(3) 0.009(3) -0.003(3) C5 0.052(5) 0.032(3) 0.060(5) 0.016(3) 0.012(4) 0.000(3) C6 0.041(4) 0.030(3) 0.079(7) 0.008(3) 0.019(4) -0.005(3) C7 0.031(3) 0.029(3) 0.069(5) -0.009(3) 0.001(3) -0.002(2) C8 0.024(3) 0.016(3) 0.051(4) -0.005(3) 0.005(2) 0.000(2) C9 0.023(3) 0.027(3) 0.038(4) -0.012(3) -0.004(3) 0.000(2) C10 0.030(3) 0.037(3) 0.024(3) -0.002(3) -0.003(2) 0.001(2) C11 0.033(3) 0.043(3) 0.055(4) -0.017(3) -0.014(3) -0.002(3) C12 0.035(4) 0.046(5) 0.044(4) 0.008(4) -0.003(3) -0.031(4) C13 0.018(3) 0.029(3) 0.044(4) 0.008(3) 0.004(3) -0.014(3) C14 0.025(3) 0.019(2) 0.039(3) 0.004(2) 0.002(2) 0.001(2) C15 0.035(3) 0.017(2) 0.033(4) 0.007(2) 0.009(3) -0.010(3) C16 0.048(4) 0.033(3) 0.041(4) -0.007(3) 0.016(4) -0.020(3) C17 0.068(6) 0.084(6) 0.054(6) 0.030(5) -0.027(5) -0.037(5) C18 0.025(3) 0.037(3) 0.077(5) 0.006(3) 0.013(3) 0.008(3) C19 0.049(4) 0.046(4) 0.029(4) 0.005(3) 0.001(3) -0.005(3) C20 0.045(4) 0.030(3) 0.091(7) 0.000(3) 0.018(4) 0.011(3) C21 0.095(6) 0.067(5) 0.055(5) -0.030(4) 0.035(5) -0.042(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0024 0.0013 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0048 0.0027 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -0.8791 6.9422 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 Ir1 C10 87.1(3) . . ? N2 Ir1 C13 130.8(3) . . ? C10 Ir1 C13 122.5(3) . . ? N2 Ir1 C15 145.4(2) . . ? C10 Ir1 C15 110.8(3) . . ? C13 Ir1 C15 64.5(3) . . ? N2 Ir1 C14 170.0(2) . . ? C10 Ir1 C14 99.6(3) . . ? C13 Ir1 C14 39.2(2) . . ? C15 Ir1 C14 38.2(2) . . ? N2 Ir1 C16 114.1(3) . . ? C10 Ir1 C16 146.8(3) . . ? C13 Ir1 C16 63.1(3) . . ? C15 Ir1 C16 38.2(2) . . ? C14 Ir1 C16 63.5(3) . . ? N2 Ir1 C12 107.5(3) . . ? C10 Ir1 C12 161.1(3) . . ? C13 Ir1 C12 38.7(3) . . ? C15 Ir1 C12 63.5(3) . . ? C14 Ir1 C12 64.4(3) . . ? C16 Ir1 C12 36.4(3) . . ? C3 N2 Ir1 133.7(5) . . ? C3 N2 H2 118(6) . . ? Ir1 N2 H2 108(6) . . ? N2 C3 C4 118.6(6) . . ? N2 C3 C8 122.2(6) . . ? C4 C3 C8 119.1(5) . . ? C5 C4 C3 122.2(7) . . ? C5 C4 H4 118.9 . . ? C3 C4 H4 118.9 . . ? C4 C5 C6 119.0(7) . . ? C4 C5 H5 120.5 . . ? C6 C5 H5 120.5 . . ? C7 C6 C5 119.8(6) . . ? C7 C6 H6 120.1 . . ? C5 C6 H6 120.1 . . ? C6 C7 C8 123.8(8) . . ? C6 C7 H7 118.1 . . ? C8 C7 H7 118.1 . . ? C3 C8 C7 116.1(7) . . ? C3 C8 C9 122.0(5) . . ? C7 C8 C9 121.9(6) . . ? C10 C9 C8 123.9(5) . . ? C10 C9 C11 118.1(6) . . ? C8 C9 C11 118.0(5) . . ? C9 C10 Ir1 130.9(5) . . ? C9 C10 H10 111(5) . . ? Ir1 C10 H10 118(5) . . ? C9 C11 H11A 109.5 . . ? C9 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C9 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C16 C12 C13 106.3(7) . . ? C16 C12 C17 128.7(9) . . ? C13 C12 C17 125.1(9) . . ? C16 C12 Ir1 70.8(4) . . ? C13 C12 Ir1 66.5(4) . . ? C17 C12 Ir1 127.2(5) . . ? C14 C13 C12 108.6(7) . . ? C14 C13 C18 124.4(7) . . ? C12 C13 C18 126.5(8) . . ? C14 C13 Ir1 71.3(4) . . ? C12 C13 Ir1 74.8(5) . . ? C18 C13 Ir1 126.0(5) . . ? C15 C14 C13 106.9(6) . . ? C15 C14 C19 126.3(6) . . ? C13 C14 C19 126.8(6) . . ? C15 C14 Ir1 70.7(3) . . ? C13 C14 Ir1 69.5(4) . . ? C19 C14 Ir1 125.2(4) . . ? C14 C15 C16 108.3(6) . . ? C14 C15 C20 125.7(7) . . ? C16 C15 C20 125.9(7) . . ? C14 C15 Ir1 71.1(3) . . ? C16 C15 Ir1 73.4(4) . . ? C20 C15 Ir1 125.5(5) . . ? C12 C16 C15 109.7(6) . . ? C12 C16 C21 127.3(9) . . ? C15 C16 C21 122.9(8) . . ? C12 C16 Ir1 72.8(4) . . ? C15 C16 Ir1 68.4(4) . . ? C21 C16 Ir1 125.9(5) . . ? C12 C17 H17A 109.5 . . ? C12 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C12 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C13 