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Information card for entry 7132207
Preview
| Coordinates | 7132207.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C19 H27 N O4 |
|---|---|
| Calculated formula | C19 H27 N O4 |
| Title of publication | Brønsted acid-catalyzed annulation reaction of hydroxamic acids: synthesis of cyclopentane-fused isoxazolidines and their benzilic amide rearrangement |
| Authors of publication | Mondal, Swati Lekha; Bhajammanavar, Vinod; Ramakrishna, Isai; Baidya, Mahiuddin |
| Journal of publication | Chemical Communications |
| Year of publication | 2023 |
| a | 26.239 ± 0.005 Å |
| b | 14.599 ± 0.003 Å |
| c | 10.4681 ± 0.0018 Å |
| α | 90° |
| β | 112.952 ± 0.008° |
| γ | 90° |
| Cell volume | 3692.5 ± 1.2 Å3 |
| Cell temperature | 298 ± 2 K |
| Ambient diffraction temperature | 298 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0557 |
| Residual factor for significantly intense reflections | 0.0453 |
| Weighted residual factors for significantly intense reflections | 0.1286 |
| Weighted residual factors for all reflections included in the refinement | 0.1419 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.078 |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 286931 (current) | 2023-10-13 | cif/ Adding structures of 7132206, 7132207 via cif-deposit CGI script. |
7132207.cif |
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