Crystallography Open Database

Information card for entry 7151050

Preview

Coordinates	7151050.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	(2R,5R,6S)-N-(2',3',4'-Tri-O-pivaloyl-a-d-arabinopyranosyl)-5,6-diallyl- 2-isopropyl-piperidin-4-one
Formula	C34 H55 N O8
Calculated formula	C34 H55 N O8
Title of publication	Stereoselective syntheses of piperidinones and their modification by organometallic coupling reactions.
Authors of publication	Kranke, Birgit; Kunz, Horst
Journal of publication	Organic & biomolecular chemistry
Year of publication	2007
Journal volume	5
Journal issue	2
Pages of publication	349 - 354
a	9.576 ± 0.002 Å
b	20.504 ± 0.005 Å
c	10.143 ± 0.003 Å
α	90°
β	112.421 ± 0.011°
γ	90°
Cell volume	1841 ± 0.8 Å³
Cell temperature	298 ± 2 K
Ambient diffraction temperature	298 ± 2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0604
Residual factor for significantly intense reflections	0.0562
Weighted residual factors for significantly intense reflections	0.1633
Weighted residual factors for all reflections included in the refinement	0.1696
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180296 (current)	2016-03-26	cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/10.	7151050.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7151050.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7151050.cif
1188	2010-06-06	cif/{1,7}/ Adding CIFs from Miguel-Quiros-2010_05, New-J-Chem-2007, Org-Biomol-Chem-2007 and RSC-2007 data extraction directories.	7151050.cif