#------------------------------------------------------------------------------ #$Date: 2021-03-23 04:42:44 +0200 (Tue, 23 Mar 2021) $ #$Revision: 263229 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/24/7242497.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7242497 loop_ _publ_author_name 'Wang, Hui-Sheng' 'Zhang, Ke' 'Wang, Jia' 'Hu, Zhaobo' 'Song, You' 'Zhang, Zaichao' 'Pan, Zhi-Quan' _publ_section_title ; Regulating the Distortion Degree of the Square Antiprism Coordination Geometry in the Dy-Na Single Ion Magnets ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D1CE00146A _journal_year 2021 _chemical_formula_sum 'C46 H44 Dy N4 Na O10' _chemical_formula_weight 998.34 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2020-12-31 deposited with the CCDC. 2021-03-22 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90.1500(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 22.3221(6) _cell_length_b 11.7740(3) _cell_length_c 16.2459(4) _cell_measurement_reflns_used 8718 _cell_measurement_temperature 173(2) _cell_measurement_theta_max 25.34 _cell_measurement_theta_min 2.74 _cell_volume 4269.74(19) _computing_cell_refinement 'Bruker SMART' _computing_data_collection 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 173(2) _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'PHOTON 100 CMOS detector' _diffrn_measurement_method 'omega scan' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0705 _diffrn_reflns_av_unetI/netI 0.0518 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_h_min -26 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 35053 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 24.997 _diffrn_reflns_theta_max 24.997 _diffrn_reflns_theta_min 2.514 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 1.825 _exptl_absorpt_correction_T_max 0.7452 _exptl_absorpt_correction_T_min 0.5682 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Bruker, 2014)' _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.553 _exptl_crystal_description plate _exptl_crystal_F_000 2020 _exptl_crystal_size_max 0.51 _exptl_crystal_size_mid 0.32 _exptl_crystal_size_min 0.06 _refine_diff_density_max 3.659 _refine_diff_density_min -1.183 _refine_diff_density_rms 0.149 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.085 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 566 _refine_ls_number_reflns 7474 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.085 _refine_ls_R_factor_all 0.0964 _refine_ls_R_factor_gt 0.0471 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0064P)^2^+30.1115P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0881 _refine_ls_wR_factor_ref 0.1019 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4608 _reflns_number_total 7474 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1ce00146a2.cif _cod_data_source_block complex_1 _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7242497 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; 1.res created by SHELXL-2014/7 TITL 1 in P2(1)/c CELL 0.71073 22.3221 11.7740 16.2459 90.000 90.150 90.000 ZERR 4.00 0.0006 0.0003 0.0004 0.000 0.001 0.000 LATT 1 SYMM -X, 0.5+Y, 0.5-Z SFAC C H N O Na Dy UNIT 184 176 16 40 4 4 L.S. 15 omit 0 50 omit -2 1 1 BOND $h acta FMAP 2 PLAN 20 FREE C15 Na1 FREE Na1 C20 TEMP -100.150 WGHT 0.006400 30.111496 FVAR 0.08945 C1 1 0.286057 0.909090 0.471097 11.00000 0.03017 0.02645 = 0.01856 -0.00277 -0.00473 0.00627 C2 1 0.340082 0.858862 0.499067 11.00000 0.03779 0.03528 = 0.02623 -0.00261 -0.00407 0.00239 C3 1 0.340498 0.771251 0.556563 11.00000 0.04093 0.04051 = 0.03742 0.00066 -0.01384 0.01393 AFIX 43 H3 2 0.377441 0.739707 0.574594 11.00000 -1.20000 AFIX 0 C4 1 0.286598 0.729872 0.587645 11.00000 0.06032 0.03327 = 0.02842 0.00483 -0.01072 -0.00164 AFIX 43 H4 2 0.286857 0.669262 0.626244 11.00000 -1.20000 AFIX 0 C5 1 0.233693 0.775856 0.562969 11.00000 0.04464 0.03709 = 0.03092 0.00265 -0.00671 -0.01114 AFIX 43 H5 2 0.197273 0.747964 0.585350 11.00000 -1.20000 AFIX 0 C6 1 0.232113 0.865034 0.504185 11.00000 0.03286 0.03108 = 0.02300 -0.00384 -0.00651 0.00109 C7 1 0.174142 0.906799 0.479369 11.00000 0.03195 0.03233 = 0.02618 0.00271 0.00641 -0.00693 AFIX 43 H7 2 0.141695 0.892902 0.515728 11.00000 -1.20000 AFIX 0 C8 1 0.102142 0.992267 0.394398 11.00000 0.01844 0.03702 = 0.01833 -0.01029 0.00502 0.00347 C9 1 0.051690 0.929843 0.421116 11.00000 0.04082 0.04048 = 0.03421 0.00130 0.00636 -0.00119 AFIX 43 H9 2 0.056549 0.867330 0.457498 11.00000 -1.20000 AFIX 0 C10 1 -0.005199 0.960743 0.393664 11.00000 0.02760 0.05786 = 0.05521 -0.00737 0.00799 -0.00263 AFIX 43 H10 2 -0.039272 0.919398 0.411702 11.00000 -1.20000 AFIX 0 C11 1 -0.012338 1.051251 0.340311 11.00000 0.02945 0.05910 = 0.05307 -0.00277 -0.00185 0.01136 AFIX 43 H11 2 -0.051307 1.072628 0.322489 11.00000 -1.20000 AFIX 0 C12 1 0.036963 1.110476 0.312956 11.00000 0.02969 0.04969 = 0.04574 -0.00152 0.00044 0.00739 AFIX 43 H12 2 0.031908 1.171082 0.274964 11.00000 -1.20000 AFIX 0 C13 1 0.094591 1.081968 0.340782 11.00000 0.02817 0.03535 = 0.02423 0.00227 0.00248 0.00562 C14 1 0.145150 1.240875 0.294746 11.00000 0.02978 0.03674 = 0.02351 0.00010 -0.00088 0.01601 AFIX 43 H14 2 0.107847 1.276671 0.305539 11.00000 -1.20000 AFIX 0 C15 1 0.251384 1.276438 0.252342 11.00000 0.04760 0.01770 = 0.02412 0.00067 -0.00222 -0.00832 C16 1 0.191080 1.313559 0.261460 11.00000 0.04785 0.03104 = 0.02179 -0.00249 -0.00040 0.00262 C17 1 0.174211 1.423970 0.237003 11.00000 0.05575 0.03623 = 0.03814 0.00147 0.00282 0.01623 AFIX 43 H17 2 0.134227 1.448305 0.246360 11.00000 -1.20000 AFIX 0 C18 1 0.213189 1.496647 0.200537 11.00000 0.07304 0.01873 = 0.02957 -0.00513 0.00118 0.01096 AFIX 43 H18 2 0.200691 1.570502 0.184380 11.00000 -1.20000 AFIX 0 C19 1 0.272411 1.460543 0.187132 11.00000 0.07775 0.02321 = 0.03091 -0.00009 0.00014 -0.00889 AFIX 43 H19 2 0.300152 1.510069 0.161188 11.00000 -1.20000 AFIX 0 C20 1 0.290219 1.354925 0.211149 11.00000 0.04532 0.03436 = 0.02682 -0.00248 -0.00690 -0.00327 C21 1 0.446749 0.855934 0.487664 11.00000 0.03345 0.07656 = 0.07789 0.01825 -0.01160 0.00790 AFIX 137 H21A 2 0.452322 0.860895 0.547411 11.00000 -1.50000 H21B 2 0.479388 0.896252 0.459964 11.00000 -1.50000 H21C 2 0.446922 0.776014 0.470812 11.00000 -1.50000 AFIX 0 C22 1 0.389298 1.381453 0.155998 11.00000 0.05824 0.05252 = 0.05103 0.00840 0.00485 -0.01886 AFIX 137 H22A 2 0.373563 1.404449 0.102148 11.00000 -1.50000 H22B 2 0.427079 1.340354 0.148591 11.00000 -1.50000 H22C 2 0.396330 1.449051 0.189867 11.00000 -1.50000 AFIX 0 C23 1 0.367659 0.888326 0.242741 11.00000 0.02055 0.03188 = 0.02102 -0.00218 -0.00320 0.00455 C24 1 0.423559 0.913245 0.205330 11.00000 0.02969 0.03672 = 0.03050 -0.00311 0.00261 -0.00256 C25 1 0.471409 0.840004 0.210291 11.00000 0.02550 0.04811 = 0.04065 0.00449 0.00357 0.00225 AFIX 43 H25 2 0.508910 0.860669 0.187186 11.00000 -1.20000 AFIX 0 C26 1 0.464687 0.734535 0.249619 11.00000 0.03504 0.05653 = 0.05268 0.00487 -0.00273 0.02109 AFIX 43 H26 2 0.497637 0.683760 0.253688 11.00000 -1.20000 AFIX 0 C27 1 0.410029 0.705443 0.282157 11.00000 0.03111 0.03867 = 0.04226 0.00501 0.00039 0.00654 AFIX 43 H27 2 0.405308 0.633406 0.307670 11.00000 -1.20000 AFIX 0 C28 1 0.361059 0.779996 0.278453 11.00000 0.02514 0.03330 = 0.02516 0.00163 -0.00068 0.00428 C29 1 0.304045 0.735389 0.303238 11.00000 0.03483 0.02222 = 0.02750 0.00533 -0.00550 0.00945 AFIX 43 H29 2 0.302719 0.657413 0.318149 11.00000 -1.20000 AFIX 0 C30 1 0.200140 0.730855 0.327974 11.00000 0.03079 0.01325 = 0.02659 -0.00407 0.00449 -0.00440 C31 1 0.198362 0.641937 0.384016 11.00000 0.03784 0.02122 = 0.03363 -0.00252 0.00076 -0.00293 AFIX 43 H31 2 0.234283 0.615466 0.408954 11.00000 -1.20000 AFIX 0 C32 1 0.143813 0.591714 0.403545 11.00000 0.04957 0.03184 = 0.03927 0.00061 0.00958 -0.01123 AFIX 43 H32 2 0.142177 0.531509 0.442405 11.00000 -1.20000 AFIX 0 C33 1 0.092054 0.630068 0.365993 11.00000 0.03498 0.03634 = 0.04415 -0.00390 0.01001 -0.00963 AFIX 43 H33 2 0.054962 0.594319 0.378140 11.00000 -1.20000 AFIX 0 C34 1 0.093353 0.719919 0.310842 