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Information card for entry 7250397
Preview
| Coordinates | 7250397.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C34 H28 Cl N2 Ni O P |
|---|---|
| Calculated formula | C34 H28 Cl N2 Ni O P |
| Title of publication | Chiral PCN pincer Ni(ii) complex-catalyzed asymmetric hydrophosphination of 2-alkenoylpyridines with diphenylphosphine |
| Authors of publication | Li, Jin-Ge; Qiu, Bing-Bo; Jiang, Hui; Song, Mao-Ping; Gong, Jun-Fang |
| Journal of publication | RSC Advances |
| Year of publication | 2025 |
| Journal volume | 15 |
| Journal issue | 20 |
| Pages of publication | 15904 - 15918 |
| a | 28.7861 ± 0.0017 Å |
| b | 9.8408 ± 0.0005 Å |
| c | 22.2091 ± 0.0017 Å |
| α | 90° |
| β | 109.059 ± 0.008° |
| γ | 90° |
| Cell volume | 5946.5 ± 0.7 Å3 |
| Cell temperature | 291.15 K |
| Ambient diffraction temperature | 291.15 K |
| Number of distinct elements | 7 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.0633 |
| Residual factor for significantly intense reflections | 0.0477 |
| Weighted residual factors for significantly intense reflections | 0.1099 |
| Weighted residual factors for all reflections included in the refinement | 0.1198 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.99 |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 299687 (current) | 2025-05-15 | cif/ Adding structures of 7250395, 7250396, 7250397 via cif-deposit CGI script. |
7250397.cif |
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Users of the data should acknowledge the original authors of the
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