#------------------------------------------------------------------------------ #$Date: 2024-11-07 01:36:04 +0200 (Thu, 07 Nov 2024) $ #$Revision: 295805 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/24/95/7249552.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7249552 loop_ _publ_author_name 'Zhang, Jie' 'Ma, Yu-Xin' 'Wu, Ming' 'He, Qing' 'Chen, Shuya' 'Ju, Ping' 'He, Yuan-Chun' 'Lei, Xiaowu' _publ_section_title ; Zero-dimensional organic--inorganic hybrid zinc halide with stable broadband blue light emissions ; _journal_name_full CrystEngComm _journal_paper_doi 10.1039/D4CE00841C _journal_year 2024 _chemical_formula_moiety 'Cl4 Zn, C6 H16 N2' _chemical_formula_sum 'C6 H16 Cl4 N2 Zn' _chemical_formula_weight 323.38 _space_group_crystal_system monoclinic _space_group_IT_number 11 _space_group_name_Hall '-P 2yb' _space_group_name_H-M_alt 'P 1 21/m 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2024-06-30 _audit_creation_method ; Olex2 1.5 (compiled 2021.12.09 svn.r5202d8cf for OlexSys, GUI svn.r6439) ; _audit_update_record ; 2024-09-26 deposited with the CCDC. 2024-10-28 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 91.2107(10) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 6.46278(8) _cell_length_b 14.69136(16) _cell_length_c 7.14340(7) _cell_measurement_reflns_used 8789 _cell_measurement_temperature 293 _cell_measurement_theta_max 74.7030 _cell_measurement_theta_min 6.0160 _cell_volume 678.093(13) _computing_cell_refinement 'CrysAlisPro 1.171.39.34b (Rigaku OD, 2017)' _computing_data_collection 'CrysAlisPro 1.171.39.34b (Rigaku OD, 2017)' _computing_data_reduction 'CrysAlisPro 1.171.39.34b (Rigaku OD, 2017)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 293 _diffrn_detector 'CCD plate' _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 93.00 157.00 0.50 0.05 -- 109.88 125.00-150.00 128 2 \w 104.00 165.00 0.50 0.05 -- 109.88 101.00-163.00 122 3 \w 93.00 156.00 0.50 0.05 -- 109.88 125.00 -30.00 126 4 \w 147.00 176.00 0.50 0.05 -- 109.88 125.00 120.00 58 5 \w 100.00 131.00 0.50 0.05 -- 109.88 125.00 120.00 62 6 \w -110.00 -62.00 0.50 0.05 -- -90.25 -74.00 106.47 96 7 \w -158.00-132.00 0.50 0.05 -- -90.25 -74.00 106.47 52 8 \w -136.00 -61.00 0.50 0.05 -- -90.25 -77.00 30.00 150 9 \w -104.00 -64.00 0.50 0.05 -- -90.25 -71.00 62.86 80 10 \w -86.00 -61.00 0.50 0.05 -- -90.25 -77.00 46.12 50 11 \w -86.00 -60.00 0.50 0.05 -- -90.25 -80.00 90.41 52 12 \w -112.00 -63.00 0.50 0.05 -- -90.25 -77.00 -60.00 98 13 \w -87.00 -61.00 0.50 0.05 -- -90.25 -79.00 -12.18 52 14 \w -105.00 -68.00 0.50 0.05 -- -90.25 -50.00 -87.61 74 15 \w -164.00-112.00 0.50 0.05 -- -90.25 -50.00 -87.61 104 16 \w -164.00-121.00 0.50 0.05 -- -90.25 -78.00-124.14 86 17 \w -159.00-134.00 0.50 0.05 -- -90.25 -75.00-168.85 50 18 \w -158.00-133.00 0.50 0.05 -- -90.25 -75.00-105.16 50 19 \w -109.00 -61.00 0.50 0.05 -- -90.25 -78.00-124.14 96 20 \w -99.00 -61.00 0.50 0.05 -- -90.25 -77.00-150.00 76 21 \w -112.00 -62.00 0.50 0.05 -- -90.25 -77.00-180.00 100 22 \w -102.00 -62.00 0.50 0.05 -- -90.25 -75.00-105.16 80 23 \w -100.00 -61.00 0.50 0.05 -- -90.25 -77.00 -30.00 78 24 \w -86.00 -61.00 0.50 0.05 -- -90.25 -77.00 0.00 50 25 \w -88.00 -63.00 0.50 0.05 -- -90.25 -77.00 60.00 50 26 \w -102.00 -61.00 0.50 0.05 -- -90.25 -77.00 150.00 82 27 \w -158.00-115.00 0.50 0.05 -- -90.25 -77.00 150.00 86 28 \w -163.00-119.00 0.50 0.05 -- -90.25 -77.00 60.00 88 29 \w -139.00-114.00 0.50 0.05 -- -90.25 -77.00 46.12 50 30 \w -119.00 -94.00 0.50 0.05 -- -90.25 -77.00 0.00 50 31 \w -142.00-110.00 0.50 0.05 -- -90.25 -77.00 -30.00 64 32 \w -162.00-136.00 0.50 0.05 -- -90.25 -77.00-180.00 52 33 \w -98.00 -63.00 0.50 0.05 -- -90.25 -75.00-168.85 70 34 \w -93.00 -68.00 0.50 0.05 -- -90.25 -59.00-104.04 50 35 \w 8.00 36.00 0.50 0.05 -- 43.18 91.00-139.90 56 36 \w 86.00 177.00 0.50 0.05 -- 109.88 30.00-180.00 182 37 \w 91.00 168.00 0.50 0.05 -- 109.88 61.00 -30.00 154 38 \w 84.00 176.00 0.50 0.05 -- 109.88 77.00 -90.00 184 39 \w 92.00 163.00 0.50 0.05 -- 109.88 61.00 60.00 142 40 \w 83.00 114.00 0.50 0.05 -- 43.18 77.00 0.00 62 41 \w 18.00 49.00 0.50 0.05 -- 43.18 77.00 0.00 62 42 \w 14.00 55.00 0.50 0.05 -- 43.18 77.00 150.00 82 43 \w -84.00 -59.00 0.50 0.05 -- -90.25 101.00-163.00 50 44 \w -83.00 -3.00 0.50 0.05 -- -43.18 101.00-163.00 160 45 \w 22.00 92.00 0.50 0.05 -- 43.18 37.00-180.00 140 46 \w 87.00 112.00 0.50 0.05 -- 43.18 57.00-120.00 50 47 \w 23.00 76.00 0.50 0.05 -- 43.18 57.00-120.00 106 48 \w 21.00 82.00 0.50 0.05 -- 43.18 77.00 60.00 122 49 \w 92.00 117.00 0.50 0.05 -- 43.18 77.00 150.00 50 50 \w 34.00 131.00 0.50 0.05 -- 109.88 -45.00-150.00 194 51 \w -111.00 -81.00 0.50 0.05 -- -43.18 -45.00 169.60 60 52 \w -117.00 -87.00 0.50 0.05 -- -43.18 -57.00 60.00 60 53 \w -52.00 -17.00 0.50 0.05 -- -43.18 -77.00 -60.00 70 54 \w -114.00 -89.00 0.50 0.05 -- -43.18 -77.00 -60.00 50 55 \w -80.00 -17.00 0.50 0.05 -- -43.18 -77.00-120.00 126 56 \w -78.00 -39.00 0.50 0.05 -- -43.18 -57.00 0.00 78 57 \w -115.00 -90.00 0.50 0.05 -- -43.18 -57.00 0.00 50 58 \w -75.00 -50.00 0.50 0.05 -- -43.18 -57.00 60.00 50 59 \w -49.00 -24.00 0.50 0.05 -- -43.18 -45.00 169.60 50 60 \w 82.00 110.00 0.50 0.05 -- 109.88-101.00 92.00 56 61 \w 49.00 76.00 0.50 0.05 -- 109.88-101.00 92.00 54 62 \w 36.00 61.00 0.50 0.05 -- 109.88 -94.00 30.00 50 63 \w 65.00 98.00 0.50 0.05 -- 109.88 -94.00 30.00 66 64 \w 36.00 118.00 0.50 0.05 -- 109.88-125.00-150.00 164 65 \w 59.00 105.00 0.50 0.05 -- 109.88 -94.00 -90.00 92 66 \w 52.00 89.00 0.50 0.05 -- 109.88 -94.00 -60.00 74 67 \w 8.00 58.00 0.50 0.05 -- 43.18-101.00 92.00 100 68 \w 33.00 90.00 0.50 0.05 -- 43.18-125.00-180.00 114 69 \w -162.00-137.00 0.50 0.05 -- -90.25 -83.00 136.17 50 70 \w -145.00 -96.00 0.50 0.05 -- -90.25-101.00 92.00 98 71 \w -123.00 -59.00 0.50 0.05 -- -90.25 -83.00 136.17 128 72 \w -85.00 -60.00 0.50 0.05 -- -90.25 -83.00 175.84 50 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0614759000 _diffrn_orient_matrix_UB_12 0.0812314000 _diffrn_orient_matrix_UB_13 0.1233084000 _diffrn_orient_matrix_UB_21 0.0348192000 _diffrn_orient_matrix_UB_22 -0.0586041000 _diffrn_orient_matrix_UB_23 0.1767448000 _diffrn_orient_matrix_UB_31 0.2277044000 _diffrn_orient_matrix_UB_32 0.0309294000 _diffrn_orient_matrix_UB_33 0.0108879000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0612 _diffrn_reflns_av_unetI/netI 0.0233 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 12887 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 66.529 _diffrn_reflns_theta_max 66.529 _diffrn_reflns_theta_min 6.024 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 9.481 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.17298 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.34b (Rigaku Oxford Diffraction, 2017) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear whiteish colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier whiteish _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.584 _exptl_crystal_description block _exptl_crystal_F_000 328 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.19 _refine_diff_density_max 1.820 _refine_diff_density_min -1.140 _refine_diff_density_rms 0.233 _refine_ls_extinction_coef 0.019(3) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2018/3 (Sheldrick 2018)' _refine_ls_goodness_of_fit_ref 1.151 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 66 _refine_ls_number_reflns 1251 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.151 _refine_ls_R_factor_all 0.0805 _refine_ls_R_factor_gt 0.0791 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1495P)^2^+3.7846P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2406 _refine_ls_wR_factor_ref 0.2427 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1227 _reflns_number_total 1251 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ce00841c2.cif _cod_data_source_block '[DMPZ]ZnCl4' _cod_original_cell_volume 678.094(13) _cod_database_code 7249552 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.266 _shelx_estimated_absorpt_t_min 0.241 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H,H) groups, All N(H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C2-C3_$1 1.39 with sigma of 0.01 C3-C2_$1 1.39 with sigma of 0.01 3.a Ternary CH refined with riding coordinates: N1(H1) 3.