#------------------------------------------------------------------------------ #$Date: 2021-06-05 21:08:10 +0300 (Sat, 05 Jun 2021) $ #$Revision: 265946 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/25/7242507.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7242507 loop_ _publ_author_name 'Yin, Meng-Ru' 'Yan, Qing-Qing' 'Li, Bin' 'Yong, Guo-Ping' _publ_section_title ; 1D ladder and 2D bilayer coordination polymers constructed from a new T-shaped ligand: luminescence, magnetic and CO2 gas adsorption properties ; _journal_issue 17 _journal_name_full CrystEngComm _journal_page_first 3196 _journal_page_last 3203 _journal_paper_doi 10.1039/D1CE00257K _journal_volume 23 _journal_year 2021 _chemical_formula_sum 'C18 H12 Co N2 O5' _chemical_formula_weight 395.23 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2021-02-22 deposited with the CCDC. 2021-03-22 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 6.3178(2) _cell_length_b 19.3847(8) _cell_length_c 27.9152(11) _cell_measurement_reflns_used 2815 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 70.0821 _cell_measurement_theta_min 4.6328 _cell_volume 3418.7(2) _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 293(2) _diffrn_measured_fraction_theta_full 0.991 _diffrn_measured_fraction_theta_max 0.974 _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0515 _diffrn_reflns_av_unetI/netI 0.0784 _diffrn_reflns_Laue_measured_fraction_full 0.991 _diffrn_reflns_Laue_measured_fraction_max 0.974 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -4 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 7698 _diffrn_reflns_point_group_measured_fraction_full 0.991 _diffrn_reflns_point_group_measured_fraction_max 0.974 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 70.069 _diffrn_reflns_theta_min 4.562 _exptl_absorpt_coefficient_mu 8.165 _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.536 _exptl_crystal_description needle _exptl_crystal_F_000 1608 _refine_diff_density_max 0.845 _refine_diff_density_min -0.565 _refine_diff_density_rms 0.089 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.109 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 236 _refine_ls_number_reflns 3158 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.109 _refine_ls_R_factor_all 0.0889 _refine_ls_R_factor_gt 0.0627 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0606P)^2^+1.7391P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1516 _refine_ls_wR_factor_ref 0.1710 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2289 _reflns_number_total 3158 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1ce00257k2.cif _cod_data_source_block 3 _cod_depositor_comments 'Adding full bibliography for 7242505--7242508.cif.' _cod_database_code 7242507 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; 2.res created by SHELXL-2014/7 TITL ymr-0826-2_a.res in Pbca REM Old TITL YMR-0826-2 in Pbca #61 REM SHELXT solution in Pbca REM R1 0.143, Rweak 0.217, Alpha 0.055, Orientation as input REM Formula found by SHELXT: C18 N2 O5 Co CELL 1.54184 6.317803 19.384705 27.915224 90 90 90 ZERR 7 0.000239 0.000817 0.001147 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O Co UNIT 140 140 21 14 7 L.S. 10 PLAN 20 BOND $H LIST 6 MORE -1 CONF fmap 2 ACTA REM REM REM WGHT 0.060600 1.739100 FVAR 0.26591 CO1 5 0.461121 0.211949 0.355418 11.00000 0.03426 0.02953 = 0.02088 0.00241 -0.00414 0.00001 O5 4 0.150850 0.243306 0.349479 11.00000 0.03365 0.04060 = 0.02592 0.00646 -0.00068 -0.00119 AFIX 7 H2 2 0.064659 0.209055 0.354788 11.00000 -1.50000 H1 2 0.125961 0.259028 0.320820 11.00000 -1.50000 AFIX 0 O2 4 0.651784 0.304865 0.234203 11.00000 0.04175 0.04371 = 0.01661 0.00064 0.00144 0.00502 O1 4 0.553144 0.225033 0.287235 11.00000 0.04374 0.03478 = 0.02330 -0.00480 0.00256 -0.00120 O3 4 -0.008833 0.312599 0.572491 11.00000 0.03886 0.05229 = 0.02474 0.00380 0.00747 -0.00643 O4 4 0.286899 0.314895 0.613233 11.00000 0.04681 0.05356 = 0.02302 0.00422 0.00414 0.00489 N1 3 0.578919 0.321504 0.358449 11.00000 0.03463 0.03134 = 0.01981 -0.00013 0.00066 0.00275 N2 3 1.117276 0.606549 0.339056 11.00000 0.04334 0.02947 = 0.03830 0.00030 0.01018 -0.00130 C1 1 0.667865 0.334533 0.315507 11.00000 0.02670 0.03283 = 0.01692 -0.00046 0.00802 0.00190 C6 1 0.509468 0.355313 0.441020 11.00000 0.04204 0.02910 = 0.02131 -0.00443 0.00800 -0.00260 C9 1 0.301932 0.333280 0.528113 11.00000 0.03523 0.03273 = 0.02036 0.00037 0.00448 0.00536 C17 1 0.619988 0.284161 0.275962 11.00000 0.03207 0.03235 = 0.02287 -0.00308 -0.00327 0.00066 C5 1 0.620285 0.366001 0.394817 11.00000 0.04272 0.03421 = 0.01811 -0.00199 0.00684 -0.00181 C3 1 0.858540 0.432255 0.345274 11.00000 0.04310 0.02999 = 0.02514 0.00144 0.00943 0.00289 C18 1 0.188866 0.319453 0.573944 11.00000 0.03954 0.02956 = 0.02606 -0.00008 0.00895 0.00425 C12 1 1.017063 0.487045 0.336532 11.00000 0.04445 0.02914 = 0.02481 -0.00091 0.00511 -0.00209 C11 1 0.301180 0.333729 0.441656 11.00000 0.04433 0.04460 = 0.01981 -0.00553 0.00228 -0.00350 AFIX 43 H11A 2 0.229706 0.326809 0.412931 11.00000 -1.20000 AFIX 0 C2 1 0.805501 0.388452 0.307590 11.00000 0.03630 0.03164 = 0.02163 0.00122 0.00577 0.00405 AFIX 43 H2A 2 0.862628 0.395559 0.277285 11.00000 -1.20000 AFIX 0 C4 1 0.759631 0.421222 0.388872 11.00000 0.04971 0.03237 = 0.02362 -0.00547 0.00867 -0.00569 AFIX 43 H4A 2 0.786244 0.450828 0.414386 11.00000 -1.20000 AFIX 0 C10 1 0.197940 0.322315 0.484580 11.00000 0.04172 0.04306 = 0.02716 -0.00405 0.00237 0.00256 AFIX 43 H10A 2 0.058209 0.307225 0.484498 11.00000 -1.20000 AFIX 0 C7 1 0.613879 0.367476 0.484506 11.00000 0.04796 0.04695 = 0.01902 -0.00157 0.00623 -0.00783 AFIX 43 H7A 2 0.752672 0.383460 0.484616 11.00000 -1.20000 AFIX 0 C13 1 0.982831 0.555087 0.349394 11.00000 0.04122 0.03327 = 0.02872 -0.00347 0.01355 0.00025 AFIX 43 H13A 2 0.859812 0.565726 0.366132 11.00000 -1.20000 AFIX 0 C8 1 0.508806 0.355515 0.527498 11.00000 0.03909 0.04547 = 0.02013 -0.00219 0.00544 -0.00410 AFIX 43 H8A 2 0.579491 0.362658 0.556297 11.00000 -1.20000 AFIX 0 C16 1 1.202108 0.471777 0.312338 11.00000 0.05162 0.03391 = 0.05382 -0.00839 0.01499 -0.00210 AFIX 43 H16A 2 1.232470 0.426662 0.303327 11.00000 -1.20000 AFIX 0 C14 1 1.290365 0.590277 0.314715 11.00000 0.04506 0.03598 = 0.07216 -0.00866 0.01941 -0.01093 AFIX 43 H14A 2 1.382531 0.625494 0.305956 11.00000 -1.20000 AFIX 0 C15 1 1.339800 0.524056 0.301866 11.00000 0.04544 0.04886 = 0.08206 -0.01719 0.03075 -0.00226 AFIX 43 H15A 2 1.466274 0.514688 0.286110 11.00000 -1.20000 AFIX 0 HKLF 4 REM ymr-0826-2_a.res in Pbca REM R1 = 0.0627 for 2289 Fo > 4sig(Fo) and 0.0889 for all 3158 data REM 236 parameters refined using 0 restraints END WGHT 0.0606 1.7434 REM Highest difference peak 0.845, deepest hole -0.565, 1-sigma level 0.089 Q1 1 0.4459 0.1573 0.3558 11.00000 0.05 0.85 Q2 1 0.4553 0.2650 0.3579 11.00000 0.05 0.77 Q3 1 0.2868 0.2431 0.3562 11.00000 0.05 0.53 Q4 1 0.2822 0.1836 0.3536 11.00000 0.05 0.51 Q5 1 0.6231 0.1785 0.3536 11.00000 0.05 0.49 Q6 1 0.6013 0.2549 0.3591 11.00000 0.05 0.49 Q7 1 1.2056 0.6192 0.2365 11.00000 0.05 0.39 Q8 1 -0.0304 0.2348 0.3576 11.00000 