11.00000 0.02940 0.03794 = 0.03873 -0.00631 0.00425 -0.00109 AFIX 43 H34 2 0.057349 0.746747 0.286336 11.00000 -1.20000 AFIX 0 C35 1 0.147738 0.770165 0.291855 11.00000 0.02019 0.02159 = 0.02170 -0.00279 0.00153 -0.00547 C36 1 0.115779 0.892852 0.184318 11.00000 0.01682 0.03117 = 0.03331 -0.00915 -0.00399 0.00074 AFIX 43 H36 2 0.084208 0.840105 0.175466 11.00000 -1.20000 AFIX 0 C37 1 0.171144 1.054805 0.121679 11.00000 0.03035 0.02801 = 0.02154 -0.00083 -0.00025 0.00820 C38 1 0.117859 0.992941 0.131150 11.00000 0.02197 0.03317 = 0.01697 -0.00020 0.00162 0.00201 C39 1 0.065768 1.020946 0.087116 11.00000 0.01808 0.05698 = 0.02838 -0.00875 -0.00827 -0.00156 AFIX 43 H39 2 0.030958 0.974998 0.091776 11.00000 -1.20000 AFIX 0 C40 1 0.065352 1.115315 0.037138 11.00000 0.03152 0.04911 = 0.03640 -0.00359 -0.01233 0.01718 AFIX 43 H40 2 0.029459 1.136837 0.009732 11.00000 -1.20000 AFIX 0 C41 1 0.117614 1.180074 0.026339 11.00000 0.03919 0.03376 = 0.03051 -0.00271 -0.00446 0.00617 AFIX 43 H41 2 0.117288 1.244797 -0.008576 11.00000 -1.20000 AFIX 0 C42 1 0.169391 1.148779 0.066913 11.00000 0.02852 0.03456 = 0.02710 -0.00686 0.00161 -0.00182 C43 1 0.470909 1.028627 0.104345 11.00000 0.03128 0.07369 = 0.03629 0.00572 0.01465 -0.01063 AFIX 137 H43A 2 0.509850 1.032495 0.132201 11.00000 -1.50000 H43B 2 0.463892 1.099332 0.073987 11.00000 -1.50000 H43C 2 0.470675 0.964484 0.065903 11.00000 -1.50000 AFIX 0 C44 1 0.225534 1.303778 0.010076 11.00000 0.06006 0.04370 = 0.03532 0.01137 -0.00739 -0.00155 AFIX 137 H44A 2 0.215394 1.283310 -0.046747 11.00000 -1.50000 H44B 2 0.265995 1.336004 0.011842 11.00000 -1.50000 H44C 2 0.196766 1.359990 0.030388 11.00000 -1.50000 AFIX 0 C45 1 0.411242 0.347760 0.873969 11.00000 0.05269 0.05993 = 0.04932 0.00164 -0.00044 0.00956 AFIX 137 H45A 2 0.422534 0.426684 0.862766 11.00000 -1.50000 H45B 2 0.392330 0.314944 0.824933 11.00000 -1.50000 H45C 2 0.447113 0.303868 0.888163 11.00000 -1.50000 AFIX 0 C46 1 0.333038 1.068313 -0.051891 11.00000 0.12215 0.05982 = 0.05869 -0.01265 -0.01271 -0.00666 AFIX 137 H46A 2 0.346467 0.990469 -0.041096 11.00000 -1.50000 H46B 2 0.347009 1.092325 -0.106315 11.00000 -1.50000 H46C 2 0.289180 1.071232 -0.050344 11.00000 -1.50000 AFIX 0 DY1 6 0.235139 1.000214 0.296240 11.00000 0.01953 0.01979 = 0.01846 0.00085 -0.00094 -0.00004 N1 3 0.162324 0.960470 0.413430 11.00000 0.02272 0.03013 = 0.02720 0.00050 0.00364 -0.00173 N2 3 0.147631 1.135113 0.311734 11.00000 0.02984 0.02724 = 0.02046 0.00322 -0.00152 0.00609 N3 3 0.254007 0.791792 0.307186 11.00000 0.02673 0.01789 = 0.03152 -0.00594 -0.00746 0.00225 N4 3 0.153474 0.870803 0.242191 11.00000 0.02326 0.02498 = 0.02618 -0.00256 0.00316 -0.00357 NA1 5 0.318637 1.115101 0.143640 11.00000 0.03481 0.03665 = 0.03063 0.00469 0.00570 -0.00185 O1 4 0.287591 0.992338 0.416379 11.00000 0.02333 0.02681 = 0.01708 0.00302 -0.00685 -0.00160 O2 4 0.271310 1.179709 0.276834 11.00000 0.03709 0.02134 = 0.03653 0.00533 -0.00608 -0.00401 O3 4 0.390974 0.906265 0.465586 11.00000 0.02785 0.05378 = 0.04573 0.00931 -0.00422 0.00688 O4 4 0.346635 1.308833 0.196181 11.00000 0.04326 0.03301 = 0.04444 0.00536 0.00019 -0.01222 O5 4 0.324733 0.963033 0.236283 11.00000 0.02185 0.03221 = 0.02452 0.00167 -0.00035 -0.00114 O6 4 0.220955 1.029845 0.159140 11.00000 0.02350 0.05005 = 0.02110 0.00763 -0.00602 -0.00502 O7 4 0.425063 1.013538 0.163581 11.00000 0.02654 0.04856 = 0.03295 0.00545 0.00846 -0.00027 O8 4 0.223244 1.203632 0.061270 11.00000 0.04247 0.03187 = 0.03207 0.00622 -0.00421 -0.00234 O9 4 0.371143 0.344615 0.939330 11.00000 0.05373 0.05193 = 0.05505 0.01578 0.01020 0.01830 AFIX 147 H9A 2 0.343643 0.392030 0.931175 11.00000 -1.50000 AFIX 0 O10 4 0.356759 1.141703 0.008767 11.00000 0.05938 0.04391 = 0.04048 0.00816 0.00334 0.00545 AFIX 3 H10A 2 0.355170 1.210873 -0.006053 11.00000 -1.20000 AFIX 0 HKLF 4 REM 1 in P2(1)/c REM R1 = 0.0471 for 4608 Fo > 4sig(Fo) and 0.0964 for all 7474 data REM 566 parameters refined using 0 restraints END WGHT 0.0438 19.1877 REM Highest difference peak 3.659, deepest hole -1.183, 1-sigma level 0.149 Q1 1 0.2942 1.0008 0.1120 11.00000 0.05 3.66 Q2 1 0.3176 0.6120 0.6448 11.00000 0.05 1.66 Q3 1 0.3258 1.0372 0.2326 11.00000 0.05 1.37 Q4 1 0.1608 1.0397 0.4089 11.00000 0.05 0.99 Q5 1 0.2191 0.9592 0.1591 11.00000 0.05 0.96 Q6 1 0.1558 1.1356 0.2449 11.00000 0.05 0.94 Q7 1 0.2403 0.9970 0.0969 11.00000 0.05 0.92 Q8 1 0.1728 0.9394 0.1232 11.00000 0.05 0.90 Q9 1 0.2511 1.2200 0.3117 11.00000 0.05 0.86 Q10 1 0.3673 0.3939 0.7402 11.00000 0.05 0.85 Q11 1 0.2910 1.4114 -0.0314 11.00000 0.05 0.77 Q12 1 0.2518 0.9977 0.0703 11.00000 0.05 0.75 Q13 1 0.3481 0.6903 0.1944 11.00000 0.05 0.74 Q14 1 0.3613 0.2853 0.7730 11.00000 0.05 0.72 Q15 1 0.2416 1.0802 0.2262 11.00000 0.05 0.72 Q16 1 0.3143 0.9742 0.1812 11.00000 0.05 0.71 Q17 1 0.0663 0.8835 0.0333 11.00000 0.05 0.71 Q18 1 0.1852 1.0477 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7 112.64 8.25 2 -9 6 -1.24 1.64 -2 -9 -6 0.67 1.90 -2 -9 -6 -0.16 0.60 -2 9 -6 1.54 1.79 2 9 6 0.07 1.86 -2 -9 -5 90.60 4.31 -2 -9 -5 99.79 7.57 2 -9 5 89.51 7.06 -2 9 -5 86.51 6.86 2 9 5 89.17 7.08 2 -9 4 6.56 2.38 -2 -9 -4 0.89 2.11 -2 -9 -4 1.07 0.97 2 9 4 4.13 3.18 -2 9 -4 -0.16 1.61 -2 -9 -3 15.16 2.14 -2 -9 -3 19.64 4.37 2 -9 3 18.17 3.44 -2 9 -3 16.38 3.86 2 9 3 19.05 4.27 -2 -9 -2 -0.59 0.98 2 -9 2 3.10 3.27 2 9 2 0.15 1.51 -2 9 -2 -1.40 1.33 -2 -9 -1 5.31 3.91 -2 -9 -1 5.84 1.75 2 -9 1 11.67 2.95 -2 9 -1 11.16 2.54 2 9 1 5.33 2.20 -2 -9 0 1.42 2.30 2 -9 0 3.38 2.11 -2 9 0 1.71 1.63 2 9 0 2.82 1.90 -2 -9 1 39.93 7.03 2 -9 -1 49.57 5.26 2 9 -1 60.39 5.57 -2 9 1 57.10 5.34 2 -9 -2 0.43 1.81 -2 -9 2 0.07 2.67 -2 9 2 1.39 1.79 2 9 -2 0.81 1.65 2 -9 -3 132.36 8.37 -2 -9 3 143.19 9.23 -2 9 3 112.83 7.50 2 9 -3 128.28 9.53 -2 -9 4 2.06 2.06 2 -9 -4 0.37 1.76 -2 9 4 2.96 1.74 2 9 -4 1.59 1.93 2 -9 -5 163.22 14.27 2 -9 -5 160.76 6.55 -2 -9 5 157.40 9.27 -2 9 5 152.78 8.58 2 9 -5 156.12 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324.77 8.98 -4 6 -2 309.50 10.40 4 6 2 333.90 11.31 4 -6 1 7.21 1.79 -4 -6 -1 5.30 1.26 -4 -6 -1 4.41 1.75 4 6 1 4.37 1.73 4 -6 0 318.91 10.48 -4 -6 0 319.54 9.66 -4 -6 0 321.45 10.75 -4 6 0 309.18 10.21 4 6 0 317.29 10.67 4 -6 -1 15.47 2.50 -4 -6 1 21.64 2.80 -4 -6 1 13.39 2.40 -4 6 1 14.44 2.20 4 6 -1 15.69 2.48 -4 -6 2 182.93 7.68 4 -6 -2 187.21 7.83 -4 -6 2 196.77 8.22 -4 6 2 192.62 7.54 4 6 -2 195.48 8.10 -4 -6 3 2.57 1.35 4 -6 -3 3.32 1.12 4 -6 -3 3.58 1.66 -4 -6 3 5.04 1.82 -4 6 3 6.38 1.64 4 6 -3 3.81 1.46 -4 -6 4 0.50 1.03 4 -6 -4 1.50 1.37 4 -6 -4 -0.25 0.90 -4 -6 4 2.88 1.41 4 6 -4 1.19 1.16 -4 6 4 1.27 1.05 -4 -6 5 -1.62 0.93 4 -6 -5 0.59 1.30 -4 -6 5 -1.12 1.09 4 -6 -5 -0.45 1.34 4 6 -5 -0.10 1.08 -4 6 5 0.04 1.47 -4 -6 6 52.86 4.91 4 -6 -6 61.53 3.93 -4 -6 6 63.75 5.13 4 -6 -6 53.01 4.80 4 6 -6 63.76 4.93 -4 6 6 65.84 4.87 4 -6 -7 2.90 0.96 4 -6 -7 4.44 1.84 -4 -6 7 4.49 1.77 -4 -6 7 3.90 1.78 -4 6 7 3.23 1.55 4 6 -7 1.88 1.33 4 -6 -8 194.07 9.22 -4 -6 8 202.20 9.22 4 -6 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2.82 2.29 4 7 12 0.60 2.42 -4 -7 -11 5.89 2.55 4 -7 11 2.55 2.19 4 7 11 4.67 2.67 4 -7 10 2.48 2.22 -4 -7 -10 4.56 2.35 4 7 10 8.02 2.80 -4 -7 -9 76.33 7.16 4 -7 9 83.71 7.06 4 7 9 83.72 7.29 -4 7 -9 83.35 6.82 -4 -7 -8 7.68 3.99 4 -7 8 3.24 2.09 4 7 8 3.02 2.33 4 -7 7 137.00 8.33 -4 -7 -7 127.12 8.26 -4 7 -7 135.32 8.02 4 7 7 140.04 8.71 -4 -7 -6 17.75 3.48 -4 -7 -6 19.87 1.68 4 -7 6 11.36 2.69 -4 7 -6 19.30 3.26 4 7 6 13.73 3.03 -4 -7 -5 160.87 5.05 4 -7 5 161.23 8.41 -4 -7 -5 172.56 9.05 4 7 5 171.62 9.02 -4 7 -5 164.67 8.33 4 -7 4 11.18 2.58 -4 -7 -4 9.33 1.59 -4 -7 -4 11.43 2.78 4 7 4 9.45 2.42 -4 7 -4 11.93 2.54 -4 -7 -3 5.76 2.03 4 -7 3 7.55 2.10 -4 -7 -3 2.02 0.98 4 7 3 3.20 1.81 -4 7 -3 1.82 1.37 -4 -7 -2 0.82 1.62 4 -7 2 3.48 1.70 -4 -7 -2 1.84 1.03 -4 7 -2 4.84 1.82 4 7 2 3.49 1.68 4 -7 1 4.92 1.77 -4 -7 -1 4.50 1.94 -4 -7 -1 3.28 1.24 4 7 1 2.19 1.62 -4 7 -1 2.76 1.45 -4 -7 0 31.80 4.11 4 -7 0 30.94 3.91 -4 -7 0 28.29 3.87 -4 7 0 32.06 3.75 4 7 0 29.58 3.81 4 -7 -1 113.84 6.67 -4 -7 1 115.28 