#------------------------------------------------------------------------------ #$Date: 2023-09-19 00:58:28 +0300 (Tue, 19 Sep 2023) $ #$Revision: 286389 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/13/21/7132141.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7132141 loop_ _publ_author_name 'Eichelmann, Robert' 'Rippel, Daniel' 'Ballmann, Joachim' 'Gade, Lutz H.' _publ_section_title ; Zipping up Tetraazaperylene: Synthesis of Tetraazacoronenes via Double Coupling in the Bay Positions ; _journal_name_full 'Chemical Communications' _journal_paper_doi 10.1039/D3CC04113A _journal_year 2023 _chemical_formula_moiety 'C74 H80 N8 O6, 1[CH2Cl2], 1[CH3OH], 0.5[OH2]' _chemical_formula_sum 'C76 H87 Cl2 N8 O7.5' _chemical_formula_weight 1303.43 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-08-15 _audit_creation_method ; Olex2 1.5 (compiled 2023.03.06 svn.rbb2c1857 for OlexSys, GUI svn.r6748) ; _audit_update_record ; 2023-08-23 deposited with the CCDC. 2023-09-18 downloaded from the CCDC. ; _cell_angle_alpha 106.6270(10) _cell_angle_beta 96.5330(10) _cell_angle_gamma 91.8250(10) _cell_formula_units_Z 2 _cell_length_a 13.3834(2) _cell_length_b 15.0836(2) _cell_length_c 17.5480(2) _cell_measurement_reflns_used 30195 _cell_measurement_temperature 120(1) _cell_measurement_theta_max 70.8230 _cell_measurement_theta_min 3.9720 _cell_volume 3364.53(8) _computing_cell_refinement 'CrysAlisPro 1.171.42.51a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.51a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.51a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 120(1) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 7.9621 _diffrn_detector_type Eos _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.983 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -22.00 54.00 1.00 4.00 -- 0.00 46.00-120.00 76 2 \w -59.00 -22.00 1.00 4.00 -- 0.00 -46.00 90.00 37 3 \w 54.00 79.00 1.00 8.00 -- 54.49 46.00-120.00 25 4 \w -16.00 78.00 1.00 8.00 -- 54.49 -46.00 90.00 94 5 \w 108.00 133.00 1.00 16.00 -- 108.98 46.00-120.00 25 6 \w 46.00 132.00 1.00 16.00 -- 108.98 -46.00 90.00 86 7 \w -19.00 23.00 1.00 4.00 -- 0.00 -46.00 90.00 42 8 \w -17.00 13.00 1.00 4.00 -- 0.00 57.00 120.00 30 9 \w 17.00 68.00 1.00 4.00 -- 0.00 57.00 120.00 51 10 \w -40.00 -1.00 1.00 4.00 -- 0.00 -77.00 60.00 39 11 \w -19.00 29.00 1.00 4.00 -- 0.00 57.00 -90.00 48 12 \w 33.00 66.00 1.00 4.00 -- 0.00 57.00 -90.00 33 13 \w -24.00 8.00 1.00 4.00 -- 18.00 104.00 84.13 32 14 \w -8.00 17.00 1.00 8.00 -- 34.00 102.00 -96.28 25 15 \w 6.00 31.00 1.00 8.00 -- 42.00 88.00-147.12 25 16 \w 6.00 31.00 1.00 8.00 -- 42.00 88.00 7.05 25 17 \w 6.00 31.00 1.00 8.00 -- 42.00 88.00 121.09 25 18 \w 13.00 38.00 1.00 8.00 -- 46.00 83.00 -80.95 25 19 \w 15.00 43.00 1.00 8.00 -- 46.00 82.00 133.44 28 20 \w 12.00 37.00 1.00 8.00 -- 46.00 84.00 -44.64 25 21 \w 13.00 38.00 1.00 8.00 -- 46.00 83.00 9.86 25 22 \w 17.00 44.00 1.00 8.00 -- 46.00 79.00 178.07 27 23 \w 14.00 39.00 1.00 8.00 -- 46.00 81.00 104.51 25 24 \w 18.00 43.00 1.00 8.00 -- 50.00 80.00-118.04 25 25 \w 19.00 44.00 1.00 8.00 -- 50.00 79.00 159.41 25 26 \w 17.00 42.00 1.00 8.00 -- 50.00 82.00 -45.67 25 27 \w 18.00 43.00 1.00 8.00 -- 50.00 81.00 57.07 25 28 \w 18.00 43.00 1.00 8.00 -- 50.00 80.00-152.97 25 29 \w 61.00 110.00 1.00 8.00 -- 54.49-125.00 90.00 49 30 \w 24.00 51.00 1.00 8.00 -- 54.49 77.00 120.00 27 31 \w 24.00 51.00 1.00 8.00 -- 54.49 77.00-150.00 27 32 \w -15.00 84.00 1.00 8.00 -- 54.49 -77.00-120.00 99 33 \w 29.00 56.00 1.00 8.00 -- 54.49 77.00-180.00 27 34 \w 25.00 51.00 1.00 8.00 -- 54.49 77.00 0.00 26 35 \w -14.00 76.00 1.00 8.00 -- 54.49 -57.00 0.00 90 36 \w 27.00 54.00 1.00 8.00 -- 54.49 77.00 -30.00 27 37 \w 43.00 70.00 1.00 8.00 -- 54.49-125.00 -90.00 27 38 \w 29.00 56.00 1.00 8.00 -- 58.00 77.00 19.28 27 39 \w 28.00 57.00 1.00 8.00 -- 58.00 77.00 55.96 29 40 \w 30.00 55.00 1.00 8.00 -- 58.00 76.00-118.86 25 41 \w 30.00 57.00 1.00 8.00 -- 58.00 77.00 -93.77 27 42 \w 28.00 55.00 1.00 8.00 -- 58.00 77.00 -70.76 27 43 \w 31.00 56.00 1.00 8.00 -- 58.00 73.00-158.93 25 44 \w 30.00 55.00 1.00 8.00 -- 58.00 76.00 78.27 25 45 \w 79.00 107.00 1.00 8.00 -- 58.00 77.00 19.28 28 46 \w 28.00 55.00 1.00 8.00 -- 58.00 77.00 90.62 27 47 \w 30.00 57.00 1.00 8.00 -- 58.00 77.00-107.97 27 48 \w 30.00 55.00 1.00 8.00 -- 58.00 75.00 91.04 25 49 \w 33.00 69.00 1.00 8.00 -- 62.00 75.00 -57.80 36 50 \w 34.00 59.00 1.00 8.00 -- 62.00 76.00 109.37 25 51 \w 34.00 64.00 1.00 8.00 -- 62.00 75.00 -16.06 30 52 \w 36.00 63.00 1.00 8.00 -- 62.00 76.00 -38.29 27 53 \w 33.00 59.00 1.00 8.00 -- 62.00 76.00-157.65 26 54 \w 33.00 59.00 1.00 8.00 -- 62.00 76.00 160.77 26 55 \w 34.00 61.00 1.00 8.00 -- 62.00 77.00 21.69 27 56 \w 35.00 62.00 1.00 8.00 -- 62.00 77.00 -3.94 27 57 \w 33.00 60.00 1.00 8.00 -- 62.00 77.00-148.38 27 58 \w 41.00 68.00 1.00 8.00 -- 62.00 70.00 -78.30 27 59 \w 38.00 65.00 1.00 8.00 -- 66.00 76.00 62.52 27 60 \w 43.00 75.00 1.00 8.00 -- 66.00 67.00 2.52 32 61 \w 36.00 63.00 1.00 8.00 -- 66.00 77.00 6.66 27 62 \w 37.00 62.00 1.00 8.00 -- 66.00 77.00 163.87 25 63 \w 43.00 70.00 1.00 8.00 -- 66.00 76.00-144.44 27 64 \w 37.00 81.00 1.00 8.00 -- 66.00 76.00 125.96 44 65 \w 40.00 67.00 1.00 8.00 -- 66.00 74.00-114.67 27 66 \w 43.00 70.00 1.00 8.00 -- 70.00 71.00 81.30 27 67 \w 40.00 67.00 1.00 8.00 -- 70.00 77.00 133.99 27 68 \w 45.00 77.00 1.00 8.00 -- 70.00 72.00 -66.88 32 69 \w 47.00 72.00 1.00 8.00 -- 70.00 67.00-113.69 25 70 \w 48.00 73.00 1.00 8.00 -- 70.00 64.00-117.32 25 71 \w 111.00 139.00 1.00 8.00 -- 70.00 75.00 41.97 28 72 \w 46.00 73.00 1.00 8.00 -- 70.00 73.00-105.45 27 73 \w 44.00 70.00 1.00 8.00 -- 70.00 71.00 -37.24 26 74 \w 43.00 70.00 1.00 8.00 -- 70.00 73.00 -52.37 27 75 \w 42.00 100.00 1.00 8.00 -- 70.00 75.00 41.97 58 76 \w 47.00 74.00 1.00 8.00 -- 74.00 75.00 -15.13 27 77 \w 47.00 78.00 1.00 8.00 -- 74.00 73.00-173.14 31 78 \w 44.00 128.00 1.00 8.00 -- 74.00 77.00 126.48 84 79 \w 46.00 73.00 1.00 8.00 -- 74.00 77.00 -41.52 27 80 \w 47.00 103.00 1.00 8.00 -- 74.00 73.00 26.19 56 81 \w 44.00 71.00 1.00 8.00 -- 74.00 77.00 75.11 27 82 \w 45.00 79.00 1.00 8.00 -- 74.00 76.00 -2.19 34 83 \w 52.00 78.00 1.00 8.00 -- 74.00 48.00-107.15 26 84 \w 50.00 79.00 1.00 8.00 -- 74.00 67.00 179.41 29 85 \w 50.00 75.00 1.00 8.00 -- 74.00 69.00 -90.68 25 86 \w 56.00 85.00 1.00 8.00 -- 74.00 56.00 66.77 29 87 \w 45.00 71.00 1.00 8.00 -- 74.00 76.00-126.45 26 88 \w 57.00 90.00 1.00 8.00 -- 78.00 68.00 95.60 33 89 \w 57.00 102.00 1.00 8.00 -- 78.00 66.00-169.62 45 90 \w 50.00 77.00 1.00 8.00 -- 78.00 76.00 -61.68 27 91 \w 54.00 117.00 1.00 8.00 -- 78.00 68.00-114.54 63 92 \w 49.00 76.00 1.00 8.00 -- 78.00 76.00 7.23 27 93 \w 53.00 82.00 1.00 16.00 -- 82.00 77.00 -38.63 29 94 \w 61.00 87.00 1.00 16.00 -- 82.00 43.00 -75.98 26 95 \w 52.00 78.00 1.00 16.00 -- 82.00 77.00 -89.59 26 96 \w 59.00 149.00 1.00 16.00 -- 82.00 68.00 -66.30 90 97 \w 61.00 88.00 1.00 16.00 -- 82.00 61.00 26.63 27 98 \w 65.00 92.00 1.00 16.00 -- 86.00 57.00 62.48 27 99 \w 58.00 130.00 1.00 16.00 -- 86.00 73.00 93.86 72 100 \w 59.00 95.00 1.00 16.00 -- 86.00 74.00 -36.43 36 101 \w 64.00 105.00 1.00 16.00 -- 86.00 62.00-127.42 41 102 \w 62.00 89.00 1.00 16.00 -- 86.00 72.00 155.48 27 103 \w 60.00 116.00 1.00 16.00 -- 86.00 75.00 -2.38 56 104 \w 58.00 87.00 1.00 16.00 -- 86.00 73.00 -16.61 29 105 \w 64.00 90.00 1.00 16.00 -- 86.00 48.00 74.10 26 106 \w 62.00 96.00 1.00 16.00 -- 90.00 73.00 112.60 34 107 \w 61.00 87.00 1.00 16.00 -- 90.00 75.00 -18.93 26 108 \w 64.00 90.00 1.00 16.00 -- 90.00 73.00 135.31 26 109 \w 61.00 91.00 1.00 16.00 -- 90.00 75.00 179.14 30 110 \w 61.00 86.00 1.00 16.00 -- 90.00 77.00 -50.07 25 111 \w 62.00 90.00 1.00 16.00 -- 90.00 76.00 -67.19 28 112 \w 61.00 88.00 1.00 16.00 -- 90.00 75.00 -91.34 27 113 \w 67.00 151.00 1.00 16.00 -- 90.00 67.00 -93.24 84 114 \w 63.00 98.00 1.00 16.00 -- 90.00 72.00 151.32 35 115 \w 64.00 96.00 1.00 16.00 -- 90.00 72.00 69.30 32 116 \w 69.00 105.00 1.00 16.00 -- 98.00 75.00 -85.05 36 117 \w 143.00 168.00 1.00 16.00 -- 98.00 76.00 -8.91 25 118 \w 69.00 123.00 1.00 16.00 -- 98.00 76.00 -8.91 54 119 \w 72.00 100.00 1.00 16.00 -- 98.00 71.00 -62.00 28 120 \w 77.00 110.00 1.00 16.00 -- 98.00 56.00 108.78 33 121 \w 74.00 109.00 1.00 16.00 -- 98.00 69.00 56.88 35 122 \w 71.00 166.00 1.00 16.00 -- 98.00 73.00 115.55 95 123 \w 78.00 111.00 1.00 16.00 -- 98.00 54.00 -19.32 33 124 \w 80.00 122.00 1.00 16.00 -- 98.00 63.00 72.73 42 125 \w 73.00 108.00 1.00 16.00 -- 102.00 77.00 -65.63 35 126 \w 82.00 168.00 1.00 16.00 -- 102.00 64.00 -27.36 86 127 \w 80.00 170.00 1.00 16.00 -- 102.00 49.00 111.35 90 128 \w 86.00 171.00 1.00 16.00 -- 106.00 57.00-164.64 85 129 \w 87.00 112.00 1.00 16.00 -- 108.98 64.00-180.00 25 130 \w 80.00 105.00 1.00 16.00 -- 108.98 77.00 0.00 25 131 \w 80.00 159.00 1.00 16.00 -- 108.98 77.00-120.00 79 132 \w 87.00 112.00 1.00 16.00 -- 108.98 64.00 90.00 25 133 \w 86.00 175.00 1.00 16.00 -- 108.98 64.00 60.00 89 134 \w 37.00 96.00 1.00 16.00 -- 108.98 -92.00 120.00 59 135 \w 100.00 168.00 1.00 16.00 -- 108.98 64.00 -90.00 68 136 \w 79.00 105.00 1.00 16.00 -- 108.98 77.00-150.00 26 137 \w 148.00 175.00 1.00 16.00 -- 108.98 77.00 30.00 27 138 \w 79.00 105.00 1.00 16.00 -- 108.98 77.00 30.00 26 139 \w 139.00 166.00 1.00 16.00 -- 108.98 76.00 133.45 27 140 \w 90.00 132.00 1.00 16.00 -- 108.98 -64.00 -30.00 42 141 \w 86.00 175.00 1.00 16.00 -- 108.98 64.00 30.00 89 142 \w 86.00 112.00 1.00 16.00 -- 108.98 64.00-120.00 26 143 \w 80.00 105.00 1.00 16.00 -- 108.98 76.00 133.45 25 144 \w 42.00 68.00 1.00 16.00 -- 108.98 -64.00 -30.00 26 145 \w 125.00 159.00 1.00 16.00 -- 108.98 111.00 90.00 34 146 \w 61.00 106.00 1.00 16.00 -- 108.98-111.00-150.00 45 147 \w 79.00 105.00 1.00 16.00 -- 108.98 77.00 -30.00 26 148 \w 84.00 113.00 1.00 16.00 -- 108.98-111.00 90.00 29 149 \w 82.00 164.00 1.00 16.00 -- 108.98 77.00 -60.00 82 150 \w 87.00 154.00 1.00 16.00 -- 108.98 63.00 22.41 67 151 \w 82.00 109.00 1.00 16.00 -- 108.98 77.00 120.00 27 152 \w 86.00 176.00 1.00 16.00 -- 108.98 64.00-150.00 90 153 \w 137.00 167.00 1.00 16.00 -- 108.98 77.00 60.00 30 154 \w 37.00 100.00 1.00 16.00 -- 108.98 -92.00-120.00 63 155 \w 126.00 153.00 1.00 16.00 -- 108.98 77.00 90.00 27 156 \w 79.00 105.00 1.00 16.00 -- 108.98 77.00 60.00 26 157 \w 79.00 105.00 1.00 16.00 -- 108.98 77.00 90.00 26 158 \w 83.00 135.00 1.00 16.00 -- 108.98 38.00-120.00 52 159 \w 145.00 173.00 1.00 16.00 -- 108.98 77.00-180.00 28 160 \w 83.00 110.00 1.00 16.00 -- 108.98 77.00 150.00 27 161 \w 38.00 109.00 1.00 