0.05 0.38 Q9 1 0.7879 0.3390 0.3073 11.00000 0.05 0.37 Q10 1 0.6854 0.3872 0.3096 11.00000 0.05 0.35 Q11 1 0.4161 0.3178 0.5301 11.00000 0.05 0.31 Q12 1 1.0362 0.6004 0.3476 11.00000 0.05 0.30 Q13 1 0.3992 0.3237 0.6165 11.00000 0.05 0.30 Q14 1 0.6453 0.4043 0.3898 11.00000 0.05 0.29 Q15 1 0.0070 0.2653 0.5709 11.00000 0.05 0.29 Q16 1 0.1600 0.2984 0.3590 11.00000 0.05 0.27 Q17 1 0.4696 0.3135 0.3589 11.00000 0.05 0.27 Q18 1 -0.0171 0.3611 0.5720 11.00000 0.05 0.26 Q19 1 0.7514 0.2736 0.3859 11.00000 0.05 0.26 Q20 1 0.5094 0.2617 0.2816 11.00000 0.05 0.25 ; _shelx_res_checksum 4574 _shelx_hkl_file ; 0 0 3 7.26 2.23 0 0 4 5284.30 55.22 0 0 5 0.02 1.12 0 0 6 7417.13 81.37 0 0 7 0.59 1.69 0 0 8 24.59 5.39 0 0 9 -0.16 1.16 0 0 10 2301.44 60.55 0 0 11 1.30 1.66 0 0 12 5.39 3.92 0 0 13 -0.26 2.22 0 0 14 2861.73 84.15 0 0 15 0.74 2.12 0 0 16 501.76 39.34 0 0 17 -3.16 2.85 0 0 -18 376.00 30.20 0 0 18 407.84 37.61 0 0 -19 4.12 5.67 0 0 -20 345.10 31.22 0 0 -21 2.74 2.40 0 0 -22 249.23 28.66 0 0 -23 6.75 5.56 0 0 -24 2971.13 101.88 0 0 -25 -5.86 5.11 0 0 -26 233.81 29.24 0 0 -27 -6.78 6.60 0 0 -28 256.51 29.83 0 0 -29 5.78 3.31 0 0 -30 188.63 23.46 0 0 -31 -3.00 3.11 0 0 -32 64.30 11.45 0 -1 2 0.79 0.57 0 1 3 -0.59 0.30 0 -1 3 -0.26 0.64 0 1 4 0.27 0.59 0 -1 4 -0.55 0.85 0 -1 5 0.92 1.31 0 1 5 0.60 1.20 0 -1 6 0.70 0.93 0 1 6 -0.16 1.03 0 -1 7 4.31 2.95 0 1 7 -0.07 0.98 0 -1 8 3.11 2.75 0 1 8 1.92 2.08 0 1 9 -0.25 1.57 0 -1 9 -0.56 1.19 0 -1 10 -1.62 2.70 0 1 10 -0.79 1.15 0 1 11 0.99 2.86 0 -1 11 0.03 1.74 0 -1 12 -0.56 3.88 0 1 12 1.10 2.75 0 1 13 0.97 2.13 0 -1 13 1.16 2.30 0 1 14 3.83 3.73 0 -1 14 -0.82 3.51 0 1 15 1.33 1.58 0 -1 15 0.42 3.38 0 -1 16 2.08 4.68 0 -1 17 -0.06 2.34 0 -1 18 1.53 1.42 0 1 -18 -0.50 2.65 0 -1 19 -0.33 3.40 0 1 -19 1.85 3.41 0 1 -20 -0.62 4.16 0 -1 -20 1.01 3.43 0 1 -21 0.83 3.41 0 -1 -21 2.55 4.97 0 1 -22 -2.34 3.94 0 -1 -22 -1.01 1.78 0 1 -23 5.58 6.20 0 -1 -23 1.46 3.02 0 -1 -24 -1.77 4.41 0 1 -24 1.82 4.61 0 1 -25 -5.72 4.44 0 -1 -25 -1.93 5.35 0 1 -26 0.27 3.15 0 -1 -26 -1.64 4.85 0 -1 -27 0.32 3.51 0 1 -27 2.69 3.86 0 1 -28 -2.91 4.74 0 -1 -28 -0.79 4.05 0 -1 -29 0.68 1.52 0 1 -29 2.90 2.52 0 1 -30 2.35 1.48 0 -1 -30 -0.09 2.51 0 1 -31 -0.34 2.32 0 -1 -31 0.62 2.29 0 1 -32 -0.42 2.33 0 -1 -32 6.85 4.28 0 -2 0 9999.00 61.43 0 -2 1 35.52 3.94 0 -2 1 29.14 3.59 0 -2 -1 27.75 3.29 0 -2 2 181.50 9.87 0 -2 -2 186.65 8.98 0 -2 3 318.47 14.13 0 -2 4 129.05 9.71 0 -2 5 931.72 28.46 0 -2 6 421.42 21.41 0 -2 7 115.19 11.68 0 -2 8 2179.49 54.72 0 2 9 277.19 19.96 0 -2 9 258.17 19.64 0 -2 10 2267.57 61.73 0 -2 11 371.17 27.45 0 -2 12 230.11 22.06 0 -2 13 183.07 21.90 0 -2 14 3701.93 97.07 0 -2 15 746.36 47.15 0 -2 16 276.14 30.00 0 -2 17 -1.42 4.57 0 2 -18 327.72 28.74 0 -2 18 341.93 35.77 0 -2 19 242.86 32.11 0 2 -19 231.39 25.51 0 2 -20 25.14 9.24 0 -2 20 30.94 11.94 0 2 -21 94.47 17.85 0 -2 21 99.48 21.64 0 -2 -22 75.29 15.59 0 2 -22 74.00 16.13 0 -2 -23 689.54 48.45 0 2 -23 681.05 48.48 0 2 -24 790.83 53.84 0 -2 -24 842.75 53.77 0 -2 -25 97.62 18.73 0 2 -25 92.76 18.65 0 -2 -26 4.60 2.87 0 2 -26 10.28 5.89 0 2 -27 76.58 17.35 0 -2 -27 86.32 17.10 0 -2 -28 454.60 38.75 0 2 -28 434.87 38.07 0 2 -29 56.70 13.47 0 -2 -29 54.36 13.49 0 -2 -30 79.90 14.75 0 2 -30 77.62 14.76 0 -2 -31 -1.85 2.02 0 2 -31 -3.03 3.29 0 2 -32 98.41 13.90 0 -2 -32 110.79 15.08 0 -3 0 1.77 1.62 0 -3 1 0.02 1.05 0 -3 -1 1.52 0.97 0 -3 -2 0.49 0.56 0 -3 2 0.50 0.95 0 -3 -3 0.17 0.40 0 -3 3 0.37 0.80 0 -3 4 0.44 1.04 0 -3 5 1.28 2.06 0 -3 6 0.44 2.15 0 -3 7 -0.44 1.54 0 -3 8 -3.48 2.28 0 -3 9 -0.65 1.73 0 -3 10 1.70 2.97 0 -3 11 -0.58 1.30 0 -3 12 0.28 4.28 0 -3 13 1.90 3.21 0 -3 14 -2.69 3.79 0 -3 15 -0.38 3.39 0 -3 16 2.71 4.68 0 -3 17 -1.63 4.07 0 -3 18 2.24 5.38 0 3 -18 1.28 0.94 0 3 -19 0.42 2.87 0 -3 19 2.03 2.62 0 -3 20 3.95 4.38 0 3 -20 -2.83 2.54 0 3 -21 4.27 1.91 0 -3 21 5.77 7.42 0 -3 22 -0.67 3.02 0 3 -22 -1.45 3.94 0 3 -23 -11.28 8.33 0 -3 -23 0.49 3.11 0 3 -24 -5.21 2.96 0 -3 -24 1.31 5.01 0 3 -25 3.22 3.76 0 -3 -25 7.66 12.26 0 3 -26 1.56 3.68 0 -3 -26 -1.32 2.39 0 -3 -27 -3.42 5.18 0 3 -27 0.36 2.83 0 3 -28 -1.50 4.95 0 -3 -28 -2.66 3.83 0 -3 -29 1.18 2.78 0 3 -29 -2.39 1.30 0 3 -30 -0.96 2.01 0 -3 -30 -4.71 4.39 0 -3 -31 -0.10 1.32 0 3 -31 1.97 2.73 0 -3 -32 0.59 2.34 0 3 -32 -1.08 1.91 0 -4 0 102.92 9.66 0 -4 1 339.20 16.96 0 -4 -1 327.54 16.16 0 -4 -2 4418.95 59.05 0 -4 2 4469.35 63.05 0 -4 3 3674.41 59.02 0 -4 -3 3450.64 54.51 0 -4 -4 737.22 26.18 0 -4 4 782.32 28.48 0 -4 5 956.92 33.39 0 -4 -5 996.68 32.07 0 -4 6 256.26 18.23 0 -4 7 134.50 13.90 0 -4 8 304.95 21.89 0 -4 9 50.04 9.60 0 -4 10 948.34 42.88 0 -4 11 12.39 5.95 0 -4 12 18.61 7.45 0 -4 13 235.51 24.65 0 -4 14 2154.87 77.98 0 -4 15 507.88 39.54 0 -4 16 504.64 42.48 0 -4 17 5.78 5.56 0 4 -17 6.23 3.98 0 -4 18 93.78 19.92 0 4 -18 82.66 14.77 0 -4 19 224.16 31.35 0 4 -19 207.26 24.50 0 4 -20 174.45 23.49 0 -4 20 176.73 29.39 0 -4 21 51.37 16.12 0 4 -21 44.27 11.94 0 4 -22 119.68 19.67 0 -4 22 138.88 26.84 0 -4 23 399.75 46.32 0 4 -23 382.27 36.62 0 4 -24 25.28 9.59 0 -4 -24 30.36 11.23 0 -4 -25 350.07 34.94 0 4 -25 334.02 34.29 0 -4 -26 22.18 8.66 0 4 -26 18.96 8.85 0 4 -27 98.70 17.42 0 -4 -27 117.05 18.98 0 4 -28 116.48 19.31 0 -4 -28 117.79 19.06 0 4 -29 273.67 27.68 0 -4 -29 315.09 30.70 0 -4 -30 29.14 9.15 0 4 -30 29.65 8.73 0 4 -31 0.73 1.68 0 -4 -31 2.05 2.93 0 -4 -32 22.08 6.64 0 4 -32 16.02 5.19 0 -5 0 1.07 1.11 0 -5 -1 0.81 0.74 0 -5 1 0.79 1.92 0 -5 -2 -0.77 0.64 0 -5 2 1.31 1.78 0 -5 3 2.57 1.92 0 -5 -3 -0.34 0.62 0 -5 4 -2.03 2.24 0 -5 -4 -1.80 1.25 0 -5 -5 -0.62 1.05 0 -5 5 -0.41 1.08 0 -5 6 -0.07 1.20 0 -5 -6 0.19 1.31 0 -5 7 -0.19 0.84 0 -5 -7 -0.29 1.26 0 -5 8 -2.24 3.08 0 -5 9 -0.75 1.93 0 -5 10 0.98 2.64 0 -5 11 1.06 1.83 0 -5 12 4.78 3.46 0 -5 13 -0.70 1.47 0 -5 14 5.59 3.93 0 -5 15 -0.42 2.20 0 -5 16 -2.81 4.63 0 5 -17 -2.29 3.29 0 -5 17 -0.66 2.79 0 -5 18 1.68 2.23 0 5 -18 1.48 3.90 0 -5 19 -0.85 4.59 0 5 -19 -2.70 3.63 0 5 -20 2.55 2.82 0 -5 20 1.18 5.07 0 5 -21 0.93 2.11 0 -5 21 1.43 6.25 0 5 -22 0.09 2.01 0 -5 22 7.17 9.08 0 -5 23 -2.56 1.51 0 5 -23 1.98 1.48 0 5 -24 -1.64 1.73 0 -5 -25 1.63 4.17 0 5 -25 -4.63 5.28 0 5 -26 -4.67 6.75 0 -5 -26 2.73 6.53 0 5 -27 -5.63 3.20 0 -5 -27 3.13 3.87 0 5 -28 4.13 1.69 0 -5 -28 4.59 4.03 0 5 -29 5.54 5.61 0 -5 -29 1.67 3.91 0 5 -30 -3.07 2.65 0 -5 -30 -2.37 2.89 0 -5 -31 -3.41 1.69 0 5 -31 -4.23 3.17 0 -5 -32 5.97 3.92 0 -6 0 1607.85 45.15 0 -6 -1 1027.80 35.21 0 -6 1 1021.02 36.52 0 -6 -2 2580.34 56.99 0 -6 2 2614.30 58.65 0 -6 -3 2213.13 53.21 0 -6 3 2223.65 55.24 0 -6 4 773.37 33.19 0 -6 -4 753.55 31.56 0 -6 -5 905.38 35.25 0 -6 5 867.23 35.98 0 -6 -6 641.55 31.05 0 -6 6 641.88 32.26 0 -6 7 23.55 6.78 0 -6 -7 19.22 4.88 0 -6 8 202.38 19.97 0 -6 -8 188.08 18.13 0 -6 9 75.03 11.97 0 -6 -9 70.39 11.48 0 -6 10 36.00 8.64 0 -6 -10 33.70 8.05 0 -6 11 16.41 6.40 0 -6 -11 11.33 4.21 0 -6 12 2.34 1.29 0 -6 13 1234.87 58.38 0 -6 14 117.78 18.95 0 -6 15 571.86 43.39 0 6 -16 435.30 31.92 0 -6 16 451.21 39.79 0 6 -17 184.18 21.77 0 -6 17 188.21 26.62 0 6 -18 24.82 8.62 0 -6 18 24.65 10.64 0 6 -19 463.95 36.86 0 -6 19 437.50 43.44 0 -6 -20 340.47 