Crystallography Open Database

Information card for entry 7222329

Preview

Coordinates	7222329.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H19 N4 O7 Pb
Calculated formula	C19 H19 N4 O7 Pb
Title of publication	Formation of Zn(ii) and Pb(ii) coordination polymers of tetrakis(4-pyridyl)cyclobutane controlled by benzene and toluene
Authors of publication	Dai, Ming; Gu, Tian-Yi; Zhao, Xin; Li, Hong-Xi; Lang, Jian-Ping
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	43
Pages of publication	8345
a	9.3515 ± 0.0006 Å
b	26.1628 ± 0.0012 Å
c	10.141 ± 0.0006 Å
α	90°
β	113.673 ± 0.007°
γ	90°
Cell volume	2272.3 ± 0.3 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0662
Residual factor for significantly intense reflections	0.0505
Weighted residual factors for significantly intense reflections	0.1198
Weighted residual factors for all reflections included in the refinement	0.1316
Goodness-of-fit parameter for all reflections included in the refinement	0.974
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7222329.cif
171054	2015-12-09	cif/ Updating files of 7222327, 7222328, 7222329, 7222330, 7222331 Original log message: Adding full bibliography for 7222327--7222331.cif.	7222329.cif
158830	2015-09-29	cif/ Adding structures of 7222327, 7222328, 7222329, 7222330, 7222331 via cif-deposit CGI script.	7222329.cif