6.79 -4 -7 1 119.10 6.23 4 7 -1 122.66 6.89 -4 7 1 115.83 6.26 -4 -7 2 -0.60 0.99 -4 -7 2 1.59 1.69 4 -7 -2 1.93 1.59 4 7 -2 1.47 1.44 -4 7 2 0.86 1.13 -4 -7 3 251.78 10.14 -4 -7 3 251.97 9.90 4 -7 -3 257.33 10.06 -4 7 3 245.62 9.47 4 7 -3 253.90 10.18 4 -7 -4 1.91 1.59 -4 -7 4 -0.29 1.28 4 -7 -4 3.75 1.25 -4 -7 4 2.42 1.75 -4 7 4 4.01 1.64 4 7 -4 3.16 1.60 4 -7 -5 214.57 9.51 -4 -7 5 206.06 9.20 -4 -7 5 209.18 9.58 4 -7 -5 218.82 7.64 -4 7 5 213.94 8.89 4 7 -5 207.65 9.38 4 -7 -6 0.83 1.59 4 -7 -6 -0.23 1.54 -4 -7 6 2.10 1.64 -4 -7 6 -0.86 1.38 4 7 -6 0.11 1.30 -4 7 6 1.71 1.44 -4 -7 7 94.06 6.61 4 -7 -7 93.12 6.72 4 -7 -7 88.64 4.46 -4 -7 7 86.76 6.70 4 7 -7 91.51 6.48 -4 7 7 104.82 6.55 4 -7 -8 18.16 1.94 4 -7 -8 17.46 3.39 -4 -7 8 14.34 2.95 -4 -7 8 17.19 3.24 -4 7 8 15.47 2.92 4 7 -8 10.23 2.41 -4 -7 9 12.29 3.51 -4 -7 9 11.41 2.65 4 -7 -9 13.36 1.48 4 -7 -9 12.41 3.04 -4 7 9 10.07 2.58 4 7 -9 13.95 2.98 -4 -7 10 16.57 3.34 -4 -7 10 11.24 2.79 4 -7 -10 12.87 3.00 4 7 -10 9.67 3.81 -4 7 10 12.09 2.82 -4 -7 11 0.15 1.84 -4 -7 11 1.00 1.80 4 -7 -11 0.60 2.05 -4 7 11 1.98 1.83 4 7 -11 -1.72 1.27 -4 -7 12 2.72 2.29 -4 -7 12 1.22 1.93 -4 -7 13 16.05 3.61 4 -7 -13 21.50 4.11 -4 -7 13 14.48 3.26 -4 7 13 16.59 3.42 4 -7 -14 1.04 1.91 -4 -7 14 -3.80 1.77 -4 -7 14 2.52 2.88 -4 7 14 0.78 2.28 -4 -7 15 76.10 7.78 -4 -7 15 86.32 10.24 -4 7 15 78.73 7.33 -4 -7 16 -5.27 2.31 -4 -7 16 1.63 2.48 4 -8 15 -3.11 2.58 -4 -8 -15 0.54 3.12 4 8 15 0.91 5.17 -4 -8 -14 67.72 8.45 4 8 14 46.21 6.66 4 -8 13 -3.55 2.27 -4 -8 -13 -1.99 2.22 4 8 13 -2.03 2.55 -4 -8 -12 69.56 8.17 4 -8 12 79.84 7.92 4 8 12 67.41 7.56 -4 -8 -11 -0.16 2.17 4 -8 11 -0.45 2.02 4 8 11 2.14 2.42 4 -8 10 63.43 6.93 -4 -8 -10 57.98 7.08 4 8 10 61.38 7.07 -4 8 -10 66.59 6.56 -4 -8 -9 -0.38 2.04 4 -8 9 0.81 1.92 4 8 9 -2.42 2.06 -4 8 -9 -1.48 1.47 4 -8 8 30.05 4.41 -4 -8 -8 48.77 5.80 4 8 8 54.63 6.27 -4 8 -8 42.71 5.12 -4 -8 -7 4.77 2.79 4 -8 7 1.72 1.86 4 8 7 5.37 2.46 -4 8 -7 4.76 2.10 -4 -8 -6 6.98 2.82 -4 -8 -6 4.83 0.94 4 -8 6 5.32 2.27 4 8 6 6.97 3.28 -4 8 -6 11.87 4.16 4 -8 5 9.13 2.55 -4 -8 -5 10.56 2.97 -4 -8 -5 5.97 1.14 -4 8 -5 3.07 1.78 4 8 5 9.31 2.75 4 -8 4 62.19 5.67 -4 -8 -4 62.18 3.73 -4 -8 -4 67.90 6.19 4 8 4 67.59 6.35 -4 8 -4 64.14 5.46 -4 -8 -3 -0.25 1.70 4 -8 3 1.70 1.89 -4 -8 -3 0.75 0.86 -4 8 -3 1.55 1.52 4 8 3 2.53 1.85 -4 -8 -2 166.14 6.91 -4 -8 -2 162.51 8.84 4 -8 2 172.20 8.82 4 8 2 161.27 8.63 -4 8 -2 166.14 8.36 -4 -8 -1 0.43 0.99 4 -8 1 -0.51 1.38 -4 -8 -1 3.11 1.91 4 8 1 3.44 1.85 -4 8 -1 3.62 1.80 4 -8 0 75.88 6.15 -4 -8 0 87.60 5.50 -4 -8 0 77.21 6.23 4 8 0 82.63 6.35 -4 8 0 86.08 5.93 4 -8 -1 -1.19 1.48 -4 -8 1 0.10 1.65 -4 -8 1 0.54 1.03 -4 8 1 -0.24 1.19 4 8 -1 0.16 1.51 4 -8 -2 19.59 3.30 -4 -8 2 21.46 3.40 -4 -8 2 16.70 2.67 -4 8 2 16.73 2.82 4 8 -2 21.49 3.37 -4 -8 3 2.05 1.72 4 -8 -3 1.82 1.75 -4 -8 3 3.25 1.46 -4 8 3 5.75 1.99 4 8 -3 4.57 2.09 -4 -8 4 1.70 1.46 4 -8 -4 0.28 1.72 4 -8 -4 3.13 1.39 -4 -8 4 1.49 1.91 -4 8 4 0.18 1.49 4 8 -4 2.25 1.56 -4 -8 5 2.96 1.59 -4 -8 5 5.34 2.01 4 -8 -5 3.13 1.28 4 -8 -5 2.74 1.95 -4 8 5 2.03 1.67 4 8 -5 3.75 1.93 4 -8 -6 23.06 3.05 -4 -8 6 13.19 2.80 4 -8 -6 23.60 3.76 -4 -8 6 15.47 4.38 4 8 -6 18.42 3.33 -4 8 6 22.22 3.32 -4 -8 7 4.57 2.13 -4 -8 7 1.89 2.29 4 -8 -7 2.61 1.94 4 8 -7 2.55 1.80 -4 8 7 3.33 1.87 4 -8 -8 88.03 3.97 -4 -8 8 84.25 6.89 4 -8 -8 86.98 7.17 -4 -8 8 82.38 7.15 4 8 -8 85.06 7.26 -4 8 8 92.99 6.74 -4 -8 9 0.97 1.86 4 -8 -9 0.13 0.49 4 -8 -9 0.96 2.00 -4 -8 9 1.15 1.94 -4 8 9 -1.82 1.62 4 8 -9 -0.23 1.29 -4 -8 10 136.76 9.55 -4 -8 10 142.85 9.07 4 -8 -10 135.35 10.95 4 8 -10 135.84 9.07 -4 8 10 145.89 10.44 -4 -8 11 2.36 2.27 4 -8 -11 8.34 2.76 -4 -8 11 2.40 2.41 -4 8 11 1.85 2.12 4 8 -11 4.57 2.57 -4 -8 12 52.17 6.46 -4 -8 12 56.46 7.21 4 -8 -12 54.46 6.71 -4 8 12 54.66 6.19 4 8 -12 49.56 6.20 -4 -8 13 8.04 2.86 4 -8 -13 6.54 2.76 -4 -8 13 9.40 3.36 -4 8 13 3.49 2.54 -4 -8 14 2.35 2.66 -4 -8 14 1.43 4.53 4 -8 -14 -1.74 2.28 -4 8 14 -3.91 2.05 4 -8 -15 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5 17 26.45 3.26 5 -6 17 -2.64 2.86 5 -6 16 74.40 8.78 5 6 16 69.49 8.73 5 -6 15 -1.15 2.32 5 6 15 -0.98 2.60 5 -6 14 16.14 4.13 5 6 14 18.23 4.39 -5 -6 -13 -1.22 1.93 5 -6 13 -2.95 2.05 5 6 13 3.84 2.64 5 -6 12 1.34 2.01 -5 -6 -12 0.48 2.17 5 6 12 2.41 2.55 -5 -6 -11 7.93 3.09 5 -6 11 6.43 2.56 5 6 11 7.98 3.09 -5 -6 -10 70.20 6.87 5 -6 10 70.09 6.57 5 6 10 69.17 6.86 5 -6 9 1.56 2.04 5 6 9 -1.55 1.98 -5 -6 -8 226.60 11.29 5 -6 8 224.47 10.60 -5 6 -8 212.48 10.05 5 6 8 234.58 11.31 5 -6 7 8.79 2.34 -5 -6 -7 10.08 2.76 -5 6 -7 5.00 2.04 5 6 7 8.64 2.60 5 -6 6 317.04 11.96 -5 -6 -6 301.69 6.85 -5 -6 -6 295.21 11.98 -5 6 -6 303.07 11.49 5 6 6 319.99 12.40 5 -6 5 7.10 1.98 -5 -6 -5 8.35 2.45 -5 -6 -5 8.32 1.16 -5 6 -5 9.88 2.30 5 6 5 8.79 2.42 -5 -6 -4 100.23 4.14 -5 -6 -4 101.08 6.57 5 -6 4 111.37 6.60 -5 6 -4 109.55 6.31 5 6 4 108.62 6.72 5 -6 3 0.16 1.06 -5 -6 -3 1.45 0.76 -5 -6 -3 2.42 1.65 5 6 3 -0.15 1.38 -5 6 -3 -0.11 1.09 -5 -6 -2 0.49 0.75 -5 -6 -2 2.48 1.71 5 -6 2 1.86 1.37 -5 6 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3.07 5 -6 -8 22.85 2.40 5 6 -8 22.95 3.40 -5 6 8 30.23 3.80 5 -6 -9 19.83 3.41 5 -6 -9 22.19 2.13 -5 -6 9 13.55 2.71 -5 -6 9 10.74 2.83 -5 6 9 15.62 2.78 5 6 -9 18.62 3.38 -5 -6 10 2.56 2.03 -5 -6 10 0.38 1.56 5 -6 -10 1.73 0.76 5 -6 -10 1.39 1.75 5 6 -10 -1.25 1.30 -5 6 10 2.62 1.70 5 -6 -11 9.74 2.54 -5 -6 11 7.99 2.56 -5 -6 11 8.48 2.77 5 6 -11 17.50 3.53 -5 6 11 15.50 2.98 -5 -6 12 68.29 6.95 5 -6 -12 60.76 6.09 -5 -6 12 70.41 6.22 -5 6 12 54.15 5.42 5 -6 -13 -0.88 1.95 -5 -6 13 1.57 2.04 -5 -6 13 4.56 2.43 -5 6 13 1.57 1.77 -5 -6 14 73.55 7.11 -5 -6 14 86.97 8.36 -5 6 14 84.42 7.79 -5 -6 15 2.23 2.23 -5 -6 15 -2.60 1.71 -5 6 15 -0.97 1.71 -5 -6 16 50.01 6.15 -5 -6 16 62.69 8.84 -5 6 16 44.16 6.09 -5 -6 17 1.84 2.83 -5 -6 17 0.25 2.19 5 -7 16 -0.61 2.21 5 -7 15 74.73 10.07 5 7 15 62.83 8.49 5 -7 14 0.01 2.56 -5 -7 -14 0.80 2.93 5 7 14 -5.06 2.40 -5 -7 -13 90.25 8.64 5 -7 13 71.90 8.11 5 7 13 69.92 8.01 -5 -7 -12 1.77 2.63 5 -7 12 2.27 2.30 5 7 12 -1.17 2.09 5 -7 11 60.18 6.56 -5 -7 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9 47.44 6.11 7 -7 8 -3.42 1.71 -7 7 -8 -0.45 1.48 7 7 8 1.63 2.32 -7 -7 -7 14.41 1.76 -7 -7 -7 10.26 2.93 7 -7 7 7.76 2.76 7 7 7 10.73 4.21 -7 7 -7 10.20 3.42 -7 -7 -6 0.58 0.88 -7 -7 -6 2.02 2.39 7 -7 6 0.62 1.82 -7 7 -6 0.12 1.46 7 7 6 0.59 1.94 -7 -7 -5 87.67 6.86 7 -7 5 96.65 7.04 -7 -7 -5 96.71 4.76 7 7 5 100.63 7.56 -7 7 -5 98.99 6.76 -7 -7 -4 -0.73 1.78 7 -7 4 0.51 1.53 -7 -7 -4 1.27 0.96 7 7 4 -0.55 1.81 -7 7 -4 -0.60 1.36 -7 -7 -3 121.78 5.62 -7 -7 -3 115.50 7.48 7 -7 3 108.72 6.96 7 7 3 132.79 8.03 -7 7 -3 116.71 6.82 -7 -7 -2 0.37 0.94 -7 -7 -2 2.00 1.81 7 -7 2 -0.03 1.37 7 7 2 0.11 1.62 -7 7 -2 -0.51 1.15 -7 -7 -1 87.53 5.31 -7 -7 -1 81.95 6.27 7 -7 1 83.31 5.72 -7 7 -1 88.43 5.67 7 7 1 100.90 6.64 -7 -7 0 11.87 2.61 -7 -7 0 13.77 2.25 7 -7 0 12.89 2.45 7 7 0 12.76 2.67 -7 7 0 13.10 2.34 7 -7 -1 73.87 5.60 -7 -7 1 66.51 5.09 7 -7 -1 67.32 5.25 -7 -7 1 74.60 5.86 -7 7 1 71.23 5.03 7 7 -1 71.60 5.62 -7 -7 2 1.22 1.57 7 -7 -2 -0.91 1.21 7 -7 -2 0.46 1.33 -7 -7 2 -0.71 0.98 -7 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29.20 4.30 8 6 6 29.67 2.47 -8 6 -6 32.67 4.25 8 -6 5 16.13 3.11 -8 -6 -5 16.03 3.15 -8 -6 -5 15.50 2.15 8 6 5 18.78 3.44 -8 6 -5 13.63 2.59 8 6 5 15.11 2.05 -8 -6 -4 105.38 6.96 -8 -6 -4 95.56 5.06 8 -6 4 98.90 6.55 8 6 4 105.43 7.20 8 6 4 95.70 4.71 -8 6 -4 99.76 6.21 -8 -6 -3 -0.80 1.49 8 -6 3 0.56 1.28 -8 -6 -3 -0.30 0.89 8 6 3 -0.20 0.81 -8 6 -3 0.78 1.25 8 6 3 0.39 1.60 -8 -6 -2 125.42 7.20 -8 -6 -2 126.71 6.02 8 -6 2 127.56 6.80 8 6 2 124.68 7.20 8 6 2 131.21 6.03 -8 6 -2 125.99 6.53 8 -6 1 2.38 1.41 -8 -6 -1 2.38 1.95 -8 -6 -1 1.70 1.67 8 6 1 3.02 1.71 -8 6 -1 2.31 1.35 -8 -6 0 152.88 7.63 8 -6 0 160.76 7.92 8 -6 0 159.95 7.30 -8 -6 0 149.73 7.12 -8 6 0 174.36 10.62 8 6 0 163.79 7.95 8 -6 -1 -0.36 1.12 -8 -6 1 0.64 0.97 -8 -6 1 0.64 1.36 8 -6 -1 0.93 1.34 -8 6 1 -0.03 0.85 8 6 -1 0.30 1.35 -8 -6 2 7.47 2.00 8 -6 -2 9.93 2.46 -8 -6 2 8.81 2.11 8 6 -2 9.74 1.98 -8 6 2 8.86 1.68 -8 -6 3 3.63 1.71 8 -6 -3 6.94 1.74 -8 -6 3 4.81 1.67 -8 6 3 4.39 1.50 8 6 -3 6.73 1.84 8 -6 -4 1.63 1.47 -8 -6 4 1.07 1.48 8 -6 -4 1.46 2.17 -8 -6 4 2.27 1.53 -8 6 4 2.57 1.20 8 6 -4 1.77 1.55 -8 -6 5 12.17 2.71 8 -6 -5 8.81 2.27 -8 -6 5 9.73 2.24 8 6 -5 8.11 2.03 -8 6 5 9.99 1.83 -8 -6 6 127.88 6.94 8 -6 -6 120.80 6.81 -8 -6 6 128.51 7.92 8 -6 -6 114.68 6.92 -8 6 6 127.15 6.02 8 6 -6 123.30 6.92 8 -6 -7 9.08 2.17 8 -6 -7 6.55 1.77 -8 -6 7 9.01 2.26 -8 -6 7 6.51 2.14 -8 6 7 6.58 1.71 8 6 -7 7.10 1.99 8 -6 -8 120.02 6.24 -8 -6 8 109.35 7.73 -8 -6 8 121.08 6.97 8 -6 -8 101.32 6.33 8 6 -8 112.28 7.01 -8 -6 9 -0.15 1.64 8 -6 -9 1.35 1.34 8 -6 -9 0.86 1.11 -8 -6 9 3.43 1.76 -8 6 9 2.21 1.37 8 6 -9 1.95 1.50 -8 -6 10 95.83 7.75 8 -6 -10 96.38 5.29 -8 -6 10 108.39 7.01 8 -6 -10 102.98 6.69 8 6 -10 96.00 7.01 -8 6 10 109.10 6.27 -8 -6 11 19.99 3.52 -8 -6 11 27.80 3.93 8 -6 -11 25.64 3.03 8 -6 -11 24.52 3.56 -8 6 11 24.19 3.42 8 6 -11 34.69 4.75 -8 -6 12 25.70 4.34 -8 -6 12 25.58 5.67 8 -6 -12 26.42 3.80 8 -6 -12 32.27 3.22 -8 6 12 19.74 3.07 -8 -6 13 -1.46 1.93 -8 -6 13 -1.41 1.61 -8 6 13 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1.35 -8 -7 -3 0.77 1.80 -8 7 -3 -0.24 1.18 8 7 3 1.35 1.90 8 -7 2 -0.67 1.24 -8 -7 -2 -0.77 0.98 -8 -7 -2 1.52 1.88 8 7 2 -1.54 1.45 -8 7 -2 -0.97 1.16 -8 -7 -1 21.85 3.39 -8 -7 -1 33.72 3.60 8 -7 1 30.08 3.81 -8 7 -1 29.66 3.73 8 7 1 33.10 4.34 8 -7 0 1.91 1.44 -8 -7 0 0.67 1.11 -8 -7 0 2.03 1.70 8 7 0 0.44 1.49 -8 7 0 2.43 1.39 8 -7 -1 138.37 7.53 -8 -7 1 142.57 7.82 -8 -7 1 134.94 7.12 8 -7 -1 126.82 7.06 -8 7 1 127.93 6.67 8 7 -1 128.68 7.55 -8 -7 2 -0.31 1.20 8 -7 -2 0.75 1.38 -8 -7 2 -0.42 1.64 8 -7 -2 2.05 1.41 8 7 -2 -0.37 1.15 -8 7 2 2.09 1.28 -8 -7 3 131.18 7.57 -8 -7 3 127.32 7.37 8 -7 -3 119.44 6.93 8 -7 -3 139.42 7.30 -8 7 3 132.29 6.64 8 7 -3 128.42 7.41 8 -7 -4 5.64 2.33 -8 -7 4 5.39 1.99 8 -7 -4 8.12 2.12 -8 -7 4 5.44 2.00 -8 7 4 5.99 1.62 8 7 -4 6.36 2.00 8 -7 -5 56.26 5.37 -8 -7 5 48.28 5.03 8 -7 -5 58.87 5.15 -8 -7 5 59.64 5.39 -8 7 5 64.60 4.75 8 7 -5 52.91 5.03 -8 -7 6 3.45 1.98 -8 -7 6 0.99 2.04 8 -7 -6 2.50 1.56 8 -7 -6 1.23 1.52 -8 7 6 1.60 1.26 8 7 -6 3.59 1.70 8 -7 -7 3.62 1.90 8 -7 -7 0.87 1.30 -8 -7 7 1.79 1.68 -8 -7 7 1.20 1.85 -8 7 7 2.09 1.52 8 7 -7 1.32 1.64 8 -7 -8 0.77 1.55 -8 -7 8 1.27 1.70 8 -7 -8 -1.10 1.05 -8 -7 8 0.47 1.84 -8 7 8 -0.90 1.20 8 7 -8 -0.23 1.37 -8 -7 9 13.99 3.26 8 -7 -9 17.28 3.16 8 -7 -9 12.94 2.04 -8 -7 9 13.00 2.96 -8 7 9 11.92 2.51 8 7 -9 12.59 2.93 8 -7 -10 4.24 1.88 -8 -7 10 2.64 2.26 -8 -7 10 1.92 2.15 8 -7 -10 1.43 1.12 -8 7 10 0.95 1.65 8 7 -10 1.06 1.79 -8 -7 11 81.94 6.83 8 -7 -11 80.17 4.63 8 -7 -11 88.14 6.72 -8 -7 11 93.43 8.09 -8 7 11 88.66 6.27 8 7 -11 83.68 7.22 8 -7 -12 0.81 0.98 -8 -7 12 1.88 2.32 8 -7 -12 3.81 2.15 -8 -7 12 1.07 2.06 8 7 -12 1.49 1.97 -8 7 12 1.39 1.81 -8 -7 13 51.68 6.06 8 -7 -13 57.81 5.92 -8 -7 13 55.88 7.04 -8 7 13 45.05 5.03 -8 -7 14 -5.62 3.25 -8 -7 14 -0.63 1.95 -8 -7 15 40.18 6.06 -8 7 15 29.64 4.24 -8 -7 16 -4.22 3.06 -8 7 16 -3.95 2.14 -8 -8 -15 1.30 3.18 -8 -8 -14 31.25 5.89 8 -8 14 34.90 6.00 8 8 14 28.87 6.03 8 -8 13 -2.04 2.63 8 8 13 -1.52 3.07 -8 -8 -12 62.34 7.79 8 -8 12 59.60 7.26 8 8 12 39.97 6.22 8 -8 11 0.31 2.57 -8 -8 -11 3.70 2.92 -8 -8 -10 11.84 3.70 8 -8 10 14.11 3.82 8 8 10 10.05 3.76 -8 -8 -9 1.04 2.48 8 -8 9 0.87 2.02 8 8 9 -0.78 2.26 8 -8 8 4.54 2.83 -8 -8 -8 -0.99 1.82 8 8 8 3.48 2.65 -8 8 -8 2.74 2.15 -8 -8 -7 3.90 1.12 -8 -8 -7 2.03 2.28 8 -8 7 5.47 2.59 -8 8 -7 6.88 2.46 8 8 7 7.16 2.92 8 -8 6 81.89 7.08 -8 -8 -6 74.47 7.15 -8 -8 -6 68.86 4.42 -8 8 -6 79.64 6.61 8 8 6 72.83 6.97 8 -8 5 6.58 2.57 -8 -8 -5 5.59 1.44 -8 -8 -5 5.57 2.79 8 8 5 2.45 2.48 -8 8 -5 2.80 2.95 -8 -8 -4 136.43 6.28 8 -8 4 137.71 9.36 -8 -8 -4 141.83 8.84 8 8 4 151.00 12.31 -8 8 -4 155.39 8.50 8 -8 3 7.04 2.40 -8 -8 -3 9.99 3.46 -8 -8 -3 11.08 1.95 -8 8 -3 11.93 2.60 8 8 3 13.67 3.39 -8 -8 -2 177.74 10.30 -8 -8 -2 168.93 7.52 8 -8 2 171.06 9.05 -8 8 -2 175.45 8.72 8 8 2 167.58 9.51 8 -8 1 7.49 2.34 -8 -8 -1 4.43 2.32 -8 -8 -1 5.35 1.78 -8 8 -1 2.89 1.78 8 8 1 2.54 2.18 8 -8 0 66.67 5.83 -8 -8 0 78.97 6.40 -8 -8 0 67.48 5.37 -8 8 0 68.42 5.42 8 8 0 60.44 5.80 -8 -8 1 10.27 2.41 8 -8 -1 9.86 2.45 -8 -8 1 12.89 3.02 8 -8 -1 13.36 2.72 8 8 -1 10.62 2.77 -8 8 1 12.24 2.50 -8 -8 2 12.14 2.52 8 -8 -2 14.69 2.81 8 -8 -2 14.64 2.92 -8 -8 2 11.41 2.83 8 8 -2 11.51 2.64 -8 8 2 14.92 2.69 8 -8 -3 8.60 2.23 8 -8 -3 8.33 2.43 -8 -8 3 6.40 2.37 -8 -8 3 5.34 2.04 -8 8 3 4.21 1.89 8 8 -3 8.34 2.25 -8 -8 4 0.04 1.63 8 -8 -4 2.30 1.85 -8 -8 4 1.72 2.11 8 -8 -4 1.19 1.49 8 8 -4 3.07 2.07 -8 8 4 1.08 1.60 -8 -8 5 20.68 3.54 8 -8 -5 33.99 4.45 -8 -8 5 20.40 3.43 8 -8 -5 18.48 3.22 -8 8 5 31.47 4.02 8 8 -5 20.42 3.64 -8 -8 6 41.73 5.57 -8 -8 6 30.90 4.96 8 -8 -6 46.13 6.27 8 -8 -6 42.93 4.95 8 8 -6 44.03 5.02 -8 8 6 43.05 4.46 8 -8 -7 30.54 4.11 -8 -8 7 21.18 4.18 8 -8 -7 29.54 4.10 -8 -8 7 21.17 3.63 8 8 -7 26.89 4.18 -8 8 7 22.40 3.27 8 -8 -8 96.58 7.03 8 -8 -8 87.99 5.68 -8 -8 8 91.13 7.06 -8 -8 8 102.96 8.02 8 8 -8 93.10 8.75 -8 8 8 110.99 6.76 8 -8 -9 0.79 1.89 8 -8 -9 1.22 1.20 -8 -8 9 1.00 2.10 -8 -8 9 1.54 2.16 -8 8 9 2.72 1.75 8 8 -9 0.20 1.70 8 -8 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31.55 4.23 10 8 -10 29.14 4.51 10 -8 -11 3.65 2.22 -10 -8 11 1.87 2.35 -10 -8 11 0.24 2.01 10 -8 -11 -0.21 1.21 10 8 -11 -2.46 1.73 -10 8 11 0.33 1.44 10 -8 -12 0.21 2.06 -10 -8 12 -2.57 1.81 -10 8 12 -2.83 1.45 10 8 -12 -0.80 2.10 10 -8 -13 1.26 1.18 10 -8 -13 6.10 3.08 -10 -8 13 4.07 2.97 -10 -8 13 1.74 2.22 10 8 -13 -0.87 2.30 -10 8 13 -3.58 1.79 10 -8 -14 -2.03 1.79 -10 -8 14 -3.61 2.54 -10 -8 14 -5.23 1.93 -10 8 14 1.36 1.94 -10 -9 -13 11.02 4.80 10 -9 13 -5.71 3.31 10 9 13 1.94 3.89 10 -9 12 -7.28 2.67 -10 -9 -12 -5.88 2.51 -10 -9 -11 29.21 5.98 10 -9 11 20.37 6.98 10 9 11 11.42 5.34 -10 -9 -10 -1.49 2.74 10 -9 10 -0.45 2.76 10 9 10 0.07 2.79 10 -9 9 76.85 8.45 -10 -9 -9 63.35 7.51 10 9 9 79.50 8.76 -10 -9 -8 -3.38 2.04 10 -9 8 -0.55 2.42 10 9 8 -5.04 2.01 10 -9 7 81.05 7.84 -10 -9 -7 80.86 4.93 -10 -9 -7 84.14 8.20 -10 9 -7 98.39 7.86 10 9 7 81.23 8.61 -10 -9 -6 -0.34 2.43 10 -9 6 -3.56 1.85 -10 -9 -6 -1.13 1.12 10 9 6 2.23 2.68 -10 9 -6 -1.55 1.52 10 -9 5 109.90 8.53 -10 -9 -5 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15 -4.40 2.94 11 -6 14 -0.15 2.92 11 6 14 -0.20 4.00 11 -6 13 0.95 2.87 11 6 13 -2.12 2.44 -11 -6 -12 11.51 3.60 11 -6 12 12.10 3.76 11 6 12 13.72 4.10 11 6 12 15.99 1.50 11 -6 11 -2.58 1.88 -11 -6 -11 0.09 2.33 11 6 11 -5.77 2.15 11 6 11 0.57 0.71 11 -6 10 114.24 9.00 -11 -6 -10 115.78 9.36 11 6 10 107.53 9.27 11 -6 9 8.38 2.88 -11 -6 -9 9.64 3.38 11 6 9 7.12 1.31 11 6 9 6.42 2.97 11 -6 8 32.69 4.89 -11 -6 -8 31.42 5.02 11 6 8 42.24 3.30 11 6 8 31.23 5.18 -11 -6 -7 1.15 1.21 11 -6 7 1.75 1.85 -11 -6 -7 2.48 2.55 11 6 7 1.00 2.29 11 6 7 -0.65 0.90 -11 -6 -6 148.71 11.37 11 -6 6 154.71 9.03 -11 -6 -6 154.02 7.21 11 6 6 150.18 6.47 11 6 6 144.78 10.22 -11 -6 -5 -0.76 1.43 -11 -6 -5 -0.29 1.58 11 -6 5 -1.13 1.27 11 6 5 -1.62 1.93 11 6 5 -0.34 0.86 11 -6 4 4.63 2.00 -11 -6 -4 11.32 2.68 -11 -6 -4 8.07 2.13 -11 6 -4 8.13 2.16 11 6 4 6.97 2.62 11 6 4 4.65 1.40 -11 -6 -3 -0.55 1.66 -11 -6 -3 -0.31 1.21 11 -6 3 0.56 1.43 11 -6 3 -1.04 1.73 11 6 3 1.90 1.50 11 6 3 0.28 1.75 -11 6 -3 1.33 1.26 -11 -6 -2 53.17 4.83 11 -6 2 59.34 5.97 -11 -6 -2 58.05 5.47 11 -6 2 53.12 4.75 -11 6 -2 47.60 4.41 11 6 2 54.75 5.46 11 6 2 60.64 4.74 -11 -6 -1 1.90 1.38 11 -6 1 1.30 1.39 11 -6 1 0.30 1.75 -11 -6 -1 -0.38 1.49 11 6 1 -0.14 1.67 11 6 1 0.66 1.15 -11 6 -1 2.28 1.35 -11 -6 0 89.71 6.22 11 -6 0 90.80 5.79 -11 -6 0 97.46 6.28 11 -6 0 101.27 6.98 -11 6 0 95.98 5.86 11 6 0 99.10 6.22 11 6 0 89.25 6.42 11 -6 -1 -0.84 0.95 -11 -6 1 0.33 1.39 -11 -6 1 -0.79 1.35 11 -6 -1 0.50 1.54 -11 6 1 0.68 1.02 11 6 -1 -1.07 1.14 11 6 -1 0.07 1.24 -11 -6 2 182.64 8.49 11 -6 -2 173.79 9.15 -11 -6 2 175.29 8.89 11 -6 -2 188.73 9.45 -11 6 2 179.01 7.17 11 6 -2 178.79 8.89 11 6 -2 192.77 8.74 11 -6 -3 3.54 1.72 -11 -6 3 6.53 2.22 11 -6 -3 9.97 2.31 -11 -6 3 3.91 1.86 11 6 -3 2.86 1.58 -11 6 3 5.06 1.36 11 6 -3 4.62 1.87 -11 -6 4 144.25 7.45 11 -6 -4 140.84 8.53 11 -6 -4 133.80 6.60 -11 -6 4 147.65 8.59 11 6 -4 150.23 8.48 11 6 -4 148.32 7.58 -11 6 4 145.66 6.17 11 -6 -5 5.59 2.18 -11 -6 5 7.55 2.23 -11 -6 5 7.87 2.23 11 -6 -5 7.17 1.93 -11 6 5 6.80 1.50 11 6 -5 6.43 2.01 11 -6 -6 9.08 2.49 -11 -6 6 8.09 2.11 -11 -6 6 6.61 2.61 11 -6 -6 15.99 2.43 11 6 -6 13.82 2.67 -11 6 6 9.35 1.71 11 -6 -7 3.32 1.45 -11 -6 7 6.65 2.40 11 -6 -7 4.49 2.00 -11 -6 7 4.63 1.89 -11 6 7 3.88 1.37 11 6 -7 4.56 1.83 11 -6 -8 1.79 1.59 11 -6 -8 2.15 1.36 -11 -6 8 4.81 1.99 -11 -6 8 1.65 1.82 -11 6 8 4.41 1.45 11 6 -8 6.23 1.86 -11 -6 9 1.92 1.73 11 -6 -9 0.66 1.41 -11 -6 9 1.49 1.84 -11 6 9 0.35 1.13 11 6 -9 0.09 1.37 -11 -6 10 11.28 3.28 11 -6 -10 8.67 2.13 -11 -6 10 6.20 2.17 11 -6 -10 6.43 1.93 11 6 -10 8.28 2.04 -11 6 10 6.61 1.75 -11 6 10 7.37 2.30 11 -6 -11 3.21 1.52 -11 -6 11 -0.93 1.90 -11 -6 11 0.69 1.69 11 6 -11 0.64 1.30 -11 6 11 -2.33 1.40 -11 6 11 -1.90 1.33 -11 -6 12 70.06 5.91 11 -6 -12 54.39 4.92 -11 -6 12 67.17 7.65 -11 6 12 53.91 4.43 -11 6 12 57.61 5.62 -11 -6 13 -1.40 1.93 11 -6 -13 -0.10 1.34 -11 -6 13 -2.65 1.51 -11 6 13 -2.45 1.46 -11 6 13 -2.06 1.47 -11 -6 14 39.75 9.21 11 -6 -14 48.72 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6.16 -11 -8 -2 90.52 7.31 11 -8 2 95.05 8.58 11 -8 2 97.66 7.29 -11 8 -2 91.49 6.53 11 8 2 91.14 7.85 11 -8 1 -1.28 1.80 -11 -8 -1 -0.24 1.32 11 -8 1 1.29 1.77 -11 -8 -1 1.29 1.97 11 8 1 -4.22 2.65 -11 8 -1 0.68 1.44 -11 -8 0 145.82 12.45 -11 -8 0 152.78 8.46 11 -8 0 158.65 8.82 11 -8 0 163.97 9.53 11 8 0 157.09 9.34 -11 8 0 155.97 8.06 -11 -8 1 4.88 1.99 11 -8 -1 4.47 2.22 11 -8 -1 2.87 2.02 -11 -8 1 0.08 2.52 11 8 -1 1.34 1.78 -11 8 1 1.45 1.61 -11 -8 2 190.77 9.82 11 -8 -2 182.03 9.82 11 -8 -2 185.38 9.27 -11 -8 2 204.54 10.87 -11 8 2 200.98 8.82 11 8 -2 184.51 9.89 -11 -8 3 3.32 2.02 11 -8 -3 3.26 2.16 11 -8 -3 3.50 1.94 -11 -8 3 7.09 2.69 11 8 -3 5.35 2.23 -11 8 3 5.88 1.93 -11 -8 4 120.06 8.16 -11 -8 4 120.16 8.52 11 -8 -4 131.30 8.45 11 -8 -4 120.12 7.49 11 8 -4 123.88 8.06 -11 8 4 123.57 6.77 11 -8 -5 2.54 1.87 -11 -8 5 2.41 2.64 11 -8 -5 3.20 2.02 -11 -8 5 4.37 1.99 -11 8 5 0.91 1.44 11 8 -5 6.08 2.38 11 -8 -6 0.47 1.79 -11 -8 6 -1.22 2.27 11 -8 -6 -1.10 1.37 -11 -8 6 3.37 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35.93 2.74 12 5 -5 43.91 5.03 12 5 -5 24.96 3.66 12 -5 -6 9.17 2.31 12 -5 -6 5.51 1.43 -12 -5 6 7.36 1.99 -12 5 6 7.40 1.36 12 5 -6 5.67 2.12 -12 5 6 7.00 2.48 12 -5 -7 0.63 1.51 12 -5 -7 2.77 1.05 -12 -5 7 1.70 1.41 -12 -5 7 2.05 1.64 -12 5 7 1.98 0.97 -12 5 7 1.07 1.98 12 5 -7 2.48 1.85 12 5 -7 1.52 1.41 12 -5 -8 3.32 1.69 -12 -5 8 1.59 1.88 -12 -5 8 1.54 1.54 12 -5 -8 1.73 1.02 12 5 -8 0.27 1.11 -12 5 8 1.59 1.89 -12 5 8 0.03 0.86 12 -5 -9 84.35 6.43 12 -5 -9 80.47 4.45 -12 -5 9 94.31 7.90 -12 -5 9 90.89 5.74 12 5 -9 89.96 6.04 -12 5 9 100.15 4.44 -12 5 9 93.74 7.18 -12 -5 10 2.91 1.63 -12 -5 10 2.91 2.21 12 -5 -10 4.57 1.90 12 5 -10 5.93 1.87 -12 5 10 7.32 1.46 -12 5 10 5.63 2.35 -12 -5 11 60.58 5.01 12 -5 -11 61.13 5.57 -12 -5 11 68.02 7.19 -12 5 11 65.72 3.94 -12 5 11 60.27 6.26 -12 -5 12 3.51 2.54 -12 -5 12 6.95 1.96 12 -5 -12 5.90 1.99 -12 5 12 4.21 2.27 -12 5 12 2.51 1.33 -12 -5 13 82.17 6.02 12 -5 -13 79.94 6.32 -12 -5 13 77.78 7.87 -12 5 13 83.18 7.29 -12 5 13 76.74 4.78 -12 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-12 -7 -4 2.45 2.22 12 -7 4 3.47 2.39 12 -7 4 2.95 2.16 -12 -7 -4 3.74 1.77 12 7 4 9.33 3.26 -12 7 -4 2.99 1.88 12 7 4 3.23 1.34 12 -7 3 20.94 3.36 -12 -7 -3 19.05 2.97 12 -7 3 14.22 3.43 12 7 3 14.28 2.35 12 7 3 15.67 3.31 -12 7 -3 15.98 2.85 12 -7 2 4.99 2.39 12 -7 2 3.51 1.89 -12 -7 -2 4.05 1.81 -12 -7 -2 5.70 2.41 -12 7 -2 3.35 1.76 12 7 2 5.19 2.65 12 7 2 3.05 1.37 -12 -7 -1 126.90 7.61 12 -7 1 141.43 7.97 12 -7 1 120.87 8.40 -12 -7 -1 126.41 7.99 12 7 1 125.86 8.25 12 7 1 122.36 7.21 -12 7 -1 125.67 7.10 12 -7 0 9.74 2.92 -12 -7 0 4.13 2.14 -12 -7 0 8.88 2.35 12 -7 0 7.30 2.13 -12 7 0 9.75 2.15 12 7 0 6.17 2.23 12 7 0 7.01 2.08 12 -7 -1 114.39 7.96 -12 -7 1 124.29 7.71 -12 -7 1 121.79 7.61 12 -7 -1 111.54 6.83 -12 7 1 126.42 6.64 12 7 -1 101.98 7.04 12 7 -1 116.31 7.47 -12 -7 2 10.27 2.55 12 -7 -2 11.96 2.81 -12 -7 2 10.66 2.77 12 -7 -2 11.72 2.51 -12 7 2 9.93 2.05 12 7 -2 12.21 2.75 12 -7 -3 105.92 7.69 -12 -7 3 113.18 7.14 -12 -7 3 101.10 7.96 12 -7 -3 103.81 6.42 12 7 -3 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19.94 3.61 -12 -8 -2 22.04 4.01 -12 8 -2 19.56 3.10 12 8 2 23.34 4.25 -12 -8 -1 0.82 1.92 12 -8 1 -0.23 1.56 -12 -8 -1 1.78 1.58 12 -8 1 3.38 2.35 -12 8 -1 1.83 1.72 12 8 1 1.89 2.22 12 -8 0 2.20 1.81 12 -8 0 8.64 4.17 -12 -8 0 4.25 1.88 -12 -8 0 4.80 2.33 -12 8 0 2.92 1.79 12 8 0 3.32 3.49 -12 -8 1 -0.31 1.67 12 -8 -1 -2.22 1.47 -12 -8 1 -2.10 2.29 12 -8 -1 -0.11 1.82 12 8 -1 -0.73 1.74 -12 8 1 -0.66 1.13 12 -8 -2 4.77 2.04 12 -8 -2 1.29 1.82 -12 -8 2 2.47 3.06 12 8 -2 7.53 2.43 -12 8 2 3.89 1.81 -12 -8 3 1.45 1.80 12 -8 -3 -0.83 1.82 -12 -8 3 2.28 3.30 12 -8 -3 1.60 1.72 -12 8 3 0.45 1.35 12 8 -3 -0.43 1.56 12 -8 -4 60.80 6.48 -12 -8 4 46.61 7.70 12 -8 -4 51.95 5.24 -12 -8 4 46.69 5.91 -12 8 4 58.23 4.75 12 8 -4 54.02 5.68 12 -8 -5 1.25 1.76 12 -8 -5 2.50 2.21 -12 -8 5 2.80 2.04 -12 8 5 4.22 1.64 12 8 -5 1.55 1.67 -12 -8 6 160.40 10.89 -12 -8 6 166.83 9.99 12 -8 -6 179.33 9.95 12 -8 -6 162.96 8.39 -12 8 6 152.98 7.45 12 8 -6 165.41 9.66 -12 -8 7 -2.24 1.69 12 -8 -7 2.20 1.92 12 -8 -7 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1.79 15 5 8 0.90 1.41 -15 -5 -7 56.67 5.46 15 -5 7 65.11 6.64 15 -5 7 72.62 7.48 -15 -5 -7 56.96 6.67 15 5 7 65.89 7.09 15 5 7 61.40 5.39 -15 -5 -6 4.75 2.17 15 -5 6 -1.91 1.58 -15 -5 -6 -0.52 1.47 15 -5 6 -0.14 1.85 15 5 6 -1.26 1.99 15 5 6 -1.79 1.25 -15 -5 -5 87.43 6.90 -15 -5 -5 78.55 9.69 15 -5 5 79.65 7.76 15 -5 5 79.95 6.64 15 5 5 77.46 6.13 15 5 5 86.47 7.50 15 -5 4 2.27 1.92 15 -5 4 1.55 2.23 -15 -5 -4 -1.37 1.77 -15 -5 -4 -0.54 1.74 15 5 4 1.07 1.91 15 5 4 1.54 1.69 -15 -5 -3 128.36 8.10 15 -5 3 122.52 7.50 15 -5 3 140.98 9.56 -15 -5 -3 145.52 9.03 15 5 3 144.44 8.36 15 5 3 141.76 8.49 15 -5 2 -0.54 1.36 -15 -5 -2 -0.31 1.57 -15 -5 -2 -0.86 1.82 15 -5 2 -0.03 2.78 15 5 2 -0.45 1.37 15 5 2 1.46 1.46 15 -5 1 7.76 3.04 15 -5 1 12.53 2.43 -15 -5 -1 12.63 2.78 -15 -5 -1 14.96 2.88 15 5 1 15.59 3.09 15 5 1 18.04 3.15 15 -5 0 0.08 1.25 -15 -5 0 -1.54 1.60 15 -5 0 1.37 2.10 -15 -5 0 -1.19 1.39 15 5 0 0.12 1.51 15 5 0 1.21 1.73 15 -5 -1 1.64 2.14 -15 -5 1 3.57 2.17 -15 -5 1 3.64 1.94 15 -5 -1 2.86 1.42 15 5 -1 2.82 1.66 15 5 -1 2.46 1.90 -15 -5 2 -0.36 1.32 -15 -5 2 0.22 1.93 15 -5 -2 1.43 2.16 15 -5 -2 0.05 1.08 15 5 -2 0.93 1.20 15 5 -2 0.35 1.49 15 -5 -3 10.70 2.99 -15 -5 3 9.44 2.92 -15 -5 3 12.61 2.47 15 -5 -3 10.97 1.93 15 5 -3 10.73 2.91 15 5 -3 10.14 2.24 -15 -5 4 -0.07 1.35 -15 -5 4 1.97 1.92 15 -5 -4 0.82 1.79 15 -5 -4 -0.07 1.08 15 5 -4 0.85 1.74 15 5 -4 1.25 1.24 -15 -5 5 84.39 7.39 15 -5 -5 85.14 7.25 15 -5 -5 80.16 3.80 -15 -5 5 80.87 5.36 15 5 -5 83.44 7.21 -15 5 5 77.93 7.47 15 5 -5 63.55 6.00 -15 -5 6 0.26 1.31 15 -5 -6 0.23 0.72 15 -5 -6 -2.92 1.30 -15 -5 6 -1.93 1.96 15 5 -6 -0.26 1.72 -15 5 6 -0.66 1.94 15 5 -6 0.87 1.90 -15 5 6 -0.60 0.56 -15 -5 7 150.43 10.06 15 -5 -7 140.58 9.15 -15 -5 7 133.74 6.62 15 -5 -7 141.13 4.39 -15 5 7 142.98 4.20 15 5 -7 123.24 8.82 -15 5 7 143.43 11.11 15 5 -7 156.41 10.05 15 -5 -8 0.40 1.64 -15 -5 8 -0.06 1.33 -15 -5 8 0.70 2.17 -15 5 8 -0.07 0.58 15 5 -8 -1.50 1.11 15 5 -8 -1.78 1.78 -15 -5 9 71.32 5.01 -15 -5 9 65.90 7.53 15 -5 -9 69.51 6.87 15 5 -9 65.85 7.08 -15 5 9 74.67 8.04 15 5 -9 66.24 5.10 -15 5 9 66.35 2.36 -15 -5 10 -1.26 2.08 15 -5 -10 2.00 3.58 -15 -5 10 0.84 1.36 -15 5 10 1.88 2.38 15 5 -10 -0.18 1.24 -15 5 10 0.47 0.52 15 -5 -11 7.21 2.70 -15 -5 11 8.47 2.06 -15 -5 11 10.03 3.39 -15 5 11 10.87 1.18 -15 5 11 7.98 2.86 15 -5 -12 1.70 1.86 -15 -5 12 -2.25 1.33 -15 -5 12 0.58 2.50 -15 5 12 -4.08 1.93 -15 5 12 0.52 0.56 15 -5 -13 6.05 2.47 -15 -5 13 3.99 2.06 -15 -5 13 4.89 3.09 -15 5 13 -4.10 