Crystallography Open Database

Information card for entry 7212921

Preview

Coordinates	7212921.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C18 H20 N2 Pb S4
Calculated formula	C18 H20 N2 Pb S4
SMILES	[Pb]12([S]=C(N(Cc3ccccc3)C)S1)[S]=C(N(Cc1ccccc1)C)S2
Title of publication	Controlled synthesis of PbS nanoparticles and the deposition of thin films by Aerosol-Assisted Chemical Vapour Deposition (AACVD)
Authors of publication	Akhtar, Javeed; Malik, Mohammad Azad; O'Brien, Paul; Helliwell, Madeleine
Journal of publication	Journal of Materials Chemistry
Year of publication	2010
Journal volume	20
Journal issue	29
Pages of publication	6116
a	10.16 ± 0.0017 Å
b	5.16 ± 0.0009 Å
c	18.758 ± 0.003 Å
α	90°
β	94.687 ± 0.004°
γ	90°
Cell volume	980.1 ± 0.3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.0132
Residual factor for significantly intense reflections	0.0129
Weighted residual factors for significantly intense reflections	0.0305
Weighted residual factors for all reflections included in the refinement	0.0306
Goodness-of-fit parameter for all reflections included in the refinement	1.073
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180460 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/29.	7212921.cif
93673	2014-01-13	cif/ Adding structures of 7212921 via cif-deposit CGI script.	7212921.cif