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C2(H2A,H2B) 3.c Idealised Me refined as rotating group: C1(H1A,H1B,H1C) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL exp_5138.res created by SHELXL-2018/3 at 10:54:36 on 30-Jun-2024 CELL 1.54184 6.462784 14.691363 7.143401 90 91.2107 90 ZERR 2 0.000084 0.000157 0.000074 0 0.001 0 LATT 1 SYMM -X,0.5+Y,-Z SFAC C H Cl N Zn UNIT 12 32 8 4 2 EQIV $1 1-X,1-Y,-Z DFIX 1.39 0.01 C2 C3_$1 DFIX 1.39 0.01 C3 C2_$1 L.S. 30 PLAN 4 SIZE 0.19 0.2 0.21 TEMP 19.85 CONF MORE -1 BOND $H fmap 2 acta SHEL 9999 0.84 OMIT 0 2 1 REM REM REM WGHT 0.149500 3.784600 EXTI 0.018503 FVAR 8.58235 ZN1 5 0.184170 0.750000 0.246876 10.50000 0.05532 0.01541 = 0.03328 0.00000 0.00518 0.00000 CL1 3 0.094828 0.605448 0.392540 11.00000 0.03809 0.02551 = 0.02772 0.00098 -0.00169 0.00269 CL3 3 0.592754 0.750000 0.222820 10.50000 0.02460 0.02452 = 0.04389 0.00000 -0.00060 0.00000 CL2 3 0.136895 0.750000 -0.107664 10.50000 0.03838 0.04677 = 0.02820 0.00000 -0.00304 0.00000 N1 4 0.542432 0.579109 -0.119509 11.00000 0.08950 0.06231 = 0.07899 -0.00019 0.00115 0.00200 AFIX 13 H1 2 0.473145 0.626145 -0.046432 11.00000 -1.20000 AFIX 0 C3 1 0.700240 0.536280 0.004751 11.00000 0.08822 0.07709 = 0.09076 -0.00364 -0.01003 0.00004 AFIX 23 H3A 2 0.773831 0.490590 -0.065801 11.00000 -1.20000 H3B 2 0.799678 0.582263 0.044143 11.00000 -1.20000 AFIX 0 C2 1 0.381551 0.504757 -0.164373 11.00000 0.09448 0.08057 = 0.07662 -0.00840 -0.01264 0.00319 AFIX 23 H2A 2 0.269120 0.531311 -0.238036 11.00000 -1.20000 H2B 2 0.445514 0.458214 -0.240149 11.00000 -1.20000 AFIX 0 C1 1 0.630188 0.626157 -0.296361 11.00000 0.14106 0.12533 = 0.12725 0.01942 0.02818 -0.02163 AFIX 137 H1A 2 0.722228 0.674366 -0.258558 11.00000 -1.50000 H1B 2 0.518166 0.650784 -0.370810 11.00000 -1.50000 H1C 2 0.704260 0.582321 -0.368726 11.00000 -1.50000 AFIX 0 HKLF 4 REM REM wR2 = 0.2427, GooF = S = 1.151, Restrained GooF = 1.151 for all data REM R1 = 0.0791 for 1227 Fo > 4sig(Fo) and 0.0805 for all 1251 data REM 66 parameters refined using 2 restraints END WGHT 0.1493 3.7868 REM Highest difference peak 1.820, deepest hole -1.140, 1-sigma level 0.233 Q1 1 0.6201 0.7500 -0.4250 10.50000 0.05 0.65 Q2 1 0.0222 0.7500 0.2233 10.50000 0.05 0.54 Q3 1 -0.0065 0.7500 0.4763 10.50000 0.05 0.54 Q4 1 0.9937 0.7500 -0.4203 10.50000 0.05 0.51 ; _shelx_res_checksum 92737 _shelx_hkl_file ; 0 0 -1 4080.03 221.180 40 0 0 1 3623.99 186.851 49 0 0 1 4340.12 220.541 54 0 0 -2 214482. 4792.13 48 0 0 2 164759. 4717.11 47 0 0 2 224852. 4736.15 54 0 0 2 181833. 4718.65 55 0 0 -2 227124. 4796.17 40 0 0 3 590.875 140.119 54 0 0 -3 321.651 119.030 40 0 0 -3 348.005 128.731 48 0 0 3 435.448 144.774 47 0 0 3 455.867 140.755 55 0 0 4 4331.66 517.146 22 0 0 4 3124.05 447.196 55 0 0 -4 3820.77 456.367 40 0 0 -4 3934.96 695.967 25 0 0 4 3710.11 384.312 59 0 0 -4 2744.79 433.564 6 0 0 -4 2957.02 554.103 9 0 0 4 4268.83 490.802 15 0 0 4 3794.03 486.880 19 0 0 5 43836.4 1799.27 59 0 0 -5 54863.4 3203.84 25 0 0 5 44803.9 2207.03 19 0 0 -5 50843.3 2853.09 9 0 0 -5 43640.6 2140.92 48 0 0 -5 56410.6 3231.49 10 0 0 -5 44562.0 2061.29 56 0 0 5 50865.3 2171.13 15 0 0 -5 42837.9 2397.42 52 0 0 5 52757.4 2483.59 46 0 0 5 47081.3 2202.75 22 0 0 6 128588. 4485.74 15 0 0 6 140031. 4986.18 19 0 0 -6 143072. 5844.82 9 0 0 6 136095. 5160.37 46 0 0 6 132728. 4636.73 36 0 0 7 2458.28 686.251 2 0 0 -7 1679.10 620.050 70 0 0 7 732.320 262.338 1 0 0 7 1332.44 393.323 36 0 0 -7 893.989 350.616 39 0 0 7 1719.81 433.312 15 0 0 7 1779.76 531.905 19 0 0 -7 1320.93 545.979 9 0 0 8 42436.5 2098.65 15 0 0 8 56218.5 2741.29 2 0 0 -8 57148.9 2977.40 70 0 0 -8 46888.3 2384.09 39 0 -1 0 200.427 48.1299 56 0 1 0 188.707 53.1782 51 0 1 1 281167. 5952.76 59 0 1 1 246769. 5949.75 47 0 1 1 227163. 5980.34 49 0 -1 -1 297628. 5992.20 48 0 1 1 258608. 6031.10 55 0 1 -1 292464. 5974.05 40 0 -1 1 297303. 6005.97 55 0 1 2 163882. 3983.49 49 0 -1 2 164746. 4021.64 55 0 -1 2 183222. 4077.35 54 0 1 -2 188279. 4037.95 40 0 -1 -2 180463. 4041.64 48 0 1 -2 174367. 4136.63 48 0 1 -2 153869. 4147.03 58 0 1 2 170961. 3928.69 59 0 1 2 135095. 3971.74 47 0 1 -3 179360. 4539.30 48 0 -1 -3 183401. 4527.30 40 0 1 3 160538. 4447.92 55 0 1 3 172285. 4213.27 59 0 1 -3 196448. 4431.12 40 0 -1 -3 167007. 4380.13 48 0 1 -3 155994. 4627.70 58 0 1 3 162102. 4476.34 47 0 -1 3 185034. 4440.61 54 0 -1 3 161524. 4381.54 55 0 -1 -4 74685.9 2631.73 48 0 1 -4 89713.0 3651.28 25 0 -1 4 82771.6 2596.96 12 0 1 4 73682.1 2698.05 19 0 1 4 73038.6 2374.63 59 0 1 -4 78512.3 3279.50 9 0 -1 -4 83915.6 3464.99 10 0 -1 4 75949.2 2712.51 22 0 -1 4 86159.5 2626.94 54 0 1 -4 81941.5 2580.54 40 0 1 4 88213.5 2721.65 15 0 -1 -4 84876.3 2733.97 40 0 -1 4 76640.1 2663.64 55 0 -1 -4 79104.4 3367.37 25 0 1 -4 77616.0 2745.99 48 0 1 -4 72258.5 2858.05 6 0 -1 -5 97127.5 4330.19 10 0 -1 -5 73039.3 2859.80 56 0 -1 -5 74510.7 2841.32 40 0 -1 -5 92996.4 3974.91 8 0 1 5 72805.1 2982.18 19 0 -1 -5 72297.2 2887.85 48 0 -1 -5 85012.5 4048.09 25 0 1 -5 101741. 4206.55 10 0 -1 5 75124.8 3112.38 46 0 -1 5 65047.5 2439.86 59 0 1 -5 67564.6 2992.00 6 0 1 5 83253.4 3278.58 46 0 -1 -5 77784.5 3568.18 9 0 1 -5 74817.3 3350.06 52 0 1 5 63483.8 2416.14 59 0 -1 5 80032.3 2926.85 15 0 1 -5 85296.8 3881.61 9 0 -1 5 73341.3 2957.42 22 0 -1 5 71605.3 2951.40 19 0 1 -5 94630.0 4289.20 25 0 1 5 77910.3 2870.85 15 0 -1 6 87623.4 3871.80 46 0 1 6 85397.2 3383.64 15 0 1 6 85411.1 3486.97 36 0 1 -6 81869.5 4012.82 52 0 -1 -6 102931. 4966.54 10 0 1 -6 83934.8 3576.96 39 0 1 6 98189.3 4132.38 46 0 -1 6 79977.1 3315.72 15 0 -1 6 80132.4 3512.42 22 0 -1 6 83852.3 3399.84 36 0 -1 6 93367.6 3834.81 19 0 1 -6 105305. 4430.07 10 0 1 -6 98293.1 4653.29 9 0 1 6 92178.3 3796.77 19 0 -1 -6 84436.9 4223.18 9 0 -1 7 28135.4 2185.66 2 0 -1 7 29201.6 2076.12 19 0 1 7 29748.8 2349.05 2 0 1 -7 27740.3 2292.90 9 0 1 7 20689.2 1510.93 15 0 1 -7 22236.8 1718.85 39 0 1 7 22814.8 1653.40 36 0 -1 7 21594.0 1564.15 15 0 -1 -7 23288.8 1735.81 39 0 -1 7 22637.7 1563.50 1 0 1 7 25716.6 1958.47 19 0 -1 -7 30063.8 2480.01 70 0 -1 -7 26790.4 2244.93 9 0 1 -8 1388.24 324.835 7 0 1 8 1734.04 479.603 2 0 1 -8 1516.57 408.701 39 0 -1 8-21.6498 1.26264 1 0 -1 8 1757.55 397.136 15 0 -1 -8 1555.63 417.538 39 0 -1 8 1798.38 473.856 2 0 -1 -8 2017.79 545.817 70 0 1 8 1859.24 397.982 15 0 2 0 240208. 5286.31 45 0 -2 0 224245. 5335.17 56 0 -2 -1 30575.1 954.336 52 0 2 1 30069.0 855.291 47 0 2 -1 32193.6 797.711 42 0 -2 -2 290016. 6210.41 48 0 2 2 253347. 6250.90 49 0 2 2 271748. 6123.57 59 0 2 -2 264934. 6394.83 58 0 -2 2 278944. 6214.13 55 0 2 2 249302. 6175.30 47 0 2 3 42577.6 1424.31 59 0 -2 -3 46726.2 1668.21 56 0 2 -3 43462.0 1803.12 58 0 2 3 42171.0 1621.79 47 0 2 -3 43815.5 1684.30 48 0 -2 3 47485.3 1647.18 54 0 -2 -3 42215.8 1519.60 48 0 -2 3 40573.1 1530.52 55 0 -2 4 87350.5 2794.93 12 0 2 4 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3 -6 -1 36635.2 2019.44 30 3 -6 -1 39883.8 2122.63 29 3 -6 -1 36494.2 1907.19 28 3 6 -1 31125.6 1713.74 27 -3 -6 1 44249.3 2100.76 53 -3 6 1 38179.7 1849.80 33 -3 6 1 39451.8 1917.10 51 -3 6 1 40817.2 2064.63 45 3 6 -1 34827.5 1632.60 44 3 -6 -1 36197.9 1685.79 44 -3 6 1 39085.0 1885.47 21 -3 6 0 144487. 4294.41 33 3 6 0 131570. 4343.62 32 3 -6 0 135160. 4305.37 31 -3 6 0 141931. 4450.70 72 3 -6 0 139918. 4381.59 28 -3 -6 0 133719. 4431.33 53 -3 6 0 133375. 4277.57 51 -3 6 0 150900. 4602.19 45 3 6 0 132828. 4020.47 44 3 -6 0 142903. 4170.19 44 -3 6 0 142950. 4386.26 21 -3 6 -1 247.199 158.916 21 -3 -6 -1 449.240 220.870 41 3 6 1 1065.33 297.245 17 3 6 1 1128.19 361.757 16 3 -6 1 313.754 194.867 31 -3 6 -1 307.363 183.419 72 3 6 1 343.717 163.990 32 -3 -6 -1 177.648 119.344 56 -3 6 -1 232.188 189.722 26 -3 6 -1 36.0964 125.211 45 -3 6 -1 272.623 181.892 42 3 6 2 134782. 4881.18 16 -3 -6 -2 145157. 4392.97 56 3 -6 2 140815. 4485.49 67 3 6 2 129959. 4288.52 67 3 -6 2 125821. 4581.22 31 -3 6 -2 136091. 4849.62 71 -3 6 -2 140429. 4723.80 26 -3 6 -2 134475. 4691.37 45 -3 6 -2 132226. 4299.34 42 -3 -6 -2 149478. 