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Information card for entry 7160546
Preview
| Coordinates | 7160546.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C26 H24 N2 O5 |
|---|---|
| Calculated formula | C26 H24 N2 O5 |
| Title of publication | Squaramide-catalyzed aza-Michael/Michael cyclization cascade reaction: one-pot enantioselective construction of highly functionalized γ-lactams. |
| Authors of publication | Wu, Sheng-Feng; Wang, Zhi-Yuan; Sun, Xing-Wen |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2025 |
| a | 11.97 ± 0.002 Å |
| b | 20.271 ± 0.004 Å |
| c | 27.852 ± 0.005 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 6758 ± 2 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0985 |
| Residual factor for significantly intense reflections | 0.0577 |
| Weighted residual factors for significantly intense reflections | 0.1452 |
| Weighted residual factors for all reflections included in the refinement | 0.186 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.083 |
| Diffraction radiation wavelength | 1.34139 Å |
| Diffraction radiation type | GaKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 299610 (current) | 2025-05-10 | cif/ Adding structures of 7160546 via cif-deposit CGI script. |
7160546.cif |
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Users of the data should acknowledge the original authors of the
structural data.