16.00 -- 108.98 -92.00 -60.00 71 162 \w 78.00 112.00 1.00 16.00 -- 108.98-111.00 -60.00 34 163 \w 89.00 175.00 1.00 16.00 -- 108.98 64.00 150.00 86 164 \w 87.00 128.00 1.00 16.00 -- 108.98 64.00 120.00 41 165 \w 88.00 147.00 1.00 16.00 -- 108.98 64.00 0.00 59 166 \w 79.00 106.00 1.00 16.00 -- 108.98 77.00-180.00 27 167 \w 41.00 91.00 1.00 16.00 -- 108.98-111.00 60.00 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, Eos' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0194145000 _diffrn_orient_matrix_UB_12 -0.0672617000 _diffrn_orient_matrix_UB_13 0.0508047000 _diffrn_orient_matrix_UB_21 0.1116555000 _diffrn_orient_matrix_UB_22 0.0003767000 _diffrn_orient_matrix_UB_23 -0.0137343000 _diffrn_orient_matrix_UB_31 0.0253366000 _diffrn_orient_matrix_UB_32 0.0830050000 _diffrn_orient_matrix_UB_33 0.0759304000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0691 _diffrn_reflns_av_unetI/netI 0.0339 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.983 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 97860 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.983 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 71.228 _diffrn_reflns_theta_min 3.331 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.369 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.659 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.51a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour red _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.287 _exptl_crystal_description needle _exptl_crystal_F_000 1386 _exptl_crystal_size_max 0.22 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.06 _refine_diff_density_max 0.564 _refine_diff_density_min -0.337 _refine_diff_density_rms 0.051 _refine_ls_extinction_coef 0.00176(16) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.027 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 926 _refine_ls_number_reflns 12847 _refine_ls_number_restraints 375 _refine_ls_restrained_S_all 1.021 _refine_ls_R_factor_all 0.0667 _refine_ls_R_factor_gt 0.0566 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0730P)^2^+2.0668P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1470 _refine_ls_wR_factor_ref 0.1546 _reflns_Friedel_coverage 0.000 _reflns_number_gt 10532 _reflns_number_total 12847 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3cc04113a2.cif _cod_data_source_block compd_2c_ga_re39 _cod_original_formula_sum 'C76 H87 Cl2 N8 O7.50' _cod_database_code 7132141 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C74 H80 N8 O6 (CH2Cl2)(OH2)(CH3OH)' _chemical_oxdiff_usercomment 're615, needle, red' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.922 _shelx_estimated_absorpt_t_min 0.753 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups, All C(H,H,H,H) groups, All C(H,H,H,H,H, H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C24-C25A \\sim C24-C25B with sigma of 0.02 C27A-C27C \\sim C27B-C27C with sigma of 0.02 C27A-C28C \\sim C27B-C28C with sigma of 0.02 C28A-C27C \\sim C28B-C27C with sigma of 0.02 C28A-C28C \\sim C28B-C28C with sigma of 0.02 C25A-C26A \\sim C25B-C26B with sigma of 0.02 C27A-C26A \\sim C27A-C26B with sigma of 0.02 C24-C26A \\sim C24-C26B with sigma of 0.02 C25A-C27A \\sim C25B-C27A with sigma of 0.02 C27A-C26A \\sim C27B-C26A with sigma of 0.02 C27A-C28A \\sim C27B-C28A with sigma of 0.02 C27A-C26B \\sim C27B-C26B with sigma of 0.02 C27A-C28A \\sim C27A-C28B with sigma of 0.02 C28A-C27B \\sim C28B-C27B with sigma of 0.02 C25A-C24 \\sim C24-C25C with sigma of 0.02 C25C-C24 \\sim C24-C25B with sigma of 0.02 C25B-C26B \\sim C25C-C26C \\sim C25A-C26A with sigma of 0.02 C26A-C27A \\sim C26B-C27B \\sim C26C-C27C with sigma of 0.02 C27A-C28A \\sim C27C-C28C \\sim C27B-C28B with sigma of 0.02 C32-C33 \\sim C33-C34 with sigma of 0.02 C29-C30 \\sim C29-C30A with sigma of 0.02 C30-C31 \\sim C30A-C31A with sigma of 0.02 C31-C32 \\sim C31A-C32A with sigma of 0.02 C32-C33 \\sim C32A-C33A with sigma of 0.02 C33-C34 \\sim C33A-C34A with sigma of 0.02 C29-C31 \\sim C29-C31A with sigma of 0.02 C30-C32 \\sim C30A-C32A with sigma of 0.02 C31-C33 \\sim C31A-C33A with sigma of 0.02 C32-C34 \\sim C32A-C34A with sigma of 0.02 3. Uiso/Uaniso restraints and constraints C25A \\sim C25C \\sim C25B \\sim C26B \\sim C26C \\sim C26A \\sim C27A \\sim C27B \\sim C27C \\sim C28B \\sim C28C \\sim C28A: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A C23 \\sim C24 \\sim C25A \\sim C25C \\sim C25B: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A C30 \\sim C31 \\sim C32 \\sim C33 \\sim C34: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 within 2A C30A \\sim C30 \\sim C29 \\sim C31A \\sim C32A \\sim C32 \\sim C34A \\sim C33A \\sim C33 \\sim C34: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02 within 2A 4. Others 1*[Sof(H24A)+Sof(H24B)+Sof(C25A)+Sof(H25A)+Sof(H25B)+Sof(C26A)+Sof(H26E)+ Sof(H26F)+Sof(C27A)+Sof(H27A)+Sof(H27B)+Sof(C28A)+Sof(H28G)+Sof(H28H)+ Sof(H28I)]+1*[Sof(H24C)+Sof(H24D)+Sof(C25B)+Sof(H25E)+Sof(H25F)+Sof(C26B)+ Sof(H26A)+Sof(H26B)+Sof(C27B)+Sof(H27C)+Sof(H27D)+Sof(C28B)+Sof(H28A)+ Sof(H28B)+Sof(H28C)]+1*[Sof(H24E)+Sof(H24F)+Sof(C25C)+Sof(H25C)+Sof(H25D)+ Sof(C26C)+Sof(H26C)+Sof(H26D)+Sof(C27C)+Sof(H27E)+Sof(H27F)+Sof(C28C)+ Sof(H28D)+Sof(H28E)+Sof(H28F)]=1 with esd of 0.0001 Sof(H24A)=Sof(H24B)=Sof(C25A)=Sof(H25A)=Sof(H25B)=Sof(C26A)=Sof(H26E)= Sof(H26F)=Sof(C27A)=Sof(H27A)=Sof(H27B)=Sof(C28A)=Sof(H28G)=Sof(H28H)= Sof(H28I)=FVAR(1) Sof(H24C)=Sof(H24D)=Sof(C25B)=Sof(H25E)=Sof(H25F)=Sof(C26B)=Sof(H26A)= Sof(H26B)=Sof(C27B)=Sof(H27C)=Sof(H27D)=Sof(C28B)=Sof(H28A)=Sof(H28B)= Sof(H28C)=FVAR(2) Sof(H24E)=Sof(H24F)=Sof(C25C)=Sof(H25C)=Sof(H25D)=Sof(C26C)=Sof(H26C)= Sof(H26D)=Sof(C27C)=Sof(H27E)=Sof(H27F)=Sof(C28C)=Sof(H28D)=Sof(H28E)= Sof(H28F)=FVAR(3) Sof(H29C)=Sof(H29D)=Sof(C30A)=Sof(H30C)=Sof(H30D)=Sof(C31A)=Sof(H31C)= Sof(H31D)=Sof(C32A)=Sof(H32C)=Sof(H32D)=Sof(C33A)=Sof(H33C)=Sof(H33D)= Sof(C34A)=Sof(H34D)=Sof(H34E)=Sof(H34F)=1-FVAR(4) Sof(H29A)=Sof(H29B)=Sof(C30)=Sof(H30A)=Sof(H30B)=Sof(C31)=Sof(H31A)=Sof(H31B)= Sof(C32)=Sof(H32A)=Sof(H32B)=Sof(C33)=Sof(H33A)=Sof(H33B)=Sof(C34)=Sof(H34A)= Sof(H34B)=Sof(H34C)=FVAR(4) 5.a Secondary CH2 refined with riding coordinates: C23(H23A,H23B), C24(H24A,H24B), C24(H24E,H24F), C24(H24C,H24D), C25A(H25A, H25B), C25C(H25C,H25D), C25B(H25E,H25F), C26B(H26A,H26B), C26C(H26C,H26D), C26A(H26E,H26F), C27A(H27A,H27B), C27B(H27C,H27D), C27C(H27E,H27F), C29(H29A, H29B), C29(H29C,H29D), C30(H30A,H30B), C31(H31A,H31B), C32(H32A,H32B), C33(H33A,H33B), C35(H35A,H35B), C36(H36A,H36B), C37(H37A,H37B), C38(H38A,H38B), C39(H39A,H39B), C41(H41A,H41B), C42(H42A,H42B), C43(H43A,H43B), C44(H44A, H44B), C45(H45A,H45B), C30A(H30C,H30D), C31A(H31C,H31D), C32A(H32C,H32D), C33A(H33C,H33D) 5.b Aromatic/amide H refined with riding coordinates: C48(H48), C49(H49), C51(H51), C52(H52), C55(H55), C56(H56), C58(H58), C59(H59), C62(H62), C63(H63), C65(H65), C66(H66), C69(H69), C70(H70), C72(H72), C73(H73) 5.c Idealised Me refined as rotating group: C28B(H28A,H28B,H28C), C28C(H28D,H28E,H28F), C28A(H28G,H28H,H28I), C34(H34A, H34B,H34C), C40(H40A,H40B,H40C), C46(H46A,H46B,H46C), C53(H53A,H53B,H53C), C60(H60A,H60B,H60C), C67(H67A,H67B,H67C), C74(H74A,H74B,H74C), C34A(H34D,H34E, H34F) ; _smtbx_masks_special_details ; A solvent mask was calculated and 131 electrons were found in a volume of 698\%A^3^ in 1 void per unit cell. This is consistent with the presence of 1[CH2Cl2], 1[CH3OH], 0.5[OH2] per Asymmetric Unit which account for 130 electrons per unit cell. ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 3.0 _shelx_res_file ; TITL ga_re39_a.res in P-1 ga_re39.res created by SHELXL-2018/3 at 15:02:43 on 15-Aug-2023 REM Old TITL ga_re39 in P-1 REM SHELXT solution in P-1: R1 0.198, Rweak 0.008, Alpha 0.054 CELL 1.54184 13.3834 15.0836 17.548 106.627 96.533 91.825 ZERR 2 0.0002 0.0002 0.0002 0.001 0.001 0.001 LATT 1 SFAC C H Cl N O UNIT 152 174 4 16 15 SADI C24 C25A C24 C25B SADI C27A C27C C27B C27C SADI C27A C28C C27B C28C SADI C28A C27C C28B C27C SADI C28A C28C C28B C28C SADI C25A C26A C25B C26B SADI C27A C26A C27A C26B SADI C24 C26A C24 C26B SADI C25A C27A C25B C27A SADI C27A C26A C27B C26A SADI C27A C28A C27B C28A SADI C27A C26B C27B C26B SADI C27A C28A C27A C28B SADI C28A C27B C28B C27B SADI C25A C24 C24 C25C SADI C25C C24 C24 C25B SADI C25B C26B C25C C26C C25A C26A SADI C26A C27A C26B C27B C26C C27C SADI C27A C28A C27C C28C C27B C28B SIMU 0.01 0.02 2 C25A > C28A SIMU C23 > C25B SIMU C30 > C34 SADI C32 C33 C33 C34 SADI C29 C30 C29 C30A SADI C30 C31 C30A C31A SADI C31 C32 C31A C32A SADI C32 C33 C32A C33A SADI C33 C34 C33A C34A SADI C29 C31 C29 C31A SADI C30 C32 C30A C32A SADI C31 C33 C31A C33A SADI C32 C34 C32A C34A SIMU 0.01 0.02 2 C30A C30 C29 C31A C32A C32 C34A C33A C33 C34 SUMP 1 0.0001 1 2 1 3 1 4 L.S. 10 0 0 PLAN 15 SIZE 0.06 0.08 0.22 TEMP -153.1(10) CONF list 4 BOND $H ABIN more -3 fmap 2 53 acta OMIT 0 -1 1 OMIT 0 1 0 OMIT 2 -3 2 REM REM REM WGHT 0.073000 2.066800 EXTI 0.001764 FVAR 3.32773 0.68838 0.15152 0.16010 0.80830 O1 5 1.043803 0.809065 0.564394 11.00000 0.03275 0.04289 = 0.03736 0.01054 0.00316 -0.01091 O2 5 0.252757 0.260393 0.614270 11.00000 0.02656 0.02946 = 0.03400 0.00480 0.00529 -0.00155 O3 5 0.914117 0.298557 0.110549 11.00000 0.02883 0.04936 = 0.02670 0.00673 0.00950 0.01217 O4 5 0.570511 -0.024757 0.193773 11.00000 0.05304 0.02856 = 0.05086 -0.00816 0.01563 0.00242 O5 5 0.846745 0.987637 1.073329 11.00000 0.08485 0.03690 = 0.04078 -0.00366 -0.02342 -0.00569 O6 5 0.405730 0.719560 1.079263 11.00000 0.04633 0.07461 = 0.02714 0.00616 0.01482 0.00774 N1 4 0.935001 0.683079 0.504283 11.00000 0.02226 0.03264 = 0.02631 0.00779 0.00102 -0.00090 N2 4 0.932606 0.772390 0.640858 11.00000 0.02144 0.02839 = 0.02685 0.00604 -0.00029 -0.00034 N3 4 0.829003 0.547884 0.446283 11.00000 0.02163 0.02716 = 0.02463 0.00619 0.00188 0.00423 N4 4 0.812086 0.739206 0.717335 11.00000 0.02016 0.02522 = 0.02450 0.00465 -0.00016 0.00299 N5 4 0.501347 0.316634 0.469389 11.00000 0.02303 0.02199 = 0.02413 0.00183 0.00294 0.00434 N6 4 0.477187 0.513167 0.737323 11.00000 0.02094 0.02384 = 0.02435 0.00296 0.00303 0.00472 N7 4 0.371703 0.290844 0.540801 11.00000 0.02225 0.02203 = 0.02415 0.00158 0.00226 0.00234 N8 4 0.360529 0.386824 0.673952 11.00000 0.02245 0.02390 = 0.02483 0.00312 0.00387 0.00275 C15 1 0.974501 0.757509 0.569292 11.00000 0.02294 0.03264 = 0.03161 0.01085 0.00022 -0.00048 C2 1 0.858297 0.620620 0.508243 11.00000 0.01889 0.02829 = 0.02518 0.00804 0.00127 0.00343 C3 1 0.815574 0.642384 