Crystallography Open Database

Information card for entry 7133340

Preview

Coordinates	7133340.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H82 N4 Si4 Yb
Calculated formula	C47 H82 N4 Si4 Yb
Title of publication	Yb/Si frustrated Lewis pairs with a labile naphthalenyl bridge.
Authors of publication	Xu, Cheng; Zhao, Sixuan; Zhang, Heng; Peng, Qian; Chen, Yaofeng
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	64
Pages of publication	8411 - 8414
a	17.9657 ± 0.0008 Å
b	22.4892 ± 0.001 Å
c	28.4392 ± 0.0014 Å
α	90°
β	90°
γ	90°
Cell volume	11490.4 ± 0.9 Å³
Cell temperature	169.98 K
Ambient diffraction temperature	169.98 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.1254
Residual factor for significantly intense reflections	0.0672
Weighted residual factors for significantly intense reflections	0.1726
Weighted residual factors for all reflections included in the refinement	0.2026
Goodness-of-fit parameter for all reflections included in the refinement	1.121
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
294423 (current)	2024-09-06	cif/ Updating files of 7133340, 7133341, 7133342, 7133343, 7133344 Original log message: Adding full bibliography for 7133340--7133344.cif.	7133340.cif
293413	2024-07-16	cif/ Adding structures of 7133340, 7133341, 7133342, 7133343, 7133344 via cif-deposit CGI script.	7133340.cif