Crystallography Open Database

Information card for entry 7700512

Preview

Coordinates	7700512.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H15 I6 N2 O4 Re Te2
Calculated formula	C12 H13 I6 N2 O4 Re Te2
Title of publication	Ionic-liquid-based synthesis of tellurium-rhenium carbonyls with specific reaction control.
Authors of publication	Wolf, Silke; Feldmann, Claus
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	41
Pages of publication	15521 - 15528
a	9.7094 ± 0.0019 Å
b	13.539 ± 0.003 Å
c	22.976 ± 0.006 Å
α	90°
β	108.62 ± 0.03°
γ	90°
Cell volume	2862.2 ± 1.2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0411
Residual factor for significantly intense reflections	0.0324
Weighted residual factors for significantly intense reflections	0.093
Weighted residual factors for all reflections included in the refinement	0.096
Goodness-of-fit parameter for all reflections included in the refinement	0.956
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
223889 (current)	2019-11-07	cif/ Updating files of 7700512, 7700513, 7700514, 7700515 Original log message: Adding full bibliography for 7700512--7700515.cif.	7700512.cif
216969	2019-07-12	cif/ Adding structures of 7700512, 7700513, 7700514, 7700515 via cif-deposit CGI script.	7700512.cif