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Information card for entry 7225653
Preview
| Coordinates | 7225653.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C15 H18 Bi2 Br11 N3 |
|---|---|
| Calculated formula | C15 H18 Bi2 Br11 N3 |
| Title of publication | Heterogeneous bromination of alkenes using Bi(III) polybromide complexes as {Br2} source |
| Authors of publication | Adonin, Sergey A.; Perekalin, Dmitry S.; Gorokh, Igor D.; Samsonenko, Denis G.; Sokolov, Maksim Nailyevich; Fedin, Vladimir P. |
| Journal of publication | RSC Adv. |
| Year of publication | 2016 |
| a | 7.8459 ± 0.0002 Å |
| b | 23.3803 ± 0.0004 Å |
| c | 9.4868 ± 0.0002 Å |
| α | 90° |
| β | 110.37 ± 0.003° |
| γ | 90° |
| Cell volume | 1631.43 ± 0.07 Å3 |
| Cell temperature | 130 ± 2 K |
| Ambient diffraction temperature | 130 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 11 |
| Hermann-Mauguin space group symbol | P 1 21/m 1 |
| Hall space group symbol | -P 2yb |
| Residual factor for all reflections | 0.0319 |
| Residual factor for significantly intense reflections | 0.0252 |
| Weighted residual factors for significantly intense reflections | 0.0532 |
| Weighted residual factors for all reflections included in the refinement | 0.0556 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.052 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 183879 (current) | 2016-06-23 | cif/ Adding structures of 7225653 via cif-deposit CGI script. |
7225653.cif |
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