37.21 0 6 -20 339.24 32.45 0 -6 20 358.31 40.93 0 -6 -21 448.45 43.32 0 -6 21 405.90 44.17 0 6 -21 431.58 36.74 0 -6 22 14.64 8.47 0 6 -22 19.92 8.45 0 -6 -22 12.27 7.33 0 6 -23 144.03 21.87 0 6 -24 34.42 10.09 0 6 -25 118.94 20.15 0 6 -26 41.20 12.07 0 -6 -26 51.88 14.38 0 -6 -27 214.79 26.24 0 6 -27 181.19 23.45 0 6 -28 4.02 3.26 0 -6 -28 4.85 5.09 0 -6 -29 446.76 34.99 0 6 -29 402.81 31.73 0 6 -30 38.18 9.16 0 -6 -30 37.38 9.78 0 6 -31 0.85 1.92 0 -6 -31 1.81 2.62 0 -6 -32 11.49 4.05 0 -7 0 41.99 9.08 0 -7 1 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9.76 2 -10 -29 48.23 9.26 2 -11 0 38.20 11.20 2 11 0 45.72 10.10 -2 -11 0 32.83 11.49 -2 -11 -1 29.82 9.42 2 -11 -1 33.18 11.92 -2 -11 1 21.66 9.01 2 11 1 21.62 7.02 2 11 -1 25.56 7.95 2 11 2 0.58 0.85 2 11 -2 3.90 3.71 -2 -11 2 -1.43 4.23 2 -11 -2 3.53 1.93 2 -11 -3 33.72 10.50 2 11 -3 41.25 10.36 -2 -11 3 39.70 11.68 2 11 3 33.92 8.38 2 11 4 423.06 31.79 -2 -11 4 414.56 40.57 2 -11 -4 431.30 39.17 2 11 -4 421.19 32.78 -2 11 5 17.08 6.61 2 11 5 16.16 6.24 2 -11 -5 14.01 8.06 2 11 -5 13.88 6.25 -2 -11 5 14.53 7.32 -2 -11 6 251.65 31.66 2 -11 -6 264.36 31.79 2 11 6 259.80 24.76 2 11 -6 257.91 26.46 2 11 7 7.16 3.96 2 11 -7 9.74 6.40 -2 -11 7 8.80 5.03 2 -11 -7 2.69 2.06 2 -11 -8 5.88 4.98 2 11 -8 7.21 5.07 2 11 8 11.05 5.34 -2 -11 8 8.01 6.76 2 11 9 34.04 9.25 2 11 -9 36.96 9.81 2 -11 -9 32.02 11.74 -2 -11 9 34.84 11.66 2 11 -10 102.69 17.16 -2 -11 10 101.72 20.66 2 11 10 106.61 15.63 2 -11 -10 104.61 21.66 2 11 10 99.50 15.54 2 11 11 1.64 3.58 2 11 -11 0.46 2.25 -2 -11 11 4.13 7.29 2 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4.22 4.28 2 14 3 2.69 3.72 2 14 -3 6.73 6.43 -2 -14 -3 0.26 4.83 2 -14 -3 2.44 5.58 -2 -14 3 -1.59 5.92 2 -14 -4 70.89 19.04 -2 14 4 68.19 14.92 2 14 4 64.29 14.42 -2 -14 4 64.99 18.13 -2 -14 -4 76.54 20.62 2 14 -4 66.23 14.60 2 -14 -5 39.67 14.43 -2 -14 -5 25.14 12.40 2 14 -5 39.15 11.17 2 14 5 38.94 11.24 -2 -14 5 30.18 12.44 2 14 6 204.46 25.21 -2 -14 6 226.24 32.87 2 -14 -6 205.82 32.01 2 14 -6 198.18 25.46 2 14 7 45.70 11.27 2 14 -7 46.74 12.02 2 -14 -7 54.08 16.90 -2 -14 7 52.23 17.06 2 14 -8 9.47 6.65 2 -14 -8 11.19 7.43 2 14 8 9.86 6.20 -2 -14 8 16.55 9.43 2 14 9 44.26 11.20 2 14 9 34.31 9.54 2 -14 -9 42.70 14.82 2 14 -9 29.38 10.27 -2 -14 9 40.34 14.75 2 14 -10 133.65 21.91 -2 -14 10 125.12 24.83 2 14 10 139.84 18.68 2 -14 -10 130.45 26.02 2 14 -11 124.28 20.38 2 14 -12 25.55 10.16 2 14 -13 -1.25 2.82 2 14 -14 121.88 20.57 2 14 -15 60.14 15.18 2 14 -16 9.22 6.03 2 14 -17 5.25 4.16 2 14 -18 89.55 16.83 2 14 -19 25.05 9.41 2 14 -20 54.20 12.96 2 14 -21 5.09 5.76 2 14 -22 -1.81 3.77 2 14 -23 4.52 4.84 2 14 -24 130.88 16.62 2 14 -25 11.39 4.53 2 -14 -25 13.52 5.38 2 15 0 13.08 7.08 -2 -15 0 12.50 8.16 -2 15 0 25.64 8.58 2 15 1 26.29 9.82 -2 -15 -1 19.67 8.86 -2 -15 1 31.47 13.91 2 15 -1 22.74 7.90 -2 15 1 21.14 6.77 -2 15 -1 33.59 10.63 -2 15 -2 34.13 10.09 2 15 2 25.98 8.56 -2 -15 -2 17.19 8.26 -2 -15 2 16.31 7.83 -2 15 2 31.41 9.62 2 15 -2 27.89 10.05 -2 15 3 6.79 5.78 2 15 -3 -2.36 4.80 -2 -15 -3 -1.15 5.77 -2 -15 3 7.03 4.81 2 15 3 1.14 4.90 -2 -15 -4 98.23 24.69 -2 -15 4 96.84 21.59 2 15 -4 125.23 20.37 2 15 4 115.42 19.86 -2 -15 -5 39.48 14.76 2 -15 -5 46.39 15.35 2 15 5 34.74 10.29 -2 -15 5 39.73 14.46 2 15 -5 48.85 12.48 2 15 -6 24.53 8.05 -2 -15 -6 26.39 11.96 -2 -15 6 19.70 8.97 2 15 6 30.08 10.20 2 -15 -6 23.72 11.79 2 15 7 65.10 14.43 2 15 -7 62.47 13.77 2 15 8 95.17 17.28 2 15 -8 114.40 20.09 2 15 -9 -4.57 2.32 2 15 9 -4.92 6.19 2 15 -10 191.74 25.43 2 15 -11 5.66 2.91 2 15 -12 11.44 6.33 2 15 -13 18.90 8.72 2 15 -14 115.83 19.28 2 15 -15 8.91 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13.21 -3 -12 4 60.65 16.60 3 -12 -4 53.02 14.81 -3 -12 -5 1.05 7.03 3 12 -5 -0.04 2.27 3 -12 -5 0.02 3.11 -3 -12 5 1.17 2.60 3 -12 -6 56.13 15.80 3 12 -6 63.83 14.16 -3 -12 6 53.93 16.05 3 12 7 4.27 3.72 3 -12 -7 11.48 7.48 3 12 -7 -1.97 3.43 -3 -12 7 10.09 6.57 -3 -12 8 166.90 28.85 3 12 8 156.22 21.77 3 -12 -8 150.05 26.95 3 12 -8 161.35 23.21 3 12 9 -0.16 2.35 3 -12 -9 6.20 7.22 3 12 -9 10.01 6.40 -3 -12 9 14.19 8.18 -3 -12 10 10.06 8.40 3 12 10 1.32 3.65 3 -12 -10 12.26 8.57 3 12 -10 5.37 4.17 3 12 -11 11.71 5.45 3 12 11 -4.37 4.58 3 12 12 208.96 23.68 3 12 -12 214.42 26.85 3 12 -13 0.12 3.86 3 12 13 4.34 5.19 3 12 -14 15.63 7.08 3 12 14 8.01 3.97 3 12 -15 -0.96 2.51 3 12 -16 123.89 20.98 3 12 -17 9.13 7.61 3 12 -18 18.12 6.79 3 12 -19 0.48 4.09 3 12 -20 92.08 16.40 3 12 -21 31.94 9.58 3 -12 -22 71.79 13.24 3 12 -22 69.53 13.73 3 12 -23 3.78 3.95 3 -12 -23 7.31 3.62 3 12 -24 18.83 6.86 3 -12 -24 5.17 2.81 3 12 -25 5.63 3.37 3 -12 -25 3.23 1.92 3 12 -26 14.46 5.19 3 13 0 -2.67 3.95 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250.88 26.50 4 -6 -13 247.51 34.71 -4 -6 13 255.92 33.47 4 -6 -14 11.69 7.41 4 6 -14 26.85 8.18 -4 -6 14 24.70 10.70 4 6 14 19.75 7.14 4 6 15 146.78 19.64 4 6 -15 156.92 21.78 4 6 -16 40.05 10.88 4 6 16 43.05 10.52 4 6 -17 15.53 8.10 4 6 17 12.31 6.24 4 6 -18 20.88 7.69 4 6 18 26.19 8.46 4 6 -19 32.97 10.87 4 6 19 28.94 8.37 4 6 -20 11.61 6.62 4 6 -21 -1.47 3.20 4 -6 -21 0.67 1.41 4 6 -22 47.88 10.90 4 -6 -22 49.77 11.89 4 6 -23 31.20 7.95 4 -6 -23 34.98 9.72 4 6 -24 2.73 2.36 4 -6 -24 5.05 4.71 4 -6 -25 70.11 11.65 4 6 -25 60.74 11.09 4 6 -26 -2.30 2.74 4 7 0 17.29 8.27 4 -7 0 23.65 6.21 -4 -7 0 19.53 9.00 4 7 0 29.64 7.78 4 -7 1 116.53 14.09 4 -7 -1 111.03 13.04 4 7 1 120.88 15.11 4 7 -1 121.27 15.64 -4 -7 -1 116.43 23.29 -4 -7 1 123.89 23.75 4 7 1 101.09 17.14 4 7 -1 108.74 17.41 4 7 2 50.45 12.71 4 7 -2 50.56 12.15 4 -7 2 57.41 10.29 4 -7 -2 50.63 8.83 4 7 2 47.17 9.93 4 -7 -2 58.95 14.27 -4 -7 -2 51.66 15.08 -4 -7 2 51.47 14.42 4 7 -2 41.98 8.70 4 7 3 113.56 14.45 4 7 -3 94.74 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35.74 10.52 4 7 -17 47.07 11.26 4 7 17 48.11 10.96 4 7 -18 20.59 8.26 4 7 18 26.97 8.35 4 7 19 147.57 16.94 4 7 -19 166.93 24.00 4 7 -20 12.38 4.74 4 7 -21 8.37 1.80 4 7 -22 0.06 2.59 4 7 -23 74.21 13.34 4 7 -24 0.40 3.03 4 7 -25 71.81 11.83 4 7 -26 -1.11 2.10 4 8 0 198.88 19.71 -4 -8 0 184.35 29.85 4 8 0 182.83 24.22 4 8 1 137.56 15.99 4 8 -1 134.46 16.41 -4 -8 -1 146.56 26.40 -4 -8 1 164.42 28.24 4 8 1 127.39 20.31 4 8 -1 118.01 18.86 4 -8 -1 141.34 22.23 4 8 2 55.64 13.01 4 8 -2 50.36 11.93 4 8 2 68.61 11.11 4 -8 -2 53.88 13.86 -4 -8 -2 58.41 16.91 -4 -8 2 61.35 16.02 4 8 -2 58.72 11.20 4 8 3 20.58 7.75 4 8 -3 18.62 7.04 4 -8 -3 17.56 8.43 -4 -8 -3 16.44 9.80 4 8 -3 16.99 5.40 -4 -8 3 12.66 6.35 4 8 -4 182.86 20.83 -4 -8 -4 171.48 30.32 -4 -8 4 174.20 28.29 4 8 4 177.33 23.92 4 8 -4 163.61 22.02 4 -8 -4 177.32 25.54 4 8 5 15.13 7.24 -4 -8 -5 21.39 9.74 4 -8 -5 13.63 7.83 4 8 -5 -0.92 6.14 -4 -8 5 17.70 8.20 4 8 6 3.19 3.24 -4 -8 -6 -0.63 7.07 4 -8 -6 -0.70 3.80 -4 -8 6 3.99 1.55 4 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5.71 2.48 4 9 -3 12.66 4.26 -4 -9 3 8.06 4.12 4 9 4 15.47 8.23 4 -9 -4 9.33 6.07 -4 -9 -4 10.30 5.20 4 9 -4 7.41 2.03 -4 -9 4 15.81 9.00 4 9 -5 307.20 26.85 -4 -9 -5 330.59 44.24 -4 -9 5 320.24 40.05 4 9 5 306.31 32.24 4 -9 -5 290.34 35.79 4 9 6 3.42 5.05 -4 -9 -6 -1.77 6.99 