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Information card for entry 7133373
Preview
| Coordinates | 7133373.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C31 H26 F N2 O P Pd |
|---|---|
| Calculated formula | C31 H26 F N2 O P Pd |
| Title of publication | Pd-catalyzed Suzuki-type cross-coupling of 2-pyridyl carbamoyl fluorides. |
| Authors of publication | Jabbarpoor, Maryam; LeBlanc, Jesse; Chen, Zichuan; Cadwallader, Dusty; Le, Christine M. |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2024 |
| Journal volume | 60 |
| Journal issue | 66 |
| Pages of publication | 8700 - 8703 |
| a | 9.6832 ± 0.0008 Å |
| b | 11.7011 ± 0.0009 Å |
| c | 13.0161 ± 0.001 Å |
| α | 73.358 ± 0.003° |
| β | 74.524 ± 0.003° |
| γ | 66.061 ± 0.003° |
| Cell volume | 1272.21 ± 0.18 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1153 |
| Residual factor for significantly intense reflections | 0.0602 |
| Weighted residual factors for significantly intense reflections | 0.09 |
| Weighted residual factors for all reflections included in the refinement | 0.1095 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.046 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 294437 (current) | 2024-09-06 | cif/ Updating files of 7133373, 7133374 Original log message: Adding full bibliography for 7133373--7133374.cif. |
7133373.cif |
| 293474 | 2024-07-20 | cif/ Adding structures of 7133373, 7133374 via cif-deposit CGI script. |
7133373.cif |
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Users of the data should acknowledge the original authors of the
structural data.