4729.34 41 3 -6 3 45927.4 2357.51 67 3 6 3 44683.4 2590.49 18 3 6 3 49996.4 2746.02 16 3 6 3 40474.7 2360.97 65 3 6 3 43929.6 2258.97 67 -3 6 -3 46006.5 2429.28 71 -3 -6 -3 46971.2 2341.96 56 -3 6 -3 45645.0 2210.77 26 3 -6 3 43516.8 2570.02 1 -3 6 -3 43708.3 2412.02 45 -3 6 -3 41924.4 2056.57 42 -3 -6 -4 1004.47 319.464 9 3 -6 4 935.776 373.995 38 3 6 4 237.097 243.172 18 3 6 4 410.479 301.504 16 3 6 4 190.224 180.717 67 3 -6 4 297.157 197.536 15 3 -6 4 428.714 255.851 31 -3 6 -4 252.104 206.079 71 3 6 4 215.248 176.008 2 3 6 4 1830.83 530.042 62 3 -6 4 532.697 304.322 1 -3 6 -4 458.695 284.890 58 -3 -6 -4 956.525 363.179 56 3 -6 4 267.287 196.435 68 -3 -6 -4 380.319 227.004 25 -3 6 -4 1432.31 435.600 6 -3 -6 -4 510.405 278.613 48 -3 6 -4 324.184 227.108 11 -3 -6 -5 26793.6 1767.75 9 -3 6 -5 27369.6 1791.19 39 3 6 5 32731.1 2313.64 18 3 6 5 28263.1 2041.99 36 -3 6 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203.592 39 -3 7 6 87.6882 166.520 20 -3 -7 6 175.902 180.386 19 3 -7 -6 264.435 204.966 37 -3 7 6 237.976 184.475 36 -3 -7 6 434.008 258.927 34 3 -7 -6 269.748 220.383 8 -3 7 6 197.984 184.168 33 3 7 -6 361.683 242.759 7 3 -7 -6 569.916 311.002 29 3 7 -6 250.497 219.660 69 3 -7 -6 471.778 263.656 28 3 7 -6 249.234 223.056 50 3 7 -5 36794.0 2160.82 39 -3 7 5 29382.3 2036.15 20 -3 7 5 29727.5 1840.69 19 3 -7 -5 33356.3 2205.39 37 -3 7 5 28655.4 1999.68 36 3 -7 -5 38787.0 2549.44 8 3 7 -5 30336.5 2330.26 69 -3 -7 5 31863.4 2253.26 34 -3 7 5 29543.1 2059.10 33 3 7 -5 40372.5 2447.40 7 3 -7 -5 38885.6 2743.45 3 -3 -7 5 29229.0 1900.22 14 3 -7 -5 38774.7 2514.55 29 3 -7 -5 35937.3 2302.91 28 -3 -7 5 30650.2 2254.88 22 -3 7 5 30129.0 1983.42 21 3 7 -4 143585. 4957.19 39 -3 7 4 124495. 4747.42 20 -3 7 4 129046. 4381.74 19 3 -7 -4 117328. 4787.34 37 -3 7 4 127435. 4684.58 72 -3 7 4 122990. 4752.00 33 -3 7 4 136259. 4982.49 36 3 7 -4 154278. 5277.63 7 3 -7 -4 136195. 5380.46 8 3 -7 -4 146628. 5794.14 3 -3 -7 4 126454. 4672.76 14 3 -7 -4 130611. 4942.84 28 -3 -7 4 126643. 5156.26 55 -3 -7 4 134653. 4798.56 12 3 7 -4 124347. 4671.02 50 -3 7 4 135640. 4691.68 49 -3 7 4 135489. 4787.40 47 -3 7 4 125164. 4693.38 21 3 7 -3 5983.35 847.098 39 -3 7 3 6466.56 849.159 20 3 -7 -3 7012.10 958.597 37 -3 7 3 7070.69 964.029 36 3 -7 -3 7906.09 1080.72 8 3 7 -3 5894.88 983.583 69 3 7 -3 7355.96 925.086 7 -3 7 3 6448.92 855.101 72 3 -7 -3 7900.11 1100.07 3 3 -7 -3 6706.71 922.313 30 -3 -7 3 6080.94 842.468 14 3 -7 -3 7641.11 1002.12 29 3 -7 -3 7552.81 950.199 28 3 -7 -3 6672.68 976.508 57 -3 -7 3 6269.48 978.684 55 3 7 -3 7008.56 888.453 50 -3 7 3 6320.80 849.627 47 -3 7 3 6287.15 854.343 33 -3 7 3 6820.96 880.145 21 -3 7 2 6862.42 804.840 20 -3 7 2 5885.00 808.110 72 -3 7 2 6544.25 889.934 36 3 7 -2 5635.36 855.751 69 3 -7 -2 4825.88 633.499 68 -3 7 2 7244.09 864.182 33 3 -7 -2 6304.01 908.774 30 3 -7 -2 6527.04 873.946 29 3 -7 -2 6401.59 813.828 28 3 7 -2 5266.32 799.424 27 -3 -7 2 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5 4244.51 687.992 38 -3 -7 -5 4352.84 798.594 8 3 7 5 4799.49 863.344 18 3 7 5 3669.44 699.912 36 -3 7 -5 5115.19 738.475 71 3 7 5 4555.19 805.117 16 3 -7 5 3578.71 673.271 15 3 7 5 4040.84 788.107 62 -3 7 -5 3874.56 678.237 6 3 -7 5 5236.34 858.048 1 -3 -7 -5 5464.87 816.588 25 -3 7 -5 4456.81 713.018 11 -3 -7 -5 4246.52 781.435 10 -3 7 -6 11940.4 951.216 9 -3 7 -6 13023.1 1109.33 39 3 7 6 13616.8 1295.81 18 3 7 6 13953.3 1180.76 16 3 -7 6 14905.8 1301.83 1 3 7 6 12314.2 1146.36 62 3 -7 6 13036.8 1140.26 15 -3 7 -6 11852.2 1103.55 6 -3 -7 -6 12823.3 1264.65 10 -3 7 -7 3736.45 444.313 39 3 -7 7 4585.38 561.864 1 -3 -8 7 590.261 165.371 38 -3 8 7 445.747 172.858 36 3 -8 -7 496.753 206.867 3 3 8 -7 489.191 182.650 50 3 8 -6 20577.5 1308.40 39 -3 -8 6 22613.8 1503.59 19 -3 8 6 22329.7 1460.46 33 3 -8 -6 22618.4 1633.49 37 -3 8 6 20995.5 1514.32 36 3 -8 -6 23353.1 1622.01 8 3 8 -6 20613.3 1603.51 69 3 -8 -6 27159.2 1886.98 3 3 8 -6 22953.9 1499.47 7 3 -8 -6 25293.8 1722.69 29 3 -8 -6 23902.6 1605.27 28 -3 -8 6 23375.0 1684.50 34 3 8 -6 21380.8 1504.02 50 -3 -8 6 22759.4 1655.55 22 3 8 -5 4970.60 747.932 39 -3 8 5 3353.92 679.841 20 3 -8 -5 3825.37 762.893 37 -3 8 5 4704.45 792.344 36 3 -8 -5 4906.45 854.870 8 3 8 -5 3928.92 806.740 69 -3 -8 5 5894.60 967.646 34 -3 8 5 4342.12 761.494 33 3 -8 -5 4265.98 851.029 3 3 8 -5 5246.36 793.132 7 -3 -8 5 3506.29 664.447 14 3 -8 -5 4916.38 791.530 28 -3 8 5 3639.26 649.670 21 3 8 -4 2262.20 536.078 39 -3 8 4 1922.39 503.151 20 -3 8 4 2457.38 612.085 36 3 8 -4 3638.54 823.543 69 3 -8 -4 2580.34 642.531 8 -3 8 4 2228.55 586.623 33 3 8 -4 2992.45 607.994 7 3 -8 -4 1687.19 492.538 29 -3 -8 4 1456.29 449.567 14 3 -8 -4 2529.95 574.963 28 3 8 -4 2125.15 604.364 27 3 -8 -4 2073.21 606.918 3 3 8 -4 2192.46 534.734 50 -3 -8 4 2499.88 563.455 12 -3 8 4 2336.94 553.652 72 -3 8 4 2861.24 641.368 21 3 8 -3 35066.5 2089.87 39 -3 8 3 34784.2 2119.28 20 3 -8 -3 30385.7 2213.38 37 -3 8 3 31333.9 2073.64 72 -3 8 3 37377.1 2270.88 33 -3 8 3 40345.4 2414.31 36 3 8 -3 30219.5 2288.73 69 3 8 -3 38086.7 1987.96 7 3 -8 -3 34211.1 2215.36 3 3 -8 -3 28624.2 2102.77 30 -3 -8 3 30207.3 2070.63 14 3 -8 -3 34373.1 2164.69 29 3 -8 -3 31756.1 1978.70 28 -3 -8 3 35604.0 2410.36 55 3 8 -3 23643.8 2003.96 27 -3 -8 3 35592.5 2112.16 12 -3 8 3 34194.2 2198.50 51 3 8 -3 27797.1 1900.27 50 -3 8 3 33032.3 1969.47 47 3 -8 -3 35353.2 2283.78 8 -3 8 3 32598.7 2121.59 21 3 8 -2 20763.0 1537.06 39 -3 8 2 18020.5 1392.48 20 3 -8 -2 13897.3 1274.78 38 3 -8 -2 15773.6 1512.64 37 -3 8 2 22215.1 1658.55 36 3 -8 -2 19957.4 1624.70 8 -3 8 2 18793.3 1520.19 33 3 8 -2 16881.9 1543.43 69 3 -8 -2 18256.3 1625.83 30 3 -8 -2 21277.8 1558.71 29 3 -8 -2 18474.4 1374.56 28 -3 -8 2 20772.7 1743.67 55 3 8 -2 14107.8 1395.25 27 -3 -8 2 20747.7 1508.85 53 -3 8 2 16492.3 1450.90 72 -3 8 2 18266.2 1494.43 51 3 8 -2 16043.0 1354.95 50 -3 8 2 19749.2 1540.13 45 -3 8 2 17986.4 1512.71 21 -3 8 1 30730.2 1717.41 20 3 -8 -1 29530.1 1909.63 38 -3 8 1 34348.2 2098.93 72 3 -8 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18712.5 1377.02 41 3 8 2 117554. 4366.27 66 3 -8 2 114989. 4725.58 38 3 8 2 100076. 4042.46 17 3 8 2 120019. 4386.62 16 3 8 2 137236. 4479.01 65 3 -8 2 118282. 4832.74 31 -3 -8 -2 116569. 4115.76 56 -3 8 -2 123990. 4300.56 26 3 8 2 93800.8 4325.80 5 -3 8 -2 108730. 3983.97 42 -3 -8 -2 136332. 4547.86 41 3 -8 3 29334.7 2145.55 38 -3 8 -3 30465.4 1908.07 71 3 8 3 33621.1 2124.44 16 3 8 3 32524.3 2077.05 65 3 -8 3 34718.3 2004.22 1 -3 8 -3 32515.8 1939.08 6 -3 -8 -3 28365.9 1942.09 56 -3 8 -3 30699.9 1802.51 26 -3 -8 -3 29658.4 2120.48 48 -3 8 -3 29218.9 1991.00 45 -3 -8 -3 26635.3 1770.47 10 -3 8 -3 28299.4 1725.25 42 3 -8 4 4002.60 765.733 38 -3 -8 -4 3314.17 689.264 8 -3 8 -4 4110.96 666.149 71 3 8 4 3826.19 744.750 16 3 -8 4 4085.03 806.703 31 3 8 4 4913.05 935.335 62 -3 8 -4 3333.97 621.612 6 3 -8 4 4564.99 745.119 1 -3 8 -4 3210.00 589.095 11 -3 -8 -4 5160.67 816.103 10 -3 8 -5 7845.31 903.895 39 3 -8 5 8234.05 951.025 38 -3 -8 -5 8133.15 1074.57 8 -3 8 -5 8311.98 927.440 71 3 8 5 9364.98 1063.21 16 3 8 5 9448.66 1203.32 62 3 -8 5 8964.10 1012.20 1 -3 8 -5 8423.74 907.185 11 -3 -8 -5 7941.50 1040.52 10 -3 8 -6 8828.50 842.703 39 -3 -8 -6 8745.79 985.205 8 -3 8 -6 8557.03 794.056 71 3 8 6 8088.91 831.093 16 3 -8 6 9835.40 933.423 1 3 8 6 9130.27 967.596 62 -3 8 -6 9399.65 901.569 6 -3 -8 -6 9747.60 954.069 24 3 -8 7 287.996 136.783 1 3 9 -7 15.6479 68.5855 50 3 9 -6 5789.83 624.125 39 -3 -9 6 6772.10 705.673 19 3 -9 -6 7023.29 848.631 37 -3 9 6 6894.48 811.218 36 3 -9 -6 6753.90 774.124 8 3 9 -6 7213.07 850.222 69 -3 -9 6 7784.06 887.970 34 3 9 -6 6719.33 689.169 7 3 -9 -6 8574.67 916.560 3 -3 9 6 5784.61 632.200 16 3 -9 -6 6562.20 752.035 28 3 9 -6 8095.51 829.668 50 -3 -9 6 7674.50 847.914 22 -3 9 5 144.930 148.589 21 3 9 -5 554.917 249.908 39 3 -9 -5 108.254 167.787 37 -3 9 5-48.2248 129.481 36 -3 -9 5 105.412 200.090 34 3 -9 -5 380.189 244.272 8 -3 9 5 131.368 179.565 33 3 9 -5 207.438 177.721 7 3 -9 -5 182.330 199.817 29 -3 -9 5 88.3610 118.629 14 3 -9 -5 578.057 271.481 28 3 -9 -5 296.099 253.658 3 -3 -9 5 80.7442 139.933 12 -3 -9 5 814.346 331.990 22 3 9 -4 16615.7 1276.71 7 3 9 -4 17917.7 1442.10 39 -3 9 4 13943.6 1374.76 20 -3 9 4 13600.6 1278.85 72 3 -9 -4 17020.6 1543.77 