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Information card for entry 7222293
Preview
| Coordinates | 7222293.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C34 H25 N3 O6 |
|---|---|
| Calculated formula | C34 H25 N3 O6 |
| SMILES | C1(=O)c2ccccc2C(=O)C21C(C#N)(C#N)C(/C=C/c1cc(C)ccc1)N(c1ccccc1)C(=C2C(=O)OC)C(=O)OC |
| Title of publication | Efficient synthesis of functionalized spiro[indoline-3,4'-pyridines] and spiro[indene-2,4'-pyridines] via three-component reaction |
| Authors of publication | Zhang, Jing; Sun, Jing; Yan, Chao Guo |
| Journal of publication | RSC Adv. |
| Year of publication | 2015 |
| a | 10.963 ± 0.002 Å |
| b | 12.057 ± 0.003 Å |
| c | 12.362 ± 0.003 Å |
| α | 83.195 ± 0.008° |
| β | 66.986 ± 0.007° |
| γ | 81.841 ± 0.007° |
| Cell volume | 1485.2 ± 0.6 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1735 |
| Residual factor for significantly intense reflections | 0.0681 |
| Weighted residual factors for significantly intense reflections | 0.1395 |
| Weighted residual factors for all reflections included in the refinement | 0.1758 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.003 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 158300 (current) | 2015-09-25 | cif/ Adding structures of 7222290, 7222291, 7222292, 7222293 via cif-deposit CGI script. |
7222293.cif |
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Users of the data should acknowledge the original authors of the
structural data.