Crystallography Open Database

Information card for entry 7214605

Preview

Coordinates	7214605.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H118 Ge6 N24 Ni4 O51 V15
Calculated formula	C36 H104 Ge6 N24 Ni4 O51 V15
Title of publication	Chain and layer networks of germanato-polyoxovanadates
Authors of publication	Wang, Jing; Näther, Christian; Speldrich, Manfred; Kögerler, Paul; Bensch, Wolfgang
Journal of publication	CrystEngComm
Year of publication	2013
Journal volume	15
Journal issue	47
Pages of publication	10238
a	26.9906 ± 0.0004 Å
b	14.7778 ± 0.0003 Å
c	24.9887 ± 0.0004 Å
α	90°
β	91.573 ± 0.001°
γ	90°
Cell volume	9963.3 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0619
Residual factor for significantly intense reflections	0.0566
Weighted residual factors for significantly intense reflections	0.1387
Weighted residual factors for all reflections included in the refinement	0.1425
Goodness-of-fit parameter for all reflections included in the refinement	1.115
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180477 (current)	2016-03-26	cif/7/21/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/21/46.	7214605.cif
110319	2014-04-18	cif/ Adding structures of 7214604, 7214605 via cif-deposit CGI script.	7214605.cif