8 3 9 -4 16150.9 1616.68 69 -3 9 4 14412.6 1410.96 33 -3 9 4 18261.4 1642.43 36 3 -9 -4 15951.7 1479.63 3 3 -9 -4 16609.6 1491.47 29 -3 -9 4 14220.7 1407.26 14 3 -9 -4 15816.6 1367.87 28 3 9 -4 11349.8 1361.70 27 -3 -9 4 17755.0 1477.46 12 3 9 -4 14877.3 1366.91 50 -3 9 4 14090.9 1374.77 21 3 9 -3 49038.1 2488.09 39 -3 9 3 40308.4 2404.00 20 3 -9 -3 43127.3 2797.38 37 -3 9 3 50078.2 2758.12 36 3 9 -3 48557.9 2847.70 69 -3 9 3 41347.6 2531.33 33 3 -9 -3 46110.3 2440.44 3 3 -9 -3 45635.4 2681.49 30 -3 -9 3 43359.9 2557.81 14 3 -9 -3 49721.3 2575.61 29 3 -9 -3 46587.4 2367.47 28 -3 -9 3 42241.3 2635.44 55 3 9 -3 37122.0 2554.72 27 -3 -9 3 49572.4 2525.00 12 -3 9 3 37259.7 2160.29 26 -3 9 3 40470.5 2511.43 51 3 9 -3 41586.3 2379.97 50 -3 9 3 40837.9 2149.76 47 -3 9 3 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27567.9 1811.76 71 3 9 0 33622.9 1972.08 66 3 9 0 21290.5 1836.28 32 3 9 0 30337.6 1725.07 65 3 -9 0 25424.8 1960.21 31 -3 9 0 30185.8 1940.77 72 -3 -9 0 31582.8 1945.26 53 -3 9 0 29279.2 1935.44 26 -3 9 0 29696.5 1701.42 51 3 9 0 31926.8 1766.08 50 -3 9 0 29215.9 1840.83 21 -3 -9 0 31953.7 1910.89 41 -3 -9 -1 360.105 224.273 41 -3 9 -1 880.601 281.970 21 3 -9 1 708.756 348.802 38 3 9 1 850.489 386.771 17 3 9 1 946.214 346.782 66 3 9 1 606.941 288.038 65 3 -9 1 954.003 403.147 31 3 9 1 976.953 374.160 62 -3 -9 -1 951.846 344.563 53 -3 9 -1 1109.22 374.408 26 3 9 1 573.511 242.780 50 3 -9 2 48112.0 2765.53 38 -3 -9 -2 42055.1 2206.06 8 3 9 2 38452.5 2346.71 17 3 9 2 44958.4 2411.02 16 3 -9 2 47231.8 2924.10 31 -3 -9 -2 43862.4 2329.44 56 -3 9 -2 49572.5 2421.81 26 3 9 2 43187.5 2678.32 5 -3 9 -2 43490.0 2394.15 45 -3 -9 -2 53584.9 2602.57 41 3 9 2 49994.8 2436.15 65 3 9 2 50395.5 2583.02 66 3 -9 3 36323.0 2320.32 38 -3 -9 -3 32796.5 2091.45 8 -3 9 -3 35345.4 2054.33 71 3 9 3 37752.0 2231.49 16 -3 9 -3 33652.3 1958.71 6 -3 -9 -3 37117.0 2281.56 56 -3 9 -3 33145.1 1896.44 26 -3 -9 -3 34732.3 2358.03 48 -3 9 -3 35658.7 1887.86 11 -3 9 -3 32926.0 2112.59 45 3 -9 4 5523.58 862.092 38 -3 -9 -4 4564.44 796.342 8 -3 9 -4 3829.13 642.401 71 3 9 4 5908.51 846.426 16 3 -9 4 3935.15 798.498 31 3 -9 4 5130.43 721.210 1 -3 9 -4 5969.61 777.926 6 -3 9 -4 4236.20 622.134 11 -3 -9 -4 5123.08 795.833 10 3 -9 5 42293.1 2194.30 38 -3 -9 -5 45811.9 2535.16 8 -3 9 -5 44787.0 2184.40 71 3 9 5 45281.7 2298.42 16 3 -9 5 47212.6 2229.78 1 -3 9 -5 42806.6 2151.01 6 -3 9 -5 41068.3 1988.37 11 3 9 5 48859.8 2710.49 62 -3 -9 -5 47850.7 2512.32 10 -3 -9 -6 2546.24 492.720 8 -3 9 -6 2274.12 376.821 71 3 9 6 3082.52 455.296 16 3 -9 6 2737.20 437.484 1 3 9 6 2734.36 506.827 62 -3 -9 -6 2884.80 479.101 24 -3 -10 6 164.140 120.535 38 3 -10 -6 204.491 125.279 8 3 -10 -6 30.4931 125.039 37 -3 10 6 168.716 150.962 36 3 10 -6-28.1748 106.968 69 3 -10 -6 94.5224 103.596 28 3 -10 -6 235.660 151.838 3 -3 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3683.45 612.176 50 -3 -11 -1 3816.78 634.664 24 -3 11 -1 3514.16 553.738 21 3 -11 2 17702.1 1502.54 38 3 11 2 17085.1 1467.56 17 -3 11 -2 15303.1 1256.94 71 3 11 2 17139.2 1346.22 66 3 11 2 15935.7 1233.11 65 3 -11 2 19021.1 1719.78 31 3 11 2 18412.8 1568.81 62 -3 11 -2 15413.2 1160.98 6 -3 11 -2 14268.5 1203.37 26 3 11 2 15945.2 1295.88 50 -3 -11 -2 16185.9 1417.12 24 3 -11 3 31532.7 1998.56 38 -3 -11 -3 29831.2 1847.25 8 3 11 3 31081.8 1892.68 16 -3 11 -3 29408.4 1669.05 6 3 11 3 26893.3 1683.88 50 -3 -11 -3 32144.2 2097.87 24 3 -11 4 74.0200 140.516 38 -3 11 -4 327.865 227.236 71 3 -11 4 276.800 202.226 31 -3 -11 -4 522.746 249.269 8 3 11 4 145.054 158.973 16 3 11 4 94.3518 163.497 62 -3 11 -4 88.4521 129.265 6 -3 -11 -4 45.2002 156.652 24 3 -11 5 63590.8 2456.03 38 -3 -11 -5 72047.2 2821.73 8 -3 11 -5 64670.7 2482.74 71 3 11 5 63977.7 2510.44 16 3 11 5 76639.9 2959.79 62 -3 -11 -5 75574.1 2808.42 13 -3 11 -5 61256.2 2394.57 6 -3 -11 -5 75256.0 2913.69 24 3 11 6 2178.84 337.224 62 3 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1056.05 2 4 -3 7 14864.8 1049.67 2 -4 -3 -7 15295.2 1234.11 10 -4 4 7 19374.9 1335.42 20 -4 -4 7 19492.1 1394.67 19 4 -4 -7 19824.9 1331.05 3 4 4 -7 18840.7 1246.20 50 -4 4 6 2518.32 566.980 20 -4 4 6 1708.40 417.517 19 4 4 -6 2222.39 546.959 70 4 -4 -6 2106.17 540.328 70 -4 4 6 2894.67 573.933 33 4 -4 -6 2118.47 649.002 28 4 -4 -6 2293.93 600.220 3 4 4 -6 2020.05 496.959 50 -4 -4 6 2066.19 499.742 22 -4 4 6 2168.34 467.436 21 -4 4 5 1023.84 371.980 20 -4 4 5 733.708 284.904 19 4 -4 -5 985.793 412.245 70 4 -4 -5 678.595 298.060 37 4 4 -5 1692.18 554.389 70 -4 -4 5 1377.87 354.611 34 -4 4 5 693.676 308.485 33 4 4 -5 531.500 390.719 7 4 -4 -5 776.671 451.541 29 4 4 -5 1309.83 350.599 3 4 -4 -5 2225.97 722.961 28 4 -4 -5 820.343 396.848 3 -4 -4 5 701.058 316.289 22 -4 4 4 2100.26 486.837 20 -4 4 4 1897.94 420.499 19 4 -4 -4 1899.39 476.303 37 4 4 -4 1985.97 576.590 70 -4 -4 4 2658.44 488.948 34 4 -4 -4 1967.08 494.235 8 4 4 -4 2001.07 618.205 7 4 -4 -4 1829.68 612.354 29 4 -4 -4 2003.26 567.190 70 -4 -4 4 1651.41 414.699 59 4 4 -4 1926.54 422.786 3 4 -4 -4 2895.68 814.755 28 -4 -4 4 2286.57 550.637 55 4 -4 -4 2064.32 632.394 3 -4 -4 4 2338.84 462.328 47 -4 4 4 2617.28 600.740 47 4 4 -4 2560.86 659.574 44 4 -4 -4 2035.35 555.881 44 -4 4 3 36322.8 1907.48 20 4 -4 -3 33318.4 1944.36 37 4 4 -3 31587.7 1787.66 3 -4 4 3 38125.8 2316.22 35 4 -4 -3 33033.1 2119.82 8 4 -4 -3 31590.4 2319.68 3 4 -4 -3 33329.7 1857.59 64 4 -4 -3 33538.2 2475.05 29 -4 -4 3 28908.9 1674.48 59 -4 -4 3 32242.6 1992.52 55 -4 -4 3 33304.2 1672.84 47 4 4 -3 35863.8 2364.90 44 4 -4 -3 34917.9 2214.50 44 -4 4 2 88520.9 3065.37 20 4 -4 -2 81458.5 3208.10 38 4 4 -2 79498.9 3084.55 3 -4 -4 2 81658.7 3203.54 35 -4 4 2 86246.2 3659.85 35 4 -4 -2 73477.4 2803.12 68 4 -4 -2 80059.8 3642.57 3 4 4 -2 89538.2 3018.93 64 4 -4 -2 82336.6 3220.82 64 -4 -4 2 76071.5 3207.85 55 -4 4 2 76571.5 3083.73 45 4 4 -2 93700.9 3767.66 44 4 -4 -2 87564.5 3525.69 44 -4 -4 1 142592. 4391.66 35 4 -4 -1 133730. 4247.67 68 4 -4 -1 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50 -4 -6 6 24151.0 1719.58 19 4 -6 -6 26683.7 1709.82 37 -4 6 6 23817.1 1609.27 33 4 6 -6 23721.5 1598.73 50 -4 -6 6 24098.5 1704.05 22 -4 6 6 21106.1 1420.06 21 -4 6 5 18974.7 1527.89 20 -4 6 5 15323.1 1202.69 19 -4 6 5 15514.5 1345.74 72 -4 -6 5 14765.7 1305.46 34 -4 6 5 17445.3 1490.68 33 4 -6 -5 18503.7 1878.39 3 4 -6 -5 21595.5 1930.20 29 4 6 -5 17120.7 1465.06 50 -4 -6 5 16775.5 1551.40 22 -4 6 5 14719.9 1343.15 21 -4 6 4 224.140 208.499 20 4 -6 -4 154.470 195.551 37 -4 6 4 489.638 253.000 36 -4 -6 4 671.287 302.356 34 4 -6 -4 390.647 302.747 8 4 -6 -4 156.858 160.905 64 4 6 -4 910.277 409.958 7 4 -6 -4 412.469 353.375 29 4 -6 -4 419.541 293.770 28 4 -6 -4 72.5876 275.603 3 4 6 -4 570.056 285.180 50 -4 6 4 180.452 221.163 21 -4 6 3 31866.6 1922.16 20 4 -6 -3 32362.8 2030.29 38 4 -6 -3 31236.0 2049.74 37 -4 6 3 30123.8 1944.69 36 4 -6 -3 31333.8 2376.06 8 4 6 -3 26592.7 2079.86 69 4 -6 -3 30672.2 2319.80 3 4 -6 -3 29259.8 1953.45 64 4 -6 -3 34405.4 2291.55 28 -4 -6 3 26624.3 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3 24601.8 1796.45 68 4 6 3 25472.8 1817.34 67 4 6 3 27610.3 1970.11 65 4 -6 3 28062.6 1960.80 31 4 6 3 24558.2 1685.42 61 -4 -6 -3 29740.1 1879.90 56 -4 6 -3 30717.1 1772.95 26 4 6 3 22470.4 1516.96 2 4 -6 3 23508.6 1598.78 2 -4 -6 -3 29211.9 1954.62 48 -4 6 -3 29888.0 2093.06 45 -4 6 -3 29028.6 1843.39 42 4 -6 4 9852.96 1073.79 38 4 6 4 12080.9 1237.81 4 -4 6 -4 13466.6 1212.18 71 4 6 4 11081.4 1250.00 16 4 -6 4 14630.9 1529.41 1 4 6 4 13572.5 1434.49 62 4 -6 4 12918.6 1226.81 61 4 6 4 11366.8 1144.87 61 -4 6 -4 12262.5 1223.25 6 -4 -6 -4 13277.7 1222.07 25 4 6 4 9604.40 999.069 2 4 -6 4 11122.3 1075.56 2 -4 6 -5 1326.27 358.326 71 4 6 5 1277.00 336.502 2 4 -6 5 1029.31 309.772 2 4 6 5 1093.35 408.313 62 4 -6 5 969.148 327.747 61 4 6 5 1002.02 326.322 61 4 -6 5 1529.36 486.892 1 -4 -6 -5 1620.51 437.455 25 -4 6 -5 1416.19 414.084 6 -4 6 -5 1365.95 390.998 11 -4 -6 -5 1092.93 397.363 10 -4 6 -6 913.454 266.580 9 4 -6 6 1470.48 399.126 1 4 6 6-20.3404 44.5797 2 4 -6 6 767.020 222.690 2 4 6 6 659.526 250.171 63 4 -6 6 654.182 225.276 61 4 6 6-23.8759 37.0030 61 -4 6 -6 740.310 295.085 6 -4 6 -6 917.019 298.064 