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Information card for entry 7132131
Preview
| Coordinates | 7132131.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C53 H67 N3 Pd |
|---|---|
| Calculated formula | C53 H67 N3 Pd |
| Title of publication | Swift C–C Bond Insertion by a 12-Electron Palladium(0) Surrogate |
| Authors of publication | Breitwieser, Kevin; Dankert, Fabian; Gruenwald, Annette; Mayer, Paula R.; Heinemann, Frank; Munz, Dominik |
| Journal of publication | Chemical Communications |
| Year of publication | 2023 |
| a | 21.1187 ± 0.0008 Å |
| b | 13.1872 ± 0.0006 Å |
| c | 32.3582 ± 0.0013 Å |
| α | 90° |
| β | 103.994 ± 0.002° |
| γ | 90° |
| Cell volume | 8744.2 ± 0.6 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0689 |
| Residual factor for significantly intense reflections | 0.066 |
| Weighted residual factors for significantly intense reflections | 0.1356 |
| Weighted residual factors for all reflections included in the refinement | 0.1364 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.474 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 286338 (current) | 2023-09-15 | cif/ Adding structures of 7132127, 7132128, 7132129, 7132130, 7132131 via cif-deposit CGI script. |
7132131.cif |
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