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Information card for entry 7158171
Preview
Coordinates | 7158171.cif |
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Original paper (by DOI) | HTML |
Formula | C39 H32 O3 P2 |
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Calculated formula | C39 H32 O3 P2 |
Title of publication | A metal-free radical cascade reaction of phosphine oxides with 2-aryloxy phenylacetylenes to synthesize diphosphonyl xanthene derivatives. |
Authors of publication | Fan, Tao; Liu, Yan; Jiang, Caina; Xu, Yanli; Chen, Yanyan |
Journal of publication | Organic & biomolecular chemistry |
Year of publication | 2021 |
Journal volume | 19 |
Journal issue | 30 |
Pages of publication | 6609 - 6612 |
a | 10.8036 ± 0.0009 Å |
b | 11.4967 ± 0.0009 Å |
c | 15.6103 ± 0.0014 Å |
α | 95.672 ± 0.007° |
β | 91.026 ± 0.007° |
γ | 113.558 ± 0.008° |
Cell volume | 1765.1 ± 0.3 Å3 |
Cell temperature | 149.99 ± 0.1 K |
Ambient diffraction temperature | 149.99 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1062 |
Residual factor for significantly intense reflections | 0.0787 |
Weighted residual factors for significantly intense reflections | 0.1988 |
Weighted residual factors for all reflections included in the refinement | 0.22 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.044 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
268946 (current) | 2021-09-06 | cif/ Updating files of 7158171 Original log message: Adding full bibliography for 7158171.cif. |
7158171.cif |
267577 | 2021-07-16 | cif/ Adding structures of 7158171 via cif-deposit CGI script. |
7158171.cif |
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