0.581462 11.00000 0.02149 0.02414 = 0.02444 0.00674 0.00158 0.00550 C4 1 0.850938 0.718169 0.648892 11.00000 0.01833 0.02379 = 0.02660 0.00647 -0.00136 0.00427 C5 1 0.721207 0.402723 0.390564 11.00000 0.02360 0.02641 = 0.02297 0.00575 0.00283 0.00749 C6 1 0.751455 0.488605 0.452584 11.00000 0.02063 0.02577 = 0.02310 0.00532 0.00199 0.00523 C8 1 0.733344 0.587178 0.585878 11.00000 0.02084 0.02296 = 0.02383 0.00591 0.00209 0.00583 C9 1 0.688426 0.609659 0.657932 11.00000 0.02043 0.02380 = 0.02193 0.00348 0.00124 0.00491 C10 1 0.729437 0.684499 0.722446 11.00000 0.01867 0.02352 = 0.02526 0.00463 -0.00006 0.00451 C11 1 0.683891 0.701820 0.795764 11.00000 0.02130 0.02571 = 0.02361 0.00297 0.00094 0.00554 C12 1 0.600563 0.645383 0.800293 11.00000 0.02328 0.02579 = 0.02074 0.00222 0.00100 0.00586 C13 1 0.559402 0.568575 0.732843 11.00000 0.01933 0.02474 = 0.02482 0.00421 0.00205 0.00507 C14 1 0.605837 0.552578 0.662924 11.00000 0.02122 0.02390 = 0.02232 0.00329 0.00146 0.00501 C16 1 0.617519 0.452293 0.525477 11.00000 0.02142 0.02346 = 0.02362 0.00397 0.00238 0.00441 C17 1 0.583871 0.370956 0.464563 11.00000 0.02131 0.02312 = 0.02352 0.00409 0.00237 0.00458 C18 1 0.642009 0.343322 0.397987 11.00000 0.02316 0.02577 = 0.02068 0.00451 0.00083 0.00765 C19 1 0.456761 0.342520 0.534998 11.00000 0.01996 0.02273 = 0.02323 0.00392 0.00113 0.00429 C20 1 0.489804 0.419764 0.601651 11.00000 0.02052 0.02267 = 0.02301 0.00345 0.00152 0.00532 C21 1 0.444443 0.443536 0.673875 11.00000 0.01936 0.02315 = 0.02386 0.00488 0.00163 0.00417 C22 1 0.324912 0.309900 0.610215 11.00000 0.02001 0.02398 = 0.02719 0.00571 0.00249 0.00422 C23 1 0.973198 0.674564 0.427368 11.00000 0.03186 0.05058 = 0.02702 0.01089 0.00298 -0.00946 AFIX 23 H23A 2 0.996127 0.737078 0.425999 11.00000 -1.20000 H23B 2 0.917039 0.650626 0.383487 11.00000 -1.20000 AFIX 0 C24 1 1.057954 0.612542 0.411888 11.00000 0.03616 0.06490 = 0.03998 0.00206 0.01238 0.00115 PART 1 AFIX 23 H24A 2 1.037314 0.549186 0.412562 21.00000 -1.20000 H24B 2 1.117104 0.636845 0.452912 21.00000 -1.20000 AFIX 23 PART 3 H24E 2 1.031425 0.552090 0.415579 41.00000 -1.20000 H24F 2 1.109518 0.637172 0.459190 41.00000 -1.20000 AFIX 23 PART 2 H24C 2 1.050059 0.571656 0.446317 31.00000 -1.20000 H24D 2 1.118488 0.654276 0.437932 31.00000 -1.20000 AFIX 0 PART 1 C25A 1 1.083290 0.611951 0.326824 21.00000 0.02431 0.03582 = 0.02957 0.00973 0.00614 0.00771 AFIX 23 H25A 2 1.022049 0.592058 0.287224 21.00000 -1.20000 H25B 2 1.106410 0.675286 0.327719 21.00000 -1.20000 AFIX 0 PART 3 C25C 1 1.117289 0.588365 0.339960 41.00000 0.03061 0.03701 = 0.04156 0.00997 0.00356 0.00748 AFIX 23 H25C 2 1.167647 0.543690 0.346870 41.00000 -1.20000 H25D 2 1.070790 0.558781 0.290388 41.00000 -1.20000 AFIX 0 PART 2 C25B 1 1.094081 0.546763 0.335248 31.00000 0.02157 0.03518 = 0.03104 0.01491 0.00317 0.00932 AFIX 23 H25E 2 1.122002 0.490854 0.345897 31.00000 -1.20000 H25F 2 1.038687 0.527652 0.290206 31.00000 -1.20000 AFIX 0 C26B 1 1.176949 0.609969 0.318121 31.00000 0.02869 0.03755 = 0.03494 0.01304 0.00612 0.00366 AFIX 23 H26A 2 1.151829 0.672430 0.324861 31.00000 -1.20000 H26B 2 1.236687 0.616331 0.358612 31.00000 -1.20000 AFIX 0 PART 3 C26C 1 1.170244 0.674960 0.332296 41.00000 0.03405 0.04195 = 0.04158 0.01048 0.00691 0.00761 AFIX 23 H26C 2 1.231523 0.692792 0.372057 41.00000 -1.20000 H26D 2 1.125140 0.726654 0.343379 41.00000 -1.20000 AFIX 0 PART 1 C26A 1 1.165302 0.545950 0.302521 21.00000 0.02540 0.03586 = 0.03188 0.00994 0.00591 0.00735 AFIX 23 H26E 2 1.223488 0.563555 0.345295 21.00000 -1.20000 H26F 2 1.139470 0.482586 0.299336 21.00000 -1.20000 AFIX 0 C27A 1 1.202324 0.543474 0.223433 21.00000 0.03278 0.03662 = 0.03264 0.00954 0.00629 0.00629 AFIX 23 H27A 2 1.143587 0.542458 0.183353 21.00000 -1.20000 H27B 2 1.236520 0.485533 0.203976 21.00000 -1.20000 AFIX 0 PART 2 C27B 1 1.209491 0.575712 0.235650 31.00000 0.03182 0.04210 = 0.03976 0.01289 0.00333 0.00629 AFIX 23 H27C 2 1.153294 0.580215 0.195350 31.00000 -1.20000 H27D 2 1.223207 0.509449 0.224978 31.00000 -1.20000 AFIX 0 PART 3 C27C 1 1.199244 0.657415 0.247885 41.00000 0.03801 0.04607 = 0.04309 0.01238 0.00560 0.00544 AFIX 23 H27E 2 1.230363 0.715921 0.243558 41.00000 -1.20000 H27F 2 1.136836 0.641302 0.209257 41.00000 -1.20000 AFIX 0 PART 2 C28B 1 1.303109 0.629333 0.225103 31.00000 0.04221 0.04736 = 0.05482 0.01751 0.00885 0.00578 AFIX 137 H28A 2 1.288309 0.693933 0.230679 31.00000 -1.50000 H28B 2 1.322594 0.601094 0.171749 31.00000 -1.50000 H28C 2 1.358501 0.627382 0.266111 31.00000 -1.50000 AFIX 0 PART 3 C28C 1 1.271880 0.580856 0.222773 41.00000 0.03587 0.05643 = 0.04721 0.01278 -0.00106 -0.00173 AFIX 137 H28D 2 1.292368 0.580296 0.170779 41.00000 -1.50000 H28E 2 1.238137 0.520660 0.218405 41.00000 -1.50000 H28F 2 1.331564 0.592674 0.263085 41.00000 -1.50000 AFIX 0 PART 1 C28A 1 1.275127 0.626229 0.229803 21.00000 0.04439 0.05423 = 0.04238 0.01096 0.01899 -0.00481 AFIX 137 H28G 2 1.299167 0.619410 0.177850 21.00000 -1.50000 H28H 2 1.332618 0.628708 0.270459 21.00000 -1.50000 H28I 2 1.240259 0.683609 0.245181 21.00000 -1.50000 AFIX 0 PART 0 C29 1 0.973317 0.852739 0.708250 11.00000 0.02469 0.02847 = 0.03179 0.00415 -0.00296 -0.00277 PART 1 AFIX 23 H29A 2 1.043654 0.868793 0.702088 51.00000 -1.20000 H29B 2 0.974513 0.835778 0.758819 51.00000 -1.20000 AFIX 23 PART 2 H29C 2 1.047873 0.857448 0.713428 -51.00000 -1.20000 H29D 2 0.952736 0.846254 0.758928 -51.00000 -1.20000 AFIX 0 PART 1 C30 1 0.911834 0.938016 0.714093 51.00000 0.03067 0.02692 = 0.03404 0.00682 -0.00100 0.00045 AFIX 23 H30A 2 0.914065 0.957528 0.664999 51.00000 -1.20000 H30B 2 0.840610 0.921191 0.717173 51.00000 -1.20000 AFIX 0 C31 1 0.951395 1.018311 0.786737 51.00000 0.03706 0.02987 = 0.04645 -0.00019 0.00259 0.00097 AFIX 23 H31A 2 1.018642 1.041354 0.779342 51.00000 -1.20000 H31B 2 0.959746 0.995787 0.834674 51.00000 -1.20000 AFIX 0 C32 1 0.882138 1.098712 0.801573 51.00000 0.05538 0.03398 = 0.06317 0.00242 -0.00006 0.00782 AFIX 23 H32A 2 0.868811 1.117531 0.751946 51.00000 -1.20000 H32B 2 0.816883 1.077109 0.813846 51.00000 -1.20000 AFIX 0 C33 1 0.926450 1.182919 0.870267 51.00000 0.05799 0.03863 = 0.08471 -0.00506 0.01235 0.00078 AFIX 23 H33A 2 0.871908 1.223355 0.888880 51.00000 -1.20000 H33B 2 0.956952 1.162062 0.915741 51.00000 -1.20000 AFIX 0 C34 1 1.005029 1.237074 0.844277 51.00000 0.06498 0.04785 = 0.11183 0.00274 -0.01062 -0.00742 AFIX 137 H34A 2 0.974589 1.258777 0.799946 51.00000 -1.50000 H34B 2 1.059485 1.197327 0.826505 51.00000 -1.50000 H34C 2 1.032365 1.290507 0.889395 51.00000 -1.50000 AFIX 0 PART 0 C35 1 0.333900 0.209086 0.473422 11.00000 0.02299 0.02384 = 0.02536 0.00207 -0.00207 0.00062 AFIX 23 H35A 2 0.336696 0.224311 0.422412 11.00000 -1.20000 H35B 2 0.262503 0.193444 0.476962 11.00000 -1.20000 AFIX 0 C36 1 0.394248 0.125239 0.472603 11.00000 0.02760 0.02398 = 0.02879 0.00438 -0.00034 0.00488 AFIX 23 H36A 2 0.466994 0.143539 0.477969 11.00000 -1.20000 H36B 2 0.382343 0.103449 0.519138 11.00000 -1.20000 AFIX 0 C37 1 0.365652 0.046647 0.396010 11.00000 0.03199 0.02509 = 0.02784 0.00437 -0.00089 0.00493 AFIX 23 H37A 2 0.368763 0.070736 0.349385 11.00000 -1.20000 H37B 2 0.295331 0.022958 0.394266 11.00000 -1.20000 AFIX 0 C38 1 0.434656 -0.032857 0.389424 11.00000 0.03489 0.02880 = 0.02963 0.00246 -0.00170 0.00675 AFIX 23 H38A 2 0.505301 -0.008170 0.394464 11.00000 -1.20000 H38B 2 0.428655 -0.058833 0.434644 11.00000 -1.20000 AFIX 0 C39 1 0.411376 -0.110180 0.311349 11.00000 0.04242 0.03173 = 0.03127 0.00232 0.00162 0.01031 AFIX 23 H39A 2 0.416309 -0.084195 0.265998 11.00000 -1.20000 H39B 2 0.341190 -0.135844 0.306687 11.00000 -1.20000 AFIX 0 C40 1 0.482206 -0.188318 0.305129 11.00000 0.05103 0.03577 = 0.04037 -0.00547 0.00103 0.01700 AFIX 137 H40A 2 0.466672 -0.234282 0.252383 11.00000 -1.50000 H40B 2 0.473435 -0.217944 0.347094 11.00000 -1.50000 H40C 2 0.552076 -0.162994 0.311911 11.00000 -1.50000 AFIX 0 C41 1 0.304573 0.408319 0.744380 11.00000 0.02227 0.02741 = 0.02620 0.00262 0.00678 0.00284 AFIX 23 H41A 2 0.232104 0.390478 0.725900 11.00000 -1.20000 H41B 2 0.311622 0.476067 0.770661 11.00000 -1.20000 AFIX 0 C42 1 0.340918 0.358865 0.805401 11.00000 0.04040 0.03788 = 0.03595 0.01320 0.01317 0.01259 AFIX 23 H42A 2 0.408659 0.385955 0.832273 11.00000 -1.20000 H42B 2 0.346836 0.292572 0.777427 11.00000 -1.20000 AFIX 0 C43 1 0.269344 0.366692 0.868360 11.00000 0.05042 0.04005 = 0.03941 0.01520 0.01825 0.00912 AFIX 23 H43A 2 0.204786 0.331717 0.841875 11.00000 -1.20000 H43B 2 0.298502 0.336688 0.908345 11.00000 -1.20000 AFIX 0 C44 1 0.247561 0.464415 0.911946 11.00000 0.04857 0.04261 = 0.03616 0.01227 0.01267 0.01196 AFIX 23 H44A 2 0.212485 0.492482 0.872690 11.00000 -1.20000 H44B 2 0.312430 0.501033 0.934192 11.00000 -1.20000 AFIX 0 C45 1 0.184174 0.472222 0.979377 11.00000 0.07729 0.05745 = 0.04604 0.01723 0.02985 0.02399 AFIX 23 H45A 2 0.123655 0.428753 0.958918 11.00000 -1.20000 H45B 2 0.223408 0.452550 1.022343 11.00000 -1.20000 AFIX 0 C46 1 0.151310 0.566418 1.014521 11.00000 0.11406 0.08305 = 0.04967 0.02357 0.03141 0.04894 AFIX 137 H46A 2 0.112421 0.586776 0.972535 11.00000 -1.50000 H46B 2 0.210594 0.609502 1.037843 11.00000 -1.50000 H46C 2 0.109165 0.565317 1.056442 11.00000 -1.50000 AFIX 0 C47 1 0.775525 0.376824 0.318499 11.00000 0.02359 0.02244 = 0.02577 0.00464 0.00422 0.00637 C48 1 0.880165 0.379920 0.324551 11.00000 0.02441 0.03164 = 0.02426 0.00478 0.00078 0.00568 AFIX 43 H48 2 0.918687 0.399688 0.376092 11.00000 -1.20000 AFIX 0 C49 1 0.929548 0.354734 0.256866 11.00000 0.02278 0.03264 = 0.02963 0.00796 0.00456 0.00885 AFIX 43 H49 2 1.001097 0.356980 0.262260 11.00000 -1.20000 AFIX 0 C50 1 0.873962 0.326291 0.181368 11.00000 0.02714 0.02758 = 0.02498 0.00580 0.00839 0.00986 C51 1 0.769133 0.324118 0.174008 11.00000 0.02707 0.02979 = 0.02339 0.00480 0.00117 0.00635 AFIX 43 H51 2 0.730769 0.305477 0.122385 11.00000 -1.20000 AFIX 0 C52 1 0.721172 0.349025 0.241653 11.00000 0.02290 0.02556 = 0.02640 0.00396 0.00307 0.00650 AFIX 43 H52 2 0.649634 0.347295 0.236023 11.00000 -1.20000 AFIX 0 C53 1 1.021425 0.305052 0.114327 11.00000 0.03026 0.06708 = 0.03821 0.01422 0.01458 0.01401 AFIX 137 H53A 2 1.040189 0.284029 0.059955 11.00000 -1.50000 H53B 2 1.050563 0.265964 0.145955 11.00000 -1.50000 H53C 2 1.047113 0.369618 0.139661 11.00000 -1.50000 AFIX 0 C54 1 0.729058 0.778696 0.866931 11.00000 0.01736 0.02999 = 0.02486 0.00088 0.00215 0.00426 C55 1 0.747428 0.867902 0.862812 11.00000 0.03056 0.03273 = 0.02813 0.00524 -0.00095 0.00261 AFIX 43 H55 