Crystallography Open Database

Information card for entry 7222327

Preview

Coordinates	7222327.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H28 N6 O6 Zn
Calculated formula	C36 H28 N6 O6 Zn
Title of publication	Formation of Zn(ii) and Pb(ii) coordination polymers of tetrakis(4-pyridyl)cyclobutane controlled by benzene and toluene
Authors of publication	Dai, Ming; Gu, Tian-Yi; Zhao, Xin; Li, Hong-Xi; Lang, Jian-Ping
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	43
Pages of publication	8345
a	17.9503 ± 0.0015 Å
b	11.2846 ± 0.0006 Å
c	9.2574 ± 0.0005 Å
α	90°
β	119.709 ± 0.007°
γ	90°
Cell volume	1628.7 ± 0.2 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	12
Hermann-Mauguin space group symbol	C 1 2/m 1
Hall space group symbol	-C 2y
Residual factor for all reflections	0.087
Residual factor for significantly intense reflections	0.0656
Weighted residual factors for significantly intense reflections	0.1461
Weighted residual factors for all reflections included in the refinement	0.1567
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7222327.cif
171054	2015-12-09	cif/ Updating files of 7222327, 7222328, 7222329, 7222330, 7222331 Original log message: Adding full bibliography for 7222327--7222331.cif.	7222327.cif
158830	2015-09-29	cif/ Adding structures of 7222327, 7222328, 7222329, 7222330, 7222331 via cif-deposit CGI script.	7222327.cif