11 -4 -6 -6 655.235 280.148 10 -4 -6 -7 615.783 208.607 39 4 -6 7 744.769 202.485 1 4 -7 -7 2128.46 343.236 3 4 7 -7 1750.98 285.362 50 -4 7 6 27436.6 1717.93 20 -4 -7 6 29692.9 1801.00 19 4 -7 -6 32457.7 1891.46 37 4 -7 -6 38619.2 2189.62 3 -4 7 6 27820.8 1683.95 33 4 -7 -6 33796.0 1915.42 28 4 7 -6 33302.3 1825.76 50 -4 -7 6 29721.7 1845.23 22 -4 7 5 23957.6 1719.72 20 -4 7 5 19689.8 1449.16 36 -4 7 5 22232.6 1594.82 72 -4 -7 5 21450.6 1624.92 34 -4 7 5 23407.8 1758.02 33 4 -7 -5 31441.4 2248.94 3 4 -7 -5 26359.5 1882.56 28 4 7 -5 24355.8 1734.67 50 -4 -7 5 26840.3 1956.40 22 -4 7 5 23098.7 1680.99 21 -4 7 4 66866.2 3168.32 20 4 -7 -4 69606.3 3474.00 37 -4 7 4 69626.3 3240.95 72 -4 7 4 62913.5 3043.23 36 4 -7 -4 66696.6 3644.02 8 -4 -7 4 65224.9 3190.56 34 4 7 -4 57946.0 3431.95 69 4 -7 -4 81431.6 3890.02 3 4 -7 -4 67121.0 3089.08 64 4 -7 -4 75517.4 3712.00 29 4 -7 -4 77432.0 3534.40 28 4 7 -4 74963.5 3343.32 50 -4 7 4 73133.4 3315.17 21 -4 7 3 1988.97 499.829 20 4 -7 -3 1699.03 475.230 38 4 -7 -3 1560.11 489.651 37 -4 7 3 1679.32 494.405 72 -4 7 3 1627.75 478.596 36 4 7 -3 1317.94 487.495 69 -4 7 3 2352.64 574.469 33 4 -7 -3 2112.04 614.637 8 4 -7 -3 1622.18 496.927 64 4 -7 -3 1825.40 516.408 28 -4 -7 3 1808.15 547.653 55 4 -7 -3 1497.06 497.992 3 -4 7 3 1769.64 511.279 51 4 7 -3 1107.71 393.268 50 -4 7 3 1358.57 444.848 47 -4 7 2 2597.16 534.140 20 4 -7 -2 2361.75 561.346 38 4 -7 -2 1696.74 487.433 37 -4 7 2 2704.36 614.751 36 4 7 -2 2406.93 595.658 69 -4 7 2 2509.70 582.970 33 4 -7 -2 2896.71 712.315 8 4 7 -2 2853.68 561.961 64 4 -7 -2 2830.35 603.812 28 -4 -7 2 2233.84 615.694 55 4 -7 -2 2339.89 554.731 3 -4 -7 2 2878.58 586.528 53 -4 7 2 2586.12 583.122 51 4 7 -2 2419.53 523.766 50 -4 7 2 2244.21 542.404 45 -4 7 2 2288.02 550.269 21 4 -7 -1 1237.12 413.693 38 4 7 -1 956.916 366.902 4 -4 7 1 1315.08 431.292 72 -4 7 1 1210.99 340.005 35 4 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93614.1 3808.22 45 -4 7 -2 87727.4 3564.49 42 -4 -7 -2 103072. 3833.47 41 4 -7 3 1576.69 519.825 38 4 -7 3 3950.50 738.770 1 -4 7 -3 3158.60 627.236 71 4 -7 3 3107.33 686.493 31 4 7 3 2450.25 658.051 62 -4 -7 -3 3442.32 645.333 56 -4 7 -3 3282.68 559.019 26 4 -7 4 186.610 177.256 38 4 7 4 310.394 253.627 4 -4 7 -4 767.363 303.269 71 4 -7 4 556.241 293.302 1 4 7 4 123.935 235.345 62 -4 7 -4 504.765 276.659 6 -4 7 -4 706.727 302.264 11 -4 -7 -4 323.166 247.948 10 4 7 5 14578.1 1175.35 4 -4 -7 -5 12424.3 1250.28 8 -4 7 -5 13288.0 1088.57 71 4 7 5 13881.3 1382.71 62 -4 7 -5 13602.7 1166.27 6 -4 7 -5 15668.2 1229.61 11 -4 -7 -5 14427.1 1326.99 10 4 -7 6 11044.0 952.477 1 -4 -7 -6 9821.10 947.234 8 4 7 6 8703.82 829.436 63 -4 7 -6 9068.47 827.842 6 -4 -7 -6 9248.29 920.063 10 -4 -8 6 8756.50 837.719 19 4 -8 -6 8363.07 887.145 37 4 -8 -6 9981.38 957.149 3 -4 8 6 8092.96 785.809 33 4 -8 -6 8758.49 838.525 28 4 8 -6 10168.9 894.080 50 -4 -8 6 8423.53 861.000 22 -4 8 5 13150.5 1222.46 20 -4 8 5 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328.529 269.550 68 4 8 1 812.968 360.940 66 4 8 1 523.010 270.317 65 4 -8 1 447.072 274.009 31 4 -8 1 586.704 309.396 64 4 8 1 448.900 301.359 62 -4 -8 -1 663.467 316.483 53 -4 8 -1 580.616 309.283 26 -4 8 -1 220.845 193.817 45 4 -8 2 4061.34 827.096 38 -4 8 -2 4016.42 738.415 71 4 -8 2 3735.70 811.733 68 4 8 2 6097.13 917.909 66 4 8 2 5332.82 818.576 65 4 -8 2 3717.78 784.634 31 4 8 2 4114.93 844.934 62 -4 8 -2 5023.85 750.866 26 -4 8 -2 4292.62 746.020 45 -4 8 -2 4291.02 722.806 42 -4 -8 -2 5360.61 808.305 41 4 -8 3 10308.2 1264.50 38 4 -8 3 10786.7 1106.20 1 -4 8 -3 11224.5 1130.95 71 4 -8 3 11338.4 1349.39 31 4 8 3 10455.9 1369.40 62 -4 8 -3 11313.6 1125.66 6 -4 8 -3 11191.0 1023.77 26 4 -8 4 9618.44 1106.85 38 4 8 4 11570.3 1288.37 4 -4 -8 -4 11585.3 1218.63 8 4 -8 4 13026.0 1189.56 1 -4 8 -4 12235.0 1090.04 71 -4 8 -4 10380.8 1010.33 11 -4 -8 -4 11556.9 1155.08 10 4 8 5 2701.98 503.558 4 4 -8 5 2974.61 521.888 1 -4 8 -5 2273.72 423.547 71 -4 -8 -5 2315.32 521.693 8 4 8 5 2121.63 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714.682 279.739 4 5 4 4 337.817 236.719 2 5 -4 4 386.255 269.965 2 5 4 4 578.625 260.770 1 5 4 4 500.112 263.819 63 5 -4 4 378.609 265.251 61 5 4 4 392.262 274.801 61 -5 4 -4 334.019 276.868 6 -5 -4 -5 47351.3 2162.53 9 5 4 5 45216.3 2275.90 63 5 -4 5 52135.3 2565.95 61 5 4 5 50819.9 2624.04 61 -5 4 -5 50125.0 2387.65 6 -5 -4 -5 46950.6 2323.44 25 5 4 5 45034.1 2338.69 2 5 -4 5 47117.3 2346.91 2 -5 4 -5 53090.2 2593.48 11 -5 -4 -5 44094.9 2353.36 10 5 4 6 2661.65 385.319 63 5 -4 6 2751.18 437.357 61 5 4 6 2793.40 457.901 61 -5 4 -6 2674.00 456.065 11 -5 -4 -6 2440.27 450.395 10 5 -4 6 3863.20 619.550 1 -5 4 -6 3019.68 477.399 9 -5 -5 6 478.635 216.439 20 -5 5 6 1175.67 318.633 20 -5 -5 6 1125.72 316.896 19 -5 5 6 889.285 295.959 33 5 -5 -6 1763.12 429.775 28 5 5 -6 1068.91 294.781 50 -5 5 5 4568.75 708.908 20 -5 -5 5 3421.97 658.847 19 -5 5 5 4463.86 697.464 72 5 -5 -5 4682.98 885.353 3 5 -5 -5 5910.96 972.883 28 5 5 -5 5548.70 764.021 50 -5 -5 5 4003.60 624.974 22 -5 5 5 4226.88 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87778.0 3712.17 68 -5 5 1 120169. 4068.92 33 5 5 -1 104706. 4105.90 66 5 5 -1 117866. 4643.34 65 5 5 -1 109288. 3911.06 64 5 5 -1 98861.2 3827.64 60 5 -5 -1 108260. 4104.35 60 -5 -5 1 88306.7 3861.47 55 5 5 -1 110602. 4342.61 44 5 -5 -1 108528. 4282.06 44 5 5 -1 108572. 4215.73 43 5 -5 -1 110987. 4213.27 43 5 5 0 31462.3 2197.92 4 5 -5 0 27033.2 1920.81 38 5 -5 0 28817.3 1907.64 68 5 5 0 32278.0 2028.42 66 5 5 0 33576.6 2182.94 65 5 -5 0 29844.7 1982.32 64 5 5 0 27309.6 1932.43 63 5 5 0 28235.4 1754.30 60 5 -5 0 28682.9 1829.42 60 -5 -5 0 28891.6 1927.55 55 -5 5 0 27906.2 1891.25 45 5 5 0 31862.7 2148.43 44 5 -5 0 33970.8 2213.37 44 -5 5 0 34638.5 1980.29 21 5 5 0 31153.0 2067.03 43 5 -5 0 33375.2 2130.77 43 -5 5 0 31411.7 2116.16 42 -5 -5 0 37956.5 2198.64 41 5 5 1 30563.3 2153.87 4 5 -5 1 26363.4 1899.99 38 5 5 1 30481.7 1980.36 66 5 5 1 31538.3 2059.17 65 5 5 1 29388.9 1836.75 64 5 -5 1 28410.1 1843.99 64 5 5 1 26411.2 1974.99 63 -5 -5 -1 31886.4 1884.13 48 5 -5 1 34050.8 2235.81 1 -5 5 -1 26973.6 1881.22 45 -5 5 -1 34204.8 2177.99 42 5 5 2 9022.45 1127.03 4 5 -5 2 7033.64 936.996 38 5 5 2 6824.72 933.747 65 5 5 2 8532.00 1003.93 64 5 -5 2 8639.69 933.323 64 5 5 2 7823.71 1059.28 63 5 -5 2 8566.23 1086.28 61 5 5 2 8100.47 1016.73 61 -5 5 -2 9585.50 1090.42 26 5 -5 2 9501.84 1275.03 1 5 -5 3 4535.99 921.435 1 5 5 3 5025.74 817.595 4 5 -5 3 4332.61 675.822 38 -5 5 -3 5174.24 821.750 71 5 -5 3 4571.86 791.471 61 5 5 3 4449.45 766.058 61 5 -5 4 1072.81 449.201 1 5 5 4 1917.62 455.980 4 -5 5 -4 1269.88 359.777 71 5 5 4 1299.33 422.982 63 5 -5 4 1733.93 463.203 61 5 5 4 1210.96 394.375 61 -5 -5 -4 1708.55 433.460 25 -5 5 -4 1699.37 459.004 6 5 5 5 17192.9 1327.47 63 5 -5 5 17690.4 1278.70 61 5 5 5 16781.6 1262.36 61 -5 5 -5 18427.3 1314.71 6 -5 -5 -5 16242.9 1225.98 25 -5 -5 -5 15029.4 1272.31 10 5 5 6 5558.69 546.638 63 5 -5 6 5194.40 484.386 61 5 -6 -6 9020.17 903.410 3 5 6 -6 7284.58 658.228 50 -5 6 5 5735.74 772.423 20 -5 -6 5 3928.68 696.206 19 -5 6 5 4601.21 698.173 72 5 -6 -5 5574.07 895.575 3 5 6 -5 5554.26 731.794 50 -5 -6 5 4244.97 666.364 22 -5 6 5 4493.84 716.131 21 -5 6 4 76537.5 3218.11 20 5 -6 -4 71349.8 3399.94 37 -5 6 4 73060.2 3259.62 72 5 -6 -4 86387.6 3947.56 3 -5 6 4 78952.3 3396.47 33 5 -6 -4 70844.7 2971.81 64 5 6 -4 80930.5 3259.25 50 -5 -6 4 65186.2 3106.39 22 -5 6 4 77133.4 3358.07 21 5 -6 -4 69839.7 2945.25 43 -5 6 3 9152.66 1008.07 20 5 -6 -3 8320.32 1100.05 37 5 -6 -3 11515.4 1344.39 3 -5 6 3 8761.12 1050.21 33 5 6 -3 6467.91 946.043 66 5 6 -3 8377.87 918.325 64 5 -6 -3 9599.06 1105.04 64 5 -6 -3 10342.9 1269.22 28 5 6 -3 10562.5 1083.07 50 -5 6 3 9626.79 1107.43 21 5 6 -3 9399.32 1019.75 43 5 -6 -3 8757.35 985.551 43 5 -6 -2 24052.8 1876.92 38 5 -6 -2 19477.6 1638.68 37 5 -6 -2 28181.5 2008.30 3 -5 6 2 28541.7 1916.93 33 5 6 -2 23100.4 1860.58 66 5 6 -2 32213.1 2176.60 65 5 6 -2 27945.4 1756.74 64 5 -6 -2 23239.9 1864.60 64 -5 6 2 27707.4 1944.26 21 5 6 -2 25726.2 1728.21 43 5 -6 -2 24972.8 1705.19 43 5 6 -1 2037.18 572.729 4 5 -6 -1 1892.40 525.727 38 -5 6 1 2688.61 576.930 35 5 -6 -1 2047.31 