2 0.732719 0.880280 0.812740 11.00000 -1.20000 AFIX 0 C56 1 0.786913 0.940158 0.930054 11.00000 0.04525 0.02853 = 0.04047 0.00517 -0.00668 -0.00267 AFIX 43 H56 2 0.798091 1.000977 0.925801 11.00000 -1.20000 AFIX 0 C57 1 0.809691 0.922488 1.003088 11.00000 0.04333 0.03404 = 0.03246 -0.00375 -0.00993 -0.00041 C58 1 0.794953 0.832665 1.007892 11.00000 0.03118 0.03668 = 0.02679 0.00372 -0.00398 0.00483 AFIX 43 H58 2 0.812879 0.819713 1.057379 11.00000 -1.20000 AFIX 0 C59 1 0.754421 0.762352 0.941092 11.00000 0.02246 0.02900 = 0.02685 0.00256 0.00225 0.00553 AFIX 43 H59 2 0.743486 0.701571 0.945496 11.00000 -1.20000 AFIX 0 C60 1 0.858507 1.081666 1.072237 11.00000 0.14036 0.03657 = 0.06412 -0.00300 -0.04360 -0.01309 AFIX 137 H60A 2 0.909431 1.087245 1.037619 11.00000 -1.50000 H60B 2 0.880092 1.121735 1.126805 11.00000 -1.50000 H60C 2 0.794072 1.100555 1.051536 11.00000 -1.50000 AFIX 0 C61 1 0.623308 0.247120 0.343498 11.00000 0.02764 0.02596 = 0.02063 0.00385 0.00494 0.00592 C62 1 0.702346 0.188365 0.333533 11.00000 0.02600 0.03156 = 0.03268 0.00542 0.00531 0.00642 AFIX 43 H62 2 0.767612 0.211371 0.360760 11.00000 -1.20000 AFIX 0 C63 1 0.688274 0.097218 0.284938 11.00000 0.03538 0.02906 = 0.04346 0.00467 0.01279 0.01013 AFIX 43 H63 2 0.743088 0.058333 0.279848 11.00000 -1.20000 AFIX 0 C64 1 0.593526 0.063282 0.243824 11.00000 0.04341 0.02467 = 0.03108 -0.00122 0.01208 0.00182 C65 1 0.513757 0.120589 0.253561 11.00000 0.03134 0.03247 = 0.02784 0.00344 0.00233 0.00031 AFIX 43 H65 2 0.448614 0.097657 0.226026 11.00000 -1.20000 AFIX 0 C66 1 0.528642 0.210829 0.303109 11.00000 0.02891 0.02812 = 0.02450 0.00369 0.00293 0.00699 AFIX 43 H66 2 0.473103 0.248789 0.309692 11.00000 -1.20000 AFIX 0 C67 1 0.650766 -0.085824 0.181134 11.00000 0.06862 0.03113 = 0.08063 -0.00701 0.02906 0.00814 AFIX 137 H67A 2 0.701494 -0.060926 0.155223 11.00000 -1.50000 H67B 2 0.623883 -0.147180 0.146695 11.00000 -1.50000 H67C 2 0.681833 -0.091148 0.232835 11.00000 -1.50000 AFIX 0 C68 1 0.549193 0.666050 0.873987 11.00000 0.02020 0.03122 = 0.01991 -0.00121 -0.00025 0.00045 C69 1 0.507478 0.750485 0.901650 11.00000 0.02653 0.03716 = 0.02549 0.00181 0.00246 0.00546 AFIX 43 H69 2 0.512102 0.795234 0.873338 11.00000 -1.20000 AFIX 0 C70 1 0.458969 0.770959 0.970075 11.00000 0.02775 0.04658 = 0.02575 -0.00325 0.00257 0.00806 AFIX 43 H70 2 0.430368 0.829002 0.987834 11.00000 -1.20000 AFIX 0 C71 1 0.452506 0.707201 1.011853 11.00000 0.02888 0.05353 = 0.01860 -0.00042 0.00319 0.00186 C72 1 0.494888 0.622438 0.985505 11.00000 0.04208 0.04997 = 0.02716 0.01072 0.00481 -0.00021 AFIX 43 H72 2 0.491761 0.578662 1.014925 11.00000 -1.20000 AFIX 0 C73 1 0.541530 0.601640 0.916699 11.00000 0.03701 0.03468 = 0.02581 0.00359 0.00368 0.00337 AFIX 43 H73 2 0.568589 0.542939 0.898377 11.00000 -1.20000 AFIX 0 C74 1 0.350878 0.800252 1.101408 11.00000 0.04587 0.08159 = 0.03142 -0.00147 0.01516 0.01260 AFIX 137 H74A 2 0.299060 0.799913 1.057095 11.00000 -1.50000 H74B 2 0.397029 0.855624 1.113385 11.00000 -1.50000 H74C 2 0.318745 0.800823 1.149002 11.00000 -1.50000 AFIX 0 C77 1 0.700047 0.509139 0.520180 11.00000 0.02187 0.02219 = 0.02227 0.00509 0.00147 0.00536 PART 2 C30A 1 0.932313 0.937263 0.691540 -51.00000 0.04159 0.03760 = 0.03797 0.00614 -0.00934 -0.00671 AFIX 23 H30C 2 0.858131 0.933951 0.690347 -51.00000 -1.20000 H30D 2 0.947804 0.939925 0.638369 -51.00000 -1.20000 AFIX 0 C31A 1 0.978313 1.024357 0.755823 -51.00000 0.05687 0.03756 = 0.05157 0.00468 -0.01008 -0.00178 AFIX 23 H31C 2 0.966445 1.019149 0.809089 -51.00000 -1.20000 H31D 2 1.052088 1.028663 0.754787 -51.00000 -1.20000 AFIX 0 C32A 1 0.935649 1.111658 0.744985 -51.00000 0.08825 0.04080 = 0.07552 0.00438 -0.01738 -0.00164 AFIX 23 H32C 2 0.945368 1.114652 0.690663 -51.00000 -1.20000 H32D 2 0.862123 1.106941 0.747098 -51.00000 -1.20000 AFIX 0 C33A 1 0.978500 1.200032 0.803782 -51.00000 0.08882 0.05194 = 0.08781 -0.00105 -0.01799 -0.00200 AFIX 23 H33C 2 0.949290 1.252499 0.787766 -51.00000 -1.20000 H33D 2 1.052241 1.205367 0.802848 -51.00000 -1.20000 AFIX 0 C34A 1 0.958004 1.206773 0.888050 -51.00000 0.06229 0.04935 = 0.09692 0.02346 -0.01528 -0.01154 AFIX 137 H34D 2 0.910577 1.155371 0.886814 -51.00000 -1.50000 H34E 2 0.928873 1.265819 0.911063 -51.00000 -1.50000 H34F 2 1.021260 1.203505 0.920963 -51.00000 -1.50000 AFIX 0 PART 0 C7 1 0.570729 0.475983 0.596387 11.00000 0.01968 0.02263 = 0.02298 0.00483 0.00117 0.00547 HKLF 4 REM ga_re39_a.res in P-1 REM wR2 = 0.1546, GooF = S = 1.027, Restrained GooF = 1.021 for all data REM R1 = 0.0566 for 10532 Fo > 4sig(Fo) and 0.0667 for all 12847 data REM 926 parameters refined using 375 restraints END WGHT 0.0730 2.0657 REM Highest difference peak 0.564, deepest hole -0.337, 1-sigma level 0.051 Q1 1 0.9229 1.2789 0.8799 11.00000 0.05 0.56 Q2 1 1.3009 0.7803 0.4539 11.00000 0.05 0.55 Q3 1 0.8596 1.1016 0.5819 11.00000 0.05 0.47 Q4 1 0.0998 0.4809 0.9752 11.00000 0.05 0.45 Q5 1 1.2461 0.7388 0.4055 11.00000 0.05 0.35 Q6 1 0.9330 1.0644 1.0430 11.00000 0.05 0.32 Q7 1 0.9035 0.9694 1.0447 11.00000 0.05 0.32 Q8 1 0.8994 1.1033 0.6413 11.00000 0.05 0.32 Q9 1 0.9237 1.2072 0.8163 11.00000 0.05 0.27 Q10 1 0.9439 1.1212 0.7975 11.00000 0.05 0.25 Q11 1 0.8371 0.6221 0.5560 11.00000 0.05 0.24 Q12 1 0.5957 0.5615 0.6801 11.00000 0.05 0.24 Q13 1 0.7198 0.5530 0.5560 11.00000 0.05 0.23 Q14 1 0.7420 0.4421 0.4230 11.00000 0.05 0.23 Q15 1 0.4710 0.4205 0.6328 11.00000 0.05 0.22 ; _shelx_res_checksum 83904 _shelx_hkl_file ; 0 0 -2 15426.6 517.550 14 0 0 -2 15902.3 576.089 10 0 0 -2 15616.3 524.421 12 0 0 2 15921.1 577.715 10 0 0 -3 7669.43 373.270 20 0 0 -3 7525.16 347.858 12 0 0 3 8227.96 349.205 11 0 0 -3 7985.17 350.503 14 0 0 -3 8442.96 417.639 10 0 0 -4 2889.28 211.548 18 0 0 -4 2675.00 231.211 26 0 0 -4 2611.68 222.403 20 0 0 4 2881.50 203.187 11 0 0 -4 2703.48 208.519 14 0 0 -4 2910.10 264.108 10 0 0 -5 7543.93 505.787 10 0 0 -5 7966.96 460.232 20 0 0 5 8161.60 398.761 11 0 0 -5 7772.70 423.988 18 0 0 -5 7964.76 436.379 14 0 0 5 7243.74 443.152 35 0 0 5 7449.77 469.871 32 0 0 -5 8037.99 467.303 26 0 0 -6 7406.60 441.043 18 0 0 -6 8191.88 504.098 20 0 0 6 7490.35 391.615 11 0 0 -6 6061.19 421.049 42 0 0 6 7871.35 516.924 32 0 0 -6 8510.91 512.960 26 0 0 -6 7981.70 461.760 14 0 0 6 7231.03 478.137 35 0 0 7 6227.08 494.072 32 0 0 7 6524.28 472.427 35 0 0 -7 6906.75 497.612 20 0 0 -7 6443.61 468.085 16 0 0 -7 5780.55 412.568 18 0 0 -7 5612.35 444.879 49 0 0 -7 5345.55 411.935 42 0 0 -7 5792.24 454.650 36 0 0 -7 6317.34 477.165 26 0 0 -8 1006.64 184.328 42 0 0 -8 1114.74 202.875 49 0 0 -8 1271.01 237.133 20 0 0 -8 1273.42 232.619 52 0 0 -8 1356.43 228.542 16 0 0 8 924.038 194.564 35 0 0 -8 1072.94 214.870 36 0 0 -8 1222.68 227.969 26 0 0 8 974.392 215.913 32 0 0 -8 943.012 186.767 74 0 0 -9 11553.3 781.815 20 0 0 9 10675.7 782.814 32 0 0 9 10800.8 743.651 35 0 0 -9 11261.1 764.395 52 0 0 -9 12148.9 776.308 16 0 0 -9 9670.07 693.604 49 0 0 -9 11981.5 768.287 21 0 0 -9 10866.3 764.541 26 0 0 -9 10379.1 734.425 36 0 0 -9 10278.3 717.256 74 0 0 -10 16457.0 1035.52 26 0 0 -10 16715.2 1024.78 52 0 0 -10 15724.8 966.680 49 0 0 -10 18707.2 1077.36 51 0 0 -10 17040.1 1020.98 16 0 0 -10 17372.8 1031.41 21 0 0 10 16075.1 991.777 35 0 0 -10 17685.4 1039.52 34 0 0 -10 16517.0 1016.18 36 0 0 10 16498.8 1071.28 32 0 0 -10 16145.0 987.080 73 0 0 -10 14717.6 947.132 74 0 0 11 1642.37 334.713 32 0 0 -11 1697.31 321.912 52 0 0 -11 1604.67 330.118 36 0 0 -11 1965.12 351.946 16 0 0 11 1594.49 327.278 29 0 0 -11 2143.01 372.878 51 0 0 -11 1808.41 347.087 21 0 0 -11 2042.34 351.865 34 0 0 -11 1619.52 318.891 79 0 0 -11 1924.55 331.858 73 0 0 -12 4139.10 552.312 21 0 0 -12 5129.27 602.230 51 0 0 -12 4992.72 603.869 36 0 0 -12 4069.42 539.519 52 0 0 -12 4941.10 602.339 34 0 0 -12 3716.50 521.866 16 0 0 -12 4322.11 540.270 79 0 0 -12 4199.26 524.943 73 0 0 12 3938.91 407.485 122 0 0 -13 1209.46 338.509 21 0 0 -13 900.000 294.072 34 0 0 -13 1177.27 317.336 16 0 0 -13 1002.44 280.846 56 0 0 -13 977.103 291.853 52 0 0 -13 1019.97 305.064 51 0 0 -13 682.333 266.698 36 0 0 -13 572.670 226.140 79 0 0 13 1071.89 246.513 122 0 0 -14 5682.12 490.957 93 0 0 -14 6225.30 722.879 60 0 0 -14 6704.57 755.892 76 0 0 -14 6096.46 744.473 34 0 0 -14 5169.80 670.175 51 0 0 -14 6196.58 739.547 56 0 0 14 4925.43 480.996 162 0 0 14 5413.96 521.220 161 0 0 14 6078.65 535.565 145 0 0 14 6068.79 532.700 122 0 0 -15 31885.1 1833.71 61 0 0 -15 31215.1 1811.96 60 0 0 -15 30655.9 1789.55 76 0 0 15 31010.0 1417.78 161 0 0 15 31096.8 1419.08 145 0 0 -15 25263.8 1714.51 34 0 0 -15 28284.0 1762.18 51 0 0 -15 30019.0 1802.58 56 0 0 -15 29821.7 1774.24 38 0 0 -16 134.020 143.991 61 0 0 -16 165.701 151.801 60 0 0 -16 480.318 219.654 76 0 0 -16 233.418 190.621 82 0 0 -16-52.2745 156.090 56 0 0 -16 166.410 170.344 55 0 0 16 31.5078 140.155 161 0 0 16 427.434 196.350 145 0 0 16-71.8706 136.876 144 0 0 -17 214.395 183.646 76 0 0 -17-110.846 175.229 82 0 0 17 155.750 138.907 161 0 0 17 210.039 136.376 144 0 0 -17 314.381 155.467 107 0 0 -17 164.244 120.609 104 0 0 18 248.898 139.188 161 0 0 18 283.741 131.294 144 0 0 -18 679.245 203.616 104 0 0 -18 263.367 119.650 107 0 0 19 1886.65 258.339 161 0 0 19 1479.57 199.378 144 0 0 20 55.1590 64.1775 161 0 -1 20-62.3458 64.9214 161 0 -1 20-14.2445 65.2490 144 0 -1 19 208.259 126.069 144 0 -1 19 85.9758 76.6302 161 0 1 -18 166.701 176.106 92 0 -1 18 296.185 177.241 161 0 -1 18 0.40120 105.946 144 0 1 -18-39.9735 115.010 107 0 1 -18-43.3677 97.6959 104 0 1 -17 1849.47 417.595 76 0 1 -17 2444.39 489.633 82 0 -1 17 2171.89 335.521 144 0 -1 17 2351.30 322.922 145 0 -1 17 2022.50 310.847 161 0 1 -17 2199.59 313.529 104 0 1 -17 2423.09 334.199 107 0 1 -16 1118.33 313.273 76 0 1 -16 1336.79 358.776 61 0 1 -16 1435.02 390.840 82 0 1 -16 981.534 323.330 60 0 1 -16 1083.53 296.927 51 0 1 -16 1228.53 333.203 55 0 1 -16 1424.01 389.901 56 0 -1 16 1395.78 263.728 145 0 -1 16 1462.17 283.340 161 0 1 -16 1339.45 265.102 104 0 1 -15 24.0749 180.517 82 0 1 -15 39.3707 165.983 76 0 1 -15 94.2481 151.236 61 0 1 -15-189.452 148.936 93 0 1 -15 29.5802 199.886 60 0 1 -15 4.89755 127.243 34 0 1 -15 50.0336 154.954 51 0 1 -15 115.802 155.644 56 0 1 -15-137.108 135.629 38 0 -1 15 204.576 122.648 145 0 -1 15 102.121 103.185 161 0 -1 15 56.2443 126.308 139 0 -1 15 306.439 179.373 122 0 1 -14 254.217 167.915 61 0 1 -14 241.599 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1428.28 387.091 35 0 7 -14 1613.78 278.282 147 0 -7 14 1362.94 266.316 163 0 7 -14 2034.61 305.909 103 0 7 -14 1974.04 314.676 