2.24 -15 5 13 3.08 0.86 -15 5 13 3.39 0.94 -15 -5 14 -3.55 2.38 15 -5 -14 -2.95 1.56 -15 5 14 0.29 0.78 -15 5 14 -1.96 1.00 15 -6 13 -5.28 2.75 15 -6 13 -2.65 2.69 15 6 13 -6.04 2.96 15 6 13 1.00 1.36 15 -6 12 32.77 7.81 15 -6 12 23.82 4.76 15 6 12 32.51 3.84 15 6 12 27.54 6.80 15 -6 11 -1.82 2.46 -15 -6 -11 12.09 3.49 15 -6 11 0.82 2.62 15 6 11 -2.75 3.23 -15 -6 -10 73.44 7.97 15 -6 10 55.90 7.48 15 -6 10 58.03 7.63 15 6 10 61.96 4.97 15 6 10 57.94 7.43 15 -6 9 -1.23 2.60 -15 -6 -9 2.42 2.53 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4 37.97 6.05 25 -4 3 3.10 1.76 -25 -4 -3 -4.17 4.62 25 -4 3 -0.70 1.81 25 -4 3 -5.94 2.67 25 4 3 2.21 2.44 25 -4 2 43.06 4.72 25 -4 2 35.57 6.29 -25 -4 -2 25.56 6.59 25 -4 2 44.78 4.71 25 4 2 25.67 3.97 25 4 2 34.80 5.90 25 -4 1 -1.06 1.47 25 -4 1 -5.99 2.62 -25 -4 -1 -4.71 3.01 25 -4 1 -0.69 1.46 25 4 1 -2.16 1.78 25 4 1 -2.96 3.94 25 -4 0 14.06 2.52 25 -4 0 5.89 3.55 25 -4 0 9.72 2.61 -25 -4 0 6.90 4.17 25 4 0 13.95 6.42 25 4 0 8.94 2.83 25 -4 -1 -0.34 2.97 -25 -4 1 -0.29 3.67 25 -4 -1 -0.99 1.09 25 -4 -1 -0.35 1.08 25 4 -1 0.54 1.61 25 4 -1 -0.34 2.62 25 -4 -2 3.79 3.02 -25 -4 2 -0.70 3.51 25 4 -2 -2.16 1.30 25 -4 -3 -2.42 2.67 -25 -4 3 -6.34 3.11 25 4 -3 -2.39 2.56 -25 -4 4 -4.36 3.55 25 -4 -4 3.86 3.14 -25 4 4 2.20 4.27 25 4 -4 7.53 3.21 25 4 -4 4.04 1.47 25 -5 2 -1.32 1.95 -25 -5 -2 -2.24 3.24 25 -5 2 -1.75 1.77 25 5 2 -3.55 1.86 25 -5 1 4.30 2.12 25 -5 1 5.00 1.97 -25 -5 -1 2.00 3.61 25 -5 1 6.07 4.05 25 5 1 5.98 4.26 25 5 1 4.03 2.39 25 -5 0 0.32 2.84 -25 -5 0 -5.68 3.22 25 -5 0 -3.30 1.26 25 5 0 2.18 2.81 25 -5 -1 41.06 3.78 -25 -5 1 30.12 6.07 25 -5 -1 27.36 5.42 25 -5 -1 41.44 3.45 25 5 -1 42.99 4.94 25 5 -1 27.47 5.18 25 -5 -2 -2.00 0.75 25 -5 -2 -1.49 2.68 25 -5 -2 -1.53 0.73 25 5 -2 -3.55 1.35 25 5 -2 -3.80 2.50 26 0 4 -1.26 2.79 26 0 4 0.09 1.69 26 0 4 -4.26 1.66 26 0 3 -2.51 1.72 26 0 3 -4.14 2.38 26 0 2 7.69 2.32 -26 0 -2 4.70 3.52 26 0 2 16.35 4.05 26 0 2 13.86 2.39 26 0 1 -1.89 1.27 26 0 0 29.48 3.46 -26 0 0 22.74 5.27 26 0 0 30.71 3.73 26 0 0 27.06 5.02 26 0 -1 -0.23 0.98 26 0 -1 -0.21 2.45 -26 0 1 -5.33 2.71 26 0 -2 53.56 7.45 -26 0 2 29.89 5.64 26 0 -3 -3.78 2.38 -26 0 4 8.14 4.31 26 0 -4 21.99 5.22 26 0 -5 -1.60 2.58 26 -1 4 2.79 1.85 26 -1 4 -3.16 2.37 26 -1 4 -1.60 1.80 26 1 4 -1.64 2.38 26 1 4 -3.16 1.85 26 -1 3 52.22 5.06 -26 -1 -3 26.99 5.78 26 -1 3 43.28 4.69 26 -1 3 40.27 6.11 26 1 3 43.07 6.29 26 1 3 31.44 4.44 26 -1 2 0.24 1.45 -26 -1 -2 -3.92 2.66 26 -1 2 -3.07 1.54 26 1 2 -0.77 2.54 26 -1 1 27.09 3.50 26 -1 1 24.80 4.64 26 -1 1 27.95 3.74 -26 -1 -1 20.46 5.28 26 1 1 33.75 5.69 26 1 1 27.28 3.70 -26 1 -1 24.42 5.60 26 1 1 23.66 3.25 26 -1 0 -1.17 2.89 -26 -1 0 -0.10 3.11 26 -1 0 -0.02 1.12 -26 1 0 -1.71 3.22 26 1 0 0.76 1.28 26 1 0 -5.53 2.36 26 1 0 -2.58 1.23 -26 -1 1 8.41 4.15 26 -1 -1 10.96 3.52 -26 1 1 9.13 4.06 26 1 -1 9.64 1.99 26 1 -1 15.07 4.09 26 1 -1 6.60 1.67 26 -1 -2 -2.26 2.37 -26 -1 2 -6.98 3.08 26 1 -2 -0.08 0.86 -26 1 2 -4.21 3.12 26 1 -2 -1.26 1.12 26 1 -2 3.72 2.63 -26 -1 3 -5.83 3.17 26 -1 -3 3.55 3.00 -26 1 3 -6.11 3.31 26 1 -3 0.38 2.97 26 -1 -4 0.92 2.56 -26 -1 4 -5.07 3.34 26 1 -4 5.10 3.32 26 -2 4 7.42 2.59 26 -2 4 7.70 3.32 26 -2 4 14.05 2.89 -26 -2 -4 0.77 3.40 26 2 4 3.07 2.70 26 2 4 3.30 2.57 26 -2 3 1.53 1.59 26 -2 3 0.68 1.69 26 -2 3 0.52 2.94 -26 -2 -3 -0.86 3.25 26 2 3 -0.17 2.49 26 -2 2 1.83 1.90 -26 -2 -2 -6.88 3.20 26 -2 2 2.54 1.81 26 -2 2 2.20 3.19 26 2 2 5.28 2.01 26 2 2 2.41 3.03 26 -2 1 -1.37 1.22 26 -2 1 -2.64 1.29 26 -2 1 -1.66 2.45 -26 -2 -1 2.33 2.96 26 2 1 -5.17 2.22 26 -2 0 11.54 3.15 -26 -2 0 9.84 4.53 26 -2 0 8.59 3.69 26 -2 0 15.95 2.16 26 2 0 16.12 3.96 26 2 0 14.42 2.54 26 -2 -1 -1.64 1.05 26 2 -1 -1.24 2.51 -26 -2 2 44.01 7.10 26 -2 -2 35.08 5.86 26 2 -2 51.48 3.51 26 2 -2 62.88 3.95 -26 2 2 44.74 7.04 26 2 -2 56.76 7.88 26 -2 -3 -0.88 2.67 -26 -2 3 -7.43 3.32 26 2 -3 1.60 2.78 26 2 -3 -1.31 0.61 -26 -2 4 31.74 9.03 26 -2 -4 24.95 4.66 -26 2 4 23.89 6.46 26 2 -4 19.49 4.77 26 -3 2 -2.42 2.83 -26 -3 -2 1.85 3.45 26 -3 2 -0.15 1.59 26 -3 2 0.05 1.77 26 3 2 -2.65 2.87 26 -3 1 17.38 4.68 26 -3 1 24.17 3.19 26 -3 1 23.14 2.93 -26 -3 -1 18.03 5.00 26 3 1 18.96 3.29 26 3 1 20.24 4.61 26 -3 0 -2.68 2.75 26 -3 0 -1.33 1.16 -26 -3 0 -2.99 3.21 26 3 0 0.33 2.46 -26 -3 1 3.25 3.59 26 -3 -1 9.49 2.25 26 -3 -1 5.97 3.75 26 3 -1 11.10 2.26 26 3 -1 11.54 3.56 26 -3 -2 1.19 2.85 26 3 -2 -1.30 1.47 26 3 -2 0.66 3.04 -26 3 2 -5.18 3.19 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 2667 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.2861(3) 0.9091(6) 0.4711(4) 0.0251(14) Uani 1 1 d . . . . . C2 C 0.3401(3) 0.8589(6) 0.4991(4) 0.0331(16) Uani 1 1 d . . . . . C3 C 0.3405(3) 0.7713(6) 0.5566(5) 0.0396(19) Uani 1 1 d . . . . . H3 H 0.3774 0.7397 0.5746 0.048 Uiso 1 1 calc R U . . . C4 C 0.2866(4) 0.7299(6) 0.5876(5) 0.0407(19) Uani 1 1 d . . . . . H4 H 0.2869 0.6693 0.6262 0.049 Uiso 1 1 calc R U . . . C5 C 0.2337(3) 0.7759(6) 0.5630(5) 0.0376(18) Uani 1 1 d . . . . . H5 H 0.1973 0.7480 0.5853 0.045 Uiso 1 1 calc R U . . . C6 C 0.2321(3) 0.8650(6) 0.5042(4) 0.0290(16) Uani 1 1 d . . . . . C7 C 0.1741(3) 0.9068(6) 0.4794(4) 0.0301(16) Uani 1 1 d . . . . . H7 H 0.1417 0.8929 0.5157 0.036 Uiso 1 1 calc R U . . . C8 C 0.1021(2) 0.9923(6) 0.3944(3) 0.0246(13) Uani 1 1 d . . . . . C9 C 0.0517(3) 0.9298(6) 0.4211(5) 0.0385(18) Uani 1 1 d . . . . . H9 H 0.0565 0.8673 0.4575 0.046 Uiso 1 1 calc R U . . . C10 C -0.0052(3) 0.9607(7) 0.3937(5) 0.047(2) Uani 1 1 d . . . . . H10 H -0.0393 0.9194 0.4117 0.056 Uiso 1 1 calc R U . . . C11 C -0.0123(3) 1.0513(7) 0.3403(5) 0.047(2) Uani 1 1 d . . . . . H11 H -0.0513 1.0726 0.3225 0.057 Uiso 1 1 calc R U . . . C12 C 0.0370(3) 1.1105(7) 0.3130(5) 0.0417(19) Uani 1 1 d . . . . . H12 H 0.0319 1.1711 0.2750 0.050 Uiso 1 1 calc R U . . . C13 C 0.0946(3) 1.0820(6) 0.3408(4) 0.0292(16) Uani 1 1 d . . . . . C14 C 0.1452(3) 1.2409(6) 0.2947(4) 0.0300(17) Uani 1 1 d . . . . . H14 H 0.1078 1.2767 0.3055 0.036 Uiso 1 1 calc R U . . . C15 C 0.2514(3) 1.2764(5) 0.2523(4) 0.0298(16) Uani 1 1 d . . . . . C16 C 0.1911(3) 1.3136(6) 0.2615(4) 0.0336(17) Uani 1 1 d . . . . . C17 C 0.1742(4) 1.4240(6) 0.2370(5) 0.043(2) Uani 1 1 d . . . . . H17 H 0.1342 1.4483 0.2464 0.052 Uiso 1 1 calc R U . . . C18 C 0.2132(3) 1.4966(7) 0.2005(4) 0.0404(17) Uani 1 1 d . . . . . H18 H 0.2007 1.5705 0.1844 0.049 Uiso 1 1 calc R U . . . C19 C 0.2724(4) 1.4605(6) 0.1871(5) 0.044(2) Uani 1 1 d . . . . . H19 H 0.3002 1.5101 0.1612 0.053 Uiso 1 1 calc R U . . . C20 C 0.2902(3) 1.3549(6) 0.2111(4) 0.0355(17) Uani 1 1 d . . . . . C21 C 0.4467(3) 0.8559(8) 0.4877(6) 0.063(3) Uani 1 1 d . . . . . H21A H 0.4523 0.8609 0.5474 0.094 Uiso 1 1 calc R U . . . H21B H 0.4794 0.8963 0.4600 0.094 Uiso 1 1 calc R U . . . H21C H 0.4469 0.7760 0.4708 0.094 Uiso 1 1 calc R U . . . C22 C 0.3893(4) 1.3815(7) 0.1560(5) 0.054(2) Uani 1 1 d . . . . . H22A H 0.3736 1.4044 0.1021 0.081 Uiso 1 1 calc R U . . . H22B H 0.4271 1.3404 0.1486 0.081 Uiso 1 1 calc R U . . . H22C H 0.3963 1.4491 0.1899 0.081 Uiso 1 1 calc R U . . . C23 C 0.3677(3) 0.8883(6) 0.2427(4) 0.0245(14) Uani 1 1 d . . . . . C24 C 0.4236(3) 0.9132(6) 0.2053(4) 0.0323(16) Uani 1 1 d . . . . . C25 C 0.4714(3) 0.8400(7) 0.2103(5) 0.0381(18) Uani 1 1 d . . . . . H25 H 0.5089 0.8607 0.1872 0.046 Uiso 1 1 calc R U . . . C26 C 0.4647(3) 0.7345(7) 0.2496(5) 0.048(2) Uani 1 1 d . . . . . H26 H 0.4976 0.6838 0.2537 0.058 Uiso 1 1 calc R U . . . C27 C 0.4100(3) 0.7054(6) 0.2822(5) 0.0373(18) Uani 1 1 d . . . . . H27 H 0.4053 0.6334 0.3077 0.045 Uiso 1 1 calc R U . . . C28 C 0.3611(3) 0.7800(6) 0.2785(4) 0.0279(15) Uani 1 1 d . . . . . C29 C 0.3040(3) 0.7354(6) 0.3032(4) 0.0282(15) Uani 1 1 d . . . . . H29 H 0.3027 0.6574 0.3181 0.034 Uiso 1 1 calc R U . . . C30 C 0.2001(3) 0.7309(5) 0.3280(4) 0.0235(14) Uani 1 1 d . . . . . C31 C 0.1984(3) 0.6419(5) 0.3840(4) 0.0309(16) Uani 1 1 d . . . . . H31 H 0.2343 0.6155 0.4090 0.037 Uiso 1 1 calc R U . . . C32 C 0.1438(3) 0.5917(6) 0.4035(5) 0.0402(19) Uani 1 1 d . . . . . H32 H 0.1422 0.5315 0.4424 0.048 