4 -9 -6 2.16 4.94 -4 -9 6 -0.52 2.88 4 -9 -7 77.42 19.12 -4 -9 7 87.00 21.38 4 9 7 73.80 15.58 4 -9 -8 0.20 3.69 -4 -9 8 10.91 8.60 4 9 8 3.26 3.31 -4 -9 9 197.16 31.57 4 9 9 186.06 24.76 4 -9 -9 152.92 27.27 -4 -9 10 56.62 16.79 4 -9 -10 54.20 16.72 4 9 10 74.64 15.60 4 9 11 8.31 2.98 4 9 -12 18.91 7.35 4 9 12 9.94 2.67 4 9 -13 54.94 12.89 4 9 13 49.55 11.29 4 9 -14 40.53 11.08 4 9 14 43.78 10.60 4 9 -15 16.95 7.72 4 9 15 22.30 7.75 4 9 -16 -1.38 2.69 4 9 16 2.77 2.89 4 9 -17 33.66 10.55 4 9 17 30.82 8.48 4 9 -18 10.31 3.72 4 9 18 17.74 6.74 4 9 -19 84.69 15.46 4 9 -20 12.24 5.55 4 9 -21 2.13 2.16 4 9 -22 -3.61 3.34 4 9 -23 44.29 9.39 4 9 -24 13.90 5.08 4 9 -25 78.72 10.81 4 10 0 38.90 10.09 -4 -10 0 57.13 18.02 4 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10 -18 30.19 8.54 4 10 -19 0.30 3.79 4 10 -20 44.65 9.91 4 10 -21 1.85 3.63 4 10 -22 3.85 3.33 4 10 -23 35.71 7.95 4 10 -24 4.20 2.56 -4 -11 0 225.17 36.64 4 11 0 157.81 22.69 4 11 1 1.89 6.31 4 11 -1 -2.12 6.36 -4 -11 -1 6.43 7.69 -4 -11 1 0.28 4.16 4 11 2 -0.90 5.40 -4 -11 -2 -0.53 3.12 -4 -11 2 -7.06 8.16 4 11 3 -0.35 2.27 4 -11 -3 8.74 7.12 -4 -11 -3 7.51 7.96 -4 -11 3 12.87 7.40 4 11 4 51.79 13.39 4 -11 -4 50.19 15.54 -4 -11 -4 56.70 19.01 -4 -11 4 53.34 18.46 4 11 5 16.61 8.42 4 -11 -5 24.74 13.13 -4 -11 -5 7.34 5.53 4 11 6 20.16 7.39 4 11 -6 26.17 6.76 4 11 7 8.29 6.38 4 11 -7 12.64 4.37 4 11 8 35.65 10.42 4 11 9 167.80 22.75 4 11 10 206.91 25.41 4 11 -10 214.48 25.15 4 11 -11 11.15 6.07 4 11 11 16.89 8.90 4 11 -12 9.31 5.38 4 11 12 2.07 6.56 4 11 -13 18.40 7.57 4 11 13 8.94 2.46 4 11 14 82.63 13.74 4 11 -14 102.60 17.54 4 11 -15 2.22 3.41 4 11 15 -0.38 2.55 4 11 -16 25.71 8.29 4 11 16 20.22 6.74 4 11 -17 3.45 2.77 4 11 -18 39.76 10.87 4 11 -19 1.43 2.53 4 11 -20 19.74 6.47 4 11 -21 5.57 3.59 4 11 -22 3.65 3.13 4 11 -23 12.55 4.28 4 12 0 5.78 2.53 4 12 1 20.09 5.37 4 12 -1 9.64 2.88 4 12 2 10.13 3.26 4 12 3 5.57 3.14 4 12 4 154.06 23.23 4 12 5 97.86 18.61 4 12 6 134.54 21.49 4 12 7 72.00 16.61 4 12 -8 -1.86 5.35 4 12 8 1.03 3.71 4 12 -9 35.49 10.31 4 12 -9 32.16 8.02 4 12 9 38.10 11.30 4 12 10 196.97 24.87 4 12 -10 184.00 23.05 4 12 -11 -1.02 4.96 4 12 11 8.65 5.20 4 12 -12 6.36 3.93 4 12 12 -6.37 5.60 4 12 -13 27.08 9.00 4 12 13 24.24 6.24 4 12 14 91.67 14.30 4 12 -14 125.08 18.55 4 12 15 64.68 11.58 4 12 -15 80.54 14.91 4 12 -16 5.38 4.40 4 12 16 9.30 4.74 4 12 -17 19.10 6.62 4 12 -18 108.73 15.92 4 12 -19 11.25 5.22 4 12 -20 62.35 11.01 4 12 -21 2.07 1.30 4 12 -22 10.75 4.01 4 13 0 23.69 6.23 4 13 1 -7.90 9.20 4 13 -1 -6.47 8.52 4 13 2 -0.33 5.85 4 13 3 2.95 1.95 4 13 4 137.49 22.43 4 13 5 9.57 6.20 4 13 6 14.64 6.48 4 13 7 27.23 10.37 4 13 8 138.74 21.17 4 13 -8 155.99 21.43 4 13 -9 15.58 6.98 4 13 9 25.07 9.15 4 13 10 209.42 24.69 4 13 -10 225.90 25.13 4 13 -11 19.03 8.25 4 13 11 14.73 6.93 4 13 -12 22.01 5.77 4 13 12 17.12 4.72 4 13 -13 2.36 2.34 4 13 13 3.75 1.18 4 13 -14 59.12 11.95 4 13 14 63.81 11.30 4 13 -15 16.19 7.31 4 13 15 9.77 4.56 4 13 -16 12.48 4.26 4 13 -17 5.29 1.48 4 13 -18 28.77 7.62 4 13 -19 0.00 1.87 4 13 -20 35.66 7.83 4 13 -20 32.48 6.32 4 14 0 62.15 16.02 4 14 1 64.13 13.59 4 14 -1 65.17 15.67 4 14 2 3.62 2.42 4 14 -2 2.03 4.49 4 14 3 27.11 9.43 4 14 4 91.60 17.33 4 14 5 11.56 7.18 4 14 6 94.18 17.95 4 14 7 2.63 2.25 4 14 -8 10.03 6.01 4 14 8 8.67 5.41 4 14 -9 25.06 8.25 4 14 9 21.89 7.43 4 14 10 155.17 20.47 4 14 -10 166.72 21.16 4 14 -11 29.79 9.54 4 14 11 23.88 7.00 4 14 -12 -1.15 3.97 4 14 12 -2.87 4.37 4 14 -13 5.52 4.37 4 14 -13 1.49 3.56 4 14 13 -5.08 3.90 4 14 -14 31.14 9.41 4 14 14 21.95 6.34 4 14 -15 6.26 4.19 4 14 -16 7.74 3.87 4 14 -17 5.14 2.28 4 14 -18 13.62 4.70 4 14 -19 4.84 2.62 4 15 0 59.57 15.32 4 15 1 7.39 5.13 4 15 -1 2.86 1.94 4 15 2 25.47 8.90 4 15 -2 27.38 9.75 4 15 3 -11.05 7.29 4 15 -3 9.08 5.43 4 15 4 132.89 20.84 4 15 5 19.49 8.18 4 15 6 94.57 17.07 4 15 7 14.91 7.72 4 15 -8 41.06 10.93 4 15 8 25.82 8.69 4 15 -9 27.62 8.75 4 15 9 12.85 6.05 4 15 -10 40.00 11.72 4 15 -10 33.86 9.06 4 15 10 32.53 9.51 4 15 -11 26.25 9.27 4 15 -11 16.43 6.41 4 15 11 3.63 3.76 4 15 -12 29.47 8.99 4 15 -12 18.89 6.57 4 15 12 15.18 4.77 4 15 -13 8.02 5.07 4 15 -13 4.59 3.19 4 15 13 4.55 1.95 4 15 -14 16.43 5.49 4 15 -15 17.36 6.09 4 15 -16 11.38 5.00 4 15 -17 -0.77 1.07 4 16 0 36.03 10.73 4 16 1 11.73 5.91 4 16 -1 11.03 6.49 4 16 2 2.50 4.00 4 16 -2 6.71 4.55 4 16 3 -2.99 3.63 4 16 -3 1.18 3.49 4 16 4 14.33 5.79 4 16 -4 23.00 9.05 4 16 5 1.14 2.57 4 16 -5 11.43 8.09 4 16 -6 49.15 13.83 4 16 6 41.60 10.60 4 16 -7 13.91 9.53 4 16 7 -0.08 3.29 4 16 -8 27.63 11.47 4 16 -8 15.73 5.97 4 16 8 13.89 6.12 4 16 -9 61.19 13.10 4 16 -9 52.18 10.77 4 16 9 48.54 11.01 4 16 -10 43.23 11.19 4 16 -10 36.58 8.78 4 16 10 32.95 8.32 4 16 -11 14.14 6.09 4 16 -11 5.59 4.34 4 16 11 5.57 2.92 4 16 -12 0.18 1.39 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7 22.10 10.78 5 1 7 21.62 8.45 5 -1 -7 11.64 6.79 5 1 -7 6.05 2.46 5 -1 7 13.10 6.04 5 1 7 10.78 5.49 5 -1 -8 4.58 3.96 5 1 -8 -0.93 3.48 5 -1 8 -3.46 4.47 5 1 8 8.02 6.24 5 -1 -9 0.48 2.86 5 1 -9 -5.59 6.06 5 -1 9 7.18 5.47 5 1 9 5.82 5.96 5 -1 -10 282.76 27.94 5 1 -10 267.53 27.27 5 -1 10 319.26 30.30 5 1 10 302.18 29.63 5 -1 -11 6.39 4.21 5 1 -11 9.59 4.48 5 -1 11 22.94 9.36 5 1 11 23.86 10.97 5 -1 -12 355.51 30.97 5 1 -12 324.21 30.23 5 -1 12 397.19 33.93 5 1 12 398.21 34.31 5 -1 -13 10.82 2.25 5 1 -13 18.05 4.58 5 -1 13 29.78 11.95 5 1 13 24.49 9.79 5 -1 -14 31.01 7.25 5 1 -14 24.42 5.68 5 -1 14 52.57 14.00 5 1 14 41.80 11.12 5 -1 -15 -5.62 8.02 5 1 -15 -4.71 9.24 5 1 15 19.20 9.86 5 -1 -16 11.87 2.53 5 1 -16 5.72 7.22 5 -1 -17 -0.91 3.45 5 1 -17 -7.90 9.35 5 1 17 12.64 7.80 5 -1 -18 -3.66 5.34 5 1 -18 -19.32 9.58 5 -1 -19 -5.04 4.86 5 1 -19 -10.73 8.93 5 -1 -20 -2.88 4.20 5 1 -20 -7.58 5.56 5 -1 -21 11.83 4.75 5 1 -21 4.31 3.97 5 -1 -22 2.04 1.38 5 1 -22 1.30 2.08 5 1 -23 4.45 1.45 5 1 -24 -3.84 2.82 5 -2 0 -5.33 6.90 5 2 0 13.07 6.66 5 -2 0 2.53 2.89 5 2 0 -1.29 4.26 5 -2 1 12.06 4.10 5 -2 -1 3.66 6.74 5 2 1 -2.88 8.01 5 2 -1 23.90 8.67 5 -2 -1 10.97 5.50 5 -2 1 12.22 5.59 5 2 1 13.05 4.96 5 2 -1 9.05 3.58 5 -2 2 83.91 13.10 5 2 -2 113.37 16.77 5 2 2 88.16 12.80 5 -2 -2 80.83 13.33 5 -2 2 98.16 15.26 5 2 2 90.62 15.94 5 2 -2 93.97 15.22 5 -2 3 9.06 4.51 5 2 3 -6.57 5.22 5 -2 -3 15.98 7.43 5 2 -3 10.02 6.83 5 -2 3 4.76 3.09 5 2 3 4.07 2.44 5 2 -3 -2.72 4.52 5 -2 4 9.35 5.67 5 2 4 -5.08 4.15 5 -2 -4 11.45 7.01 5 2 -4 6.60 3.40 5 -2 4 0.84 3.73 5 2 4 -2.34 4.19 5 -2 5 51.22 11.88 5 2 5 46.86 10.50 5 -2 -5 40.84 10.55 5 2 -5 29.82 8.02 5 -2 5 42.67 10.38 5 2 5 31.07 8.97 5 -2 6 83.30 14.89 5 2 6 77.95 12.77 5 -2 -6 81.34 15.02 5 2 -6 64.93 12.75 5 2 6 94.34 18.10 5 -2 6 76.88 14.07 5 -2 7 41.15 11.70 5 2 7 37.54 11.02 5 -2 -7 22.15 7.45 5 2 -7 20.56 5.90 5 -2 7 23.60 8.51 5 2 7 22.91 8.94 5 2 8 90.71 15.02 5 -2 -8 79.13 14.17 5 2 -8 66.81 13.25 5 -2 8 89.05 16.09 5 2 8 81.79 16.34 5 -2 -9 -4.33 3.94 5 2 -9 -2.57 8.24 5 -2 9 5.99 6.45 5 2 9 4.02 3.99 5 -2 -10 -3.61 1.58 5 2 -10 -7.33 9.18 5 -2 10 13.12 8.51 5 2 10 3.54 6.03 5 -2 -11 144.13 19.06 5 2 -11 111.28 16.91 5 -2 11 144.66 21.42 5 2 11 141.61 21.32 5 -2 -12 44.34 10.50 