C18 H18A 109.5 . . ? C13 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C13 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C14 C19 H19A 109.5 . . ? C14 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? C14 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C16 C21 H21A 109.5 . . ? C16 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C16 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ir1 N2 1.937(5) . ? Ir1 C10 1.972(6) . ? Ir1 C13 2.147(7) . ? Ir1 C15 2.167(6) . ? Ir1 C14 2.171(6) . ? Ir1 C16 2.233(7) . ? Ir1 C12 2.259(8) . ? N2 C3 1.366(7) . ? N2 H2 0.79(3) . ? C3 C4 1.409(9) . ? C3 C8 1.418(9) . ? C4 C5 1.369(9) . ? C4 H4 0.9400 . ? C5 C6 1.395(13) . ? C5 H5 0.9400 . ? C6 C7 1.350(13) . ? C6 H6 0.9400 . ? C7 C8 1.419(9) . ? C7 H7 0.9400 . ? C8 C9 1.439(8) . ? C9 C10 1.360(9) . ? C9 C11 1.537(8) . ? C10 H10 0.83(9) . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C11 H11C 0.9700 . ? C12 C16 1.405(12) . ? C12 C13 1.462(10) . ? C12 C17 1.485(13) . ? C13 C14 1.447(9) . ? C13 C18 1.498(9) . ? C14 C15 1.419(9) . ? C14 C19 1.490(9) . ? C15 C16 1.443(9) . ? C15 C20 1.518(10) . ? C16 C21 1.503(10) . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 H17C 0.9700 . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C18 H18C 0.9700 . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C19 H19C 0.9700 . ? C20 H20A 0.9700 . ? C20 H20B 0.9700 . ? C20 H20C 0.9700 . ? C21 H21A 0.9700 . ? C21 H21B 0.9700 . ? C21 H21C 0.9700 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ir1 N2 C3 C4 176.5(5) . . . . ? Ir1 N2 C3 C8 -2.5(9) . . . . ? N2 C3 C4 C5 -177.9(6) . . . . ? C8 C3 C4 C5 1.1(9) . . . . ? C3 C4 C5 C6 -0.4(10) . . . . ? C4 C5 C6 C7 -0.7(11) . . . . ? C5 C6 C7 C8 1.0(10) . . . . ? N2 C3 C8 C7 178.1(5) . . . . ? C4 C3 C8 C7 -0.8(8) . . . . ? N2 C3 C8 C9 -1.1(9) . . . . ? C4 C3 C8 C9 180.0(5) . . . . ? C6 C7 C8 C3 -0.2(9) . . . . ? C6 C7 C8 C9 179.0(6) . . . . ? C3 C8 C9 C10 3.1(9) . . . . ? C7 C8 C9 C10 -176.1(6) . . . . ? C3 C8 C9 C11 -178.1(5) . . . . ? C7 C8 C9 C11 2.7(8) . . . . ? C8 C9 C10 Ir1 -1.7(10) . . . . ? C11 C9 C10 Ir1 179.5(5) . . . . ? C16 C12 C13 C14 -3.9(7) . . . . ? C17 C12 C13 C14 176.1(7) . . . . ? Ir1 C12 C13 C14 -63.8(4) . . . . ? C16 C12 C13 C18 -176.2(6) . . . . ? C17 C12 C13 C18 3.8(10) . . . . ? Ir1 C12 C13 C18 123.9(7) . . . . ? C16 C12 C13 Ir1 60.0(4) . . . . ? C17 C12 C13 Ir1 -120.0(7) . . . . ? C12 C13 C14 C15 4.9(7) . . . . ? C18 C13 C14 C15 177.4(6) . . . . ? Ir1 C13 C14 C15 -61.2(4) . . . . ? C12 C13 C14 C19 -174.6(6) . . . . ? C18 C13 C14 C19 -2.1(10) . . . . ? Ir1 C13 C14 C19 119.3(6) . . . . ? C12 C13 C14 Ir1 66.1(5) . . . . ? C18 C13 C14 Ir1 -121.4(6) . . . . ? C13 C14 C15 C16 -4.0(7) . . . . ? C19 C14 C15 C16 175.5(6) . . . . ? Ir1 C14 C15 C16 -64.4(4) . . . . ? C13 C14 C15 C20 -178.9(6) . . . . ? C19 C14 C15 C20 0.6(10) . . . . ? Ir1 C14 C15 C20 120.7(7) . . . . ? C13 C14 C15 Ir1 60.4(4) . . . . ? C19 C14 C15 Ir1 -120.1(6) . . . . ? C13 C12 C16 C15 1.4(7) . . . . ? C17 C12 C16 C15 -178.6(7) . . . . ? Ir1 C12 C16 C15 58.6(5) . . . . ? C13 C12 C16 C21 -179.6(6) . . . . ? C17 C12 C16 C21 0.4(12) . . . . ? Ir1 C12 C16 C21 -122.4(7) . . . . ? C13 C12 C16 Ir1 -57.2(4) . . . . ? C17 C12 C16 Ir1 122.8(8) . . . . ? C14 C15 C16 C12 1.7(7) . . . . ? C20 C15 C16 C12 176.6(6) . . . . ? Ir1 C15 C16 C12 -61.3(5) . . . . ? C14 C15 C16 C21 -177.4(6) . . . . ? C20 C15 C16 C21 -2.5(10) . . . . ? Ir1 C15 C16 C21 119.7(7) . . . . ? C14 C15 C16 Ir1 62.9(4) . . . . ? C20 C15 C16 Ir1 -122.2(7) . . . . ?