Crystallography Open Database

Information card for entry 7700472

Preview

Coordinates	7700472.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H30 Al N2 O P Se
Calculated formula	C27 H30 Al N2 O P Se
Title of publication	Aluminium complex as an efficient catalyst for the chemo-selective reduction of amides to amines.
Authors of publication	Das, Suman; Karmakar, Himadri; Bhattacharjee, Jayeeta; Panda, Tarun K.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	31
Pages of publication	11978 - 11984
a	9.8019 ± 0.0013 Å
b	10.1178 ± 0.0013 Å
c	13.545 ± 0.0019 Å
α	89.947 ± 0.011°
β	83.892 ± 0.011°
γ	81.113 ± 0.011°
Cell volume	1319.5 ± 0.3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1274
Residual factor for significantly intense reflections	0.0729
Weighted residual factors for significantly intense reflections	0.1764
Weighted residual factors for all reflections included in the refinement	0.2092
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
224366 (current)	2019-11-08	cif/ Updating files of 7700471, 7700472, 7700473 Original log message: Adding full bibliography for 7700471--7700473.cif.	7700472.cif
216850	2019-07-09	cif/ Adding structures of 7700471, 7700472, 7700473 via cif-deposit CGI script.	7700472.cif