Uiso 1 1 calc R U . . . C33 C 0.0921(3) 0.6301(6) 0.3660(5) 0.0385(18) Uani 1 1 d . . . . . H33 H 0.0550 0.5943 0.3781 0.046 Uiso 1 1 calc R U . . . C34 C 0.0934(3) 0.7199(6) 0.3108(5) 0.0353(17) Uani 1 1 d . . . . . H34 H 0.0573 0.7467 0.2863 0.042 Uiso 1 1 calc R U . . . C35 C 0.1477(3) 0.7702(5) 0.2919(4) 0.0212(14) Uani 1 1 d . . . . . C36 C 0.1158(3) 0.8929(6) 0.1843(4) 0.0271(15) Uani 1 1 d . . . . . H36 H 0.0842 0.8401 0.1755 0.033 Uiso 1 1 calc R U . . . C37 C 0.1711(3) 1.0548(6) 0.1217(4) 0.0266(15) Uani 1 1 d . . . . . C38 C 0.1179(2) 0.9929(6) 0.1311(3) 0.0240(13) Uani 1 1 d . . . . . C39 C 0.0658(3) 1.0209(7) 0.0871(4) 0.0345(18) Uani 1 1 d . . . . . H39 H 0.0310 0.9750 0.0918 0.041 Uiso 1 1 calc R U . . . C40 C 0.0654(3) 1.1153(7) 0.0371(5) 0.0390(19) Uani 1 1 d . . . . . H40 H 0.0295 1.1368 0.0097 0.047 Uiso 1 1 calc R U . . . C41 C 0.1176(3) 1.1801(6) 0.0263(4) 0.0345(17) Uani 1 1 d . . . . . H41 H 0.1173 1.2448 -0.0086 0.041 Uiso 1 1 calc R U . . . C42 C 0.1694(3) 1.1488(6) 0.0669(4) 0.0301(16) Uani 1 1 d . . . . . C43 C 0.4709(3) 1.0286(7) 0.1043(5) 0.047(2) Uani 1 1 d . . . . . H43A H 0.5099 1.0325 0.1322 0.071 Uiso 1 1 calc R U . . . H43B H 0.4639 1.0993 0.0740 0.071 Uiso 1 1 calc R U . . . H43C H 0.4707 0.9645 0.0659 0.071 Uiso 1 1 calc R U . . . C44 C 0.2255(4) 1.3038(7) 0.0101(5) 0.046(2) Uani 1 1 d . . . . . H44A H 0.2154 1.2833 -0.0467 0.070 Uiso 1 1 calc R U . . . H44B H 0.2660 1.3360 0.0118 0.070 Uiso 1 1 calc R U . . . H44C H 0.1968 1.3600 0.0304 0.070 Uiso 1 1 calc R U . . . C45 C 0.4112(4) 0.3478(8) 0.8740(5) 0.054(2) Uani 1 1 d . . . . . H45A H 0.4225 0.4267 0.8628 0.081 Uiso 1 1 calc R U . . . H45B H 0.3923 0.3149 0.8249 0.081 Uiso 1 1 calc R U . . . H45C H 0.4471 0.3039 0.8882 0.081 Uiso 1 1 calc R U . . . C46 C 0.3330(5) 1.0683(9) -0.0519(6) 0.080(3) Uani 1 1 d . . . . . H46A H 0.3465 0.9905 -0.0411 0.120 Uiso 1 1 calc R U . . . H46B H 0.3470 1.0923 -0.1063 0.120 Uiso 1 1 calc R U . . . H46C H 0.2892 1.0712 -0.0503 0.120 Uiso 1 1 calc R U . . . Dy1 Dy 0.23514(2) 1.00021(3) 0.29624(2) 0.01926(9) Uani 1 1 d . . . . . N1 N 0.1623(2) 0.9605(5) 0.4134(3) 0.0267(13) Uani 1 1 d . . . . . N2 N 0.1476(2) 1.1351(5) 0.3117(3) 0.0258(12) Uani 1 1 d . . . . . N3 N 0.2540(2) 0.7918(4) 0.3072(3) 0.0254(13) Uani 1 1 d . . . . . N4 N 0.1535(2) 0.8708(4) 0.2422(3) 0.0248(12) Uani 1 1 d . . . . . Na1 Na 0.31864(12) 1.1151(2) 0.14364(17) 0.0340(6) Uani 1 1 d . . . . . O1 O 0.28759(16) 0.9923(4) 0.4164(2) 0.0224(9) Uani 1 1 d . . . . . O2 O 0.2713(2) 1.1797(4) 0.2768(3) 0.0317(11) Uani 1 1 d . . . . . O3 O 0.3910(2) 0.9063(5) 0.4656(3) 0.0425(13) Uani 1 1 d . . . . . O4 O 0.3466(2) 1.3088(4) 0.1962(3) 0.0402(13) Uani 1 1 d . . . . . O5 O 0.32473(18) 0.9630(4) 0.2363(3) 0.0262(10) Uani 1 1 d . . . . . O6 O 0.22095(19) 1.0298(4) 0.1591(3) 0.0316(12) Uani 1 1 d . . . . . O7 O 0.42506(19) 1.0135(4) 0.1636(3) 0.0360(12) Uani 1 1 d . . . . . O8 O 0.2232(2) 1.2036(4) 0.0613(3) 0.0355(12) Uani 1 1 d . . . . . O9 O 0.3711(3) 0.3446(5) 0.9393(4) 0.0536(16) Uani 1 1 d . . . . . H9A H 0.3436 0.3920 0.9312 0.080 Uiso 1 1 calc R U . . . O10 O 0.3568(2) 1.1417(5) 0.0088(3) 0.0479(14) Uani 1 1 d . . . . . H10A H 0.3552 1.2109 -0.0061 0.057 Uiso 1 1 d R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.030(4) 0.026(3) 0.019(3) -0.003(3) -0.005(3) 0.006(3) C2 0.038(4) 0.035(4) 0.026(4) -0.003(3) -0.004(3) 0.002(3) C3 0.041(4) 0.041(4) 0.037(4) 0.001(4) -0.014(4) 0.014(4) C4 0.060(5) 0.033(4) 0.028(4) 0.005(3) -0.011(4) -0.002(4) C5 0.045(4) 0.037(4) 0.031(4) 0.003(4) -0.007(3) -0.011(4) C6 0.033(4) 0.031(4) 0.023(4) -0.004(3) -0.007(3) 0.001(3) C7 0.032(4) 0.032(4) 0.026(4) 0.003(3) 0.006(3) -0.007(3) C8 0.018(3) 0.037(4) 0.018(3) -0.010(3) 0.005(2) 0.003(3) C9 0.041(4) 0.040(5) 0.034(4) 0.001(4) 0.006(4) -0.001(3) C10 0.028(4) 0.058(5) 0.055(5) -0.007(4) 0.008(4) -0.003(4) C11 0.029(4) 0.059(5) 0.053(5) -0.003(5) -0.002(4) 0.011(4) C12 0.030(4) 0.050(5) 0.046(5) -0.002(4) 0.000(4) 0.007(4) C13 0.028(4) 0.035(4) 0.024(4) 0.002(3) 0.002(3) 0.006(3) C14 0.030(4) 0.037(4) 0.024(4) 0.000(3) -0.001(3) 0.016(3) C15 0.048(4) 0.018(3) 0.024(4) 0.001(3) -0.002(3) -0.008(3) C16 0.048(5) 0.031(4) 0.022(4) -0.002(3) 0.000(3) 0.003(3) C17 0.056(5) 0.036(4) 0.038(5) 0.001(4) 0.003(4) 0.016(4) C18 0.073(5) 0.019(3) 0.030(4) -0.005(4) 0.001(3) 0.011(4) C19 0.078(6) 0.023(4) 0.031(4) 0.000(3) 0.000(4) -0.009(4) C20 0.045(4) 0.034(4) 0.027(4) -0.002(3) -0.007(3) -0.003(3) C21 0.033(5) 0.077(7) 0.078(7) 0.018(6) -0.012(4) 0.008(4) C22 0.058(5) 0.053(5) 0.051(5) 0.008(4) 0.005(4) -0.019(4) C23 0.021(3) 0.032(4) 0.021(3) -0.002(3) -0.003(3) 0.005(3) C24 0.030(4) 0.037(4) 0.030(4) -0.003(3) 0.003(3) -0.003(3) C25 0.026(4) 0.048(5) 0.041(5) 0.004(4) 0.004(3) 0.002(3) C26 0.035(5) 0.057(5) 0.053(5) 0.005(4) -0.003(4) 0.021(4) C27 0.031(4) 0.039(4) 0.042(5) 0.005(4) 0.000(3) 0.007(3) C28 0.025(3) 0.033(4) 0.025(4) 0.002(3) -0.001(3) 0.004(3) C29 0.035(4) 0.022(3) 0.027(4) 0.005(3) -0.005(3) 0.009(3) C30 0.031(4) 0.013(3) 0.027(4) -0.004(3) 0.004(3) -0.004(3) C31 0.038(4) 0.021(4) 0.034(4) -0.003(3) 0.001(3) -0.003(3) C32 0.050(5) 0.032(4) 0.039(5) 0.001(4) 0.010(4) -0.011(4) C33 0.035(4) 0.036(4) 0.044(5) -0.004(4) 0.010(4) -0.010(3) C34 0.029(4) 0.038(4) 0.039(4) -0.006(4) 0.004(3) -0.001(3) C35 0.020(3) 0.022(3) 0.022(4) -0.003(3) 0.002(3) -0.005(3) C36 0.017(3) 0.031(4) 0.033(4) -0.009(3) -0.004(3) 0.001(3) C37 0.030(4) 0.028(4) 0.022(3) -0.001(3) 0.000(3) 0.008(3) C38 0.022(3) 0.033(3) 0.017(3) 0.000(3) 0.002(2) 0.002(3) C39 0.018(3) 0.057(6) 0.028(4) -0.009(4) -0.008(3) -0.002(3) C40 0.032(4) 0.049(5) 0.036(4) -0.004(4) -0.012(3) 0.017(4) C41 0.039(4) 0.034(4) 0.031(4) -0.003(3) -0.004(3) 0.006(3) C42 0.029(4) 0.035(4) 0.027(4) -0.007(3) 0.002(3) -0.002(3) C43 0.031(4) 0.074(7) 0.036(4) 0.006(4) 0.015(3) -0.011(4) C44 0.060(5) 0.044(5) 0.035(5) 0.011(4) -0.007(4) -0.002(4) C45 0.053(5) 0.060(6) 0.049(5) 0.002(5) 0.000(4) 0.010(4) C46 0.122(10) 0.060(7) 0.059(7) -0.013(6) -0.013(6) -0.007(6) Dy1 0.01953(14) 0.01979(14) 0.01846(14) 0.00085(15) -0.00094(10) -0.00004(15) N1 0.023(3) 0.030(3) 0.027(3) 0.000(2) 0.004(2) -0.002(2) N2 0.030(3) 0.027(3) 0.020(3) 0.003(2) -0.002(2) 0.006(2) N3 0.027(3) 0.018(3) 0.032(3) -0.006(2) -0.007(2) 0.002(2) N4 0.023(3) 0.025(3) 0.026(3) -0.003(2) 0.003(2) -0.004(2) Na1 0.0348(15) 0.0366(16) 0.0306(15) 0.0047(13) 0.0057(12) -0.0019(12) O1 0.023(2) 0.027(2) 0.017(2) 0.003(2) -0.0068(16) -0.002(2) O2 0.037(3) 0.021(3) 0.037(3) 0.005(2) -0.006(2) -0.004(2) O3 0.028(3) 0.054(3) 0.046(3) 0.009(3) -0.004(2) 0.007(2) O4 0.043(3) 0.033(3) 0.044(3) 0.005(2) 0.000(2) -0.012(2) O5 0.022(2) 0.032(3) 0.025(2) 0.002(2) -0.0004(19) -0.0011(18) O6 0.024(2) 0.050(3) 0.021(2) 0.008(2) -0.0060(19) -0.005(2) O7 0.027(2) 0.049(3) 0.033(3) 0.005(3) 0.008(2) 0.000(2) O8 0.042(3) 0.032(3) 0.032(3) 0.006(2) -0.004(2) -0.002(2) O9 0.054(4) 0.052(4) 0.055(4) 0.016(3) 0.010(3) 0.018(3) O10 0.059(4) 0.044(3) 0.040(3) 0.008(3) 0.003(3) 0.005(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Na Na 0.0362 0.0249 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 C1 C6 123.3(6) . . ? O1 C1 C2 120.1(6) . . ? C6 C1 C2 116.7(6) . . ? O3 C2 C3 124.1(7) . . ? O3 C2 C1 114.0(6) . . ? C3 C2 C1 121.9(7) . . ? C4 C3 C2 119.9(7) . . ? C4 C3 H3 120.1 . . ? C2 C3 H3 120.1 . . ? C5 C4 C3 120.3(7) . . ? C5 C4 H4 119.9 . . ? C3 C4 H4 119.9 . . ? C4 C5 C6 120.9(7) . . ? C4 C5 H5 119.6 . . ? C6 C5 H5 119.6 . . ? C1 C6 C5 120.4(6) . . ? C1 C6 C7 122.1(6) . . ? C5 C6 C7 117.5(6) . . ? N1 C7 C6 126.1(6) . . ? N1 C7 H7 116.9 . . ? C6 C7 H7 116.9 . . ? C13 C8 C9 119.7(6) . . ? C13 C8 N1 116.8(5) . . ? C9 C8 N1 123.2(7) . . ? C10 C9 C8 119.5(7) . . ? C10 C9 H9 120.3 . . ? C8 C9 H9 120.3 . . ? C11 C10 C9 120.4(7) . . ? C11 C10 H10 119.8 . . ? C9 C10 H10 119.8 . . ? C12 C11 C10 120.1(7) . . ? C12 C11 H11 119.9 . . ? C10 C11 H11 119.9 . . ? C11 C12 C13 120.5(8) . . ? C11 C12 H12 119.8 . . ? C13 C12 H12 119.8 . . ? C8 C13 C12 119.8(6) . . ? C8 C13 N2 116.5(6) . . ? C12 C13 N2 123.5(6) . . ? N2 C14 C16 129.0(6) . . ? N2 C14 H14 