Crystallography Open Database

Information card for entry 7222331

Preview

Coordinates	7222331.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H22 N6 O7 Pb
Calculated formula	C24 H21.38 N6 O7 Pb
Title of publication	Formation of Zn(ii) and Pb(ii) coordination polymers of tetrakis(4-pyridyl)cyclobutane controlled by benzene and toluene
Authors of publication	Dai, Ming; Gu, Tian-Yi; Zhao, Xin; Li, Hong-Xi; Lang, Jian-Ping
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	43
Pages of publication	8345
a	12.0677 ± 0.0004 Å
b	18.149 ± 0.0004 Å
c	12.1215 ± 0.0004 Å
α	90°
β	110.818 ± 0.004°
γ	90°
Cell volume	2481.49 ± 0.14 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0347
Residual factor for significantly intense reflections	0.0269
Weighted residual factors for significantly intense reflections	0.0634
Weighted residual factors for all reflections included in the refinement	0.066
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	7222331.cif
171054	2015-12-09	cif/ Updating files of 7222327, 7222328, 7222329, 7222330, 7222331 Original log message: Adding full bibliography for 7222327--7222331.cif.	7222331.cif
158830	2015-09-29	cif/ Adding structures of 7222327, 7222328, 7222329, 7222330, 7222331 via cif-deposit CGI script.	7222331.cif