Crystallography Open Database

Information card for entry 7225203

Preview

Coordinates	7225203.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H38 Cu2 Mo16 N24 O57
Calculated formula	C32 H32 Cu2 Mo16 N24 O57
Title of publication	Diverse polyoxometalate-based metal‒organic complexes constructed by a tetrazole- and pyridyl-containing asymmetric amide ligand or its in situ transformed ligand
Authors of publication	Wang, Xiu-Li; Rong, Xing; Liu, Dan-Na; Lin, Hong-Yan; Liu, Guo-Cheng; Wang, Xiang; Song, Ge
Journal of publication	CrystEngComm
Year of publication	2016
Journal volume	18
Journal issue	27
Pages of publication	5101
a	26.9829 ± 0.001 Å
b	37.6059 ± 0.0015 Å
c	19.3314 ± 0.0007 Å
α	90°
β	90°
γ	90°
Cell volume	19615.9 ± 1.3 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	6
Space group number	64
Hermann-Mauguin space group symbol	C m c e
Hall space group symbol	-C 2ac 2
Residual factor for all reflections	0.0828
Residual factor for significantly intense reflections	0.0561
Weighted residual factors for significantly intense reflections	0.1605
Weighted residual factors for all reflections included in the refinement	0.1743
Goodness-of-fit parameter for all reflections included in the refinement	1.081
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
185230 (current)	2016-08-07	cif/ Updating files of 7225203, 7225204, 7225205, 7225206 Original log message: Adding full bibliography for 7225203--7225206.cif.	7225203.cif
182891	2016-05-12	cif/ Adding structures of 7225203, 7225204, 7225205, 7225206 via cif-deposit CGI script.	7225203.cif