5 2 -12 11.39 7.69 5 -2 12 58.25 14.43 5 2 12 47.93 13.25 5 -2 -13 20.19 4.52 5 2 -13 9.73 5.65 5 -2 13 44.94 14.64 5 2 13 39.16 12.38 5 -2 -14 13.98 4.29 5 2 -14 3.31 7.84 5 2 14 14.59 6.66 5 -2 -15 19.51 6.65 5 2 -15 3.51 9.26 5 2 15 29.54 9.28 5 -2 -16 110.57 16.18 5 2 16 113.47 17.81 5 2 -16 62.02 9.86 5 -2 -17 10.12 3.51 5 2 17 28.42 9.70 5 -2 -18 9.38 4.91 5 2 18 17.80 7.60 5 -2 -19 28.10 7.42 5 2 -19 -13.86 8.62 5 -2 -20 59.33 10.36 5 2 -20 20.99 3.77 5 2 -21 17.02 4.84 5 2 -22 24.96 6.57 5 2 -23 0.31 2.48 5 2 -24 -0.89 2.56 5 -3 0 -5.77 5.50 5 3 0 9.49 7.18 5 -3 0 1.83 2.60 5 3 0 -3.35 5.08 5 -3 1 2.44 2.60 5 -3 -1 -7.70 5.58 5 3 1 4.77 3.83 5 3 -1 19.51 8.63 5 -3 1 9.73 5.58 5 3 1 -6.39 6.88 5 3 -1 -1.28 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3 12 38.45 12.60 5 -3 -13 152.57 19.33 5 3 13 164.14 23.49 5 3 -13 94.30 14.55 5 -3 -14 6.52 5.58 5 3 14 7.97 6.50 5 -3 -15 70.77 12.75 5 3 15 67.87 12.74 5 -3 -16 13.70 6.51 5 3 16 18.60 7.31 5 -3 -17 58.35 10.83 5 3 17 63.95 12.94 5 -3 -18 5.35 4.52 5 3 18 7.97 6.02 5 3 -19 -27.48 11.18 5 3 -20 -22.20 9.22 5 3 -21 -0.98 5.97 5 3 -22 -0.55 3.10 5 3 -23 -2.42 2.52 5 3 -24 10.31 4.17 5 -4 0 -3.20 4.15 5 4 0 15.24 8.18 5 -4 0 8.13 6.45 5 4 0 -5.52 7.45 5 -4 1 107.37 15.40 5 -4 -1 103.01 14.45 5 4 1 111.72 15.44 5 4 -1 116.96 17.38 5 -4 1 119.51 16.01 5 4 -1 95.06 16.22 5 4 1 90.84 15.19 5 -4 2 23.28 7.81 5 -4 -2 8.13 2.36 5 4 2 5.32 6.16 5 4 -2 22.62 7.30 5 -4 2 21.72 8.47 5 4 2 10.58 3.49 5 4 -2 9.99 2.82 5 -4 3 199.08 21.12 5 4 3 170.61 18.41 5 -4 -3 194.62 19.31 5 4 -3 182.59 21.59 5 -4 3 187.82 21.16 5 4 3 174.68 22.84 5 4 -3 168.06 21.35 5 -4 4 20.71 8.63 5 4 4 -11.60 6.36 5 -4 -4 -11.73 7.86 5 4 -4 -3.65 4.34 5 -4 4 11.22 7.67 5 4 4 -7.96 8.25 5 4 -4 -3.83 4.50 5 -4 5 17.93 10.04 5 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10.62 5 5 -1 53.66 12.47 5 5 1 62.02 13.84 5 5 -1 60.51 15.04 5 -5 2 15.77 7.76 5 -5 -2 4.23 2.06 5 5 2 -7.02 8.36 5 5 -2 8.90 5.64 5 5 2 3.80 2.77 5 5 -2 14.38 7.72 5 -5 3 109.55 16.10 5 -5 -3 78.89 12.32 5 5 3 79.02 11.75 5 5 -3 88.86 14.66 5 5 -3 92.20 17.47 5 5 3 85.09 14.89 5 -5 4 20.74 9.03 5 5 4 -6.09 6.44 5 -5 -4 -7.63 6.88 5 5 -4 -11.20 6.71 5 5 4 -4.53 6.99 5 5 -4 12.09 7.84 5 5 5 2.26 3.62 5 -5 -5 -5.91 5.34 5 5 -5 2.39 2.94 5 5 5 -4.48 7.13 5 5 -5 12.20 7.02 5 5 6 69.58 12.83 5 -5 -6 51.27 8.15 5 5 -6 57.33 11.70 5 5 6 59.89 12.34 5 -5 -7 6.27 4.71 5 5 -7 8.91 3.61 5 5 7 16.49 5.09 5 5 8 146.43 17.10 5 -5 -8 114.64 15.55 5 5 -8 95.00 16.01 5 5 8 118.52 18.29 5 -5 -9 120.61 16.47 5 5 -9 81.11 13.62 5 5 9 111.10 18.62 5 -5 -10 230.80 22.02 5 5 -10 165.28 20.21 5 5 10 211.70 25.55 5 -5 -11 18.40 8.10 5 5 -11 -2.54 7.15 5 5 11 8.73 5.41 5 5 -12 6.61 8.21 5 5 12 58.82 13.19 5 5 13 288.74 29.00 5 5 -13 144.43 15.67 5 5 14 88.97 15.72 5 5 -14 -2.78 12.20 5 5 15 14.30 8.61 5 5 16 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51.72 10.61 5 10 9 39.14 9.35 5 10 -9 47.06 11.01 5 10 -10 -1.01 3.13 5 10 10 -6.90 7.13 5 10 -11 16.79 5.73 5 10 11 7.76 3.43 5 10 -12 141.95 17.70 5 10 12 133.68 18.71 5 10 -13 4.20 3.47 5 10 13 15.62 6.76 5 10 -14 -3.73 3.98 5 10 14 1.34 2.53 5 10 -15 6.71 2.52 5 10 15 14.44 6.24 5 10 -16 107.19 14.07 5 10 16 102.42 13.63 5 10 -17 16.46 5.20 5 10 17 21.48 5.92 5 10 -18 45.45 9.32 5 10 18 42.60 7.50 5 10 -19 3.86 2.09 5 10 -20 -0.98 2.00 5 10 -21 48.98 7.44 5 11 0 -2.53 3.18 5 11 1 -1.35 6.36 5 11 -1 -0.38 4.51 5 11 -2 6.66 4.21 5 11 2 16.60 7.51 5 11 -3 21.16 7.08 5 11 3 45.47 12.16 5 11 -4 12.34 6.47 5 11 4 41.07 12.41 5 11 -5 3.44 4.54 5 11 -5 2.17 1.47 5 11 5 0.72 7.19 5 11 -6 4.71 3.98 5 11 -6 26.68 7.63 5 11 6 38.79 12.43 5 11 -7 6.50 3.68 5 11 -7 22.89 6.85 5 11 7 19.31 7.21 5 11 -8 16.43 5.59 5 11 8 3.05 7.75 5 11 -8 -0.36 6.12 5 11 -9 12.68 4.97 5 11 9 1.20 6.54 5 11 -9 4.94 1.27 5 11 -10 30.85 7.93 5 11 10 22.49 7.73 5 11 -11 0.61 2.65 5 11 11 0.73 1.66 5 11 -12 -1.13 2.03 5 11 12 0.16 1.17 5 11 -13 19.88 5.55 5 11 13 20.67 6.81 5 11 -14 9.87 2.80 5 11 14 11.75 4.57 5 11 -15 22.63 6.13 5 11 15 23.38 7.18 5 11 -16 17.71 5.35 5 11 16 27.52 7.44 5 11 -17 -0.07 2.47 5 11 17 2.29 1.92 5 11 -18 2.32 1.41 5 11 -19 8.66 3.28 5 12 0 -4.14 3.67 5 12 1 2.20 2.67 5 12 -1 -0.61 3.41 5 12 -2 76.46 14.97 5 12 2 120.98 19.71 5 12 -3 -9.11 9.83 5 12 3 5.92 7.15 5 12 -4 0.01 3.48 5 12 4 7.68 5.70 5 12 -5 -5.30 8.36 5 12 5 9.38 7.09 5 12 -6 47.50 10.50 5 12 6 153.05 21.74 5 12 -7 4.40 2.26 5 12 7 10.60 3.63 5 12 -8 53.25 11.28 5 12 8 58.46 11.82 5 12 -9 8.40 4.38 5 12 9 -4.27 5.85 5 12 -9 6.47 4.33 5 12 -10 45.22 9.07 5 12 10 36.18 8.18 5 12 -10 33.75 7.92 5 12 -11 8.19 4.10 5 12 11 2.51 3.88 5 12 -12 97.56 12.70 5 12 12 83.00 13.27 5 12 -13 39.67 7.88 5 12 13 34.94 8.17 5 12 -14 8.44 3.80 5 12 14 7.85 4.82 5 12 -15 -2.65 3.28 5 12 15 2.47 2.64 5 12 -16 56.94 8.69 5 12 16 56.81 8.78 5 12 -17 -1.54 1.57 5 13 0 -5.15 4.80 5 13 1 35.48 10.85 5 13 -1 23.22 8.10 5 13 -2 47.76 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6 0 2 8.82 6.21 6 0 2 2.86 5.05 6 0 3 11.53 8.28 6 0 3 7.05 4.91 6 0 4 22.96 10.82 6 0 4 10.00 6.63 6 0 -5 -31.79 14.79 6 0 5 1.91 2.55 6 0 -6 -0.92 5.27 6 0 6 13.74 5.47 6 0 -7 36.18 11.62 6 0 7 7.35 7.05 6 0 -8 145.35 20.16 6 0 8 116.11 18.01 6 0 -9 31.33 10.81 6 0 9 8.95 8.42 6 0 -10 84.56 15.37 6 0 10 74.70 15.44 6 0 -11 27.21 11.55 6 0 11 16.31 8.87 6 0 -12 71.89 14.12 6 0 12 66.07 14.66 6 0 -13 32.06 10.04 6 0 -14 27.13 8.95 6 0 -15 16.14 6.96 6 0 -16 6.60 5.38 6 0 -17 8.16 4.82 6 0 -18 24.45 6.28 6 0 -19 5.87 3.38 6 -1 0 390.25 30.25 6 1 0 395.87 30.54 6 -1 0 376.08 29.08 6 1 0 382.87 31.19 6 -1 1 5.67 6.37 6 1 1 -3.28 3.42 6 -1 -1 -0.63 4.46 6 1 -1 -11.40 7.64 6 -1 1 6.54 6.00 6 1 -1 4.52 4.61 6 1 1 10.44 7.67 6 -1 2 19.34 8.90 6 1 2 9.97 5.50 6 -1 -2 -0.83 2.49 6 -1 2 8.78 5.92 6 1 2 16.67 8.47 6 -1 3 12.87 8.13 6 1 3 10.82 8.99 6 -1 -3 1.92 4.13 6 1 -3 -11.05 10.87 6 -1 3 9.35 7.29 6 1 3 17.60 8.85 6 -1 4 187.89 21.17 6 1 4 175.70 20.60 6 -1 -4 133.14 16.91 6 1 -4 121.63 14.74 6 -1 4 142.56 19.54 6 1 4 139.63 19.58 6 -1 -5 3.96 7.17 6 -1 5 28.93 10.47 6 1 5 29.33 9.49 6 1 -6 45.97 12.19 6 -1 6 31.18 10.10 6 1 6 23.47 8.56 6 1 -7 22.00 10.67 6 -1 7 11.52 8.37 6 -1 -8 133.79 17.39 6 1 -8 145.10 20.94 6 -1 8 142.23 20.61 6 1 8 141.79 19.69 6 -1 -9 55.06 12.53 6 1 -9 37.70 12.43 6 -1 9 38.00 11.99 6 1 9 40.40 12.52 6 -1 -10 152.20 19.51 6 1 -10 148.37 19.55 6 -1 10 161.58 21.49 6 1 10 135.76 18.75 6 -1 -11 25.14 10.28 6 1 -11 19.74 8.38 6 1 11 14.01 9.44 6 -1 -12 28.86 9.83 6 1 -12 25.76 9.74 6 1 12 24.96 9.02 6 -1 -13 26.57 8.70 6 1 -13 15.87 8.54 6 1 13 23.04 8.96 6 -1 -14 74.72 12.71 6 1 -14 69.95 12.63 6 -1 -15 17.43 7.30 6 1 -15 16.05 6.53 6 -1 -16 22.72 8.01 6 1 -16 19.25 6.95 6 -1 -17 10.27 5.39 6 1 -17 10.51 4.58 6 -1 -18 34.22 6.96 6 1 -18 25.11 6.48 6 -1 -19 -6.25 3.65 6 1 -19 5.17 2.65 6 1 -20 32.61 6.47 6 -2 0 13.57 7.04 6 2 0 5.98 5.43 6 2 0 24.94 9.58 6 -2 1 8.49 7.04 6 -2 -1 -8.82 4.60 6 2 1 -3.19 5.63 6 2 -1 -19.02 9.09 6 -2 1 10.10 5.98 6 2 -1 3.26 5.89 6 2 1 10.44 7.06 6 -2 2 25.47 9.82 6 2 2 14.12 4.90 6 -2 -2 7.69 4.02 6 2 -2 -5.58 8.78 6 -2 2 23.57 9.12 6 2 -2 20.63 7.81 6 2 2 26.80 9.39 6 -2 3 66.71 