501.126 68 -5 6 1 2651.08 561.752 33 5 6 -1 2592.09 620.998 66 5 6 -1 2572.57 634.565 65 5 6 -1 3049.48 589.906 64 5 6 -1 2312.44 486.444 60 5 -6 -1 2906.72 580.227 60 -5 -6 1 1756.57 526.845 55 -5 6 1 3255.31 648.732 21 5 6 -1 2492.87 529.468 43 5 -6 -1 2217.58 514.431 43 5 -6 0 2375.55 601.372 38 5 6 0 2036.90 583.981 4 -5 6 0 2537.55 597.554 72 5 -6 0 2025.22 522.857 68 5 6 0 1909.03 532.729 66 5 6 0 1763.55 510.833 65 5 6 0 2921.92 587.893 64 5 -6 0 2237.70 572.435 64 5 6 0 2589.60 573.020 63 5 6 0 2003.52 430.451 60 5 -6 0 2378.55 495.536 60 -5 6 0 2768.60 580.031 45 -5 6 0 3218.22 625.404 21 -5 6 0 2323.38 580.781 42 -5 -6 0 3608.60 670.587 41 5 -6 1 5953.10 946.788 38 -5 6 -1 6902.88 904.289 72 5 6 1 5162.03 845.908 66 5 6 1 6996.47 980.969 65 5 6 1 6622.58 913.107 64 5 -6 1 6915.61 926.390 64 5 6 1 6246.26 972.338 63 -5 -6 -1 6729.01 960.668 53 -5 6 -1 7426.50 1039.31 26 -5 -6 -1 6579.64 897.758 48 -5 6 -1 7069.56 921.991 45 5 6 2 54728.2 3114.81 4 5 -6 2 46969.7 2785.53 38 -5 6 -2 61125.7 3144.38 71 5 6 2 60011.0 3013.41 65 5 6 2 59462.7 2944.59 64 5 -6 2 55638.6 2604.79 64 5 -6 2 60679.0 2847.63 61 5 6 2 55095.9 2678.15 61 -5 6 -2 67470.0 2982.95 26 5 -6 2 65282.6 3200.78 1 5 6 3 37569.6 2370.51 4 5 -6 3 29117.6 1972.21 38 -5 6 -3 40994.0 2253.89 71 5 -6 3 34899.1 2074.12 61 5 6 3 35003.9 2041.53 61 -5 6 -3 40055.9 2293.25 6 5 -6 3 47255.3 2687.54 1 5 6 4 37573.4 2157.94 4 -5 6 -4 38419.6 1965.85 71 5 6 4 39080.3 2376.98 63 5 -6 4 37856.7 2022.56 61 5 6 4 36350.6 1987.05 61 -5 6 -4 39497.0 2127.19 6 -5 6 -4 42202.3 2233.01 11 -5 -6 -4 38526.5 2133.83 10 5 -6 5 2599.20 526.470 1 -5 -6 -5 2262.00 475.383 8 5 6 5 2065.71 465.615 63 5 -6 5 1597.44 332.010 61 -5 6 -5 1980.66 410.718 6 -5 6 -5 2450.05 452.727 11 -5 -6 -5 1900.24 428.318 10 5 6 6 220.016 127.179 63 5 -6 6 314.401 152.444 1 5 7 -6 6541.51 579.242 65 5 7 -6 5787.47 500.218 50 -5 7 5 6033.58 760.658 20 -5 -7 5 5985.03 812.621 19 5 -7 -5 5957.24 837.216 37 -5 7 5 5577.78 710.531 72 5 -7 -5 6881.45 867.659 3 5 -7 -5 5853.35 780.197 28 5 7 -5 6846.67 737.558 50 -5 -7 5 5688.70 753.160 22 -5 7 5 5632.17 754.132 21 -5 7 4 564.729 272.796 20 5 -7 -4 918.944 393.124 37 -5 7 4 595.056 309.474 72 -5 7 4 790.161 338.100 33 5 7 -4 340.702 209.123 66 5 -7 -4 899.067 320.810 64 5 -7 -4 417.642 259.619 28 5 -7 -4 778.259 345.674 3 5 7 -4 819.219 294.536 50 -5 -7 4 737.416 327.560 22 -5 7 4 744.327 338.393 21 -5 7 3 92216.2 3619.03 20 5 -7 -3 78161.8 3828.62 37 -5 7 3 87447.4 3839.14 72 5 -7 -3 102041. 3984.51 3 -5 7 3 94823.3 3934.76 33 5 7 -3 75777.0 3695.15 66 5 7 -3 80413.9 3352.71 64 5 -7 -3 85908.3 3891.28 64 5 -7 -3 93476.3 3930.47 28 5 7 -3 97036.7 3574.41 50 -5 7 3 98276.4 3995.34 21 5 -7 -2 20860.4 1774.55 38 5 -7 -2 17382.2 1603.16 37 -5 7 2 23826.2 1867.92 72 5 -7 -2 22741.6 1639.01 3 -5 7 2 24344.2 1819.00 33 5 7 -2 22031.5 1852.65 66 5 7 -2 25654.2 1853.40 65 5 7 -2 21251.9 1585.59 64 5 -7 -2 21238.3 1871.53 64 -5 7 2 23965.6 1843.26 21 5 7 -1 32217.7 2338.49 4 5 -7 -1 29869.4 2244.23 38 -5 7 1 39166.0 2449.42 72 -5 7 1 31127.2 1998.00 36 -5 7 1 39701.4 2258.54 33 5 7 -1 36497.6 2418.18 66 5 7 -1 38134.9 2307.78 65 5 7 -1 35428.1 2138.41 64 -5 7 1 37920.6 2354.34 21 5 7 0 10374.8 1367.15 4 -5 7 0 12330.2 1314.72 72 5 7 0 12363.0 1369.17 66 5 7 0 13213.8 1314.79 65 5 7 0 12839.5 1254.31 64 5 -7 0 11954.8 1358.24 64 -5 7 0 10549.8 1160.97 21 5 -7 1 1186.33 494.340 38 -5 7 -1 2211.73 519.912 72 5 7 1 1257.25 449.306 66 5 7 1 1481.52 453.803 65 5 7 1 1539.52 478.381 64 5 -7 1 1213.90 415.904 64 5 7 1 1271.94 454.530 63 -5 7 -1 1866.90 515.500 26 5 7 2 59481.1 3393.17 4 5 -7 2 57528.0 3228.65 38 -5 7 -2 68812.5 3241.93 71 5 7 2 70454.4 3292.22 65 -5 7 -2 72243.7 3048.46 26 5 7 3 32220.1 2266.33 4 5 -7 3 28213.1 1998.49 38 -5 7 -3 33451.3 1957.11 71 -5 7 -3 34828.0 2033.81 6 5 -7 3 38502.6 2154.35 1 5 7 4 86.8888 178.135 4 -5 7 -4 206.634 158.479 71 -5 7 -4 204.684 183.142 6 -5 7 -4 34.0157 105.451 11 5 -7 4 192.169 197.546 1 -5 -7 -4 107.478 146.904 10 -5 -7 -5 22719.1 1454.13 8 5 7 5 23651.4 1532.74 63 -5 7 -5 24142.7 1343.15 6 -5 7 -5 22071.9 1276.17 11 -5 -7 -5 22419.7 1384.96 10 5 -7 5 26836.7 1456.30 1 -5 7 -5 22148.5 1218.41 9 5 -8 -5 2592.03 521.736 37 5 -8 -5 2862.00 473.123 3 5 -8 -5 2673.88 470.361 28 5 8 -5 3099.14 448.081 50 -5 8 5 2767.16 469.008 21 -5 8 4 41034.9 2131.82 20 5 -8 -4 42678.1 2536.82 37 -5 8 4 39530.2 2245.74 72 5 -8 -4 46874.1 2252.03 3 -5 8 4 42868.4 2346.00 33 5 8 -4 42392.9 2223.28 66 5 -8 -4 40373.7 2174.86 64 5 -8 -4 46111.6 2295.62 28 -5 8 4 37961.0 2043.18 26 5 8 -4 49563.4 2183.28 50 -5 -8 4 42874.4 2352.45 22 -5 8 4 44494.9 2388.23 21 -5 8 3 1818.68 447.261 20 5 -8 -3 2713.27 646.863 37 -5 8 3 2270.76 571.279 72 -5 8 3 2263.03 488.864 36 -5 8 3 2054.56 538.148 33 5 8 -3 2486.75 578.722 66 5 -8 -3 2209.35 590.826 64 5 -8 -3 2214.88 480.983 3 5 8 -3 2299.72 465.311 50 -5 8 3 2781.36 643.223 21 5 -8 -2 23746.2 1905.44 38 5 -8 -2 20116.0 1744.67 37 -5 8 2 27448.8 2023.66 72 -5 8 2 26876.9 1788.47 36 -5 8 2 28311.7 1963.36 33 5 8 -2 29281.8 2082.79 66 5 -8 -2 22258.7 2021.17 64 -5 8 2 28087.3 2052.00 21 5 8 -1 288.604 253.608 4 5 -8 -1 733.775 367.416 38 -5 8 1 1138.71 483.574 72 -5 8 1 1337.91 399.781 36 -5 8 1 974.093 356.961 33 5 8 -1 1545.50 486.161 66 5 8 -1 1290.73 438.618 64 5 -8 -1 606.491 376.929 64 -5 8 1 844.276 383.941 21 5 8 0 9344.41 1308.00 4 5 -8 0 10395.2 1339.63 38 -5 8 0 11828.3 1281.68 72 5 8 0 12744.9 1384.98 66 5 8 0 11679.9 1253.73 64 5 -8 0 13077.9 1468.58 64 -5 8 0 11592.5 1314.04 26 -5 8 0 13057.9 1232.75 21 5 8 1 8359.24 1258.74 4 5 -8 1 9542.86 1297.47 38 -5 8 -1 9845.22 1027.72 72 5 -8 1 9883.38 1175.33 64 5 8 1 10569.5 1187.39 63 -5 8 -1 11038.2 1185.47 26 5 8 2 47264.9 3029.87 4 5 -8 2 41500.1 2720.66 38 -5 8 -2 61695.2 2843.90 71 -5 8 -2 56231.0 2538.73 26 5 8 3 24318.8 1969.49 4 5 -8 3 22207.5 1744.30 38 -5 -8 -3 26084.6 1651.76 8 -5 8 -3 28044.8 1664.15 71 -5 8 -3 26578.5 1442.51 26 5 8 4 26687.1 1691.65 4 -5 -8 -4 26878.8 1544.06 8 -5 8 -4 27081.5 1336.97 71 -5 8 -4 24362.1 1347.26 6 -5 8 -4 25423.6 1342.40 11 5 -8 4 27831.9 1398.43 1 5 8 5 2673.07 478.146 63 -5 8 -5 2680.31 391.258 6 5 -8 5 2813.20 379.737 1 5 -9 -5 6662.44 563.480 3 5 9 -5 8698.42 686.342 65 5 9 -5 7505.96 576.224 50 -5 9 4 579.388 251.334 21 5 -9 -4 900.291 349.054 37 -5 9 4 236.980 182.259 72 -5 9 4 693.278 294.134 33 5 9 -4 580.002 239.868 66 5 9 -4 948.503 292.606 65 5 -9 -4 730.723 285.661 64 5 -9 -4 729.986 231.184 3 5 9 -4 1026.57 278.734 50 -5 -9 4 849.729 303.258 22 5 -9 -3 12277.5 1327.97 37 -5 9 3 11328.5 1181.82 72 -5 9 3 11988.8 1078.11 36 -5 -9 3 11383.1 1137.25 34 -5 9 3 11543.5 1171.79 33 5 9 -3 12670.3 1223.55 66 5 9 -3 13663.1 1161.58 65 5 -9 -3 10803.2 1271.70 64 -5 9 3 10523.5 1088.93 26 5 9 -3 13659.4 1039.33 50 -5 9 3 11945.4 1215.75 21 -5 9 2 2780.36 648.052 21 5 -9 -2 2487.42 584.325 38 5 -9 -2 1749.29 498.614 37 -5 9 2 2835.24 647.865 72 -5 9 2 2322.53 512.987 36 -5 9 2 2483.80 570.880 33 5 9 -2 2787.89 633.587 66 5 9 -2 2910.98 567.671 65 5 -9 -2 2555.19 690.538 64 -5 9 2 2109.27 547.217 26 5 9 -1 50183.0 2749.68 4 5 -9 -1 51104.3 2945.13 38 -5 9 1 52238.6 2881.90 72 -5 9 1 49115.5 2459.92 36 -5 9 1 50577.7 2479.72 33 5 9 -1 56167.7 2933.50 66 5 9 -1 58432.7 2685.23 65 5 -9 -1 44682.3 2950.34 64 -5 9 1 56702.2 2839.99 21 5 9 0 13852.7 1523.83 4 5 -9 0 14909.7 1574.81 38 -5 9 0 14815.7 1376.63 72 -5 9 0 15688.5 1459.93 71 5 9 0 15224.8 1312.44 65 5 -9 0 12800.2 1444.12 64 -5 9 0 14212.3 1403.52 26 -5 9 0 17130.0 1316.42 21 5 9 1 24856.1 2149.69 4 5 -9 1 27302.7 2141.27 38 -5 9 -1 28100.1 1917.61 71 5 9 1 32219.5 2132.36 66 5 9 1 30990.4 1894.47 65 5 -9 1 30028.0 1997.62 64 5 9 1 26147.8 1740.19 63 -5 9 -1 29483.7 1894.61 26 5 -9 2 1899.39 533.516 38 5 9 2 1852.05 570.055 4 -5 9 -2 1872.61 454.343 71 5 9 2 1793.66 453.071 65 5 9 2 1905.37 495.485 63 -5 9 -2 2585.41 489.085 26 -5 9 -2 1953.74 448.117 6 5 9 3 4456.15 816.314 4 5 -9 3 4532.44 721.474 38 -5 9 -3 4230.51 595.731 71 -5 9 -3 4299.53 600.961 6 -5 9 -3 3404.13 482.663 26 -5 9 -3 3443.65 524.120 11 5 9 4 2679.08 526.260 4 -5 -9 -4 2654.59 450.561 8 -5 9 -4 2543.80 395.078 71 5 9 4 2706.33 516.319 63 -5 9 -4 2272.62 392.252 