107 0 7 -14 2062.36 305.004 126 0 -7 14 1875.18 305.076 122 0 7 -14 1982.40 293.178 118 0 -7 14 1941.53 293.886 127 0 7 -14 1916.41 319.535 104 0 7 -14 1704.57 282.857 123 0 -7 13 1294.01 354.677 35 0 7 -13 1188.24 357.484 60 0 7 -13 925.246 234.840 100 0 -7 13 663.454 307.006 78 0 7 -13 933.356 284.119 92 0 7 -13 353.562 163.030 61 0 7 -13 909.501 311.412 82 0 7 -13 773.160 190.480 107 0 -7 13 1071.84 229.420 127 0 7 -13 953.036 229.563 104 0 7 -13 818.761 197.257 103 0 7 -13 656.064 201.857 123 0 7 -13 835.756 204.142 126 0 7 -13 827.414 221.705 118 0 -7 13 1280.46 251.713 122 0 7 -12 78.5602 161.252 92 0 7 -12 137.880 158.277 61 0 7 -12-93.4177 190.512 60 0 -7 12 139.506 190.696 78 0 7 -12 124.266 122.757 82 0 7 -12 60.6588 133.070 100 0 7 -12-27.9358 116.258 126 0 -7 12 56.0878 94.4993 122 0 7 -12 14.2428 133.905 104 0 7 -12 18.3602 97.5858 103 0 7 -12 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191.930 89 0 -8 7 615.018 154.428 102 0 -8 6 2727.73 405.288 77 0 -8 6 3477.60 457.822 84 0 -8 6 2521.62 374.214 78 0 8 -6 2363.59 267.900 96 0 8 -6 2678.92 390.854 4 0 -8 6 1850.95 298.362 57 0 -8 6 2397.92 373.188 53 0 -8 6 2155.96 324.392 31 0 -8 6 2494.20 368.393 43 0 -8 6 2104.92 314.604 28 0 -8 5 2954.26 420.946 77 0 -8 5 2272.97 388.017 84 0 -8 5 2284.47 373.791 78 0 8 -5 2339.20 258.478 96 0 -8 5 2559.34 372.910 53 0 -8 5 2079.47 313.356 28 0 -8 5 2470.94 392.135 33 0 -8 5 2550.97 359.565 31 0 -8 5 2004.22 305.205 15 0 8 -5 2758.93 385.830 4 0 -8 5 2392.67 357.549 43 0 -8 4 2206.97 360.809 62 0 -8 4 1947.07 314.735 78 0 8 -4 1868.90 235.119 96 0 -8 4 1851.36 306.227 84 0 -8 4 2658.04 380.637 33 0 -8 4 2104.75 326.699 53 0 -8 4 1927.07 330.313 43 0 8 -4 2297.16 352.051 4 0 -8 4 1982.76 299.598 31 0 -8 4 2126.06 303.197 15 0 -8 4 2519.10 346.831 28 0 -8 3 5792.94 525.348 64 0 -8 3 6649.56 588.604 62 0 8 -3 6484.48 439.843 96 0 -8 3 6977.77 611.932 84 0 -8 3 5369.90 519.828 78 0 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438.140 29 -1 -3 -10 603.232 199.622 36 -1 -3 -10 626.402 205.656 20 1 3 10 580.541 232.792 29 -1 -3 -10 744.330 230.106 21 1 3 10 445.371 212.175 32 -1 -3 -10 674.246 212.084 16 -1 -3 -11 15245.9 1108.73 34 -1 -3 -11 13146.5 1066.76 16 1 3 11 15730.8 1221.66 29 -1 -3 -11 15427.2 1132.87 21 -1 -3 -11 15435.3 1089.95 51 1 3 11 14878.6 1152.79 32 1 3 12-66.6910 86.2636 146 1 3 12-312.870 166.008 162 1 3 12 67.9130 123.435 154 1 3 12-27.7050 97.1347 167 1 3 12 9.27753 120.069 161 -1 -3 -12-10.8008 104.671 21 -1 -3 -12 44.3215 123.568 34 1 3 12 15.8548 105.042 29 1 3 13-6.00976 99.6028 167 1 3 13 356.896 177.953 161 1 3 13 275.632 146.282 154 1 3 13 272.990 154.766 162 1 3 13 439.820 237.930 29 -1 -3 -13 68.0154 105.796 56 -1 -3 -13 90.7733 91.9546 34 -1 -3 -13 175.128 150.946 38 -1 -3 -14 498.558 213.397 61 -1 -3 -14 385.041 188.020 56 1 3 14 445.378 192.732 161 1 3 14 409.815 177.745 167 1 3 14 383.146 165.253 154 1 3 14 500.686 198.354 162 1 3 15 6496.03 587.474 162 1 3 15 5944.97 552.706 167 1 3 15 6633.21 584.673 161 1 3 16-106.778 136.259 161 1 3 16-38.5021 113.032 162 1 3 17 1135.52 234.206 162 1 3 17 1233.65 211.931 161 1 3 18 2152.37 266.618 161 1 4 -21 146.508 76.4079 147 -1 -4 21-33.5093 63.4415 144 -1 -4 20 92.7395 76.7952 144 1 4 -20-32.4737 90.3031 147 1 4 -20 123.047 92.0491 118 -1 -4 19 1792.64 261.874 145 1 4 -19 2047.96 281.678 147 -1 -4 19 1714.64 241.464 139 1 4 -19 1814.28 272.827 103 1 4 -19 1401.93 236.613 104 1 4 -19 1419.63 257.081 107 1 4 -19 1511.34 229.210 126 1 4 -18-123.054 149.964 82 1 4 -18 169.441 208.304 76 1 4 -18 127.814 109.350 100 1 4 -18 607.827 296.813 92 -1 -4 18 193.020 125.439 139 -1 -4 18 323.516 150.564 145 -1 -4 18 259.556 131.259 122 1 4 -18-57.9314 130.005 103 1 4 -18 192.801 98.9337 123 1 4 -18 32.5420 104.755 126 1 4 -18 84.0001 109.663 104 1 4 -18 294.541 140.463 107 1 4 -17 854.714 291.761 76 1 4 -17 850.530 296.961 60 1 4 -17 1064.36 302.670 82 1 4 -17 1198.69 236.992 100 1 4 -17 1098.88 317.323 92 1 4 -17 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744.864 235.294 79 1 4 -13 558.642 258.730 61 1 4 -13 463.095 137.208 110 -1 -4 13 408.000 171.069 122 -1 -4 13 502.301 180.908 127 1 4 -12 7624.83 735.772 51 1 4 -12 7090.62 699.492 34 1 4 -12 7782.28 692.343 38 1 4 -12 7043.83 691.239 56 1 4 -12 6228.66 646.169 21 -1 -4 12 7702.91 756.078 35 1 4 -12 8229.47 736.735 82 1 4 -12 8076.51 722.474 61 -1 -4 12 8323.37 765.310 78 1 4 -12 7336.06 531.126 100 1 4 -12 7041.74 688.476 76 1 4 -12 6967.46 732.121 79 1 4 -12 7405.56 531.627 93 1 4 -12 7158.01 694.468 60 1 4 -12 6696.85 516.326 110 1 4 -11 6376.27 639.489 51 1 4 -11 5952.11 589.507 34 1 4 -11 5928.92 601.837 56 1 4 -11 5394.34 546.598 21 1 4 -11 5939.93 618.270 79 1 4 -11 5777.70 589.011 60 1 4 -11 6337.05 609.737 61 1 4 -11 6206.03 617.482 76 1 4 -11 5536.98 596.944 73 1 4 -11 5733.50 440.220 93 1 4 -11 5549.34 436.521 100 -1 -4 11 6376.27 644.018 78 1 4 -11 5076.37 424.133 110 1 4 -10 52326.5 2104.89 76 1 4 -10 50095.7 2129.76 79 1 4 -10 49870.6 2079.12 73 -1 -4 10 55664.1 2178.62 78 1 4 -10 55309.2 2109.61 60 1 4 -10 49025.7 1758.36 93 1 4 -10 47475.8 1752.29 100 1 4 -10 51920.9 2051.34 61 1 4 -10 53899.8 2089.09 34 1 4 -10 54511.1 2126.92 51 1 4 -10 53100.2 2087.38 56 1 4 -10 48107.9 1978.65 21 1 4 -9 14622.0 937.925 79 1 4 -9 16074.7 918.554 60 1 4 -9 14716.2 910.269 73 -1 -4 9 16229.8 973.532 78 1 4 -9 16078.5 932.472 76 1 4 -9 15484.2 884.334 61 1 4 -9 14900.4 894.744 56 1 4 -9 15619.5 902.513 34 1 4 -9 16399.9 954.386 51 1 4 -9 15334.2 862.477 21 1 4 -8 971.671 224.071 61 1 4 -8 1036.24 208.254 60 1 4 -8 1204.43 250.256 73 1 4 -8 1037.32 226.335 76 -1 -4 8 1033.29 244.940 78 1 4 -8 1114.99 247.088 79 1 4 -8 1326.45 250.051 34 1 4 -8 1309.03 218.573 21 1 4 -8 1614.32 267.052 51 1 4 -8 1051.53 222.909 56 1 4 -7 5420.61 461.342 73 1 4 -7 5306.55 433.684 61 1 4 -7 5615.82 457.801 60 1 4 -7 5476.95 439.432 34 1 4 -7 5507.04 468.237 51 1 4 -7 4323.24 346.694 4 1 4 -7 5243.38 404.409 21 1 4 -7 5425.22 452.394 56 1 4 -6 4735.05 392.419 60 1 4 -6 4767.46 356.386 21 1 4 -6 5159.42 402.669 34 -1 -4 6 3936.83 438.720 1 1 4 -6 4624.13 389.367 56 -1 -4 6 5083.44 505.873 7 1 4 -6 4196.61 334.362 4 1 4 -6 4837.37 417.061 51 -1 -4 5 11795.0 547.853 28 1 4 -5 14238.0 679.539 34 1 4 -5 13867.4 661.951 4 1 4 -5 14619.1 731.801 51 -1 -4 5 15327.0 912.782 7 -1 -4 5 14608.8 871.997 1 -1 -4 4 99609.3 3264.23 7 -1 -4 4 96292.4 2895.19 33 -1 -4 4 94541.3 3221.16 1 1 4 -4 91914.8 2873.81 4 1 4 -4 95851.1 3281.62 9 -1 -4 3 56432.4 2141.67 7 -1 -4 3 59926.3 1828.29 22 1 4 -3 50336.7 1785.93 4 1 4 -3 55319.9 2094.79 9 -1 -4 3 56655.4 2118.37 1 -1 -4 3 55264.0 1811.08 33 -1 -4 2 33005.3 1188.22 22 1 4 -2 33421.8 1397.00 9 -1 -4 2 31807.8 1454.05 7 -1 -4 1 122151. 3641.66 30 -1 -4 1 128871. 3668.67 19 1 4 -1 136043. 3892.49 9 -1 -4 1 124077. 3999.07 7 -1 -4 1 114985. 3799.30 9 -1 -4 0 25996.3 990.156 30 -1 -4 0 26806.7 995.054 17 -1 -4 0 25750.6 944.066 23 1 4 0 23158.1 976.172 4 1 4 0 23013.1 983.521 29 -1 -4 0 27550.1 1010.01 19 -1 -4 0 26478.2 1255.75 1 -1 -4 0 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315.543 161 -2 6 12 28774.2 1358.80 161 -2 6 12 29005.3 1390.58 146 -2 6 12 30056.2 1369.47 154 -2 6 11 117.792 123.776 146 -2 6 11 348.509 154.728 154 -2 6 11 327.363 128.680 161 -2 6 11 457.363 206.042 32 2 -6 -11 632.776 271.195 49 2 -6 -11 376.353 212.352 26 -2 6 11 260.038 161.742 29 -2 6 10 152.979 85.3085 161 -2 6 10 57.0706 94.3075 154 -2 6 10 191.821 135.767 146 2 -6 -10-50.8702 156.247 18 2 -6 -10 189.934 150.667 20 2 -6 -10 205.591 127.541 42 -2 6 10 80.8445 116.529 29 -2 6 10 181.526 188.814 32 2 -6 -10 33.4828 90.6459 26 2 -6 -9 1709.70 359.059 41 2 -6 -9 1487.32 353.621 18 -2 6 9 1275.40 355.556 29 -2 6 9 1536.84 343.249 32 2 -6 -8 105.395 140.453 18 -2 6 8 52.7252 107.111 32 2 -6 -8-36.9820 87.8127 14 2 -6 -8 59.0961 133.185 24 -2 6 8 93.3683 177.042 29 2 -6 -7 3095.72 466.746 14 2 -6 -7 3630.70 505.257 18 -2 6 7 3690.25 488.411 32 -2 6 7 3736.14 554.865 29 -2 6 7 3269.90 482.667 37 2 -6 -7 3661.10 498.497 15 2 -6 -7 4221.11 524.580 24 -2 6 6 6465.68 658.942 37 2 -6 -6 7023.53 673.468 15 -2 6 6 6642.37 628.834 32 2 -6 -6 6463.29 612.507 28 2 -6 -6 6757.45 611.362 31 -2 6 6 6828.59 715.616 29 2 -6 -6 7030.17 662.764 24 2 -6 -6 6306.14 644.021 14 2 -6 -5 236.009 138.667 14 -2 6 5 116.912 170.732 29 2 -6 -5 100.642 126.675 31 2 -6 -5 109.797 111.486 15 2 -6 -5 174.455 103.305 24 2 -6 -5 21.7329 90.8798 28 2 -6 -5-35.1677 76.5028 43 -2 6 5-29.7171 136.468 32 -2 6 5-6.44623 110.006 37 -2 6 4 522.637 167.733 32 2 -6 -4 544.876 161.044 33 2 -6 -4 525.607 181.841 31 2 -6 -4 485.471 158.826 22 2 -6 -4 524.945 165.721 14 2 -6 -4 653.370 196.083 15 2 -6 -4 546.669 179.216 28 -2 6 4 530.465 204.862 29 2 -6 -4 459.281 155.002 43 -2 6 4 642.418 202.057 37 2 -6 -3 179.394 107.823 22 2 -6 -3-33.9269 97.1326 33 -2 6 3 7.72226 113.892 29 2 -6 -3 77.8013 63.1998 25 -2 6 3 102.526 92.5874 4 2 -6 -3 170.545 104.304 43 -2 6 3 90.7935 121.412 32 2 -6 -3 62.5323 104.966 31 2 -6 -3 131.431 131.438 28 -2 6 3 143.814 143.525 37 2 -6 -3 137.614 106.909 15 2 -6 -2 70.3322 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630.344 15 2 -6 1 8234.55 587.532 43 2 -6 1 7528.11 568.383 62 -2 6 -2 13273.0 743.563 45 -2 6 -2 15501.3 844.333 4 2 -6 2 15716.7 846.228 28 2 -6 2 14280.3 829.984 53 2 -6 2 14868.7 829.182 57 2 -6 2 15821.2 842.065 31 2 -6 2 16085.2 855.764 43 2 -6 3 11626.6 737.631 53 2 -6 3 12582.3 757.795 43 2 -6 3 11264.9 718.399 57 -2 6 -3 13257.7 761.091 4 -2 6 -3 10855.0 671.943 45 2 -6 3 12274.9 733.303 31 2 -6 4 1024.28 210.389 31 2 -6 4 760.639 220.887 53 -2 6 -4 1020.74 266.724 4 -2 6 -4 716.369 181.611 45 2 -6 4 704.572 196.667 57 2 -6 4 522.824 146.106 24 2 -6 4 705.170 180.070 63 2 -6 5 1938.76 276.801 57 -2 6 -5 2260.03 310.379 4 2 -6 5 1984.23 323.446 77 2 -6 5 2065.86 324.605 84 2 -6 5 1904.91 273.668 63 -2 6 -6 17981.9 962.149 4 -2 6 -6 17140.4 996.756 82 2 -6 6 15730.5 975.970 77 -2 6 -7 17982.8 971.576 4 2 -6 7 16642.1 1041.97 89 2 -6 7 16575.7 978.972 78 -2 6 -7 18669.0 1062.65 82 -2 6 -7 16161.1 968.912 80 -2 6 -7 16835.6 1033.21 92 -2 6 -8 30023.8 1417.89 55 2 -6 8 28281.4 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144.979 104 -2 6 -11 298.916 131.836 107 -2 6 -11 614.211 183.244 103 -2 6 -12 299.233 203.363 38 2 -6 12 289.468 154.329 35 -2 6 -12 460.859 205.252 55 -2 6 -12 318.814 185.972 61 -2 6 -12 67.6139 183.039 92 -2 6 -12 481.304 174.919 100 -2 6 -12 451.350 205.136 80 -2 6 -12 418.777 184.592 82 -2 6 -12 187.748 204.471 60 -2 6 -12 451.117 182.276 118 -2 6 -12 496.624 164.861 107 -2 6 -12 376.385 139.618 123 -2 6 -12 486.223 161.894 104 -2 6 -12 621.528 176.404 103 2 -6 12 490.308 158.738 122 2 -6 12 402.327 162.336 127 -2 6 -13 1345.49 344.895 60 -2 6 -13 1641.91 400.378 92 -2 6 -13 1890.85 423.852 82 -2 6 -13 1504.68 363.892 80 -2 6 -13 1896.79 274.610 100 -2 6 -13 1448.59 378.504 55 -2 6 -13 1411.44 357.896 38 2 -6 13 1536.45 394.152 35 2 -6 13 1531.89 291.729 163 -2 6 -13 1601.79 280.051 107 -2 6 -13 1043.66 243.686 126 2 -6 13 1763.41 276.163 122 -2 6 -13 1242.63 237.382 123 -2 6 -13 1653.19 276.376 104 -2 6 -13 1435.14 258.890 118 -2 6 -13 1754.51 291.282 103 -2 6 -14 248.165 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248.935 18 2 -5 -10 660.321 273.031 20 -2 5 10 662.886 254.022 32 2 -5 -10 1005.30 291.054 42 2 -5 -10 951.344 283.859 26 2 -5 -9 1894.50 374.466 18 2 -5 -9 1610.24 359.279 14 -2 5 9 1705.15 383.436 29 -2 5 9 2105.41 399.767 32 2 -5 -9 1946.07 369.796 41 2 -5 -9 1673.00 369.186 20 2 -5 -8 8594.49 792.894 14 2 -5 -8 9178.13 815.498 18 -2 5 8 8776.61 777.882 32 -2 5 8 8705.95 830.896 29 2 -5 -8 8726.67 749.567 47 2 -5 -8 8784.22 748.253 24 2 -5 -7 3067.87 443.089 14 -2 5 7 3721.14 508.838 29 -2 5 7 3762.22 456.021 32 2 -5 -7 3715.71 489.532 18 -2 5 7 3412.26 471.470 37 2 -5 -7 3385.00 435.609 15 2 -5 -7 3487.24 436.737 24 2 -5 -6 4517.90 461.468 31 2 -5 -6 5168.83 531.404 15 2 -5 -6 5208.83 541.142 14 -2 5 6 4733.64 499.250 32 -2 5 6 5160.38 565.958 29 2 -5 -6 5097.29 517.215 24 2 -5 -6 5052.22 490.871 28 -2 5 6 5538.09 555.339 37 -2 5 5-75.4650 129.032 37 -2 5 5-22.2487 99.4097 29 2 -5 -5-66.8386 100.993 14 2 -5 -5 212.046 169.092 15 2 -5 -5-33.4384 95.0534 31 2 -5 -5 42.9834 88.0729 28 -2 5 5 36.2790 108.347 32 2 -5 -5-65.9679 84.7648 43 2 -5 -5 96.2469 107.619 24 -2 5 4 282.180 150.244 29 -2 5 4 514.732 151.754 32 2 -5 -4 300.741 121.440 31 2 -5 -4 313.845 128.015 15 2 -5 -4 337.390 117.712 43 2 -5 -4 423.279 174.972 28 2 -5 -4 326.320 127.179 33 2 -5 -4 331.009 122.020 22 -2 5 4 479.427 188.943 37 2 -5 -4 361.825 147.841 14 2 -5 -3 84.2741 126.327 1 2 -5 -3 147.457 119.440 13 2 -5 -3 0.10994 91.9209 22 2 -5 -3 233.994 131.277 43 2 -5 -3 145.146 118.473 33 -2 5 3 54.6398 110.413 29 -2 5 3 256.116 143.110 32 2 -5 -3 79.4732 105.635 15 -2 5 3 59.3714 116.407 1 2 -5 -3 90.4460 85.3312 28 2 -5 -3 74.9988 92.3606 31 2 -5 -3 131.601 81.1480 25 -2 5 3 185.974 112.548 4 2 -5 -2 15037.3 821.137 13 -2 5 2 17280.4 931.782 29 -2 5 2 17627.3 870.510 32 2 -5 -2 15208.1 797.173 33 2 -5 -2 15613.7 829.993 31 -2 5 2 13748.1 1001.61 1 2 -5 -2 13134.0 1038.20 1 2 -5 -2 17482.9 872.050 28 -2 5 2 16380.1 835.044 4 2 -5 -2 15224.3 739.377 25 2 -5 -2 15366.5 833.674 43 2 -5 -2 17492.2 882.534 15 2 -5 -2 17021.0 821.580 22 2 -5 -1 343.087 146.675 53 2 -5 -1 256.261 120.827 15 2 -5 -1 287.745 113.674 33 2 -5 -1 210.719 107.634 43 -2 5 1 267.129 141.831 4 2 -5 -1 235.256 158.282 1 -2 5 1 233.117 96.4945 32 2 -5 -1 237.578 120.632 28 2 -5 -1 247.834 94.1791 31 2 -5 -1 308.239 129.897 22 -2 5 1 291.144 172.219 1 2 -5 -1 272.000 86.1450 13 -2 5 0 61822.4 2577.17 1 2 -5 0 77986.0 2356.50 15 2 -5 0 64426.5 2285.61 53 -2 5 0 72750.0 2325.71 32 2 -5 0 65395.4 2254.52 33 -2 5 0 69888.5 2304.37 4 2 -5 0 67750.8 2273.27 31 2 -5 0 59766.0 2670.87 1 2 -5 0 69658.7 2282.08 28 2 -5 0 63164.3 2626.79 11 2 -5 0 67522.7 2288.07 43 2 -5 1 917.823 182.126 15 2 -5 1 886.268 183.915 33 -2 5 -1 716.223 150.439 4 -2 5 -1 678.429 139.007 45 2 -5 1 748.677 153.933 57 2 -5 1 797.190 169.636 31 2 -5 1 771.768 160.824 53 2 -5 1 767.276 219.577 11 2 -5 1 567.791 209.529 1 2 -5 1 957.393 176.243 28 -2 5 -1 697.821 123.649 9 2 -5 1 793.370 168.785 43 -2 5 -1 627.278 185.559 1 2 -5 2 53427.9 1916.68 53 2 -5 2 57196.7 1898.59 28 2 -5 2 49078.3 2279.10 1 -2 5 -2 48757.1 2154.03 1 -2 5 -2 56930.5 1921.10 4 2 -5 2 53002.6 1893.19 57 2 -5 2 50741.5 2165.63 11 -2 5 -2 50165.9 1812.62 45 2 -5 2 54038.8 1894.69 31 2 -5 2 55826.9 1921.55 43 -2 5 -3 9948.21 789.307 1 2 -5 3 10811.2 641.642 57 2 -5 3 11216.4 671.384 53 2 -5 3 11530.3 648.020 31 2 -5 3 9563.02 848.708 1 -2 5 -3 10291.9 637.416 4 2 -5 3 11505.7 672.463 43 2 -5 3 9807.71 770.698 11 2 -5 3 10121.5 563.547 24 2 -5 4 7744.52 668.716 11 2 -5 4 10131.5 631.904 53 2 -5 4 8821.21 577.122 57 2 -5 4 8365.78 795.433 1 -2 5 -4 8131.62 718.178 1 -2 5 -4 10415.1 625.700 4 2 -5 4 8239.21 484.006 24 -2 5 -5 31496.2 1586.40 1 2 -5 5 28202.2 1447.55 11 2 -5 5 29170.2 1660.99 1 -2 5 -6 491.339 177.414 55 -2 5 -6 493.727 146.858 4 -2 5 -6 462.162 196.340 1 2 -5 6 438.754 202.838 1 -2 5 -6 520.881 143.521 82 -2 5 -6 543.049 181.483 60 -2 5 -7 3801.41 422.697 38 -2 5 -7 3269.83 383.587 55 -2 5 -7 3213.76 392.800 80 2 -5 7 3232.05 398.936 78 -2 5 -7 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72.4402 37 2 -2 -6 70.2050 73.6449 14 -2 2 6 292.253 126.618 32 -2 2 6 128.934 112.058 11 2 -2 -6 167.254 95.5928 47 2 -2 -6 143.967 94.3389 18 2 -2 -6 109.666 84.1945 15 -2 2 6 64.4609 91.8362 29 2 -2 -6 17.4206 96.3511 12 2 -2 -6 94.9063 62.5156 24 2 -2 -5 79.2871 69.3499 18 -2 2 5 91.6539 89.6534 29 2 -2 -5 87.0885 51.9600 15 -2 2 5 136.303 103.335 37 2 -2 -5 149.565 64.8960 28 2 -2 -5 162.858 114.889 12 -2 2 5 120.488 82.1908 11 2 -2 -5 162.661 100.672 24 -2 2 5 129.779 66.6689 1 -2 2 5 95.3462 67.8694 32 2 -2 -5 131.502 78.8239 40 2 -2 -5 87.1391 66.5741 14 -2 2 4 519.234 112.110 37 -2 2 4 560.410 129.620 32 2 -2 -4 522.818 109.895 15 2 -2 -4 492.790 101.215 28 2 -2 -4 453.890 108.043 14 2 -2 -4 401.513 139.715 12 -2 2 4 481.520 167.493 11 2 -2 -4 499.127 91.0612 22 -2 2 4 563.294 138.443 29 2 -2 -4 515.821 119.625 24 -2 2 4 497.823 126.663 1 2 -2 -4 494.799 119.747 40 2 -2 -3 18139.0 690.774 9 2 -2 -3 19083.4 767.013 15 -2 2 3 16229.8 771.021 29 2 -2 -3 17304.5 757.264 24 -2 2 3 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543.398 73.1959 12 2 -2 5 636.271 203.450 10 -2 2 -5 715.627 152.121 51 2 -2 6 59645.8 1981.59 35 -2 2 -6 56751.3 1943.93 34 2 -2 6 49311.5 2247.06 10 -2 2 -6 52462.1 1920.22 51 -2 2 -6 53941.7 1939.42 56 -2 2 -6 57315.2 1937.41 38 -2 2 -6 53792.6 1909.93 55 -2 2 -6 50091.5 1822.51 1 -2 2 -6 54338.4 1947.26 60 -2 2 -6 53093.9 1927.71 61 -2 2 -7 741.064 187.278 21 2 -2 7 774.757 192.915 35 -2 2 -7 991.879 216.033 34 -2 2 -7 804.329 182.183 38 -2 2 -7 996.708 210.430 56 2 -2 7 797.969 255.448 10 -2 2 -7 819.465 196.571 51 -2 2 -7 509.955 174.574 60 -2 2 -7 654.598 187.309 61 -2 2 -8 5618.38 505.926 38 -2 2 -8 5884.40 526.117 34 -2 2 -8 5336.73 492.796 21 -2 2 -8 5734.62 516.013 51 2 -2 8 6315.50 561.334 35 -2 2 -8 6051.82 529.796 56 -2 2 -8 6217.33 541.941 60 -2 2 -8 5820.89 519.273 61 -2 2 -8 5481.58 510.327 82 -2 2 -8 5198.83 500.074 76 -2 2 -9 272.739 140.259 38 -2 2 -9 231.480 145.757 51 -2 2 -9 298.767 163.948 34 2 -2 9 288.291 140.846 35 -2 2 -9-19.2704 142.233 56 -2 2 -9 190.554 129.349 21 -2 2 -9 126.106 115.213 76 -2 2 -9 307.335 143.951 60 -2 2 -9 299.420 175.230 61 -2 2 -9 115.247 132.182 82 -2 2 -10 2614.51 377.653 38 -2 2 -10 2334.06 373.517 21 -2 2 -10 2475.50 397.511 51 -2 2 -10 2685.05 396.103 56 -2 2 -10 2530.16 402.009 34 2 -2 10 2817.94 412.974 35 -2 2 -10 2394.30 374.069 82 -2 2 -10 2601.33 392.823 60 -2 2 -10 2323.66 387.390 76 -2 2 -10 2756.24 405.737 61 -2 2 -11 388.694 177.529 56 -2 2 -11 398.709 202.446 55 2 -2 11 525.779 212.743 35 -2 2 -11 640.901 247.428 34 -2 2 -11 590.668 207.829 51 -2 2 -11 609.164 213.675 38 -2 2 -11 800.118 245.861 82 -2 2 -11 514.793 220.800 76 -2 2 -11 314.880 143.282 60 -2 2 -11 635.837 220.432 61 -2 2 -11 670.721 144.019 104 2 -2 12 2572.86 454.227 35 -2 2 -12 2152.99 408.837 34 -2 2 -12 2219.31 411.423 55 -2 2 -12 2725.02 445.629 38 -2 2 -12 2642.18 444.525 56 -2 2 -12 2329.64 428.060 51 -2 2 -12 2693.15 460.608 61 -2 2 -12 2541.47 440.383 60 -2 2 -12 2704.39 449.169 82 -2 2 -12 2662.28 439.652 76 -2 2 -12 2581.68 309.884 104 2 -2 12 2245.26 306.724 122 -2 2 -13 2183.78 419.851 38 -2 2 -13 2537.65 457.314 55 2 -2 13 2116.30 429.787 35 -2 2 -13 2235.07 425.922 51 -2 2 -13 2187.75 436.784 56 -2 2 -13 1908.44 405.255 61 -2 2 -13 1854.52 385.548 82 -2 2 -13 1877.21 403.871 60 -2 2 -13 2177.72 435.455 76 -2 2 -13 1813.79 260.551 104 -2 2 -13 1875.32 262.433 107 2 -2 13 2001.91 289.647 122 -2 2 -14 13551.3 1107.84 82 -2 2 -14 13057.5 1109.36 92 -2 2 -14 11728.9 1055.33 61 -2 2 -14 11923.4 1031.60 76 -2 2 -14 12142.8 1073.25 60 -2 2 -14 11751.1 1045.83 38 -2 2 -14 12821.6 1101.86 56 2 -2 14 10390.3 1025.93 35 -2 2 -14 12640.1 1069.19 55 2 -2 14 9372.58 706.615 145 2 -2 14 10452.9 751.603 161 2 -2 14 11786.5 805.944 139 2 -2 14 10004.4 773.103 167 -2 2 -14 12154.8 758.146 104 2 -2 14 13423.0 811.345 122 -2 2 -14 12552.9 764.157 107 -2 2 -15 32728.2 1881.43 82 -2 2 -15 29390.2 1758.55 76 -2 2 -15 27466.1 1748.06 60 -2 2 -15 29897.4 1825.12 61 -2 2 -15 33797.5 1905.53 92 -2 2 -15 27698.3 1756.23 38 -2 2 -15 28632.4 1788.80 56 -2 2 -15 29515.9 1784.64 55 2 -2 15 31047.3 1442.93 139 2 -2 15 29341.3 1435.53 167 2 -2 15 28925.7 1385.22 161 2 -2 15 27372.1 1335.32 145 -2 2 -15 30029.0 1339.75 107 -2 2 -15 29018.5 1335.35 104 -2 2 -16 187.135 286.144 92 -2 2 -16-90.4015 173.668 82 -2 2 -16 476.719 280.187 61 -2 2 -16-85.8668 178.270 76 -2 2 -16-46.6490 205.688 60 -2 2 -16 204.942 158.891 55 -2 2 -16 170.416 177.478 56 2 -2 16 58.1566 133.346 161 2 -2 16 70.5785 107.750 139 2 -2 16 244.117 150.311 144 2 -2 16 207.384 217.214 167 -2 2 -16 380.329 158.088 103 -2 2 -16 388.932 172.569 107 -2 2 -16 71.7051 127.055 104 -2 2 -17 13579.6 1138.71 92 -2 2 -17 11819.1 1039.94 80 -2 2 -17 11435.5 1044.85 82 2 -2 17 13284.3 822.297 144 2 -2 17 11787.9 764.264 161 2 -2 17 12529.0 796.713 167 -2 2 -17 14519.9 834.199 103 -2 2 -18 10300.5 671.028 97 2 -2 18 10475.5 679.310 144 2 -2 18 9117.89 631.330 161 -2 2 -18 9668.25 653.173 103 -2 2 -18 11130.9 670.183 118 2 -2 19-24.4093 69.7327 161 2 -2 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148 2 9 11 3634.78 403.144 162 2 9 12 451.294 149.840 148 2 9 12 156.185 126.707 162 2 9 13 707.560 152.348 148 2 9 13 910.111 194.867 162 -2 -10 20 48.7207 61.7694 139 2 10 -20 26.0884 56.8820 165 2 10 -20-8.23008 73.5141 126 -2 -10 19 1135.89 191.903 139 2 10 -19 1579.53 226.132 147 2 10 -19 1356.49 197.061 165 2 10 -19 881.227 161.804 118 2 10 -19 1424.71 212.248 126 -2 -10 19 1304.12 199.076 122 2 10 -18 1534.43 244.618 147 2 10 -18 1284.64 217.331 165 -2 -10 18 1032.30 217.642 163 2 10 -18 1039.17 199.234 123 2 10 -18 961.402 202.119 126 2 10 -18 950.565 186.493 118 -2 -10 18 855.193 198.779 122 -2 -10 17 984.036 215.898 163 2 10 -17 997.486 246.316 147 2 10 -17 1135.24 239.353 126 2 10 -17 1315.98 235.177 123 -2 -10 17 1013.06 214.140 122 -2 -10 17 1240.52 233.495 127 2 10 -17 1081.07 213.113 118 2 10 -16 343.927 153.430 149 -2 -10 16 161.303 129.153 163 2 10 -16 395.854 160.622 147 2 10 -16 305.753 132.213 126 2 10 -16 360.776 156.193 118 2 10 -16 296.679 168.072 123 -2 -10 16 397.263 179.387 127 -2 -10 16 412.244 169.431 122 -2 -10 15 1044.94 377.878 78 -2 -10 15 1100.35 275.311 163 2 10 -15 1074.57 230.809 149 2 10 -15 1075.06 265.827 147 -2 -10 15 1251.09 245.243 127 -2 -10 15 1058.98 226.262 122 2 10 -15 1029.82 222.356 126 2 10 -15 1049.75 231.446 123 -2 -10 14-49.6864 161.221 78 2 10 -14 90.1972 127.935 147 -2 -10 14 366.719 170.512 163 2 10 -14 85.4296 102.808 149 -2 -10 14 154.905 118.247 160 -2 -10 14 103.037 111.056 127 2 10 -14 119.571 123.066 123 2 10 -14 54.0455 161.573 126 -2 -10 14 3.33741 129.526 122 -2 -10 13 1635.96 417.366 78 2 10 -13 1737.45 275.759 96 -2 -10 13 2027.38 319.502 160 -2 -10 13 1928.47 316.693 163 2 10 -13 1702.51 282.965 149 2 10 -13 1999.02 326.564 147 2 10 -13 1786.66 282.111 123 -2 -10 13 1820.37 296.264 122 2 10 -13 1968.49 314.076 126 -2 -10 13 1920.60 292.401 127 -2 -10 12 682.230 304.894 78 2 10 -12 786.150 189.534 96 -2 -10 12 719.342 218.818 164 2 10 -12 597.600 202.470 147 -2 -10 12 375.865 185.893 163 2 10 -12 454.814 184.490 149 -2 -10 12 502.589 196.812 160 -2 -10 12 533.291 167.216 122 2 10 -12 461.269 179.901 123 -2 -10 12 416.373 179.943 127 2 10 -12 638.521 219.225 126 -2 -10 11 199.741 257.256 78 2 10 -11 56.5353 87.4078 96 2 10 -11-1.08216 121.480 147 -2 -10 11 211.407 161.911 164 2 10 -11-52.9100 122.011 149 -2 -10 11 113.550 160.083 160 -2 -10 11 198.922 176.560 163 -2 -10 11 162.488 131.282 143 2 10 -11 31.9198 109.043 126 -2 -10 11 223.002 124.163 127 -2 -10 11 195.208 139.208 122 2 10 -11 200.704 161.602 123 -2 -10 11 130.353 145.044 114 -2 -10 10 1901.05 399.202 84 2 10 -10 2182.59 300.135 96 -2 -10 10 1553.50 398.274 78 2 10 -10 1433.21 277.357 126 -2 -10 10 2833.88 360.830 102 -2 -10 10 2040.10 324.403 114 -2 -10 10 1669.91 265.839 122 2 10 -10 1817.91 287.241 123 2 10 -9 145.686 156.213 4 -2 -10 9 351.293 202.170 84 2 10 -9 375.164 162.966 96 -2 -10 9 532.666 211.935 89 -2 -10 9 410.704 217.873 78 -2 -10 9 134.008 89.8308 122 2 10 -9 513.716 175.342 123 -2 -10 9 423.575 168.148 114 2 10 -9 241.809 155.067 126 -2 -10 9 307.169 153.446 102 2 10 -8 2044.85 382.291 4 2 10 -8 2387.31 302.243 96 -2 -10 8 2318.88 436.719 84 -2 -10 8 2451.55 417.399 89 -2 -10 8 1664.03 387.985 78 -2 -10 8 2079.01 399.657 77 -2 -10 8 1475.91 246.489 122 -2 -10 8 2159.64 317.364 102 -2 -10 8 2257.23 322.923 114 2 10 -8 2073.78 292.129 123 -2 -10 8 2287.70 303.468 109 -2 -10 8 2366.92 330.899 108 2 10 -7 5467.28 636.659 4 -2 -10 7 6149.49 693.682 84 -2 -10 7 5916.13 675.032 78 2 10 -7 6514.40 507.691 96 -2 -10 7 6179.21 680.766 77 -2 -10 7 6684.41 518.338 102 -2 -10 7 6418.13 519.455 114 -2 -10 7 5500.85 492.434 108 -2 -10 6 10380.8 897.138 33 -2 -10 6 10133.0 838.525 53 -2 -10 6 9864.67 832.673 43 2 10 -6 11821.1 942.373 4 -2 -10 6 12487.5 961.329 78 -2 -10 6 13301.4 1007.85 84 -2 -10 6 12501.8 973.911 77 2 10 -6 12703.4 714.425 96 -2 -10 6 12141.7 982.029 62 -2 -10 6 11438.6 709.898 102 -2 -10 6 11652.4 722.628 114 -2 -10 6 11276.4 713.588 108 -2 -10 5 5247.90 610.651 33 -2 -10 5 4593.44 532.400 28 -2 -10 5 4937.77 562.800 43 2 10 -5 4702.05 578.531 4 -2 -10 5 4480.97 550.765 64 2 10 -5 5527.84 450.590 96 -2 -10 5 5479.89 625.527 62 -2 -10 5 4494.04 562.860 78 -2 -10 5 5477.70 621.070 84 -2 -10 5 5679.79 460.201 102 -2 -10 5 4907.56 442.118 114 -2 -10 5 5349.31 458.148 108 -2 -10 4 2226.05 423.240 22 2 10 -4 2530.48 426.155 4 -2 -10 4 1702.07 323.277 15 -2 -10 4 2318.44 406.729 54 -2 -10 4 2185.41 373.217 28 -2 -10 4 2199.88 417.136 33 -2 -10 4 1894.99 361.668 78 2 10 -4 2287.68 300.166 96 -2 -10 4 2539.29 416.272 64 -2 -10 4 2460.97 426.824 62 -2 -10 4 2217.78 286.834 108 -2 -10 3 531.500 232.083 22 -2 -10 3 239.127 157.074 28 -2 -10 3 262.580 161.521 33 -2 -10 3 185.751 132.097 15 2 10 -3 274.515 155.109 4 -2 -10 3 510.099 266.114 54 -2 -10 3 449.341 206.532 62 -2 -10 3 319.872 210.613 67 2 10 -3 485.115 147.348 96 -2 -10 3-121.843 194.434 78 -2 -10 3 445.945 197.443 64 -2 -10 3 382.391 136.764 108 -2 -10 2 6122.20 632.193 78 2 10 -2 7342.85 523.922 96 -2 -10 2 7061.62 706.163 62 -2 -10 2 5914.64 644.440 67 -2 -10 2 5698.64 619.214 64 -2 -10 2 6748.65 707.824 54 2 10 -2 5639.76 650.026 4 -2 -10 2 5381.42 608.701 15 -2 -10 2 6836.95 698.019 33 -2 -10 2 6683.18 696.053 22 -2 -10 1 883.390 261.796 62 -2 -10 1 1012.14 291.810 67 -2 -10 1 810.597 232.656 64 -2 -10 1 763.349 238.591 78 -2 -10 1 938.296 278.135 22 -2 -10 1 1004.90 284.755 33 -2 -10 1 707.168 217.444 25 -2 -10 1 1223.43 334.700 54 2 10 -1 734.417 268.235 4 -2 -10 1 1004.28 269.843 15 -2 -10 0 3016.49 467.269 67 -2 -10 0 3307.63 465.926 78 -2 -10 0 3414.46 517.608 62 -2 -10 0 3142.58 501.949 22 -2 -10 0 3283.43 514.015 33 2 10 0 3575.88 506.504 4 -2 -10 0 3523.32 522.072 54 -2 -10 0 3057.98 489.692 25 -2 -10 -1 11299.7 913.132 67 -2 -10 -1 13139.6 1023.88 33 2 10 1 9876.46 945.081 29 -2 -10 -1 13344.7 1032.19 54 -2 -10 -1 12384.2 1004.10 25 -2 -10 -1 12068.9 1011.26 22 2 10 1 11050.8 933.577 4 -2 -10 -2 14371.5 1039.43 67 -2 -10 -2 14169.8 1105.36 25 -2 -10 -2 14027.3 1111.35 22 -2 -10 -2 13391.7 1098.05 15 2 10 2 11913.2 1076.35 29 2 10 2 12623.9 1012.57 4 -2 -10 -2 15067.6 1115.81 54 -2 -10 -3-124.856 209.702 22 -2 -10 -3 42.1569 139.032 19 -2 -10 -3-106.674 186.131 54 -2 -10 -3-26.8389 108.510 15 2 10 3-47.6185 154.690 29 -2 -10 -3-27.2675 167.205 25 2 10 3-53.3782 120.860 148 2 10 3 29.6379 92.5343 134 2 10 4 2811.33 528.308 29 -2 -10 -4 2929.47 493.037 54 -2 -10 -4 2472.71 455.104 25 -2 -10 -4 1990.36 436.688 22 2 10 4 2298.66 344.310 146 2 10 4 3084.05 378.084 134 2 10 4 2848.31 382.579 148 -2 -10 -5 1585.21 377.835 54 -2 -10 -5 810.081 262.235 33 -2 -10 -5 1101.51 341.078 28 2 10 5 1526.60 439.277 29 -2 -10 -5 888.088 284.754 25 2 10 5 1508.77 273.448 134 2 10 5 1403.40 280.748 148 2 10 5 1582.55 276.986 146 -2 -10 -6-43.5639 176.477 33 2 10 6 311.086 270.715 29 2 10 6 119.612 152.013 134 2 10 6 162.887 123.112 146 2 10 6 77.2966 120.006 148 2 10 7-34.0276 123.336 146 2 10 7-7.39280 134.373 148 2 10 7-33.6751 145.436 134 2 10 8 5786.04 524.712 134 2 10 8 5257.22 509.768 146 2 10 8 5319.42 532.722 148 2 10 9 2358.27 309.724 162 2 10 9 2365.08 317.420 134 2 10 9 2582.32 357.857 148 2 10 9 2824.70 369.197 146 2 10 10 1975.95 298.045 162 2 10 10 1972.89 280.074 134 2 10 10 2254.95 306.083 146 2 10 10 1985.11 308.188 148 2 10 11 208.467 140.083 162 2 10 11 126.467 100.217 146 2 10 11 147.905 122.416 148 2 10 12 230.790 112.027 148 -2 -11 20 128.399 64.9384 139 -2 -11 19 32.6474 77.4495 139 2 11 -19 153.708 83.4655 165 -2 -11 19 62.6392 59.1834 163 -2 -11 19-120.085 91.6985 122 2 11 -19 88.4814 94.2277 126 -2 -11 18 3264.66 322.990 163 2 11 -18 2683.36 278.520 165 -2 -11 18 3249.26 329.666 122 2 11 -17-47.0923 122.792 147 -2 -11 17-18.3673 111.291 163 2 11 -17 116.652 90.6107 165 -2 -11 17-130.135 111.647 122 2 11 -17-97.7540 110.178 126 -2 -11 17 296.192 136.652 127 2 11 -17 98.7655 117.864 123 -2 -11 16 3045.13 393.685 163 2 11 -16 3400.02 392.334 147 2 11 -16 3051.31 332.225 149 -2 -11 16 3636.80 371.612 122 -2 -11 16 3477.73 367.812 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700.313 78 2 11 -6 5981.63 493.195 96 -2 -11 6 5292.62 486.121 114 -2 -11 6 5339.24 481.643 102 -2 -11 6 5238.66 481.297 108 -2 -11 5 6160.74 666.404 31 -2 -11 5 7146.85 771.572 33 2 11 -5 7487.86 785.222 4 -2 -11 5 7016.69 734.982 53 -2 -11 5 5630.16 650.202 28 -2 -11 5 6888.68 726.707 43 -2 -11 5 7943.16 805.895 84 -2 -11 5 7211.77 769.346 62 2 11 -5 8713.39 605.657 96 -2 -11 5 7425.56 753.242 78 -2 -11 5 7764.10 572.774 114 -2 -11 5 7294.84 562.838 108 -2 -11 5 7679.94 577.297 102 -2 -11 4 5744.93 651.700 31 -2 -11 4 5885.85 712.241 54 -2 -11 4 6691.46 745.852 33 -2 -11 4 5303.42 627.630 28 -2 -11 4 6721.03 726.614 43 2 11 -4 5900.55 691.268 4 -2 -11 4 6185.92 677.143 78 2 11 -4 7719.52 569.650 96 -2 -11 4 5804.39 654.275 64 -2 -11 4 6883.26 761.003 62 -2 -11 4 7075.54 753.020 84 -2 -11 4 7427.80 551.989 102 -2 -11 4 6058.87 503.121 108 -2 -11 4 6768.29 549.032 114 -2 -11 3 112.680 187.434 22 -2 -11 3 448.555 247.848 33 -2 -11 3 99.8956 146.402 15 2 11 -3 416.255 246.102 4 -2 -11 3 127.073 105.808 28 -2 -11 3 443.319 238.154 54 -2 -11 3 35.7182 114.604 64 -2 -11 3 154.727 171.272 62 -2 -11 3 187.957 158.501 78 2 11 -3 98.3330 96.2971 96 -2 -11 3 147.351 121.390 108 -2 -11 2 1502.32 352.425 22 2 11 -2 1963.66 402.750 4 -2 -11 2 2218.86 428.228 33 -2 -11 2 1539.78 349.107 28 -2 -11 2 2020.84 411.317 54 -2 -11 2 1501.38 334.726 15 -2 -11 2 2173.00 436.176 67 -2 -11 2 2602.38 487.535 62 -2 -11 2 2095.26 394.050 78 -2 -11 2 2269.95 301.808 108 -2 -11 1 4870.52 603.292 67 -2 -11 1 5562.48 683.077 62 -2 -11 1 5952.57 709.923 33 -2 -11 1 4435.77 597.284 28 -2 -11 1 4635.67 622.971 15 2 11 -1 5222.45 639.608 4 -2 -11 1 5036.67 659.956 54 -2 -11 1 4461.39 635.047 22 -2 -11 0 2182.39 391.790 67 -2 -11 0 1907.82 419.161 62 -2 -11 0 2222.83 432.696 22 -2 -11 0 1787.69 408.373 33 -2 -11 0 1614.68 375.072 15 -2 -11 0 2403.46 462.640 54 -2 -11 0 1857.87 388.735 28 2 11 0 2060.67 422.362 4 -2 -11 -1 2164.66 445.891 62 2 11 1 873.011 218.910 148 2 11 1 1320.18 244.509 149 2 11 1 1578.68 270.033 134 -2 -11 -1 1399.76 346.658 28 -2 -11 -1 1119.47 351.682 22 2 11 1 1023.14 280.810 4 -2 -11 -1 1255.34 348.317 33 -2 -11 -1 1575.10 360.522 54 -2 -11 -1 1172.45 318.708 25 2 11 1 1150.37 219.056 6 -2 -11 -2 454.842 276.389 62 2 11 2 446.919 159.334 134 2 11 2 540.124 191.299 148 -2 -11 -2 394.922 245.419 54 -2 -11 -2 184.062 207.816 33 -2 -11 -2-76.0798 126.777 28 -2 -11 -2 227.426 205.371 25 -2 -11 -2 243.115 201.929 22 -2 -11 -3 2583.96 487.048 62 2 11 3 2501.91 360.492 148 2 11 3 2638.40 352.287 134 -2 -11 -3 3040.02 530.700 33 -2 -11 -3 1522.20 374.574 25 -2 -11 -3 2390.46 462.432 54 -2 -11 -3 2130.92 459.469 28 -2 -11 -4 2538.88 479.984 62 2 11 4 1796.82 465.771 29 -2 -11 -4 1965.62 448.073 33 -2 -11 -4 2501.22 512.297 54 2 11 4 2478.52 343.169 134 2 11 4 1920.67 346.635 148 2 11 4 2181.09 339.025 146 2 11 5 159.905 157.148 146 2 11 5-222.655 166.950 148 2 11 5 209.868 183.973 134 2 11 6 2582.43 364.340 146 2 11 6 2462.47 354.464 134 2 11 6 2282.71 364.729 148 2 11 7 282.067 160.278 146 2 11 7 192.375 137.716 