13.38 6 2 3 55.11 13.00 6 -2 -3 34.43 7.39 6 2 -3 21.57 7.30 6 -2 3 47.50 12.92 6 2 3 50.78 13.11 6 -2 4 35.49 12.28 6 2 4 16.23 8.06 6 -2 -4 -11.24 7.91 6 2 -4 -21.02 11.70 6 -2 4 16.94 9.40 6 2 4 17.38 8.87 6 2 5 19.93 10.14 6 2 -5 37.26 13.18 6 -2 5 16.17 8.32 6 2 5 11.91 8.52 6 2 6 46.08 12.08 6 2 -6 42.67 13.89 6 -2 6 32.16 11.48 6 2 6 16.71 8.98 6 2 -7 18.01 11.60 6 -2 7 26.45 9.51 6 2 7 18.44 8.29 6 2 -8 16.11 11.05 6 2 8 1.27 4.21 6 -2 -9 -1.97 7.60 6 2 -9 29.49 12.54 6 2 9 20.02 7.64 6 -2 -10 -2.22 3.63 6 2 -10 16.43 9.48 6 2 10 18.82 9.02 6 -2 -11 2.96 4.30 6 2 -11 12.51 7.05 6 2 11 9.69 6.38 6 -2 -12 23.16 7.53 6 2 -12 24.64 9.44 6 2 12 20.41 9.04 6 -2 -13 11.99 5.20 6 2 -13 28.19 9.77 6 2 13 14.10 8.47 6 -2 -14 7.48 4.34 6 2 14 11.39 8.22 6 -2 -15 34.27 7.19 6 2 -15 54.38 10.84 6 -2 -16 -14.12 5.05 6 2 -16 16.68 6.49 6 -2 -17 -12.85 5.61 6 2 -17 -0.64 1.33 6 2 -18 -2.52 2.42 6 2 -19 1.13 2.22 6 2 -20 3.50 2.28 6 -3 0 267.78 24.26 6 3 0 233.44 23.00 6 3 0 232.39 25.46 6 -3 1 19.18 8.31 6 -3 -1 13.23 6.62 6 3 1 -7.52 7.29 6 3 -1 -3.62 8.46 6 3 -1 12.63 7.28 6 3 1 11.00 5.82 6 -3 2 66.77 14.10 6 -3 -2 51.90 10.41 6 3 2 39.33 9.08 6 3 -2 52.53 11.39 6 3 2 50.12 12.82 6 -3 3 82.21 15.57 6 3 3 64.46 13.05 6 -3 -3 68.60 12.37 6 3 3 58.54 13.59 6 3 4 170.41 19.51 6 -3 -4 152.33 18.24 6 3 -4 161.97 20.23 6 3 4 155.62 20.74 6 3 5 102.98 16.47 6 3 -5 121.71 20.84 6 -3 -5 80.60 12.66 6 3 5 104.40 17.32 6 3 6 134.68 17.54 6 -3 -6 104.63 14.65 6 3 -6 136.46 19.90 6 3 6 125.25 19.74 6 -3 -7 -8.32 7.34 6 3 7 8.13 7.47 6 3 -8 33.84 12.26 6 3 8 36.50 12.42 6 -3 -9 147.59 17.27 6 3 -9 164.40 21.62 6 3 9 168.92 21.64 6 -3 -10 256.10 23.00 6 3 -10 266.59 25.48 6 3 10 295.71 27.61 6 3 -11 28.37 10.12 6 3 11 10.17 5.69 6 -3 -12 -9.56 6.88 6 3 12 9.08 5.64 6 -3 -13 7.69 2.31 6 3 13 28.63 9.28 6 -3 -14 68.61 10.57 6 3 -14 76.31 13.59 6 3 14 81.78 14.81 6 -3 -15 25.09 4.64 6 3 -15 32.65 8.26 6 3 -16 18.78 5.21 6 3 -17 -4.87 4.46 6 3 -18 6.81 1.08 6 3 -19 17.72 4.76 6 3 -20 16.91 4.43 6 -4 0 21.08 9.42 6 4 0 2.19 5.86 6 4 0 6.62 5.90 6 -4 -1 7.86 6.10 6 4 1 1.82 2.80 6 4 -1 -9.74 8.17 6 4 1 1.11 3.27 6 4 -1 3.46 4.55 6 -4 -2 17.16 6.43 6 4 2 13.02 5.83 6 4 2 12.92 7.15 6 4 -2 8.53 5.86 6 4 3 36.93 10.47 6 -4 -3 33.77 9.17 6 4 -3 11.17 8.23 6 4 3 35.30 10.28 6 4 -3 31.75 9.42 6 4 4 47.05 11.14 6 -4 -4 35.99 8.51 6 4 -4 38.61 9.08 6 4 4 40.01 11.49 6 4 5 16.80 9.05 6 -4 -5 4.62 3.46 6 4 -5 28.66 12.68 6 4 5 9.61 7.63 6 -4 -6 11.83 3.64 6 4 -6 38.87 12.84 6 4 6 26.33 10.04 6 -4 -7 2.58 2.78 6 4 -7 18.66 11.11 6 4 7 19.85 9.95 6 -4 -8 -1.61 4.77 6 4 -8 35.61 13.27 6 4 8 26.98 10.46 6 -4 -9 -6.15 5.39 6 4 -9 23.78 11.38 6 4 9 13.36 10.29 6 -4 -10 -1.77 3.43 6 4 -10 17.35 10.54 6 4 10 18.00 9.37 6 -4 -11 19.09 4.80 6 4 11 20.31 7.82 6 -4 -12 3.06 1.72 6 4 12 11.91 5.73 6 -4 -13 0.47 3.21 6 4 -13 16.27 6.92 6 4 13 8.69 5.70 6 4 -14 13.77 5.95 6 4 14 14.11 6.37 6 4 -15 -0.57 5.37 6 4 15 57.55 11.23 6 4 -16 -16.39 6.72 6 4 16 24.74 7.97 6 4 -17 -10.55 4.32 6 4 -18 -6.99 3.61 6 4 -19 0.01 0.83 6 4 -20 18.04 4.72 6 5 0 2.34 4.77 6 5 0 2.44 1.82 6 -5 -1 198.15 20.53 6 5 1 144.95 17.56 6 5 -1 131.32 16.88 6 5 1 157.02 21.56 6 5 -1 158.31 20.78 6 5 2 -2.69 3.60 6 5 -2 -8.38 8.53 6 5 2 -0.43 3.96 6 5 -2 1.83 2.99 6 -5 -3 134.21 16.80 6 5 3 107.94 14.98 6 5 -3 75.60 9.55 6 5 3 123.27 18.88 6 5 -3 110.02 16.88 6 5 4 21.02 8.60 6 -5 -4 22.09 7.83 6 5 -4 16.81 4.21 6 5 4 4.62 2.71 6 5 5 365.92 26.94 6 -5 -5 343.14 26.59 6 5 -5 348.31 29.19 6 5 5 359.57 31.96 6 -5 -6 3.73 4.25 6 5 -6 26.17 11.13 6 5 6 9.79 8.61 6 -5 -7 43.52 9.91 6 5 -7 47.26 13.19 6 5 7 47.54 12.26 6 -5 -8 16.21 5.14 6 5 -8 29.09 10.34 6 5 8 23.42 9.29 6 -5 -9 104.27 13.44 6 5 -9 104.23 16.84 6 5 9 133.24 19.29 6 -5 -10 50.17 9.35 6 5 -10 45.88 12.52 6 5 10 54.30 12.92 6 5 -11 19.50 8.35 6 5 11 21.48 9.75 6 5 -12 1.57 2.18 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17.54 6.26 6 6 -15 -8.13 4.85 6 6 15 8.05 4.56 6 6 -16 10.88 4.29 6 6 16 20.91 7.07 6 6 -17 -1.71 3.02 6 6 -18 0.23 1.70 6 6 -19 7.93 3.29 6 7 0 0.90 1.73 6 7 0 -4.90 5.72 6 7 1 29.39 7.72 6 7 -1 22.46 4.61 6 7 1 18.18 3.06 6 7 -1 19.99 4.94 6 7 2 9.90 6.01 6 7 -2 -13.95 7.37 6 7 2 -6.36 5.31 6 7 -2 -9.39 7.29 6 7 3 134.53 16.18 6 7 -3 98.57 13.02 6 7 3 119.02 17.35 6 7 -3 102.43 15.94 6 7 4 0.57 2.35 6 7 -4 -3.29 4.62 6 7 -5 158.79 18.20 6 7 5 178.04 22.25 6 7 -5 144.57 18.16 6 7 -6 31.11 9.60 6 7 6 9.73 6.74 6 7 -7 7.76 5.13 6 7 7 5.25 5.96 6 7 -8 7.92 6.46 6 7 8 3.02 4.94 6 7 -9 118.51 16.31 6 7 9 164.15 20.40 6 7 -10 12.61 5.53 6 7 10 17.74 7.99 6 7 -11 21.21 6.21 6 7 11 32.78 10.33 6 7 -12 7.03 2.51 6 7 12 21.78 8.38 6 7 -13 16.39 4.82 6 7 13 24.34 7.06 6 7 -14 1.76 1.13 6 7 14 4.98 3.28 6 7 -15 37.00 7.40 6 7 15 58.92 10.13 6 7 -16 -0.39 1.25 6 7 16 9.02 4.60 6 7 -17 16.84 4.77 6 7 -18 6.99 3.17 6 8 0 5.51 3.60 6 8 0 1.92 3.66 6 8 1 1.96 1.57 6 8 -1 0.50 2.17 6 8 1 -11.20 7.66 6 8 -1 -6.90 6.54 6 8 -2 -6.07 5.00 6 8 2 -8.39 7.40 6 8 -2 -7.23 5.76 6 8 -3 -8.77 5.94 6 8 3 2.19 2.06 6 8 -3 -11.27 7.46 6 8 -4 4.36 4.30 6 8 4 7.74 2.24 6 8 -4 0.01 5.66 6 8 5 -2.66 4.98 6 8 -5 -0.95 3.07 6 8 -6 22.89 7.79 6 8 6 8.76 4.85 6 8 -7 17.20 6.32 6 8 7 0.43 2.70 6 8 -8 9.40 4.94 6 8 8 5.38 3.72 6 8 -9 6.73 4.45 6 8 9 16.68 7.02 6 8 -10 5.42 4.23 6 8 10 9.29 5.74 6 8 -11 15.58 5.40 6 8 11 30.75 9.18 6 8 -12 12.73 4.97 6 8 12 25.19 7.82 6 8 -13 1.60 2.38 6 8 13 1.50 3.23 6 8 -14 1.40 1.83 6 8 14 6.31 4.07 6 8 -15 6.28 3.24 6 8 15 12.55 4.91 6 8 -16 0.73 2.40 6 8 16 7.83 3.80 6 8 -17 0.72 2.04 6 9 0 34.75 7.80 6 9 0 12.31 5.25 6 9 1 14.18 5.40 6 9 -1 9.58 3.74 6 9 1 -8.89 6.83 6 9 -1 -8.79 7.95 6 9 -2 7.70 3.17 6 9 2 5.29 2.19 6 9 -3 36.34 7.29 6 9 3 28.68 7.28 6 9 -3 11.76 3.33 6 9 -4 5.79 3.39 6 9 4 14.18 4.96 6 9 -5 59.61 9.72 6 9 5 70.93 13.31 6 9 -5 49.74 9.57 6 9 -6 -5.89 6.71 6 9 6 10.41 6.18 6 9 -7 -2.07 3.95 6 9 7 -3.70 4.13 6 9 -8 6.16 4.58 6 9 8 9.31 5.96 6 9 -9 48.63 9.67 6 9 9 51.95 11.05 6 9 -10 37.51 8.64 6 9 10 31.37 8.88 6 9 -11 110.73 13.33 6 9 11 98.08 14.14 6 9 -12 18.03 6.12 6 9 12 20.01 7.15 6 9 -13 45.40 8.04 6 9 13 49.42 9.39 6 9 -14 15.41 4.70 6 9 14 10.92 4.20 6 9 -15 17.89 4.94 6 9 15 23.75 6.13 6 9 -16 6.05 3.42 6 10 0 -11.97 8.03 6 10 1 -7.29 7.32 6 10 -1 -12.02 8.51 6 10 -2 6.59 3.70 6 10 2 -8.06 6.98 6 10 -2 -17.11 9.63 6 10 3 -0.02 3.94 6 10 -3 -11.44 8.33 6 10 -4 1.89 2.52 6 10 4 -2.89 4.52 6 10 -5 -6.28 4.54 6 10 5 -3.98 4.62 6 10 -5 -7.66 5.40 6 10 -6 5.69 1.45 6 10 6 15.35 6.73 6 10 -6 12.02 4.44 6 10 -7 -4.21 4.32 6 10 7 9.11 4.86 6 10 -8 -12.69 5.94 6 10 8 3.19 3.10 6 10 -9 -2.96 1.57 6 10 9 3.68 3.39 6 10 -10 6.45 3.27 6 10 10 9.78 5.33 6 10 -11 16.56 5.59 6 10 11 15.35 6.12 6 10 -12 12.39 4.39 6 10 12 7.38 3.83 6 10 -13 14.97 4.89 6 10 13 9.58 4.25 6 10 -14 4.39 3.00 6 10 14 2.77 2.72 6 11 0 31.00 5.63 6 11 1 -6.31 5.99 6 11 -1 -18.22 8.87 6 11 2 2.36 4.26 6 11 -2 -10.90 6.73 6 11 3 -1.92 3.64 6 11 -3 -9.66 5.95 6 11 4 18.38 5.69 6 11 -4 3.96 2.19 6 11 5 34.43 8.53 6 11 -5 18.42 5.45 6 11 6 15.53 5.44 6 11 -6 7.64 3.89 6 11 -7 -2.56 2.63 6 11 7 1.35 2.39 6 11 -8 25.68 5.43 6 11 8 31.42 8.20 6 11 -9 -3.17 3.43 6 11 9 3.85 3.14 6 11 -10 