6 -5 9 -4 1886.26 333.822 11 5 9 5 4660.91 538.027 63 5 10 -5 4061.78 406.407 65 5 -10 -4 6178.52 746.133 37 -5 10 4 5129.38 526.282 36 5 10 -4 5333.24 610.577 66 5 10 -4 5545.81 607.947 65 5 -10 -4 4955.20 610.055 64 5 10 -4 6100.01 568.275 50 -5 -10 4 4867.41 626.800 22 -5 10 4 5193.57 622.594 21 5 -10 -3 7499.34 926.985 37 -5 10 3 6462.54 734.436 36 -5 10 3 7835.29 886.737 72 -5 -10 3 7466.54 857.791 34 -5 10 3 8215.18 880.574 33 5 10 -3 7982.02 877.834 66 5 10 -3 8999.24 854.707 65 5 -10 -3 8923.27 1054.29 64 -5 10 3 6938.59 771.186 26 5 10 -3 7661.70 708.654 50 -5 10 3 7966.18 898.835 21 5 -10 -2 8128.52 949.679 38 5 -10 -2 7196.22 883.967 37 -5 10 2 7739.96 952.297 72 -5 10 2 7063.03 824.961 36 5 10 -2 10670.0 1088.72 66 5 10 -2 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1848.53 368.242 71 5 10 3 1983.51 432.424 63 -5 10 -3 1801.27 363.345 6 5 10 4 267.924 184.530 4 5 -10 4 19.1919 29.7661 38 -5 10 -4 227.714 124.765 71 5 10 4 372.729 179.837 63 -5 10 -4 177.711 122.400 6 -5 -10 -4 496.592 205.034 24 5 -11 -4 2697.16 399.920 37 -5 11 4 2105.40 272.634 36 5 11 -4 2227.89 334.476 66 5 11 -4 2736.04 361.074 65 5 -11 -4 2508.05 344.038 64 5 -11 -3 3890.83 539.009 37 -5 11 3 3100.33 442.033 36 -5 -11 3 3029.46 476.597 34 5 11 -3 4079.98 551.178 66 5 11 -3 3757.34 492.653 65 5 -11 -3 3722.98 593.727 64 -5 11 3 3046.28 410.329 26 -5 11 3 3042.56 475.366 21 -5 11 2 8490.47 787.496 36 5 11 -2 10259.2 944.630 66 5 11 -2 8994.20 801.940 65 5 -11 -2 11053.6 1128.26 64 -5 -11 2 8356.37 758.748 12 -5 11 2 7790.75 795.047 26 -5 11 2 9016.59 876.588 21 5 11 -1 72311.1 2756.40 4 5 -11 -1 79009.6 3178.95 38 -5 11 1 65929.9 2663.31 71 -5 11 1 68490.3 2755.63 36 5 11 -1 73956.9 2805.37 65 5 -11 -1 72766.9 3263.61 64 -5 11 1 69019.4 2914.99 26 -5 11 1 75846.9 2879.57 21 5 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902.167 368.445 64 6 -5 -2 1048.55 414.744 3 6 5 -2 1276.87 415.040 43 6 -5 -2 1128.43 389.957 43 -6 5 2 1055.65 386.890 21 -6 5 1 612.642 345.319 72 6 5 -1 2241.22 497.541 66 6 5 -1 418.920 269.733 65 6 5 -1 1293.76 383.031 64 6 5 -1 610.935 289.788 60 6 -5 -1 806.375 333.418 60 6 5 -1 1154.15 404.459 43 6 -5 -1 925.142 362.312 43 -6 5 1 863.908 364.802 21 6 -5 0 367.027 243.890 38 -6 5 0 741.831 342.831 72 6 5 0 660.410 289.574 66 6 5 0 436.406 281.271 65 6 -5 0 391.767 251.821 64 6 5 0 528.986 295.672 63 6 5 0 156.959 161.089 60 6 -5 0 430.053 249.487 60 6 5 1 1737.34 558.968 4 6 -5 1 2004.35 526.925 38 6 5 1 2589.45 568.218 65 6 5 1 2421.12 539.153 64 6 -5 1 2317.41 532.512 64 6 5 1 1810.53 537.465 63 6 5 1 2063.76 463.880 60 6 -5 1 2490.11 531.310 60 -6 5 -1 2536.58 600.533 26 6 5 2 6076.38 931.913 4 6 -5 2 6764.92 877.070 38 -6 5 -2 8678.56 1065.65 71 6 5 2 7274.59 946.878 64 6 -5 2 6949.92 813.353 64 6 5 2 7284.72 1046.22 63 -6 5 -3 1580.84 388.023 71 6 5 3 1439.54 443.182 63 6 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9383.88 949.081 60 6 -6 -1 11922.8 1118.26 60 -6 6 1 12379.3 1284.99 21 6 -6 0 2452.41 621.674 38 -6 6 0 3025.60 659.548 72 6 6 0 2902.10 625.603 66 6 6 0 4746.33 800.151 65 6 -6 0 2855.58 641.524 64 6 6 0 3454.33 643.841 63 6 -6 0 2767.66 530.753 60 6 6 0 2159.72 447.919 60 -6 6 0 3316.93 743.974 26 6 -6 1 798.781 369.561 38 6 6 1 777.715 333.087 65 6 6 1 866.593 353.933 64 6 -6 1 1351.91 425.220 64 6 6 1 1089.77 422.635 63 6 6 1 894.817 280.822 60 6 -6 1 858.620 306.358 60 -6 6 -1 979.572 382.991 26 6 6 2 5451.76 901.536 4 6 -6 2 3735.77 675.744 38 -6 6 -2 5822.67 828.098 71 6 6 2 4675.46 836.894 63 6 6 2 4789.34 612.129 60 6 -6 2 4749.13 625.420 60 6 6 3 134.970 170.773 4 -6 6 -3 29.8483 113.298 71 6 -6 3 107.970 147.557 1 6 6 3-48.7928 169.071 63 6 6 3 96.7613 118.541 60 6 -6 3 98.9917 127.193 60 -6 6 -3-33.9292 157.733 6 6 -6 4 490.702 206.956 1 6 6 4-15.4260 0.09833 60 -6 6 -4 394.653 183.310 6 -6 6 -4 499.242 195.276 11 6 6 5 10582.7 788.405 63 -6 7 4 404.651 215.832 21 -6 7 4 656.450 269.444 72 -6 7 4 542.862 232.455 33 6 7 -4 607.646 238.650 65 6 -7 -4 657.493 228.857 64 6 -7 -4 852.958 261.098 3 6 -7 -3 7734.00 767.030 3 -6 7 3 9667.36 1009.87 33 6 7 -3 10436.0 1000.69 65 6 -7 -3 10877.3 1093.86 64 -6 7 3 9354.02 1041.28 21 -6 7 2 12066.6 1282.80 72 -6 7 2 11497.8 1134.51 33 6 7 -2 9024.05 1024.74 66 6 7 -2 12962.5 1207.79 65 6 7 -2 10616.6 1086.18 64 6 -7 -2 10693.4 1227.50 64 -6 7 2 11905.3 1242.11 21 6 -7 -1 4708.16 866.180 38 -6 7 1 5494.84 891.384 72 6 7 -1 3989.03 722.683 66 6 7 -1 5795.05 838.980 65 6 7 -1 5157.84 780.013 64 6 -7 -1 5074.90 861.782 64 -6 7 1 6738.30 1009.46 26 -6 7 1 5318.22 814.307 21 6 -7 0 6161.48 1008.26 38 -6 7 0 9194.22 1067.14 72 6 7 0 8577.30 1080.49 66 6 7 0 10163.3 1102.08 65 6 7 0 7758.41 997.178 64 6 -7 0 7668.10 1043.55 64 -6 7 0 8680.46 1123.20 26 6 -7 1 7153.74 1043.53 38 -6 7 -1 11097.3 1216.51 71 6 7 1 11497.5 1163.07 65 6 -7 1 9228.25 1045.84 64 6 7 1 8854.30 1049.45 63 -6 7 -1 11093.6 1118.36 26 6 7 2 56.0757 150.535 4 6 -7 2 90.4377 156.711 38 -6 7 -2 113.355 143.451 71 6 7 2 388.491 249.598 63 -6 7 -2 163.123 133.256 26 6 7 3 12772.2 1213.89 4 -6 7 -3 11830.4 896.431 71 6 7 3 11810.7 1150.09 63 -6 7 -3 11736.0 938.883 6 6 8 -4 8373.90 691.912 65 6 -8 -4 6834.62 615.311 64 -6 8 3 329.824 212.528 21 -6 8 3 446.878 221.250 33 6 8 -3 28.8477 77.5442 66 6 8 -3 505.026 220.819 65 6 -8 -3 470.189 257.640 64 -6 8 3 525.242 242.704 26 -6 -8 3 430.898 211.821 22 -6 8 2 1482.92 448.487 72 6 8 -2 2039.04 482.326 66 6 8 -2 2906.70 528.360 65 6 -8 -2 2340.58 563.877 64 -6 8 2 2521.53 560.285 26 -6 8 2 2862.38 569.788 21 6 -8 -1 6947.52 1024.42 38 -6 8 1 6775.72 930.294 72 6 8 -1 6783.47 931.329 66 6 8 -1 9289.34 966.959 65 6 -8 -1 6288.16 955.933 64 -6 8 1 7117.21 974.926 26 -6 8 1 7639.31 893.259 21 -6 8 0 1656.31 418.527 72 -6 8 0 2268.65 561.194 71 6 8 0 1596.41 481.697 66 6 8 0 2219.61 510.056 65 6 -8 0 1583.24 460.069 64 -6 8 0 2512.00 563.207 26 6 8 1 117.855 182.665 4 6 -8 1 51.8492 160.733 38 -6 8 -1 125.928 159.372 71 6 8 1 421.614 258.921 65 6 -8 1 220.246 188.693 64 6 8 1 234.216 186.980 63 -6 8 -1 175.736 154.091 26 6 8 2 4150.36 763.292 4 6 -8 2 3413.62 623.586 38 -6 8 -2 3524.06 556.009 71 6 8 2 4515.11 690.032 63 -6 8 -2 3334.87 463.959 26 6 8 3 120.972 153.062 4 6 -8 3-25.4129 39.3819 38 -6 8 -3 44.3062 76.7627 71 6 8 3 102.747 118.676 63 -6 8 -3 210.707 135.747 11 6 8 4 502.941 200.142 63 6 9 -4 2609.13 332.450 65 -6 9 3 1351.31 323.641 21 6 9 -3 925.181 247.029 66 6 9 -3 1308.80 299.730 65 6 -9 -3 1453.82 364.098 64 -6 9 2 1754.46 417.206 72 -6 9 2 1623.55 360.892 71 6 9 -2 1967.88 432.289 66 6 9 -2 1985.00 395.146 65 6 -9 -2 2437.86 534.700 64 -6 9 2 1798.34 418.133 26 -6 9 2 2276.04 451.680 21 6 -9 -1 2039.14 513.238 38 -6 9 1 1903.33 441.710 72 -6 9 1 2122.00 476.528 71 6 9 -1 2194.02 492.765 66 6 9 -1 2404.67 453.684 65 6 -9 -1 2166.75 532.735 64 -6 9 1 2146.59 491.056 26 -6 9 1 2234.74 426.726 21 -6 9 0 152.891 196.550 71 -6 9 0 148.920 127.722 36 6 9 0 377.985 252.141 66 6 9 0 615.190 255.920 65 6 -9 0 630.891 273.334 64 -6 9 0 517.361 268.674 26 6 9 1 540.658 305.168 4 6 -9 1 1050.96 372.091 38 -6 9 -1 720.274 222.645 36 6 9 1 989.607 321.074 65 6 -9 1 1092.97 298.246 64 -6 9 -1 782.219 258.497 26 6 9 2 5971.91 847.328 4 6 -9 2 6892.88 797.656 38 -6 9 -2 6254.29 668.801 71 6 9 2 6634.69 688.909 63 -6 9 -2 6433.31 668.690 6 -6 9 -2 5889.50 568.834 26 6 -9 3-19.2487 42.1837 38 6 9 3 2234.24 375.220 63 6 10 -3 3512.13 396.697 66 6 -10 -3 5352.85 557.804 64 6 10 -2 494.666 209.890 66 6 -10 -2 500.566 227.628 64 -6 10 2 471.981 192.748 26 -6 10 1 551.790 220.177 71 6 10 -1 660.588 253.564 66 6 -10 -1 463.882 241.121 64 6 -10 0 10666.4 1029.25 38 -6 10 0 9754.85 873.193 71 -6 10 0 8677.44 708.250 36 6 10 0 10614.6 988.124 66 6 -10 0 10818.6 927.321 64 -6 10 0 11630.4 951.846 26 6 10 1 18570.3 1310.52 4 6 -10 1 19069.6 1271.18 38 -6 10 -1 16516.3 1041.30 71 -6 10 -1 15751.4 876.345 36 -6 10 -1 15928.2 981.193 6 -6 10 -1 16722.8 993.131 26 6 -10 2 306.293 172.409 38 -6 10 -2 186.119 124.114 71 -6 10 -2 256.524 119.151 36 6 10 2-14.7584 0.11473 63 6 11 -3 155.797 84.5463 65 6 11 -2 3213.20 398.159 66 6 11 -2 3542.42 398.252 65 6 -11 -2 3434.20 441.648 64 6 11 -1 8329.51 720.313 66 6 11 -1 7483.10 