Crystallography Open Database

Information card for entry 7134798

Preview

Coordinates	7134798.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C47 H57 Bi Cl2 N2 O2
Calculated formula	C47 H57 Bi Cl2 N2 O2
Title of publication	Synthesis and structural characterization of Sb(iii) and Bi(iii) complexes with an N2O2-type tetradentate dipyrrin ligand
Authors of publication	Agou, Tomohiro; Kuroiwa, Shunsuke; Moriyama, Ryo; Kuroda, Takuma; Kubo, Kazuya; Fukumoto, Hiroki; Morita, Masato; Inoue, Ryo; Nabeshima, Tatsuya
Journal of publication	Chemical Communications
Year of publication	2025
Journal volume	61
Journal issue	39
Pages of publication	7141 - 7144
a	13.8968 ± 0.001 Å
b	14.1548 ± 0.001 Å
c	14.2678 ± 0.001 Å
α	62.515 ± 0.007°
β	80.924 ± 0.006°
γ	62.258 ± 0.007°
Cell volume	2197.8 ± 0.3 Å³
Cell temperature	213 K
Ambient diffraction temperature	213 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1462
Residual factor for significantly intense reflections	0.0991
Weighted residual factors for significantly intense reflections	0.2315
Weighted residual factors for all reflections included in the refinement	0.2579
Goodness-of-fit parameter for all reflections included in the refinement	1.104
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
300319 (current)	2025-07-04	cif/ Adding structures of 7134797, 7134798 via cif-deposit CGI script.	7134798.cif