134 2 11 7 313.068 145.011 148 2 11 8 1443.52 267.390 146 2 11 8 1161.15 242.248 134 2 11 8 1237.60 292.080 148 2 11 9 796.830 178.599 146 2 11 9 1149.30 232.168 148 2 11 9 1102.38 204.531 134 2 11 10 19.5095 67.3117 146 2 11 10 10.7858 95.3849 148 2 11 11-203.769 122.555 148 -2 -12 19 15.8907 55.5632 163 -2 -12 19 148.904 79.2979 139 2 12 -19 114.439 76.4610 126 -2 -12 18 1318.56 192.857 163 -2 -12 18 1256.79 189.437 122 2 12 -18 1660.26 232.155 126 -2 -12 17 3119.91 332.590 163 2 12 -17 3342.35 349.961 126 -2 -12 17 2421.21 285.307 122 -2 -12 16 1777.58 273.529 163 2 12 -16 1531.54 233.654 149 -2 -12 16 1638.86 246.299 127 -2 -12 16 1268.24 210.996 122 -2 -12 15-69.8926 133.758 78 2 12 -15 338.182 141.766 149 -2 -12 15 334.234 182.669 163 2 12 -15 361.287 193.797 126 -2 -12 15 229.510 125.380 122 -2 -12 15 84.7869 107.345 127 -2 -12 14 131.003 125.404 78 -2 -12 14 186.202 164.146 163 -2 -12 14 169.444 148.607 160 2 12 -14-122.634 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213.165 143 -2 -12 10 465.392 201.251 114 2 12 -10 278.253 155.372 126 -2 -12 9 2338.02 504.448 78 -2 -12 9 3463.13 582.963 84 2 12 -9 2918.87 372.780 96 -2 -12 9 2876.18 505.193 89 2 12 -9 2311.96 311.854 6 2 12 -9 1786.04 423.389 4 -2 -12 9 3026.87 380.459 143 2 12 -9 2025.20 310.090 135 -2 -12 9 2134.77 306.848 151 2 12 -9 2591.53 354.307 149 -2 -12 9 3116.05 400.808 160 -2 -12 9 2362.42 378.881 163 2 12 -9 3004.73 376.220 126 -2 -12 9 3272.11 419.246 102 -2 -12 9 2746.05 357.801 109 -2 -12 9 3003.81 398.694 114 2 12 -8 248.247 156.344 96 -2 -12 8 166.441 183.342 84 -2 -12 8 196.805 128.917 77 -2 -12 8 157.657 144.764 89 -2 -12 8-62.2589 162.837 78 2 12 -8 95.9261 123.518 4 2 12 -8 14.3121 111.144 6 2 12 -8 212.250 127.188 149 -2 -12 8 97.0026 145.706 143 2 12 -8 270.809 175.157 135 -2 -12 8 479.028 222.068 102 -2 -12 8 218.171 135.312 109 -2 -12 8-57.1545 142.338 114 2 12 -8 270.128 183.358 126 2 12 -7 311.805 136.121 96 -2 -12 7 172.356 215.546 84 -2 -12 7 411.219 214.729 78 -2 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318.569 166 -4 13 -10 2039.68 321.595 165 4 -13 10 2414.07 333.008 163 -4 13 -10 2161.14 326.871 118 4 -13 10 2256.41 378.654 128 4 -13 10 2395.13 389.505 129 -4 13 -10 2102.92 323.690 126 -4 13 -11 517.845 197.054 165 4 -13 11 73.4654 137.411 166 4 -13 11 294.556 170.310 163 -4 13 -11 294.080 125.425 118 4 -13 11 261.255 157.741 128 4 -13 11 463.654 197.326 129 -4 13 -11 18.6385 123.619 126 -4 13 -11-112.327 110.641 103 -4 13 -12-158.664 153.571 165 4 -13 12-278.424 154.072 163 -4 13 -12 275.071 123.964 103 -4 13 -12 66.7947 122.965 118 4 -13 12-146.988 132.883 128 -4 13 -12 79.2520 144.601 126 -4 13 -13 27.9648 116.167 165 4 -13 13 39.8640 117.527 163 -4 13 -13-155.409 130.885 103 -4 13 -13 121.760 114.456 126 -4 13 -13 122.844 130.640 118 4 -13 13 124.126 110.680 128 -4 13 -14 1263.36 236.927 165 4 -13 14 1275.63 239.110 163 -4 13 -14 1048.53 215.012 103 -4 13 -14 1413.91 234.198 118 -4 13 -14 1205.58 230.270 126 4 -13 15 98.7956 120.608 163 -4 13 -15 178.224 128.221 165 -4 13 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368.660 6 4 -12 1 2220.59 462.911 57 4 -12 1 2118.96 468.641 3 4 -12 1 1623.48 412.679 24 4 -12 1 2405.05 524.582 63 4 -12 1 2554.02 495.288 77 4 -12 1 2075.51 482.612 89 -4 12 -1 2575.88 371.468 126 4 -12 1 2547.81 348.173 109 4 -12 2 30465.8 1858.41 63 4 -12 2 32308.7 1914.14 77 4 -12 2 31392.5 1883.09 89 -4 12 -2 31058.7 1395.42 6 4 -12 2 25007.1 1690.10 40 4 -12 2 25997.6 1754.28 3 4 -12 2 29277.5 1821.10 57 -4 12 -2 25310.0 1269.83 165 4 -12 2 30858.2 1403.47 109 -4 12 -2 31941.2 1421.79 126 4 -12 3 6170.39 786.756 63 4 -12 3 7260.26 885.997 77 4 -12 3 7473.83 875.415 89 -4 12 -3 6200.81 553.677 6 4 -12 3 7523.85 867.905 57 4 -12 3 5555.55 729.867 40 4 -12 3 4974.03 723.618 3 -4 12 -3 5148.78 508.958 165 4 -12 3 6252.73 590.849 109 -4 12 -3 8054.52 645.826 126 4 -12 4 3738.93 594.122 87 4 -12 4 3824.37 617.031 63 4 -12 4 3757.00 612.006 89 4 -12 4 3972.21 648.498 77 -4 12 -4 3451.99 413.996 6 4 -12 4 2856.15 533.610 3 -4 12 -4 3094.49 374.540 165 -4 12 -4 3306.21 399.625 149 4 -12 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118 -4 12 -11 729.108 199.186 126 -4 12 -12 490.827 282.632 165 4 -12 12 484.712 172.890 163 4 -12 12 381.635 166.678 128 -4 12 -12 388.607 168.397 103 -4 12 -12 506.471 190.798 118 -4 12 -12 626.432 207.744 126 -4 12 -13 8029.23 603.494 165 4 -12 13 7152.96 591.207 163 -4 12 -13 7464.41 600.670 118 4 -12 13 6240.29 549.500 128 -4 12 -13 6772.44 572.840 103 -4 12 -13 7340.81 591.403 126 4 -12 14 1649.66 259.040 139 -4 12 -14 2528.57 328.804 165 4 -12 14 2386.35 329.406 163 -4 12 -14 2135.25 308.701 118 -4 12 -14 1717.07 274.757 103 -4 12 -14 2307.79 301.635 130 -4 12 -14 1965.96 296.438 126 4 -12 15 262.002 131.250 139 4 -12 15 153.564 138.591 163 -4 12 -15-19.2794 120.311 165 -4 12 -15 22.1924 118.640 118 -4 12 -15 107.696 99.1470 103 -4 12 -15 168.377 127.055 126 4 -12 16 545.260 157.042 163 -4 12 -16 307.922 120.739 150 -4 12 -16 347.215 118.222 165 4 -12 16 205.373 96.5337 139 -4 12 -16 535.041 165.285 118 -4 12 -16 544.232 142.493 126 4 -12 17 427.195 120.072 139 -4 12 -17 583.196 157.670 165 4 -12 17 425.095 120.812 163 -4 12 -17 193.526 70.8141 118 4 -12 18-62.2107 72.2572 163 -4 12 -18 64.4450 79.7995 165 -4 11 12 60.1883 68.8402 154 -4 11 12 130.640 82.2768 162 -4 11 11 1247.68 195.460 154 -4 11 11 912.659 165.759 162 -4 11 11 1291.78 210.715 146 -4 11 10 669.954 162.032 154 -4 11 10 575.051 151.658 146 -4 11 10 492.817 127.808 162 -4 11 9 128.798 108.535 154 -4 11 9 167.753 126.838 162 -4 11 9 80.4867 80.3152 146 -4 11 8 856.105 197.487 154 -4 11 8 656.747 196.268 146 4 -11 -7 200.024 171.682 65 4 -11 -7 306.092 227.315 87 -4 11 7 485.168 200.010 154 -4 11 7 483.704 159.781 146 4 -11 -6 940.038 352.087 87 4 -11 -6 648.369 289.812 65 4 -11 -6 410.337 200.187 70 4 -11 -6 841.011 303.048 69 -4 11 6 730.039 186.287 154 -4 11 6 1118.86 243.814 146 4 -11 -5 111.012 216.744 70 4 -11 -5-95.0982 173.435 63 4 -11 -5 257.944 208.597 65 4 -11 -5 144.668 135.685 57 4 -11 -5 104.630 177.010 47 4 -11 -5 111.484 440.950 40 -4 11 5 68.1621 113.630 146 -4 11 5-8.85374 104.413 154 4 -11 -4 350.787 186.199 63 4 -11 -4 471.271 201.909 83 -4 11 4 448.346 261.539 37 4 -11 -4 297.581 216.124 57 4 -11 -4 450.515 271.247 47 4 -11 -4 281.257 235.004 40 -4 11 4 150.839 94.5755 146 -4 11 4 163.899 133.110 154 -4 11 4 475.336 173.193 117 4 -11 -3 14396.9 1253.31 63 -4 11 3 12922.4 1164.63 37 4 -11 -3 13938.1 1251.68 40 4 -11 -3 13231.6 1186.98 57 4 -11 -3 12594.8 1196.09 47 4 -11 -3 14036.0 1227.42 53 4 -11 -3 12964.1 1212.14 24 -4 11 3 13100.2 845.469 154 -4 11 3 12753.0 857.156 146 -4 11 3 15325.9 923.428 117 -4 11 2 5029.28 489.342 6 -4 11 2 5933.30 749.270 37 4 -11 -2 4579.05 650.748 3 -4 11 2 4518.86 626.621 32 4 -11 -2 5927.53 779.145 53 4 -11 -2 5790.90 765.160 57 4 -11 -2 5304.46 750.856 24 4 -11 -2 5844.12 780.152 40 4 -11 -2 6331.73 795.585 63 -4 11 2 6284.89 566.903 117 -4 11 1 25616.9 1316.92 6 -4 11 1 30601.0 1837.10 37 -4 11 1 26488.7 1654.19 32 4 -11 -1 27977.3 1768.74 3 4 -11 -1 29810.8 1841.00 57 4 -11 -1 32674.3 1928.68 53 4 -11 -1 27638.1 1795.52 24 4 -11 -1 30074.8 1881.17 40 4 -11 -1 31674.3 1876.07 63 4 -11 -1 28101.3 1726.22 89 4 -11 -1 30530.7 1820.18 77 -4 11 1 31429.7 1448.31 117 -4 11 1 32540.4 1420.76 126 -4 11 0 4391.08 467.232 6 -4 11 0 4068.09 597.998 32 4 -11 0 3852.05 595.492 3 4 -11 0 5143.83 716.893 53 4 -11 0 4718.84 671.712 57 4 -11 0 4239.75 639.498 24 4 -11 0 5220.62 708.777 40 4 -11 0 4843.50 658.846 63 4 -11 0 4374.77 648.620 77 4 -11 0 5005.54 674.568 89 4 -11 0 4742.54 469.167 109 -4 11 0 4978.25 490.135 126 -4 11 -1 20403.4 1411.52 32 4 -11 1 22069.0 1529.78 3 4 -11 1 25195.9 1594.37 57 4 -11 1 19396.5 1426.37 24 4 -11 1 22229.6 1531.51 40 4 -11 1 23778.4 1562.55 63 4 -11 1 26404.9 1628.94 77 4 -11 1 22963.7 1515.19 89 4 -11 1 23252.8 1152.61 109 -4 11 -1 23198.0 1173.42 126 4 -11 2 21625.6 1479.84 57 -4 11 -2 20050.7 1382.18 32 4 -11 2 17709.0 1334.45 24 4 -11 2 19767.7 1409.68 40 4 -11 2 23539.0 1533.85 77 4 -11 2 23301.4 1514.67 63 4 -11 2 23234.5 1528.41 89 4 -11 2 22100.2 1118.21 109 -4 11 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347.452 194.222 3 -4 11 -7 650.361 220.739 165 4 -11 7 803.590 252.466 166 -4 11 -7 354.696 146.035 103 -4 11 -7 488.142 178.846 118 4 -11 7 534.877 185.635 109 4 -11 7 413.736 160.794 129 4 -11 7 422.317 203.337 128 -4 11 -7 556.882 198.441 126 4 -11 8 18562.6 1387.30 89 -4 11 -8 14430.7 895.127 6 4 -11 8 12017.0 1096.89 3 4 -11 8 15424.6 984.664 166 -4 11 -8 15578.5 940.695 165 4 -11 8 14088.6 902.214 160 -4 11 -8 17618.7 972.332 103 -4 11 -8 17225.9 972.703 126 -4 11 -8 17574.0 972.112 118 4 -11 8 16019.7 1002.58 128 4 -11 8 15134.8 930.356 129 4 -11 9 2069.62 451.224 89 4 -11 9 1298.28 264.345 163 -4 11 -9 1503.09 305.893 165 4 -11 9 1264.79 283.640 166 4 -11 9 1572.01 315.075 128 -4 11 -9 1255.68 260.190 130 -4 11 -9 1529.33 273.053 118 -4 11 -9 1725.71 289.328 103 -4 11 -9 1760.51 300.810 126 4 -11 9 1796.77 325.321 129 4 -11 10 2517.96 504.989 89 -4 11 -10 3016.08 398.939 165 4 -11 10 2669.08 384.367 163 4 -11 10 3305.05 443.138 166 -4 11 -10 3896.81 438.629 126 -4 11 -10 3095.23 407.100 103 -4 11 -10 2615.50 382.444 130 -4 11 -10 3483.50 408.517 118 4 -11 10 3149.39 423.908 129 4 -11 10 2913.98 410.691 128 -4 11 -11 2052.27 347.344 165 4 -11 11 2309.29 374.044 163 4 -11 11 1949.64 328.558 166 -4 11 -11 2184.99 345.322 103 -4 11 -11 2206.50 353.249 118 -4 11 -11 1830.06 322.199 130 4 -11 11 1345.28 291.414 128 4 -11 11 1562.61 294.940 129 -4 11 -11 2363.48 351.734 126 -4 11 -12 1548.88 315.810 165 4 -11 12 1575.99 312.687 163 -4 11 -12 1646.46 274.448 150 -4 11 -12 1807.79 305.927 118 -4 11 -12 1666.72 283.429 130 4 -11 12 1572.50 298.153 128 -4 11 -12 1466.31 271.222 103 -4 11 -12 1288.72 272.393 126 -4 11 -13 3057.62 370.171 150 4 -11 13 2698.59 356.524 139 -4 11 -13 3343.97 404.906 165 4 -11 13 3189.70 408.604 163 -4 11 -13 3162.05 412.802 103 -4 11 -13 2943.95 369.205 118 -4 11 -13 3105.35 386.491 130 4 -11 13 2581.58 362.276 128 -4 11 -13 3141.47 388.921 126 4 -11 14 5396.94 492.846 139 4 -11 14 6696.63 566.198 163 -4 11 -14 5440.57 503.217 150 -4 11 -14 6845.48 559.481 165 -4 11 -14 5582.48 544.832 103 -4 11 -14 6091.81 538.368 130 -4 11 -14 5866.55 522.264 118 -4 11 -14 6049.74 531.297 126 4 -11 15 1915.83 326.469 163 4 -11 15 2047.87 300.143 139 -4 11 -15 2201.27 291.711 150 -4 11 -15 1963.87 310.769 165 -4 11 -15 2124.20 320.