627.847 65 6 -11 -1 7672.35 690.780 64 6 -11 0 1352.82 323.054 38 -6 11 0 754.081 178.452 36 6 11 0 1029.36 246.107 65 6 -11 0 758.657 202.350 64 -6 11 -1 683.968 167.336 36 6 -11 2 12487.1 785.000 38 6 12 -1 510.005 141.265 65 6 -12 -1 224.873 102.719 64 -7 0 3 27028.3 1490.87 33 7 0 -3 32935.7 1601.05 64 7 0 -2 17164.5 1252.29 64 7 0 -2 27324.8 2562.05 43 7 0 -1 33844.1 1918.99 64 7 0 -1 44962.0 3161.86 60 7 0 0 550.593 248.236 64 7 0 0 662.523 480.331 60 7 0 1 216.950 177.210 64 7 0 1-80.4653 374.084 60 7 0 2 19403.4 1410.83 64 7 0 2 23482.1 2135.14 60 7 0 3 9786.63 1223.31 60 7 0 4 1356.97 374.655 60 -7 1 3 1474.54 335.884 33 7 -1 -3 2003.12 393.372 64 7 1 -3 1330.33 314.187 64 7 -1 -3 2221.49 652.436 43 7 1 -2 14758.7 1150.75 64 7 -1 -2 15846.4 1207.45 64 7 1 -1 2546.18 507.144 64 7 -1 -1 2940.74 544.049 64 7 1 0 1679.19 413.880 64 7 -1 0 2128.14 475.369 64 7 -1 0 2398.53 754.748 60 7 1 1 108.631 158.715 64 7 -1 1 36.4198 126.204 64 7 -1 1 152.214 312.036 60 7 1 2 18054.2 1308.06 64 7 -1 2 21608.7 1923.06 60 7 -1 3 14831.4 1404.87 60 -7 1 -3 11742.2 1024.29 11 7 1 4 13723.3 1115.68 60 7 -1 4 12662.6 1033.98 60 7 2 -3 12834.8 953.498 64 7 -2 -3 12631.3 977.920 64 -7 2 3 11651.1 997.502 21 7 -2 -3 15367.7 1493.45 43 7 2 -2 518.073 235.504 64 7 -2 -2 273.566 183.766 64 7 2 -2 459.496 375.380 43 7 -2 -2 560.818 361.404 43 -7 2 2 417.586 211.361 21 7 2 -1 22159.8 1507.67 64 7 2 -1 25198.7 1999.96 60 7 2 0 6277.27 791.094 64 7 -2 0 5597.08 758.337 64 7 2 0 5769.54 978.763 60 7 2 1 9798.91 989.346 64 7 -2 1 9240.30 960.921 64 7 2 1 9745.61 1235.60 60 7 -2 1 9848.29 1298.27 60 7 2 2 74.4221 172.990 64 7 -2 2-32.0995 0.06947 64 7 2 2 106.048 201.269 60 7 -2 2 106.106 246.636 60 -7 2 -2 279.599 187.613 6 7 2 3 384.714 238.947 60 7 -2 3 312.750 242.435 60 7 2 4 876.688 261.121 60 7 -2 4 994.184 259.119 60 -7 3 3 494.584 239.676 72 7 3 -3 149.488 139.239 64 7 -3 -3 139.235 136.495 64 7 3 -3 290.411 248.782 43 7 -3 -3 40.8683 141.645 43 -7 3 3 93.0468 135.977 21 7 3 -2 520.225 231.131 64 7 -3 -2 496.192 233.252 64 7 3 -2 589.709 329.653 43 -7 3 2 435.317 220.404 21 -7 3 1 4243.24 671.166 72 7 3 -1 4128.16 651.124 64 7 3 -1 4177.09 726.694 60 7 -3 -1 4907.52 858.581 60 7 3 0 35966.9 2008.29 64 7 -3 0 37744.3 2092.76 64 7 3 0 36954.0 2223.62 60 7 -3 0 43101.1 2523.87 60 -7 3 0 39832.1 2264.80 26 7 3 1 555.711 281.712 64 7 -3 1 922.782 328.978 64 7 3 1 845.661 345.235 60 7 -3 1 825.146 383.866 60 7 3 2 25125.0 1628.25 64 7 3 2 26375.3 1842.47 63 -7 3 -2 23782.8 1538.72 6 7 3 2 23973.4 1657.77 60 7 -3 2 23630.5 1649.91 60 7 3 3 95.6954 130.792 60 7 -3 3 58.8056 128.883 60 -7 4 3 1790.67 415.827 72 7 -4 -3 1956.80 392.234 64 7 4 -3 1452.61 318.521 64 -7 4 2 1188.19 361.907 72 7 4 -2 943.127 303.121 64 7 -4 -2 1359.02 378.147 64 -7 4 2 770.028 270.412 21 -7 4 1 34774.3 2006.63 72 7 4 -1 33962.2 1916.82 64 7 -4 0 13584.9 1213.95 64 7 4 0 12896.5 1133.71 60 7 -4 0 13662.1 1228.09 60 -7 4 0 12134.6 1185.25 26 -7 4 -1 30697.0 1909.05 71 7 4 1 26143.3 1684.94 64 7 -4 1 27931.0 1692.40 64 7 -4 1 28126.2 1722.00 60 7 4 2 1846.15 502.311 63 -7 4 -2 2514.05 468.877 6 7 4 2 1602.49 377.052 60 7 -4 2 1920.18 413.773 60 7 4 3 654.058 292.900 63 7 4 3 669.123 213.493 60 7 -4 3 613.007 197.007 60 7 -5 -3 776.406 251.090 64 -7 5 2 5361.99 738.946 72 7 5 -2 5694.00 693.625 64 7 -5 -2 5237.86 718.993 64 -7 5 1 148.197 181.555 72 7 5 -1-27.4658 60.1914 65 7 5 -1 365.605 265.736 64 -7 5 1 382.493 279.412 26 7 -5 0 10302.4 1029.60 64 7 5 0 7951.07 769.031 60 7 -5 0 8696.30 837.057 60 -7 5 0 9242.05 950.987 26 -7 5 -1 1042.75 332.156 71 7 5 1 990.405 346.376 64 7 -5 1 879.734 299.420 64 7 5 1 971.964 276.861 60 7 -5 1 1001.54 299.397 60 7 5 2 16302.3 1347.64 63 7 5 2 12428.1 886.522 60 7 -5 2 12620.8 897.420 60 -7 5 -2 15282.9 1078.00 6 7 5 3 2941.42 512.147 63 7 -6 -3 23139.5 1288.36 64 7 -6 -2 3751.38 600.763 64 -7 6 2 3665.83 590.179 26 7 6 -1 18141.3 1224.00 65 7 -6 -1 21347.2 1501.52 64 -7 6 1 21371.2 1488.55 26 -7 6 0 862.632 321.878 71 7 6 0 593.476 255.808 65 7 -6 0 943.022 308.221 64 -7 6 0 600.789 250.311 26 -7 6 -1 124.985 136.953 71 7 6 1-17.8274 0.07705 60 7 7 -2 12681.3 863.522 65 7 -7 -2 16796.3 1179.37 64 -7 7 1 7817.13 830.404 71 7 7 -1 7167.21 691.530 65 7 -7 -1 7371.90 818.651 64 -7 7 0 534.303 234.174 71 7 7 0 867.881 262.914 65 7 -7 0 1146.92 316.171 64 7 -7 1-18.0577 39.5753 64 7 -8 -2 2323.19 368.452 64 7 8 -1 11323.9 788.752 65 7 -8 -1 13745.3 958.040 64 7 -8 0 511.707 179.752 64 7 -9 -1 315.514 125.557 64 8 0 -1 10201.7 894.962 64 8 0 0 123.312 151.090 64 8 0 1 22735.7 1711.90 60 8 1 -1 11343.1 932.067 64 8 1 0 5900.56 706.981 64 8 -1 0 5880.74 698.389 64 8 1 1 674.066 319.741 60 8 -1 1 980.595 341.226 60 8 2 -1 239.958 160.097 64 8 2 0 496.217 226.289 64 8 -2 0 281.757 169.272 64 0 0 0 0.00 0.00 0 TITL exp_5138 in P2(1)/m REM P2(1)/m (#11 in standard setting) CELL 1.54184 6.462784 14.691363 7.143401 90.0000 91.2107 90.0000 ZERR 3.00 0.000084 0.000157 0.000074 0.0000 0.0010 0.0000 LATT 1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 33.00 30.00 3.00 3.00 TREF HKLF 4 END ; _shelx_hkl_checksum 86039 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.724 _oxdiff_exptl_absorpt_empirical_full_min 0.633 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.1842(2) 0.750000 0.24688(17) 0.0346(7) Uani 1 2 d S T P . . Cl1 Cl 0.0948(2) 0.60545(10) 0.3925(2) 0.0305(6) Uani 1 1 d . . . . . Cl3 Cl 0.5928(3) 0.750000 0.2228(3) 0.0310(7) Uani 1 2 d S T P . . Cl2 Cl 0.1369(4) 0.750000 -0.1077(3) 0.0378(7) Uani 1 2 d S T P . . N1 N 0.5424(17) 0.5791(7) -0.1195(15) 0.077(3) Uani 1 1 d . . . . . H1 H 0.473145 0.626145 -0.046432 0.092 Uiso 1 1 calc R U . . . C3 C 0.700(2) 0.5363(10) 0.0048(17) 0.086(4) Uani 1 1 d D . . . . H3A H 0.773831 0.490590 -0.065801 0.103 Uiso 1 1 calc R U . . . H3B H 0.799678 0.582263 0.044143 0.103 Uiso 1 1 calc R U . . . C2 C 0.382(2) 0.5048(9) -0.1644(16) 0.084(4) Uani 1 1 d D . . . . H2A H 0.269120 0.531311 -0.238036 0.101 Uiso 1 1 calc R U . . . H2B H 0.445514 0.458214 -0.240149 0.101 Uiso 1 1 calc R U . . . C1 C 0.630(3) 0.6262(16) -0.296(3) 0.131(7) Uani 1 1 d . . . . . H1A H 0.722228 0.674366 -0.258558 0.196 Uiso 1 1 calc R U . . . H1B H 0.518166 0.650784 -0.370810 0.196 Uiso 1 1 calc R U . . . H1C H 0.704260 0.582321 -0.368726 0.196 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.0553(11) 0.0154(8) 0.0333(9) 0.000 0.0052(6) 0.000 Cl1 0.0381(10) 0.0255(10) 0.0277(9) 0.0010(6) -0.0017(6) 0.0027(6) Cl3 0.0246(11) 0.0245(12) 0.0439(13) 0.000 -0.0006(8) 0.000 Cl2 0.0384(13) 0.0468(15) 0.0282(12) 0.000 -0.0030(9) 0.000 N1 0.089(7) 0.062(6) 0.079(6) 0.000(5) 0.001(5) 0.002(5) C3 0.088(8) 0.077(8) 0.091(9) -0.004(7) -0.010(7) 0.000(7) C2 0.094(9) 0.081(9) 0.077(7) -0.008(7) -0.013(6) 0.003(7) C1 0.141(16) 0.125(17) 0.127(14) 0.019(13) 0.028(12) -0.022(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn -1.5491 0.6778 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Zn1 Cl1 121.04(9) 4_575 . ? Cl1 Zn1 Cl3 105.83(6) . . ? Cl1 Zn1 Cl3 105.83(6) 4_575 . ? Cl1 Zn1 Cl2 113.58(5) 4_575 . ? Cl1 Zn1 Cl2 113.58(5) . . ? Cl2 Zn1 Cl3 91.97(8) . . ? C3 N1 H1 107.3 . . ? C3 N1 C2 106.1(9) . . ? C3 N1 C1 114.7(11) . . ? C2 N1 H1 107.3 . . ? C2 N1 C1 113.7(11) . . ? C1 N1 H1 107.3 . . ? N1 C3 H3A 108.8 . . ? N1 C3 H3B 108.8 . . ? H3A C3 H3B 107.7 . . ? C2 C3 N1 113.8(12) 3_665 . ? C2 C3 H3A 108.8 3_665 . ? C2 C3 H3B 108.8 3_665 . ? N1 C2 H2A 108.8 . . ? N1 C2 H2B 108.8 . . ? C3 C2 N1 113.6(11) 3_665 . ? C3 C2 H2A 108.8 3_665 . ? C3 C2 H2B 108.8 3_665 . ? H2A C2 H2B 107.7 . . ? N1 C1 H1A 109.5 . . ? N1 C1 H1B 109.5 . . ? N1 C1 H1C 109.5 . . ? H1A C1 H1B 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn1 Cl1 2.4395(16) 4_575 ? Zn1 Cl1 2.4396(16) . ? Zn1 Cl3 2.650(2) . ? Zn1 Cl2 2.545(3) . ? N1 H1 0.9800 . ? N1 C3 1.478(17) . ? N1 C2 1.537(16) . ? N1 C1 1.56(2) . ? C3 H3A 0.9700 . ? C3 H3B 0.9700 . ? C3 C2 1.403(7) 3_665 ? C2 H2A 0.9700 . ? C2 H2B 0.9700 . ? C1 H1A 0.9600 . ? C1 H1B 0.9600 . ? C1 H1C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C3 N1 C2 C3 54.2(17) . . . 3_665 ? C2 N1 C3 C2 -54.3(16) . . . 3_665 ? C1 N1 C3 C2 179.3(14) . . . 3_665 ? C1 N1 C2 C3 -178.8(14) . . . 3_665 ?