Crystallography Open Database

Information card for entry 7243749

Preview

Coordinates	7243749.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C13 H13 Mo4 N4 Ni O17
Calculated formula	C13 H13 Mo4 N4 Ni O17
Title of publication	A series of polyoxometalate-based hybrid complexes constructed by a tripodal ligand containing mixed N/O donors
Authors of publication	Ying, Jun; Jin, Liang; Yu, Hai-Yan; Tian, Ai-Xiang; Wang, Xiu-Li
Journal of publication	CrystEngComm
Year of publication	2021
Journal volume	23
Journal issue	44
Pages of publication	7846 - 7854
a	9.5458 ± 0.0005 Å
b	11.1569 ± 0.0006 Å
c	12.2071 ± 0.0007 Å
α	83.619 ± 0.001°
β	68.162 ± 0.001°
γ	74.084 ± 0.001°
Cell volume	1160.46 ± 0.11 Å³
Cell temperature	273.15 K
Ambient diffraction temperature	273.15 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.027
Residual factor for significantly intense reflections	0.0219
Weighted residual factors for significantly intense reflections	0.052
Weighted residual factors for all reflections included in the refinement	0.0541
Goodness-of-fit parameter for all reflections included in the refinement	1.032
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
271153 (current)	2021-12-07	cif/ Updating files of 7243745, 7243746, 7243747, 7243748, 7243749, 7243750 Original log message: Adding full bibliography for 7243745--7243750.cif.	7243749.cif
269981	2021-10-17	cif/ Adding structures of 7243745, 7243746, 7243747, 7243748, 7243749, 7243750 via cif-deposit CGI script.	7243749.cif