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Information card for entry 7134802
Preview
| Coordinates | 7134802.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C23 H17 F |
|---|---|
| Calculated formula | C23 H17 F |
| Title of publication | Palladium-catalyzed sequential [3+2] cyclization/C–H activation of o-iodostyrenes with cyclopropenones as C2 synthons |
| Authors of publication | Sun, Jie; Zhang, Shaojie; Wang, Ruixue; Lv, Zeng; Wu, Xin-Xing |
| Journal of publication | Chemical Communications |
| Year of publication | 2025 |
| Journal volume | 61 |
| Journal issue | 45 |
| Pages of publication | 8200 - 8203 |
| a | 11.689 ± 0.002 Å |
| b | 17.293 ± 0.003 Å |
| c | 8.4188 ± 0.0014 Å |
| α | 90° |
| β | 102.698 ± 0.002° |
| γ | 90° |
| Cell volume | 1660.1 ± 0.5 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.0729 |
| Residual factor for significantly intense reflections | 0.0491 |
| Weighted residual factors for significantly intense reflections | 0.1549 |
| Weighted residual factors for all reflections included in the refinement | 0.1773 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.273 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 300323 (current) | 2025-07-04 | cif/ Adding structures of 7134802 via cif-deposit CGI script. |
7134802.cif |
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Users of the data should acknowledge the original authors of the
structural data.