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Information card for entry 7233415
Preview
| Coordinates | 7233415.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H36 O Si2 |
|---|---|
| Calculated formula | C32 H36 O Si2 |
| Title of publication | Asymmetric retro-[1,4]-Brook rearrangement of 3-silyl allyloxysilanes via chirality transfer from silicon to carbon |
| Authors of publication | Wu, Ya; Chen, Hua; Yang, Wenyu; Fan, Yu; Gao, Lu; Su, Zhishan; Hu, Changwei; Song, Zhenlei |
| Journal of publication | RSC Advances |
| Year of publication | 2019 |
| Journal volume | 9 |
| Journal issue | 45 |
| Pages of publication | 26209 |
| a | 10.5099 ± 0.0002 Å |
| b | 14.8311 ± 0.0003 Å |
| c | 18.254 ± 0.0003 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2845.31 ± 0.09 Å3 |
| Cell temperature | 293 K |
| Ambient diffraction temperature | 293 K |
| Number of distinct elements | 4 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0365 |
| Residual factor for significantly intense reflections | 0.0352 |
| Weighted residual factors for significantly intense reflections | 0.0991 |
| Weighted residual factors for all reflections included in the refinement | 0.1009 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.059 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54178 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 217655 (current) | 2019-08-22 | cif/ Adding structures of 7233414, 7233415 via cif-deposit CGI script. |
7233415.cif |
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Users of the data should acknowledge the original authors of the
structural data.