115.5 . . ? C16 C14 H14 115.5 . . ? O2 C15 C16 124.5(6) . . ? O2 C15 C20 120.4(6) . . ? C16 C15 C20 115.1(6) . . ? C17 C16 C15 120.4(7) . . ? C17 C16 C14 117.6(7) . . ? C15 C16 C14 122.0(6) . . ? C18 C17 C16 122.2(7) . . ? C18 C17 H17 118.9 . . ? C16 C17 H17 118.9 . . ? C17 C18 C19 118.7(7) . . ? C17 C18 H18 120.6 . . ? C19 C18 H18 120.6 . . ? C20 C19 C18 120.4(7) . . ? C20 C19 H19 119.8 . . ? C18 C19 H19 119.8 . . ? C19 C20 O4 124.7(7) . . ? C19 C20 C15 123.1(7) . . ? O4 C20 C15 112.2(6) . . ? O3 C21 H21A 109.5 . . ? O3 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? O3 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? O4 C22 H22A 109.5 . . ? O4 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? O4 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? O5 C23 C28 124.5(6) . . ? O5 C23 C24 118.2(6) . . ? C28 C23 C24 117.1(6) . . ? O7 C24 C25 123.6(6) . . ? O7 C24 C23 114.5(6) . . ? C25 C24 C23 121.9(7) . . ? C24 C25 C26 119.8(7) . . ? C24 C25 H25 120.1 . . ? C26 C25 H25 120.1 . . ? C27 C26 C25 119.4(7) . . ? C27 C26 H26 120.3 . . ? C25 C26 H26 120.3 . . ? C26 C27 C28 121.3(7) . . ? C26 C27 H27 119.3 . . ? C28 C27 H27 119.3 . . ? C23 C28 C27 120.1(6) . . ? C23 C28 C29 122.7(6) . . ? C27 C28 C29 116.8(6) . . ? N3 C29 C28 126.1(6) . . ? N3 C29 H29 117.0 . . ? C28 C29 H29 117.0 . . ? C35 C30 C31 120.2(6) . . ? C35 C30 N3 116.0(6) . . ? C31 C30 N3 123.7(6) . . ? C30 C31 C32 119.8(7) . . ? C30 C31 H31 120.1 . . ? C32 C31 H31 120.1 . . ? C33 C32 C31 119.5(7) . . ? C33 C32 H32 120.3 . . ? C31 C32 H32 120.3 . . ? C34 C33 C32 121.1(7) . . ? C34 C33 H33 119.5 . . ? C32 C33 H33 119.5 . . ? C33 C34 C35 119.3(7) . . ? C33 C34 H34 120.4 . . ? C35 C34 H34 120.4 . . ? C30 C35 C34 120.1(6) . . ? C30 C35 N4 115.8(5) . . ? C34 C35 N4 123.7(6) . . ? N4 C36 C38 124.9(6) . . ? N4 C36 H36 117.5 . . ? C38 C36 H36 117.5 . . ? O6 C37 C38 123.7(6) . . ? O6 C37 C42 119.4(6) . . ? C38 C37 C42 116.8(6) . . ? C37 C38 C39 121.6(6) . . ? C37 C38 C36 120.8(6) . . ? C39 C38 C36 117.6(6) . . ? C40 C39 C38 119.7(7) . . ? C40 C39 H39 120.2 . . ? C38 C39 H39 120.2 . . ? C39 C40 C41 120.5(7) . . ? C39 C40 H40 119.8 . . ? C41 C40 H40 119.8 . . ? C42 C41 C40 119.4(7) . . ? C42 C41 H41 120.3 . . ? C40 C41 H41 120.3 . . ? O8 C42 C41 125.3(7) . . ? O8 C42 C37 112.8(6) . . ? C41 C42 C37 122.0(6) . . ? O7 C43 H43A 109.5 . . ? O7 C43 H43B 109.5 . . ? H43A C43 H43B 109.5 . . ? O7 C43 H43C 109.5 . . ? H43A C43 H43C 109.5 . . ? H43B C43 H43C 109.5 . . ? O8 C44 H44A 109.5 . . ? O8 C44 H44B 109.5 . . ? H44A C44 H44B 109.5 . . ? O8 C44 H44C 109.5 . . ? H44A C44 H44C 109.5 . . ? H44B C44 H44C 109.5 . . ? O9 C45 H45A 109.5 . . ? O9 C45 H45B 109.5 . . ? H45A C45 H45B 109.5 . . ? O9 C45 H45C 109.5 . . ? H45A C45 H45C 109.5 . . ? H45B C45 H45C 109.5 . . ? O10 C46 H46A 109.5 . . ? O10 C46 H46B 109.5 . . ? H46A C46 H46B 109.5 . . ? O10 C46 H46C 109.5 . . ? H46A C46 H46C 109.5 . . ? H46B C46 H46C 109.5 . . ? O5 Dy1 O6 74.34(15) . . ? O5 Dy1 O1 84.74(15) . . ? O6 Dy1 O1 156.31(14) . . ? O5 Dy1 O2 78.87(16) . . ? O6 Dy1 O2 76.79(17) . . ? O1 Dy1 O2 88.56(17) . . ? O5 Dy1 N3 72.07(16) . . ? O6 Dy1 N3 104.09(17) . . ? O1 Dy1 N3 79.19(17) . . ? O2 Dy1 N3 149.28(17) . . ? O5 Dy1 N4 111.69(16) . . ? O6 Dy1 N4 69.79(16) . . ? O1 Dy1 N4 129.91(17) . . ? O2 Dy1 N4 139.77(17) . . ? N3 Dy1 N4 63.52(17) . . ? O5 Dy1 N2 147.68(16) . . ? O6 Dy1 N2 84.01(16) . . ? O1 Dy1 N2 109.62(16) . . ? O2 Dy1 N2 72.92(17) . . ? N3 Dy1 N2 137.74(17) . . ? N4 Dy1 N2 81.77(17) . . ? O5 Dy1 N1 148.13(16) . . ? O6 Dy1 N1 132.19(16) . . ? O1 Dy1 N1 71.31(16) . . ? O2 Dy1 N1 119.94(17) . . ? N3 Dy1 N1 82.77(17) . . ? N4 Dy1 N1 71.86(17) . . ? N2 Dy1 N1 63.08(17) . . ? O5 Dy1 Na1 43.59(12) . . ? O6 Dy1 Na1 45.40(12) . . ? O1 Dy1 Na1 111.17(11) . . ? O2 Dy1 Na1 48.26(13) . . ? N3 Dy1 Na1 110.59(13) . . ? N4 Dy1 Na1 112.56(13) . . ? N2 Dy1 Na1 104.39(13) . . ? N1 Dy1 Na1 166.61(13) . . ? C7 N1 C8 120.4(5) . . ? C7 N1 Dy1 126.1(4) . . ? C8 N1 Dy1 113.0(4) . . ? C14 N2 C13 117.8(6) . . ? C14 N2 Dy1 128.6(5) . . ? C13 N2 Dy1 113.6(4) . . ? C29 N3 C30 118.3(5) . . ? C29 N3 Dy1 130.0(4) . . ? C30 N3 Dy1 111.4(4) . . ? C36 N4 C35 121.1(6) . . ? C36 N4 Dy1 126.9(4) . . ? C35 N4 Dy1 111.5(4) . . ? O5 Na1 O10 132.3(2) . . ? O5 Na1 O6 70.50(16) . . ? O10 Na1 O6 118.5(2) . . ? O5 Na1 O4 117.47(19) . . ? O10 Na1 O4 96.0(2) . . ? O6 Na1 O4 124.45(19) . . ? O5 Na1 O2 72.77(16) . . ? O10 Na1 O2 154.5(2) . . ? O6 Na1 O2 69.89(16) . . ? O4 Na1 O2 62.63(16) . . ? O5 Na1 O7 62.04(15) . . ? O10 Na1 O7 81.40(18) . . ? O6 Na1 O7 127.07(19) . . ? O4 Na1 O7 98.30(19) . . ? O2 Na1 O7 113.79(18) . . ? O5 Na1 O8 130.78(18) . . ? O10 Na1 O8 77.13(18) . . ? O6 Na1 O8 60.30(16) . . ? O4 Na1 O8 90.74(18) . . ? O2 Na1 O8 88.71(17) . . ? O7 Na1 O8 157.47(18) . . ? O5 Na1 Dy1 41.91(11) . . ? O10 Na1 Dy1 158.08(18) . . ? O6 Na1 Dy1 42.16(11) . . ? O4 Na1 Dy1 104.51(14) . . ? O2 Na1 Dy1 42.41(11) . . ? O7 Na1 Dy1 102.87(13) . . ? O8 Na1 Dy1 94.68(12) . . ? C1 O1 Dy1 126.3(4) . . ? C15 O2 Dy1 137.7(4) . . ? C15 O2 Na1 98.4(4) . . ? Dy1 O2 Na1 89.33(17) . . ? C2 O3 C21 116.9(6) . . ? C20 O4 C22 116.6(6) . . ? C20 O4 Na1 100.9(4) . . ? C22 O4 Na1 123.4(5) . . ? C23 O5 Dy1 138.0(4) . . ? C23 O5 Na1 127.5(4) . . ? Dy1 O5 Na1 94.50(17) . . ? C37 O6 Dy1 127.6(4) . . ? C37 O6 Na1 129.0(4) . . ? Dy1 O6 Na1 92.43(17) . . ? C24 O7 C43 117.7(6) . . ? C24 O7 Na1 115.1(4) . . ? C43 O7 Na1 120.2(4) . . ? C42 O8 C44 117.2(6) . . ? C42 O8 Na1 118.2(4) . . ? C44 O8 Na1 124.6(4) . . ? C45 O9 H9A 109.5 . . ? C46 O10 Na1 115.4(6) . . ? C46 O10 H10A 111.9 . . ? Na1 O10 H10A 111.9 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 O1 1.324(8) . ? C1 C6 1.418(9) . ? C1 C2 1.417(9) . ? C2 O3 1.379(8) . ? C2 C3 1.392(10) . ? C3 C4 1.394(10) . ? C3 H3 0.9500 . ? C4 C5 1.359(10) . ? C4 H4 0.9500 . ? C5 C6 1.420(10) . ? C5 H5 0.9500 . ? C6 C7 1.441(9) . ? C7 N1 1.271(8) . ? C7 H7 0.9500 . ? C8 C13 1.379(10) . ? C8 C9 1.414(9) . ? C8 N1 1.428(8) . ? C9 C10 1.393(11) . ? C9 H9 0.9500 . ? C10 C11 1.383(11) . ? C10 H10 0.9500 . ? C11 C12 1.377(11) . ? C11 H11 0.9500 . ? C12 C13 1.403(10) . ? C12 H12 0.9500 . ? C13 N2 1.421(8) . ? C14 N2 1.277(8) . ? C14 C16 1.442(10) . ? C14 H14 0.9500 . ? C15 O2 1.285(8) . ? C15 C16 1.423(10) . ? C15 C20 1.434(9) . ? C16 C17 1.410(10) . ? C17 C18 1.358(10) . ? C17 H17 0.9500 . ? C18 C19 1.406(11) . ? C18 H18 0.9500 . ? C19 C20 1.362(10) . ? C19 H19 0.9500 . ? C20 O4 1.393(9) . ? C21 O3 1.424(9) . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 O4 1.438(8) . ? C22 H22A 0.9800 . ? C22 H22B 0.9800 . ? C22 H22C 0.9800 . ? C23 O5 1.305(7) . ? C23 C28 1.409(9) . ? C23 C24 1.420(9) . ? C24 O7 1.362(8) . ? C24 C25 1.375(10) . ? C25 C26 1.405(11) . ? C25 H25 0.9500 . ? C26 C27 1.374(10) . ? C26 H26 0.9500 . ? C27 C28 1.403(9) . ? C27 H27 0.9500 . ? C28 C29 1.435(9) . ? C29 N3 1.301(8) . ? C29 H29 0.9500 . ? C30 C35 1.387(9) . ? C30 C31 1.388(9) . ? C30 N3 1.441(8) . ? C31 C32 1.391(9) . ? C31 H31 0.9500 . ? C32 C33 1.381(11) . ? C32 H32 0.9500 . ? C33 C34 1.387(10) . ? C33 H33 0.9500 . ? C34 C35 1.386(9) . ? C34 H34 0.9500 . ? C35 N4 1.439(8) . ? C36 N4 1.287(8) . ? C36 C38 1.462(10) . ? C36 H36 0.9500 . ? C37 O6 1.300(8) . ? C37 C38 1.404(9) . ? C37 C42 1.420(9) . ? C38 C39 1.403(8) . ? C39 C40 1.376(10) . ? C39 H39 0.9500 . ? C40 C41 1.405(10) . ? C40 H40 0.9500 . ? C41 C42 1.379(10) . ? C41 H41 0.9500 . ? C42 O8 1.368(8) . ? C43 O7 1.418(7) . ? C43 H43A 0.9800 . ? C43 H43B 0.9800 . ? C43 H43C 0.9800 . ? C44 O8 1.444(9) . ? C44 H44A 0.9800 . ? C44 H44B 0.9800 . ? C44 H44C 0.9800 . ? C45 O9 1.391(9) . ? C45 H45A 0.9800 . ? C45 H45B 0.9800 . ? C45 H45C 0.9800 . ? C46 O10 1.413(11) . ? C46 H46A 0.9800 . ? C46 H46B 0.9800 . ? C46 H46C 0.9800 . ? Dy1 O5 2.269(4) . ? Dy1 O6 2.276(4) . ? Dy1 O1 2.275(4) . ? Dy1 O2 2.285(4) . ? Dy1 N3 2.496(5) . ? Dy1 N4 2.531(5) . ? Dy1 N2 2.531(5) . ? Dy1 N1 2.550(5) . ? Dy1 Na1 3.387(3) . ? Na1 O5 2.343(5) . ? Na1 O10 2.373(6) . ? Na1 O6 2.414(5) . ? Na1 O4 2.514(6) . ? Na1 O2 2.528(5) . ? Na1 O7 2.679(5) . ? Na1 O8 2.720(6) . ? O9 H9A 0.8400 . ? O10 H10A 0.8500 . ?