24.25 4.92 6 11 10 31.09 7.67 6 11 -11 64.81 8.26 6 11 11 73.03 10.93 6 11 12 3.60 2.94 6 11 13 16.11 4.50 6 12 0 -10.38 5.76 6 12 1 -5.94 5.87 6 12 -1 -5.42 5.29 6 12 2 -6.45 5.55 6 12 -2 -3.36 4.14 6 12 3 -1.36 2.75 6 12 -3 3.23 2.67 6 12 4 -4.92 4.22 6 12 -4 17.37 5.83 6 12 5 0.01 1.86 6 12 -5 11.25 4.67 6 12 6 2.37 1.43 6 12 -6 10.87 4.47 6 12 7 -5.11 4.63 6 12 8 1.86 2.76 6 12 9 15.78 5.29 6 12 10 2.21 2.12 6 12 11 10.06 4.05 6 13 0 81.06 12.23 6 13 1 -4.56 3.73 6 13 -1 2.99 2.11 6 13 2 10.44 4.02 6 13 -2 11.24 4.89 6 13 3 -5.66 3.77 6 13 -3 12.11 5.01 6 13 4 20.13 5.65 6 13 -4 37.86 7.90 6 13 5 1.55 2.26 6 13 -5 14.19 4.98 6 13 6 22.67 5.91 6 13 7 2.11 2.69 6 13 8 31.22 7.03 6 13 9 8.17 3.68 6 14 0 0.92 1.57 6 14 1 2.73 2.35 6 14 -1 4.69 3.12 6 14 2 3.00 2.16 6 14 -2 6.48 3.18 6 14 3 5.23 3.19 6 14 -3 8.65 4.15 6 14 4 3.90 2.94 6 14 5 2.15 2.66 6 14 6 7.10 3.41 7 0 0 51.58 10.81 7 0 -1 35.56 9.40 7 0 -2 152.46 16.62 7 0 -3 14.56 6.06 7 0 -4 32.73 7.89 7 0 -5 10.48 5.08 7 0 -6 68.36 10.25 7 0 -7 4.41 2.80 7 0 -8 45.28 8.58 7 0 -9 0.28 1.47 7 0 -10 75.22 10.11 7 0 -11 6.02 3.62 7 0 -12 61.03 8.69 7 0 -13 1.87 1.53 7 1 0 32.45 8.66 7 -1 -1 24.67 8.21 7 1 -1 37.01 9.27 7 -1 -2 35.08 9.02 7 1 -2 38.19 9.81 7 -1 -3 48.92 9.63 7 1 -3 24.40 6.93 7 -1 -4 41.36 8.99 7 1 -4 24.34 6.95 7 -1 -5 25.77 7.74 7 1 -5 12.62 5.11 7 -1 -6 17.55 6.14 7 1 -6 16.64 6.01 7 -1 -7 25.00 6.49 7 1 -7 5.72 2.87 7 -1 -8 25.13 6.56 7 1 -8 9.54 3.82 7 -1 -9 11.33 4.67 7 1 -9 1.69 3.17 7 -1 -10 13.80 4.83 7 1 -10 2.07 1.34 7 -1 -11 23.80 5.61 7 1 -11 10.39 3.67 7 -1 -12 74.44 9.10 7 1 -12 55.56 8.03 7 1 -13 14.39 4.12 7 2 0 24.30 7.82 7 2 1 50.07 10.25 7 2 -1 20.93 7.67 7 -2 -2 113.13 13.91 7 2 -2 95.18 13.13 7 2 2 83.78 12.10 7 -2 -3 52.16 9.69 7 2 -3 34.70 7.94 7 2 3 41.02 9.40 7 2 -4 15.18 4.97 7 2 4 25.37 7.69 7 -2 -5 13.23 5.99 7 2 -5 5.54 3.13 7 2 5 16.64 6.86 7 -2 -6 70.98 10.64 7 2 -6 28.21 5.96 7 -2 -7 22.87 6.49 7 2 -7 -3.62 3.06 7 -2 -8 71.42 10.32 7 2 -8 40.14 7.05 7 -2 -9 30.32 6.66 7 2 -9 6.43 3.43 7 -2 -10 23.44 5.91 7 2 -10 -0.91 3.45 7 -2 -11 13.96 4.86 7 2 -11 -8.12 3.63 7 2 -12 54.07 8.06 7 2 -13 -2.43 3.10 7 3 0 24.32 7.44 7 3 1 33.35 8.82 7 3 -1 23.38 7.48 7 3 1 20.56 6.41 7 3 -2 37.54 9.32 7 3 2 45.12 9.32 7 3 -3 24.09 6.79 7 3 3 19.88 7.33 7 3 -4 23.50 6.66 7 3 4 26.10 7.34 7 3 -5 3.86 3.38 7 3 5 17.59 6.63 7 -3 -6 18.35 6.68 7 3 6 19.11 6.94 7 -3 -7 24.20 6.37 7 3 7 19.88 6.89 7 -3 -8 15.79 5.81 7 3 8 24.60 7.74 7 -3 -9 21.63 5.69 7 3 -9 -9.15 4.36 7 -3 -10 15.95 4.87 7 3 -10 -5.07 4.29 7 3 -11 2.68 0.76 7 3 -12 0.46 1.57 7 3 -13 -7.08 3.27 7 4 0 28.78 8.15 7 4 1 42.72 9.08 7 4 -1 23.55 7.84 7 4 1 20.89 6.37 7 4 -2 48.25 9.79 7 4 2 53.26 9.92 7 4 -3 92.36 12.16 7 4 3 84.76 11.80 7 4 -4 59.70 10.11 7 4 4 59.47 10.40 7 4 -5 13.89 5.51 7 4 5 24.73 7.55 7 4 -6 4.26 3.26 7 4 6 19.73 6.79 7 4 -7 58.87 8.92 7 4 7 103.04 13.27 7 4 -8 9.48 3.28 7 4 8 35.27 8.00 7 4 -9 10.87 3.80 7 4 9 42.82 8.47 7 4 -10 -0.24 2.24 7 4 -11 -5.84 3.44 7 4 -12 4.95 1.13 7 4 -13 -3.14 2.81 7 5 0 21.37 7.22 7 5 0 9.17 4.03 7 5 -1 21.88 6.42 7 5 1 12.51 5.37 7 5 -2 22.81 6.26 7 5 2 21.14 6.36 7 5 -3 13.17 5.34 7 5 3 11.99 5.51 7 5 -4 9.29 4.19 7 5 4 8.47 4.54 7 5 -5 23.45 6.19 7 5 5 31.05 7.77 7 5 -6 -0.39 1.24 7 5 6 10.07 5.06 7 5 -7 -1.41 1.57 7 5 7 17.62 6.45 7 5 -8 -0.14 1.01 7 5 8 10.68 5.04 7 5 -9 -4.20 2.77 7 5 9 10.42 4.66 7 5 -10 -5.98 3.90 7 5 10 12.84 5.64 7 5 -11 -4.06 3.33 7 5 -12 -3.88 2.41 7 6 0 21.37 5.83 7 6 0 3.98 3.01 7 6 -1 33.52 7.09 7 6 1 23.90 5.84 7 6 -2 10.18 4.49 7 6 2 10.26 4.87 7 6 -3 42.64 7.97 7 6 3 35.95 7.51 7 6 -4 0.74 2.03 7 6 4 9.33 4.47 7 6 -5 13.09 4.41 7 6 5 14.67 5.19 7 6 -6 9.26 4.10 7 6 6 10.35 4.45 7 6 -7 87.11 10.42 7 6 7 108.62 12.70 7 6 -8 -0.66 1.40 7 6 8 7.23 4.42 7 6 -9 6.17 2.58 7 6 9 20.91 5.96 7 6 -10 -2.67 2.49 7 6 10 11.87 4.74 7 6 -11 9.41 3.03 7 7 0 2.16 2.14 7 7 -1 20.69 5.43 7 7 1 7.81 3.77 7 7 -2 13.02 4.56 7 7 2 4.72 3.35 7 7 -3 8.47 3.37 7 7 3 4.88 3.43 7 7 -4 10.64 4.14 7 7 4 4.57 2.79 7 7 -5 5.73 2.99 7 7 5 5.46 3.18 7 7 -6 0.68 1.75 7 7 6 -0.61 0.93 7 7 -7 4.09 2.54 7 7 7 6.89 3.84 7 7 -8 2.67 2.02 7 7 8 7.66 4.16 7 7 -9 4.04 2.07 7 7 9 11.38 4.39 7 8 1 6.10 2.39 7 8 2 0.74 0.71 7 8 -3 29.45 5.74 7 8 3 14.32 4.09 7 8 -4 8.21 3.28 7 8 4 9.17 3.97 7 8 5 6.37 2.41 7 8 6 4.92 3.43 7 8 7 87.87 10.42 7 8 8 6.80 3.00 0 0 0 0.00 0.00 TITL YMR-0826-2 in Pbca REM Pbca (#61 in standard setting) CELL 1.54184 6.317803 19.384705 27.915224 90.0000 90.0000 90.0000 ZERR 7.00 0.000239 0.000817 0.001147 0.0000 0.0000 0.0000 LATT 1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O Co UNIT 140.00 140.00 21.00 14.00 7.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 59219 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.46112(13) 0.21195(4) 0.35542(3) 0.0282(3) Uani 1 1 d . . . . . O5 O 0.1508(5) 0.24331(18) 0.34948(12) 0.0334(8) Uani 1 1 d . . . . . H2 H 0.0647 0.2091 0.3548 0.050 Uiso 1 1 d R U . . . H1 H 0.1260 0.2590 0.3208 0.050 Uiso 1 1 d R U . . . O2 O 0.6518(5) 0.30487(18) 0.23420(11) 0.0340(8) Uani 1 1 d . . . . . O1 O 0.5531(6) 0.22503(17) 0.28723(12) 0.0339(8) Uani 1 1 d . . . . . O3 O -0.0088(6) 0.3126(2) 0.57249(12) 0.0386(9) Uani 1 1 d . . . . . O4 O 0.2869(6) 0.31490(19) 0.61323(12) 0.0411(9) Uani 1 1 d . . . . . N1 N 0.5789(6) 0.3215(2) 0.35845(13) 0.0286(9) Uani 1 1 d . . . . . N2 N 1.1173(7) 0.6065(2) 0.33906(16) 0.0370(10) Uani 1 1 d . . . . . C1 C 0.6679(7) 0.3345(2) 0.31551(16) 0.0255(10) Uani 1 1 d . . . . . C6 C 0.5095(8) 0.3553(3) 0.44102(17) 0.0308(11) Uani 1 1 d . . . . . C9 C 0.3019(8) 0.3333(2) 0.52811(16) 0.0294(11) Uani 1 1 d . . . . . C17 C 0.6200(8) 0.2842(2) 0.27596(17) 0.0291(11) Uani 1 1 d . . . . . C5 C 0.6203(8) 0.3660(3) 0.39482(17) 0.0317(11) Uani 1 1 d . . . . . C3 C 0.8585(8) 0.4323(3) 0.34527(17) 0.0327(11) Uani 1 1 d . . . . . C18 C 0.1889(8) 0.3195(2) 0.57394(18) 0.0317(11) Uani 1 1 d . . . . . C12 C 1.0171(8) 0.4870(3) 0.33653(18) 0.0328(12) Uani 1 1 d . . . . . C11 C 0.3012(9) 0.3337(3) 0.44166(17) 0.0362(12) Uani 1 1 d . . . . . H11A H 0.2297 0.3268 0.4129 0.043 Uiso 1 1 calc R U . . . C2 C 0.8055(8) 0.3885(2) 0.30759(17) 0.0299(11) Uani 1 1 d . . . . . H2A H 0.8626 0.3956 0.2773 0.036 Uiso 1 1 calc R U . . . C4 C 0.7596(8) 0.4212(2) 0.38887(18) 0.0352(12) Uani 1 1 d . . . . . H4A H 0.7862 0.4508 0.4144 0.042 Uiso 1 1 calc R U . . . C10 C 0.1979(9) 0.3223(3) 0.48458(18) 0.0373(12) Uani 1 1 d . . . . . H10A H 0.0582 0.3072 0.4845 0.045 Uiso 1 1 calc R U . . . C7 C 0.6139(9) 0.3675(3) 0.48451(17) 0.0380(12) Uani 1 1 d . . . . . H7A H 0.7527 0.3835 0.4846 0.046 Uiso 1 1 calc R U . . . C13 C 0.9828(8) 0.5551(3) 0.34939(18) 0.0344(12) Uani 1 1 d . . . . . H13A H 0.8598 0.5657 0.3661 0.041 Uiso 1 1 calc R U . . . C8 C 0.5088(8) 0.3555(3) 0.52750(18) 0.0349(12) Uani 1 1 d . . . . . H8A H 0.5795 0.3627 0.5563 0.042 Uiso 1 1 calc R U . . . C16 C 1.2021(9) 0.4718(3) 0.3123(2) 0.0465(15) Uani 1 1 d . . . . . H16A H 1.2325 0.4267 0.3033 0.056 Uiso 1 1 calc R U . . . C14 C 1.2904(9) 0.5903(3) 0.3147(2) 0.0511(16) Uani 1 1 d . . . . . H14A H 1.3825 0.6255 0.3060 0.061 Uiso 1 1 calc R U . . . C15 C 1.3398(10) 0.5241(3) 