Crystallography Open Database

Information card for entry 7700496

Preview

Coordinates	7700496.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H18 B F4 N O2 W
Calculated formula	C23 H18 B F4 N O2 W
Title of publication	Propene complexes of molybdenum and tungsten stabilized by intramolecular coordination of the 1-(quinol-8-yl)indenyl ligand.
Authors of publication	Mrózek, Ondřej; Dostál, Libor; Císařová, Ivana; Honzíček, Jan; Vinklárek, Jaromír
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	32
Pages of publication	12210 - 12218
a	28.4483 ± 0.0016 Å
b	8.0338 ± 0.0004 Å
c	21.5649 ± 0.0011 Å
α	90°
β	123.377 ± 0.002°
γ	90°
Cell volume	4115.7 ± 0.4 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0647
Residual factor for significantly intense reflections	0.0556
Weighted residual factors for significantly intense reflections	0.1279
Weighted residual factors for all reflections included in the refinement	0.1322
Goodness-of-fit parameter for all reflections included in the refinement	1.148
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
223912 (current)	2019-11-07	cif/ Updating files of 7700495, 7700496, 7700497, 7700498, 7700499 Original log message: Adding full bibliography for 7700495--7700499.cif.	7700496.cif
216944	2019-07-11	cif/ Adding structures of 7700495, 7700496, 7700497, 7700498, 7700499 via cif-deposit CGI script.	7700496.cif