0.3019(3) 0.0588(19) Uani 1 1 d . . . . . H15A H 1.4663 0.5147 0.2861 0.071 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.0343(4) 0.0295(5) 0.0209(4) 0.0024(3) -0.0041(3) 0.0000(3) O5 0.0337(19) 0.041(2) 0.0259(17) 0.0065(15) -0.0007(15) -0.0012(16) O2 0.042(2) 0.044(2) 0.0166(16) 0.0006(15) 0.0014(15) 0.0050(16) O1 0.044(2) 0.0348(19) 0.0233(18) -0.0048(15) 0.0026(16) -0.0012(16) O3 0.039(2) 0.052(2) 0.0247(19) 0.0038(17) 0.0075(16) -0.0064(17) O4 0.047(2) 0.054(2) 0.0230(18) 0.0042(17) 0.0041(17) 0.0049(19) N1 0.035(2) 0.031(2) 0.020(2) -0.0001(16) 0.0007(17) 0.0028(18) N2 0.043(3) 0.029(2) 0.038(2) 0.000(2) 0.010(2) -0.001(2) C1 0.027(3) 0.033(2) 0.017(2) -0.0005(19) 0.0080(19) 0.002(2) C6 0.042(3) 0.029(3) 0.021(2) -0.004(2) 0.008(2) -0.003(2) C9 0.035(3) 0.033(3) 0.020(2) 0.000(2) 0.004(2) 0.005(2) C17 0.032(2) 0.032(3) 0.023(2) -0.003(2) -0.003(2) 0.001(2) C5 0.043(3) 0.034(3) 0.018(2) -0.002(2) 0.007(2) -0.002(2) C3 0.043(3) 0.030(3) 0.025(2) 0.001(2) 0.009(2) 0.003(2) C18 0.040(3) 0.030(3) 0.026(2) 0.000(2) 0.009(2) 0.004(2) C12 0.044(3) 0.029(3) 0.025(2) -0.001(2) 0.005(2) -0.002(2) C11 0.044(3) 0.045(3) 0.020(2) -0.006(2) 0.002(2) -0.003(3) C2 0.036(3) 0.032(2) 0.022(2) 0.001(2) 0.006(2) 0.004(2) C4 0.050(3) 0.032(3) 0.024(2) -0.005(2) 0.009(2) -0.006(2) C10 0.042(3) 0.043(3) 0.027(3) -0.004(2) 0.002(2) 0.003(2) C7 0.048(3) 0.047(3) 0.019(2) -0.002(2) 0.006(2) -0.008(3) C13 0.041(3) 0.033(3) 0.029(3) -0.003(2) 0.014(2) 0.000(2) C8 0.039(3) 0.045(3) 0.020(2) -0.002(2) 0.005(2) -0.004(2) C16 0.052(4) 0.034(3) 0.054(4) -0.008(3) 0.015(3) -0.002(3) C14 0.045(3) 0.036(3) 0.072(4) -0.009(3) 0.019(3) -0.011(3) C15 0.045(4) 0.049(4) 0.082(5) -0.017(3) 0.031(4) -0.002(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Co1 O5 99.33(14) . . ? O1 Co1 O3 157.20(15) . 4_556 ? O5 Co1 O3 103.46(14) . 4_556 ? O1 Co1 N2 89.16(16) . 8_755 ? O5 Co1 N2 92.53(16) . 8_755 ? O3 Co1 N2 90.52(16) 4_556 8_755 ? O1 Co1 N1 79.67(14) . . ? O5 Co1 N1 92.25(14) . . ? O3 Co1 N1 98.60(15) 4_556 . ? N2 Co1 N1 168.43(16) 8_755 . ? O1 Co1 O4 97.50(14) . 4_556 ? O5 Co1 O4 161.98(13) . 4_556 ? O3 Co1 O4 59.79(13) 4_556 4_556 ? N2 Co1 O4 94.13(15) 8_755 4_556 ? N1 Co1 O4 84.44(14) . 4_556 ? O1 Co1 C18 127.48(16) . 4_556 ? O5 Co1 C18 132.77(16) . 4_556 ? O3 Co1 C18 29.85(15) 4_556 4_556 ? N2 Co1 C18 93.92(16) 8_755 4_556 ? N1 Co1 C18 90.56(15) . 4_556 ? O4 Co1 C18 29.98(14) 4_556 4_556 ? Co1 O5 H2 110.9 . . ? Co1 O5 H1 110.4 . . ? H2 O5 H1 108.1 . . ? C17 O1 Co1 116.7(3) . . ? C18 O3 Co1 94.8(3) . 4_456 ? C18 O4 Co1 84.7(3) . 4_456 ? C1 N1 C5 117.8(4) . . ? C1 N1 Co1 106.3(3) . . ? C5 N1 Co1 133.7(3) . . ? C14 N2 C13 117.1(4) . . ? C14 N2 Co1 121.7(4) . 8_765 ? C13 N2 Co1 121.0(3) . 8_765 ? N1 C1 C2 123.2(4) . . ? N1 C1 C17 116.6(4) . . ? C2 C1 C17 120.1(4) . . ? C11 C6 C7 119.2(5) . . ? C11 C6 C5 120.2(5) . . ? C7 C6 C5 120.5(4) . . ? C8 C9 C10 118.9(5) . . ? C8 C9 C18 121.5(5) . . ? C10 C9 C18 119.6(5) . . ? O2 C17 O1 125.4(4) . . ? O2 C17 C1 116.4(4) . . ? O1 C17 C1 118.3(4) . . ? N1 C5 C4 121.3(4) . . ? N1 C5 C6 118.1(4) . . ? C4 C5 C6 120.6(4) . . ? C4 C3 C2 117.5(5) . . ? C4 C3 C12 124.1(5) . . ? C2 C3 C12 118.4(4) . . ? O3 C18 O4 120.5(5) . . ? O3 C18 C9 117.9(5) . . ? O4 C18 C9 121.6(5) . . ? O3 C18 Co1 55.3(3) . 4_456 ? O4 C18 Co1 65.3(3) . 4_456 ? C9 C18 Co1 172.3(4) . 4_456 ? C16 C12 C13 117.6(5) . . ? C16 C12 C3 120.0(5) . . ? C13 C12 C3 122.4(5) . . ? C6 C11 C10 120.6(5) . . ? C6 C11 H11A 119.7 . . ? C10 C11 H11A 119.7 . . ? C1 C2 C3 119.6(4) . . ? C1 C2 H2A 120.2 . . ? C3 C2 H2A 120.2 . . ? C3 C4 C5 120.5(5) . . ? C3 C4 H4A 119.7 . . ? C5 C4 H4A 119.7 . . ? C11 C10 C9 120.5(5) . . ? C11 C10 H10A 119.7 . . ? C9 C10 H10A 119.7 . . ? C8 C7 C6 119.6(5) . . ? C8 C7 H7A 120.2 . . ? C6 C7 H7A 120.2 . . ? N2 C13 C12 123.6(5) . . ? N2 C13 H13A 118.2 . . ? C12 C13 H13A 118.2 . . ? C9 C8 C7 121.1(5) . . ? C9 C8 H8A 119.5 . . ? C7 C8 H8A 119.5 . . ? C15 C16 C12 118.9(5) . . ? C15 C16 H16A 120.5 . . ? C12 C16 H16A 120.5 . . ? N2 C14 C15 123.1(5) . . ? N2 C14 H14A 118.5 . . ? C15 C14 H14A 118.5 . . ? C16 C15 C14 119.6(5) . . ? C16 C15 H15A 120.2 . . ? C14 C15 H15A 120.2 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 O1 2.006(3) . ? Co1 O5 2.059(3) . ? Co1 O3 2.077(4) 4_556 ? Co1 N2 2.151(4) 8_755 ? Co1 N1 2.252(4) . ? Co1 O4 2.296(4) 4_556 ? Co1 C18 2.516(5) 4_556 ? O5 H2 0.8714 . ? O5 H1 0.8704 . ? O2 C17 1.249(6) . ? O1 C17 1.261(6) . ? O3 C18 1.257(6) . ? O3 Co1 2.077(4) 4_456 ? O4 C18 1.263(6) . ? O4 Co1 2.296(4) 4_456 ? N1 C1 1.348(6) . ? N1 C5 1.358(6) . ? N2 C14 1.326(7) . ? N2 C13 1.342(6) . ? N2 Co1 2.151(4) 8_765 ? C1 C2 1.377(6) . ? C1 C17 1.505(6) . ? C6 C11 1.381(7) . ? C6 C7 1.402(7) . ? C6 C5 1.482(6) . ? C9 C8 1.376(7) . ? C9 C10 1.398(7) . ? C9 C18 1.490(6) . ? C5 C4 1.396(7) . ? C3 C4 1.385(6) . ? C3 C2 1.393(7) . ? C3 C12 1.480(7) . ? C18 Co1 2.516(5) 4_456 ? C12 C16 1.382(7) . ? C12 C13 1.384(7) . ? C11 C10 1.382(7) . ? C11 H11A 0.9300 . ? C2 H2A 0.9300 . ? C4 H4A 0.9300 . ? C10 H10A 0.9300 . ? C7 C8 1.391(7) . ? C7 H7A 0.9300 . ? C13 H13A 0.9300 . ? C8 H8A 0.9300 . ? C16 C15 1.367(8) . ? C16 H16A 0.9300 . ? C14 C15 1.369(8) . ? C14 H14A 0.9300 . ? C15 H15A 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 N1 C1 C2 3.3(7) . . . . ? Co1 N1 C1 C2 -162.2(4) . . . . ? C5 N1 C1 C17 179.7(4) . . . . ? Co1 N1 C1 C17 14.3(5) . . . . ? Co1 O1 C17 O2 -168.0(4) . . . . ? Co1 O1 C17 C1 12.5(6) . . . . ? N1 C1 C17 O2 161.2(4) . . . . ? C2 C1 C17 O2 -22.2(7) . . . . ? N1 C1 C17 O1 -19.2(7) . . . . ? C2 C1 C17 O1 157.4(4) . . . . ? C1 N1 C5 C4 -3.6(7) . . . . ? Co1 N1 C5 C4 156.9(4) . . . . ? C1 N1 C5 C6 175.1(4) . . . . ? Co1 N1 C5 C6 -24.4(7) . . . . ? C11 C6 C5 N1 -37.6(7) . . . . ? C7 C6 C5 N1 142.9(5) . . . . ? C11 C6 C5 C4 141.1(5) . . . . ? C7 C6 C5 C4 -38.4(7) . . . . ? Co1 O3 C18 O4 -4.5(5) 4_456 . . . ? Co1 O3 C18 C9 175.7(4) 4_456 . . . ? Co1 O4 C18 O3 4.1(5) 4_456 . . . ? Co1 O4 C18 C9 -176.1(4) 4_456 . . . ? C8 C9 C18 O3 166.3(5) . . . . ? C10 C9 C18 O3 -14.9(7) . . . . ? C8 C9 C18 O4 -13.5(7) . . . . ? C10 C9 C18 O4 165.3(5) . . . . ? C4 C3 C12 C16 134.0(6) . . . . ? C2 C3 C12 C16 -45.6(7) . . . . ? C4 C3 C12 C13 -49.7(8) . . . . ? C2 C3 C12 C13 130.7(5) . . . . ? C7 C6 C11 C10 -1.8(8) . . . . ? C5 C6 C11 C10 178.7(5) . . . . ? N1 C1 C2 C3 0.3(7) . . . . ? C17 C1 C2 C3 -176.1(4) . . . . ? C4 C3 C2 C1 -3.4(7) . . . . ? C12 C3 C2 C1 176.2(4) . . . . ? C2 C3 C4 C5 3.0(8) . . . . ? C12 C3 C4 C5 -176.5(5) . . . . ? N1 C5 C4 C3 0.5(8) . . . . ? C6 C5 C4 C3 -178.2(5) . . . . ? C6 C11 C10 C9 0.8(8) . . . . ? C8 C9 C10 C11 -0.1(8) . . . . ? C18 C9 C10 C11 -178.9(5) . . . . ? C11 C6 C7 C8 2.1(8) . . . . ? C5 C6 C7 C8 -178.4(5) . . . . ? C14 N2 C13 C12 0.7(8) . . . . ? Co1 N2 C13 C12 174.9(4) 8_765 . . . ? C16 C12 C13 N2 1.0(8) . . . . ? C3 C12 C13 N2 -175.4(5) . . . . ? C10 C9 C8 C7 0.4(8) . . . . ? C18 C9 C8 C7 179.2(5) . . . . ? C6 C7 C8 C9 -1.4(8) . . . . ? C13 C12 C16 C15 -0.8(9) . . . . ? C3 C12 C16 C15 175.7(6) . . . . ? C13 N2 C14 C15 -2.8(10) . . . . ? Co1 N2 C14 C15 -177.0(6) 8_765 . . . ? C12 C16 C15 C14 -1.1(11) . . . . ? N2 C14 C15 C16 3.1(11) . . . . ?